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Prof.Mainak Ghosal
[MIE,MISC,MIAStruct.E,FIV]
–PRESENTER
&
Prof.Arun Kr. Chakraborty
Dep’t of Civil Engineering,IIEST,Shibpur,India.
(Formerly Bengal Engineering & Science University)
22nd -- 24th June,2016
 Has written over 150 Technical Reports
 Has Authored over 15 Technical Papers
 Formerly Asst. Engineer,PHED,Gov. of
W.B
 Adjunct Professor,JIS College of
Engineering
 Consultant/Registered Valuer,CBDT,Gov.
of India
 Research Scholar, Dep't of Civil
Engg.,IIEST,Shibpur
 Is a Life Member of –
* Indian Science Congress
* Institution of Engineers[I]
* Indian Concrete Institute
* Indian Association of Structural Engineers
* Institution of Valuers
* Consulting Engineers Association of India
& Several other Organizations……
 “The construction
industry was the only
industry to identify
nanotechnology as a
promising emerging
technology in the UK
Delphi Survey in the early
1990s…
“Application of Nanotechnology
in Construction”, Materials and
Structures, 37, 649 (2004),
Springer
 By 2030 India’s Population is
expected to cross 1.5 billion
mark - surpass China in
terms of Population….means
a 800 million square meters
of residential & commercial
space needs to be built
annually up to 2030
 Death in every minute due to
Water Scarcity/related
disease…. Concrete is next to
Water in Consumption….
Nano Addition decreases
water Demand
BEFORE NANO-TECHNOLOGY AFTER NANO-TECHNOLOGY
Admixtures+
Nano
FRESH PROPERTIES HARDENED PROPERTIES
SOURCES OF
NANO MATERIALS
1.NANO SILICA[Mean Dia~35 nm]-
1st nano-product that replaced micro-silica
No Admixtures/Plasticizers required
2.CARBON NANOTUBES[Mean Dia=20-40nm]-
Crack controlling
SHM
3. NANO TITANIUM DI-OXIDE[Mean Dia=30-40nm]-
Self cleaning properties
 Improves the materials’ bulk properties.
 To obtain thinner final elements(more
Floor Space) and quicker setting time.
 Brings down Weight & Cost Effective.
 Allows For Rationalization Of Design.
 Lowered levels of environmental
contamination.
 Improved Carbon Ratings.
Conventional
Glass
Self
Cleaning
Glass
SCOPE OF WORK:-
The AIM is to Investigate the
INFLUENCES of Nano-
Additions on Ordinary Cement
& BLENDED Cements
Testing of Nano-materials (nS,
CNT & n-TiO2) for7, 28,90,180 &
365 days compressive strength
for OPC/PPC/PSC
Mortar[Cement:Sand=1:3] at
OPTIMIZED additions
% Nano
additions in
OPCement
7 Days
Strength
(% incr.)
28 Days
Strength
(% incr.)
90 Days
Strength
(% incr.)
180 Days
Strength
(% incr.)
365 Days
Strength
(% incr.)
0% nS
21.08 MPa
(--)
31.89MPa
(--)
31.20MPa
(--)
30.01MPa
(--)
30.01MPa
(---)
0.5% nS
23.85MPa
(13.14%)
35.1MPa
(11.35%)
41.30MPa
(32.37%)
27.47MPa
(-9.24%)
26.76MPa
(-4.29%)
0.75% nS
27.73MPa
(31.54%)
42.27MPa
(32.55%)
49.85MPa
(59.78%)
32.52MPa
(8.36%)
31.5MPa
(4.96%)
1.0% nS
25.07MPa
(18.93%)
37.36MPa
(17.15%)
42.98MPa
(37.76%)
33.68MPa
(12.23%)
32.41MPa
(8.0%)
1.25% nS
23.17MPa
(9.91%)
30.85MPa
(-3.26%)
39.45MPa
(26.44%)
35.24MPa
(17.43%)
31.3MPa
(4.29%)
1.50% nS 23.81MPa
(12.95%)
37.79MPa
(18.50%)
33.42MPa
(7.12%)
31.23MPa
(4.07%)
29.12MPa
(-2.96%)
% Nano
additions in
PPC
7 Days
Strength
(% incr.)
28 Days
Strength
(% incr.)
90 Days
Strength
(% incr.)
180 Days
Strength
(% incr.)
365 Days
Strength
(% incr.)
