This document discusses a student's project on bio-processing of textiles using enzymes. It includes sections on the objectives of studying the bio-polishing effect of enzymes on knit fabric and the washing effect on denim. The methodology, introduction to enzymes and their industrial applications, and specific experiments on bio-polishing knit fabric are described. The effects of varying the enzyme concentration, temperature, pH, and other factors are summarized.
Wrinkle free resin finishing is a process to apply chemical resin onto fabrics functioning crosslinking between hydrogen bonds in order to enhance stability, on other words, fabrics are prevent to wrinkling. The ability of a fabric to recover to a definite degree is called crease recovery of the fabric.Tendency of fabrics made by cellulose, regenerated cellulose and blends with synthetic fibers to wrinkle after washing, tumble drying and wearing are higher. Today everybody wishes for that his/her dress retains just ironed shape. Wrinkle free finishes provide wrinkle free and soft look fabric. Wrinkle free finishes are broadly used in the textile industry to impart wrinkle-resistance to cellulosic materials such as cotton fabric.
This presentation is about Plasma technology in textile. Plasma technology improves many sites in textile. It improves the dying speed, Desizing, reduces crease, improve surface energy and soo on.
Pretreatment ,Impurities in natural fibre; Chemistry and practice of preparatory processes for cotton, wool and silk; Mercerization of cotton; Preparatory processes for manmade fibres and their blends,Carbonization ,Scouring barium acitivity number .
Presentation on Enzymes, Denim Stone Washing and Bio PolishingMd. Sirajul Islam
Questions:
WHAT ARE ENZYMES?
USAGE OF ENZYMES IN TEXTILE INDUSTRY?
Advantages of using Enzymes?
Properties of enzymes used in textiles?
The main characteristics imparted to the fabric during bio polishing treatment?
It has great effect of hot brand reactive dye on cotton fabric with exhaustion method. Migration method is more acceptable for proper color fixation in a dyeing process. Another way when we followed ISO method has create a lot of problem such as wash fastness variation rubbing fastness variation, uneven dyeing etc. If we want to get perfect dyeing than we must maintain migration method.
Different kinds of enzyme on textile substrates Azmir Latif Beg
Enzymes are proteins with highly specialized catalytic functions, produced by all living organisms. The textile industry has used enzymes to remove hairiness of fabric. The textile industry has become familiar with the use of celluloses for stone-washing blue jeans, and more recently for finishing of fabrics and garments made on cotton, linen and other cellulose fibers. In the modern textile technology finishing process, employing environmentally friendly, fully biodegradable enzymes can replace a number of mechanical and chemical operations which have hitherto been applied to improve the comfort and quality of textile materials.
Wrinkle free resin finishing is a process to apply chemical resin onto fabrics functioning crosslinking between hydrogen bonds in order to enhance stability, on other words, fabrics are prevent to wrinkling. The ability of a fabric to recover to a definite degree is called crease recovery of the fabric.Tendency of fabrics made by cellulose, regenerated cellulose and blends with synthetic fibers to wrinkle after washing, tumble drying and wearing are higher. Today everybody wishes for that his/her dress retains just ironed shape. Wrinkle free finishes provide wrinkle free and soft look fabric. Wrinkle free finishes are broadly used in the textile industry to impart wrinkle-resistance to cellulosic materials such as cotton fabric.
This presentation is about Plasma technology in textile. Plasma technology improves many sites in textile. It improves the dying speed, Desizing, reduces crease, improve surface energy and soo on.
Pretreatment ,Impurities in natural fibre; Chemistry and practice of preparatory processes for cotton, wool and silk; Mercerization of cotton; Preparatory processes for manmade fibres and their blends,Carbonization ,Scouring barium acitivity number .
Presentation on Enzymes, Denim Stone Washing and Bio PolishingMd. Sirajul Islam
Questions:
WHAT ARE ENZYMES?
USAGE OF ENZYMES IN TEXTILE INDUSTRY?
Advantages of using Enzymes?
Properties of enzymes used in textiles?
The main characteristics imparted to the fabric during bio polishing treatment?
It has great effect of hot brand reactive dye on cotton fabric with exhaustion method. Migration method is more acceptable for proper color fixation in a dyeing process. Another way when we followed ISO method has create a lot of problem such as wash fastness variation rubbing fastness variation, uneven dyeing etc. If we want to get perfect dyeing than we must maintain migration method.