0% nS
11.36 MPa
(--)
22.44 MPa
(--)
25.96 MPa
(--)
27.08 MPa
(--)
23.52MPa
(---)
0.5% nS
8.93MPa
(-21.39%)
27.16 MPa
(21.03%)
22.45 MPa
(-13.52%)
26.11MPa
(-3.58%)
21.26MPa
(9.61%)
0.75% nS
23.66MPa
(108.27%)
27.45 MPa
(22.32%)
33.17 MPa
(27.77%)
27.0 MPa
(-0.30%)
35.54MPa
(51.11%)
1.0% nS
25.07MPa
(18.93%)
37.36MPa
(17.15%)
42.98MPa
(37.76%)
33.68MPa
(12.23%)
32.41MPa
(8.0%)
1.25% nS
23.17MPa
(9.91%)
30.85MPa
(-3.26%)
39.45MPa
(26.44%)
35.24MPa
(17.43%)
31.3MPa
(4.29%)
1.50% nS 23.81MPa
(12.95%)
37.79MPa
(18.50%)
33.42MPa
(7.12%)
31.23MPa
(4.07%)
29.12MPa
(-2.96%)
% Nano
additions in
PSC
7 Days
Strength
(% incr.)
28 Days
Strength
(% incr.)
90 Days
Strength
(% incr.)
180 Days
Strength
(% incr.)
365 Days
Strength
(% incr.)
0% nS
22.89 MPa
(--)
28.93 MPa
(--)
26.79 MPa
(--)
19.95 MPa
(--)
32.65MPa
(---)
0.5% nS
22.81MPa
(-0.35%)
30.56MPa
(18.93%)
26.31MPa
(5.63%)
24.63MPa
(23.46%)
41.24 MPa
(26.31%)
0.75% nS
19.45 MPa
(-15.02%)
27.56 MPa
(-4.73%)
22.89 MPa
(14.55%)
20.63MPa
(3.41%)
23.47MPa
(-28.11%)
1.0% nS
21.54MPa
(-5.89%)
29.88 MPa
(3.28%)
36.22 MPa
(35.20%)
23.48MPa
(17.69%)
18.11MPa
(-44.53%)
1.25% nS
19.62 MPa
(-14.28%)
18.62 MPa
(-39.63%)
22.84 MPa
(-14.74%)
14.74 MPa
(-26.12%)
23.81MPa
(-27.08%)
1.50% nS 14.39MPa
(-37.13%)
14.80 MPa
(-48.83%)
18.74 MPa
(-42.96%)
14.86 MPa
(-25.51%)
16.84 MPa
(-48.42%)
% Nano
additions in
OPCement
7 Days
Compressiv
e Str
(% incr.)
28 Days
Compressive
Str
(% incr.)
90 Days
Compressive
Str
(% incr.)
180 Days
Compressive
Str
(% incr.)
365 Days
Strength
(% incr.)
0%
CNT/TiO2
21.08MPa
(--)
31.89MPa
(--)
31.20MPa
(--)
30.01MPa
(--)
30.01MPa
(--)
0.02%CNT 17.69MPa
(-16.08%)
43.75MPa
(37.19%)
35.59MPa
(14.07%)
30.89MPa
(0%)
28.53MPa
(-4.93%)
0.05%CNT
27.19MPa
(28.98%)
34.88MPa
(9.37%)
31.85MPa
(2.08%)
38.55MPa
(3%)
41.69MPa
(38.92%)
0.1%CNT 21.69MPa
(2.89%)
24.83MPa
(-22.14%)
31.50MPa
(0.96%)
30.16MPa
(0%)
50.78MPa
(69.21%)
1%TiO2
25.24MPa
(19.73%)
36.71MPa
(12.59%)
35.92MPa
(15.13%)
33.42MPa
(11.36%)
41.16MPa
(37.15%)
2.5%TiO2
20.34MPa
(-3.51%)
34.97MPa
(9.58%)
37.80MPa
(21.15%)
40.95MPa
(36.45%)
28.16MPa
(-6.16%)
DISCUSSIONS &
CONCLUSIONS
Nano-Additions never resulted in any
appreciable change in PHYSICAL
CHARACTERISTICS of Cement –
COLOUR,SHAPE,SIZE,WEIGHT,DENSITY
Nano-Additions in PCE for
CNT/TiO2 REDUCED THE SETTING
TIME[From 3 Days to 1.5 Day]
OPTIMIZATIONS for Nano
Materials in Ordinary Cement
Mortar -nS, CNT & TiO2 are
0.75%,0.02% & 1% w.r.to Cement
weight at 28 Days
 Results indicate that for OPC,
slight increase of Ns/CNT dose
from the optimized one gives an
overall increase in strength in
Long Term
For PPC & PSC optimizations are
0.75% nS & 0.5% nS which remains
fixed for both Short & Long Terms
Further research on MICRO
STRUCTURAL studies are necessary
for Characterization of Nano
Materials -XRD,SEM-EDS,TEM,AFM
in Cement Concrete
THANK YOU!