Different kinds of enzyme on textile substrates Azmir Latif Beg
Enzymes are proteins with highly specialized catalytic functions, produced by all living organisms. The textile industry has used enzymes to remove hairiness of fabric. The textile industry has become familiar with the use of celluloses for stone-washing blue jeans, and more recently for finishing of fabrics and garments made on cotton, linen and other cellulose fibers. In the modern textile technology finishing process, employing environmentally friendly, fully biodegradable enzymes can replace a number of mechanical and chemical operations which have hitherto been applied to improve the comfort and quality of textile materials.
Influence of enzyme and silicone wash on the physico mechanical properties of...Elias Khalil (ইলিয়াস খলিল)
Garments washing is one of the most important finishing treatments applied on apparels which have vital use to create special outlooks and improving the fashion. Technologically washing is one of the most important fashion elements for clothing industry and production of washed garments depends on the machine quality. In order to achieve an optimum effect of washing process, on the woven fabric in different washing time, Enzyme Wash and then Silicone wash were carried out for cotton fabric. However, there are some of the comments that when the garments have longer washing time, use of the chemical on the washing procedure will affect the physical and mechanical performance. The aim of this study is to determine the effects of industrial enzyme silicone wash combined with silicone wash. For this study currently fashionable regular Non- denim (100% cotton with twill 3/1 weave construction) trouser was chosen. The selected Non-denim trouser has been processed by enzyme and then silicone wash. In order to evaluate the washing effects on Non-denim trouser, changes of fabric handle, fabric specification (ends/inch, picks/inch, surface density, warp & weft yarn linear density), fabric strength has been determined during and after washing
In this context, there is a need to use “biodetergent or biocleaners”, which offer a better option to the synthetic detergents with respect to their biodegradability, low toxicity, non-corrosiveness environmental-friendliness, enhanced cleaning properties and their increased efficiency and stability in different formulations.
To counter these limitations, enzyme-based detergents are fast emerging as an alternative to synthetic detergents owing to their
biodegradability,
low toxicity,
non- corrosiveness,
environmental friendliness,
enhanced cleaning properties,
increased efficiency and stability in different formulations.
They are therefore also being referred to as “green chemicals”
Presently, proteases, amylases, lipases and cellulases make up the major portion of the market for industrial enzymes in cleaning applications.
Protease enzymes were first hydrolases introduced into detergent formulations specifically for the degradation of protein-based stains. Proteases have been classified according to the nucleophile or reactive component found at their catalytic sites
Cosmetic shop management system project report.pdfKamal Acharya
Buying new cosmetic products is difficult. It can even be scary for those who have sensitive skin and are prone to skin trouble. The information needed to alleviate this problem is on the back of each product, but it's thought to interpret those ingredient lists unless you have a background in chemistry.
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Data file handling has been effectively used in the program.
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Final project report on grocery store management system..pdfKamal Acharya
In today’s fast-changing business environment, it’s extremely important to be able to respond to client needs in the most effective and timely manner. If your customers wish to see your business online and have instant access to your products or services.
Online Grocery Store is an e-commerce website, which retails various grocery products. This project allows viewing various products available enables registered users to purchase desired products instantly using Paytm, UPI payment processor (Instant Pay) and also can place order by using Cash on Delivery (Pay Later) option. This project provides an easy access to Administrators and Managers to view orders placed using Pay Later and Instant Pay options.
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This document will discuss each of the underlying technologies to create and implement an e- commerce website.
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Advancements in technology unveil a myriad of electrical and electronic breakthroughs geared towards efficiently harnessing limited resources to meet human energy demands. The optimization of hybrid solar PV panels and pumped hydro energy supply systems plays a pivotal role in utilizing natural resources effectively. This initiative not only benefits humanity but also fosters environmental sustainability. The study investigated the design optimization of these hybrid systems, focusing on understanding solar radiation patterns, identifying geographical influences on solar radiation, formulating a mathematical model for system optimization, and determining the optimal configuration of PV panels and pumped hydro storage. Through a comparative analysis approach and eight weeks of data collection, the study addressed key research questions related to solar radiation patterns and optimal system design. The findings highlighted regions with heightened solar radiation levels, showcasing substantial potential for power generation and emphasizing the system's efficiency. Optimizing system design significantly boosted power generation, promoted renewable energy utilization, and enhanced energy storage capacity. The study underscored the benefits of optimizing hybrid solar PV panels and pumped hydro energy supply systems for sustainable energy usage. Optimizing the design of solar PV panels and pumped hydro energy supply systems as examined across diverse climatic conditions in a developing country, not only enhances power generation but also improves the integration of renewable energy sources and boosts energy storage capacities, particularly beneficial for less economically prosperous regions. Additionally, the study provides valuable insights for advancing energy research in economically viable areas. Recommendations included conducting site-specific assessments, utilizing advanced modeling tools, implementing regular maintenance protocols, and enhancing communication among system components.
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We used HTML/PHP as front end and MYSQL as back end for developing our project. HTML is primarily a visual design environment. We can create a android application by designing the form and that make up the user interface. Adding android application code to the form and the objects such as buttons and text boxes on them and adding any required support code in additional modular.
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2. Md. Rafsan Jany
Id # 2007200400024
6th Batch
Supervisor: Dr. Shah Mohammad Fatah-ur-
Rahman
Associate
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Professor
4. Acknowledgement
The department of Textile Engineering of Southeast University has given me
the field to perform the project with the ‘Bio-processing of Textiles’.
I am deeply indebted to our honorable supervising teacher Dr. Shah
Mohammad Fatah-ur-Rahman, Associate Professor and my entire course
teacher of textile department as their rendered them hand for all kind of help
to me.
I would also like to thank Engr. Md. Faridul Hasan, Executive, Dyeing,
Viyellatex Group Ltd. for helping by giving me information about the project.
The encouragement as a continued source of inspiration provided by my
parents is fully appreciated.
Finally I would like to acknowledge that I remain responsible for the
inadequacies and errors, which doubtlessly remain.
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5. Abstract
Now a days the whole universe is concern about the
hygiene and they are looking for eco-friendly processes
everywhere. Textile processing is responsible for polluting the
environment at a large degree. Use of Cellulase enzyme for
denim washing is a standard eco-friendly technique to achieve
desired appearance and washing of denim and also the desired
appearance of the knit fabric. Applications of enzymes to replace
harsh chemicals and other difficulties for the processing
industries have been practiced for decades.
I have studied the bio-polishing effect of knit fabric &
washing effect of denim fabric with Cellulase enzyme under
different condition.
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6. Objectives of the project
To know the effect of bio-polishing on knit fabric/garment.
To know the effect of enzyme washing on denim fabric/garment.
To find out the washing technique by which faded/old look effect
is created in the garments.
Limitation
It is based on knit fabric.
All the experiments had done by cellulase enzyme.
Only Focused on bio-polishing & enzyme wash only.
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7. Methodology
Visited to different washing
Industries and knit dyeing
industries
Observed Different processes of
bio-polishing &enzyme washing
(cellulase enzyme)
Observed the effect of enzyme
on fabric and garments.
Group discussion done
Selected the suitable Process
and Recipe for Enzyme
application on Textile Processing
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8. Introduction
Bio-processing can simply be defined as the
application of living organisms and their components
to industrial products and processes. It is not an industry
in itself, but an important technology that will have a
large impact on many industrial sectors in the future.
Bio-processing is the application of biological
organisms, systems or processes to manufacturing
industries. Bio-processing firms will rely mainly on
inexpensive substrates for biosynthesis, processes that will
function at low temperatures, and will consume little
energy.
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9. Enzyme
Enzymes are proteins that catalyze chemical reactions. Mainly
they are consist of long chains of amino acids held together by
peptide bonds Like all catalysts, enzymes work by lowering the
activation energy for a reaction and thus dramatically accelerating
the rate of the reaction. However, enzymes do differ from most
other catalysts by being much more specific. Enzymes are known
to catalyze about 4,000 biochemical reactions.
Enzyme are proteins produced by living organisms. Some enzyme
replicated in the lab or engineered to perform in a particular task.
Practically most catalyst have a limited stability & after certain
time they lose their activity & are not usable again. Generally
most enzyme are used only once & discard after they have done
their job.
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10. Cont….
Different types of enzymes are suitable for different stains.
Enzyme washing process breaks the stain down into smaller
molecules which can be removed by conventional soap or with
water.
I worked only with cellulase enzyme . I tried to know the
effect of bio-polishing & enzyme washing.
Enzyme works at low temperature & also environment friendly.
Many detergent products mix enzyme into their formulas , to
ensure that they are effective at all temperature & on all
stains.
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11. ETYMOLOGY & HISTORY
In 1876 German physiologist Wilhelm Kühne (1837–1900)
proposed that the name 'enzyme' be used as the new term to
denote phenomena previously known as 'unorganised ferments',
that is, ferments isolated from the viable organisms in which they
were formed. The word itself means 'in yeast' and is derived from
the Greek 'en' meaning 'in', and 'zyme' meaning 'yeast' or
'leaven'.