mainakghosal2010@gmail.com
www.ermainakghosal.weebly.com

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Golden Jubilee of Goa Engineering College's International Conference on Advances in Concrete Technology, Materials and Construction Practices

  • 1. Prof.Mainak Ghosal [MIE,MISC,MIAStruct.E,FIV] –PRESENTER & Prof.Arun Kr. Chakraborty Dep’t of Civil Engineering,IIEST,Shibpur,India. (Formerly Bengal Engineering & Science University) 22nd -- 24th June,2016
  • 2.  Has written over 150 Technical Reports  Has Authored over 15 Technical Papers  Formerly Asst. Engineer,PHED,Gov. of W.B  Adjunct Professor,JIS College of Engineering  Consultant/Registered Valuer,CBDT,Gov. of India  Research Scholar, Dep't of Civil Engg.,IIEST,Shibpur  Is a Life Member of – * Indian Science Congress * Institution of Engineers[I] * Indian Concrete Institute * Indian Association of Structural Engineers * Institution of Valuers * Consulting Engineers Association of India & Several other Organizations……
  • 3.  “The construction industry was the only industry to identify nanotechnology as a promising emerging technology in the UK Delphi Survey in the early 1990s… “Application of Nanotechnology in Construction”, Materials and Structures, 37, 649 (2004), Springer  By 2030 India’s Population is expected to cross 1.5 billion mark - surpass China in terms of Population….means a 800 million square meters of residential & commercial space needs to be built annually up to 2030  Death in every minute due to Water Scarcity/related disease…. Concrete is next to Water in Consumption…. Nano Addition decreases water Demand
  • 7. SOURCES OF NANO MATERIALS 1.NANO SILICA[Mean Dia~35 nm]- 1st nano-product that replaced micro-silica No Admixtures/Plasticizers required 2.CARBON NANOTUBES[Mean Dia=20-40nm]- Crack controlling SHM 3. NANO TITANIUM DI-OXIDE[Mean Dia=30-40nm]- Self cleaning properties
  • 8.
  • 9.  Improves the materials’ bulk properties.  To obtain thinner final elements(more Floor Space) and quicker setting time.  Brings down Weight & Cost Effective.  Allows For Rationalization Of Design.  Lowered levels of environmental contamination.  Improved Carbon Ratings. Conventional Glass Self Cleaning Glass
  • 10. SCOPE OF WORK:- The AIM is to Investigate the INFLUENCES of Nano- Additions on Ordinary Cement & BLENDED Cements Testing of Nano-materials (nS, CNT & n-TiO2) for7, 28,90,180 & 365 days compressive strength for OPC/PPC/PSC Mortar[Cement:Sand=1:3] at OPTIMIZED additions
  • 11. % Nano additions in OPCement 7 Days Strength (% incr.) 28 Days Strength (% incr.) 90 Days Strength (% incr.) 180 Days Strength (% incr.) 365 Days Strength (% incr.) 0% nS 21.08 MPa (--) 31.89MPa (--) 31.20MPa (--) 30.01MPa (--) 30.01MPa (---) 0.5% nS 23.85MPa (13.14%) 35.1MPa (11.35%) 41.30MPa (32.37%) 27.47MPa (-9.24%) 26.76MPa (-4.29%) 0.75% nS 27.73MPa (31.54%) 42.27MPa (32.55%) 49.85MPa (59.78%) 32.52MPa (8.36%) 31.5MPa (4.96%) 1.0% nS 25.07MPa (18.93%) 37.36MPa (17.15%) 42.98MPa (37.76%) 33.68MPa (12.23%) 32.41MPa (8.0%) 1.25% nS 23.17MPa (9.91%) 30.85MPa (-3.26%) 39.45MPa (26.44%) 35.24MPa (17.43%) 31.3MPa (4.29%) 1.50% nS 23.81MPa (12.95%) 37.79MPa (18.50%) 33.42MPa (7.12%) 31.23MPa (4.07%) 29.12MPa (-2.96%)