Enzymes are usually named according to the reaction they carry
out. Typically the suffix -ase is reaction or the type of added to
the name of the substrate.
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12. ENZYME & INDUTRIAL APPLICATION
Industrial enzymes can be produced in an
ecologically sound way where the waste
sludge is recycled as fertilizer.
Industrial application of enzymes started:
Amylase Desizing (1952).
Protease Wool (1984).
Cellulase Bio-stoning (1987).
Catalase Bleach cleanup (1993).
Laccase Denim Bleaching (1996).
Peroxidase Enzymatic Rinse
(1999).
Pectate Lyase Bio-scouring
(2003).
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13. Enzymes for Textile
There are lot of enzymes like amylases,
cellulases, catalase, pectinase and protease
for various textile wet-processing
applications like desizing, bio-polishing,
denim finishing, bleach clean-up, bio-scouring
and de-wooling.
14. Sources of Enzymes
Animal Enzyme
Enzyme Source
Catalase Liver
Lipase Pancreas
Protease Pancreas
Bacterial Enzyme
-amylase Bacillus
Protease Bacillus
Plant Enzyme
Protease Carica papaya
Successful enzymes for textile bio-processing
has yet to be synthesized .
15. DIFFERENT TYPES OF ENZYME:
Proteases:
Proteases are the most widely used enzymes in the detergent
industry. Proteases hydrolyze proteins and break them down
into more soluble polypeptides or free amino acids. As a
result of the combined effect of surfactants and enzymes,
stubborn stains can be removed from fibres.
Lipases:
oily and fatty stains have always been troublesome to remove.
The trend towards lower washing temperatures has made the
removal of grease spots an even bigger problem .The lipase is
capable of removing fatty stains such as fats, butter, salad oil,
sauces and the tough stains on collars and cuffs.
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16. Amylases:
Amylases are used to remove residues of starch-based foods
like potatoes, spaghetti, custards, gravies and chocolate. This
type of enzyme can be used in laundry detergents as well as in
dishwashing detergents.
Cellulases:
Cellulase enzyme has properties enabling it to modify the
structure of cellulose fibre on cotton and cotton blends. When
it is added to a detergent, it results into the following effects:
1. Color brightening
2. Softening
3. Soil removal
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17. How does enzyme work????
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18. Lock & key model
Induced model
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19. Bio-polishing of knit fabric
Stage-1: One bath Scouring and Peroxide bleaching
Recipe:
Anti-foaming 0.07gm/l
Rucozen WBX (Detergent) 0.5gm/l
Stabilizer SOF 0.5gm/l
Primasol jet (Anti-creasing) 1.5gm/l
Securon 540 (Sequestering) 1gm/l
Caustic 2gm/l
H2O2 2.5gm/l
pH 10-11
Temperature 1050C
Time 50min
9/25/2014 Bio-processing of Textiles 19
Stage-2: Bio-polishing
Recipe:
BP Nano 0.9gm/l
Acetic acid 1gm/l
T-100 (Peroxide killer) 0.08gm/l
Securon 540 0.25gm/l
pH 4.5-5
Temperature 550C-600C
Time 40-60min
20. Process flw chart
Fresh water and fabric
Load at 450C
Temperature raise to
600C
Detergent & Peroxide
Stabilizer (Inject)
Run for 5 min
Inject Caustic and run
5 min
Raise temperature to
700C
H2O2 inject and run 5
min
Temperature raise to
1050C
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Bio-polishing
before dyeing
Bio-polishing
after dyeing
21. Run for 30 min
Lower the
temperature to 800C
Bath drain
BP Nano & Acetic
acid
Securon 540 &
Peroxide killer inject
Temperature raise to
550C
Run for 60 min
Rinsing and unload
the fabric.
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22. Process variables
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Concentration
Temperature
pH
Time
M : L Rnatio
Mechanical Agitation
To achieve optimum bio-polishing, the process variables have been
varied as mentioned below
Concentration of enzyme: 0.5%, 1%, 2%, 2.5%, 3% & 4%.
Temperature: 400C, 45 0C, 500C, 550C & 600C.
pH: 3-4, 4-5 & 5-6.
M: L: 1:5, 1:10, 1:15 & 1:20.
Mechanical Agitation: Vigorous Stirring, Medium Stirring &
Without Stirring.