  • 12. % Nano additions in PPC 7 Days Strength (% incr.) 28 Days Strength (% incr.) 90 Days Strength (% incr.) 180 Days Strength (% incr.) 365 Days Strength (% incr.) 0% nS 11.36 MPa (--) 22.44 MPa (--) 25.96 MPa (--) 27.08 MPa (--) 23.52MPa (---) 0.5% nS 8.93MPa (-21.39%) 27.16 MPa (21.03%) 22.45 MPa (-13.52%) 26.11MPa (-3.58%) 21.26MPa (9.61%) 0.75% nS 23.66MPa (108.27%) 27.45 MPa (22.32%) 33.17 MPa (27.77%) 27.0 MPa (-0.30%) 35.54MPa (51.11%) 1.0% nS 25.07MPa (18.93%) 37.36MPa (17.15%) 42.98MPa (37.76%) 33.68MPa (12.23%) 32.41MPa (8.0%) 1.25% nS 23.17MPa (9.91%) 30.85MPa (-3.26%) 39.45MPa (26.44%) 35.24MPa (17.43%) 31.3MPa (4.29%) 1.50% nS 23.81MPa (12.95%) 37.79MPa (18.50%) 33.42MPa (7.12%) 31.23MPa (4.07%) 29.12MPa (-2.96%)
  • 13. % Nano additions in PSC 7 Days Strength (% incr.) 28 Days Strength (% incr.) 90 Days Strength (% incr.) 180 Days Strength (% incr.) 365 Days Strength (% incr.) 0% nS 22.89 MPa (--) 28.93 MPa (--) 26.79 MPa (--) 19.95 MPa (--) 32.65MPa (---) 0.5% nS 22.81MPa (-0.35%) 30.56MPa (18.93%) 26.31MPa (5.63%) 24.63MPa (23.46%) 41.24 MPa (26.31%) 0.75% nS 19.45 MPa (-15.02%) 27.56 MPa (-4.73%) 22.89 MPa (14.55%) 20.63MPa (3.41%) 23.47MPa (-28.11%) 1.0% nS 21.54MPa (-5.89%) 29.88 MPa (3.28%) 36.22 MPa (35.20%) 23.48MPa (17.69%) 18.11MPa (-44.53%) 1.25% nS 19.62 MPa (-14.28%) 18.62 MPa (-39.63%) 22.84 MPa (-14.74%) 14.74 MPa (-26.12%) 23.81MPa (-27.08%) 1.50% nS 14.39MPa (-37.13%) 14.80 MPa (-48.83%) 18.74 MPa (-42.96%) 14.86 MPa (-25.51%) 16.84 MPa (-48.42%)
  • 14. % Nano additions in OPCement 7 Days Compressiv e Str (% incr.) 28 Days Compressive Str (% incr.) 90 Days Compressive Str (% incr.) 180 Days Compressive Str (% incr.) 365 Days Strength (% incr.) 0% CNT/TiO2 21.08MPa (--) 31.89MPa (--) 31.20MPa (--) 30.01MPa (--) 30.01MPa (--) 0.02%CNT 17.69MPa (-16.08%) 43.75MPa (37.19%) 35.59MPa (14.07%) 30.89MPa (0%) 28.53MPa (-4.93%) 0.05%CNT 27.19MPa (28.98%) 34.88MPa (9.37%) 31.85MPa (2.08%) 38.55MPa (3%) 41.69MPa (38.92%) 0.1%CNT 21.69MPa (2.89%) 24.83MPa (-22.14%) 31.50MPa (0.96%) 30.16MPa (0%) 50.78MPa (69.21%) 1%TiO2 25.24MPa (19.73%) 36.71MPa (12.59%) 35.92MPa (15.13%) 33.42MPa (11.36%) 41.16MPa (37.15%) 2.5%TiO2 20.34MPa (-3.51%) 34.97MPa (9.58%) 37.80MPa (21.15%) 40.95MPa (36.45%) 28.16MPa (-6.16%)
  • 15. DISCUSSIONS & CONCLUSIONS Nano-Additions never resulted in any appreciable change in PHYSICAL CHARACTERISTICS of Cement – COLOUR,SHAPE,SIZE,WEIGHT,DENSITY Nano-Additions in PCE for CNT/TiO2 REDUCED THE SETTING TIME[From 3 Days to 1.5 Day] OPTIMIZATIONS for Nano Materials in Ordinary Cement Mortar -nS, CNT & TiO2 are 0.75%,0.02% & 1% w.r.to Cement weight at 28 Days  Results indicate that for OPC, slight increase of Ns/CNT dose from the optimized one gives an overall increase in strength in Long Term For PPC & PSC optimizations are 0.75% nS & 0.5% nS which remains fixed for both Short & Long Terms Further research on MICRO STRUCTURAL studies are necessary for Characterization of Nano Materials -XRD,SEM-EDS,TEM,AFM in Cement Concrete