23. Effects of Bio-polishing experimented
Effects of concentration of enzyme on bio-polishing
Effects of Temperature of enzyme on bio-polishing
Effects of pH of enzyme on bio-polishing
Effects of M:L of enzyme on bio-polishing
Effects of duration of enzyme on bio-polishing
Effects of Enzyme treatment on dyeing property (3%
shade)
9/25/2014 Bio-processing of Textiles 23
24. Effects of concentration
Effects of Temperature
9/25/2014 Bio-processing of Textiles 24
Properties
Result
Concentration of Enzyme
0.5% 1% 1.5% 2%
2.5
%
3%
3.5
%
Weight loss (%) 0.36 0.77 0.88 1.46 2.09 2.12 2.07
Abrasion (mm) 0.04 0.06 0.07 0.08 0.08 0.09 0.09
Wash fastness 4-5 4-5 4-5 4-5 4-5 4-5 4-5
Pilling rating 3 3 4 4 4 4 4
Properties
Result
Temperature
400C 450C 500C 550C
Weight loss (%) 0.75 1.03 1.45 2.56
Abrasion (mm) 0.04 0.06 0.07 0.08
Wash fastness 4-5 4-5 4-5 4-5
Pilling rating 3 4 4 4
25. Effects of pH
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Properties
Result
pH
3-4 4-5 5-6 6-7 7-8
Weight loss (%) 0.47 1.21 1.1 0.93 0.86
Abrasion (mm) 0.03 0.08 0.06 0.05 0.04
Wash fastness 3 3 4 3 3
Pilling rating 3 4 4 4 4
Effects of M:L
Properties
Result
M: L Ratio
1:5 1:10 1:15 1:20
Weight loss (%) 1.06 1.12 0.62 0.51
Abrasion (mm) 0.03 0.04 0.06 0.06
Wash fastness 4-5 4-5 4 4
Pilling rating 4 4 3 3
27. Discussions
The best result is obtained at 3% concentration of enzyme.
1:10 M: L ratio gives the best result.
At pH range of 4-5, enzyme shows maximum activity.
At 550C temperature, enzyme activity is maximum.
Mechanical agitation supports enzyme activity.
Depth of shade increases when enzyme treatment is given before
dyeing and the depth decreases when enzyme treatment is given after
dyeing.
Pilling tendency decreases with application of enzyme.
One bath application saves energy, time & cost. But the bio-polishing
effect is not as good as the two bath method.
Wash fastness of the enzyme treated sample before dyeing is very
poor.
Wash fastness of the enzyme treated sample after dyeing is good.
Wash fastness of one bath enzyme treated sample is moderate.
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28. Advantages of bio-polishing
Hairiness fluffs and pills are removed.
Material sticking (the burr effect) is prevented.
Improved handle
Achievement of surface smoothness and a clear structural appearance.
Improved luster.
Material texture relaxation
Increased flexibility and therefore a soft handle even with over end
products and mercerized fabric.
Improved sew ability.
Fast to washing, low pilling tendency, no napping in use, or during care
operation.
Stone wash effect without pumice stone and dyestuff destroying
chemicals.
Poor quality, uneven, napped, knoppy material surface (i.e.) typical second
quality goods are converted into elegant, lustrous, soft, top quality with a fine,
high quality surface appearance.
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30. Material selection:
Bio-processing of
Textiles
9/25/2014
3
0
Enzyme Wash (Denim)
Denim fabric composition: 100% cotton Indigo dye.
Weave: twill 3/1 weave
Ends/inch: 50-51
Picks/inch: 41-42
Surface density (gm/m2): 352-353
Warp linear density (Ne): 6-7
Weft linear density (Ne): 1 1-12
The denim garments have been processed by various
types of enzyme washing and finally softening method as
mentioned below.
31. Method of desizing
Table1: Recipe of desizing
Process parameter Amount
Soda ash 400gm
Caustic soda 400gm
Temperature 700C
Time 15min
Method of enzymatic wash
Table 2:Recipe of enzyme wash
Process parameter Amount
SL enzyme 400gm
Acetic acid 200gm
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Anti back staining
agent
200gm
Temperature 400C
Time 12min
32. Method of softening
Table 3: Recipe of fabric softening
Process parameter Amount
Softener(Cationic) 200gm
Wash 2 times
Temperature Room temp.
Time 5min
After softening the apparel was washed off
for two times.
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33. Changes of fabric specification
after washing
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35. Discussion
Denim trousers were chosen as apparel and after washing,
changes on characteristics of denim trousers has been
observed.
It is concluded that after enzyme wash the denim fabric
changed from harsh to softer. Due to abrasion damage
ends/inch and picks/inch of denim fabric has been increased
and as a result surface density of fabric increased. Again
tensile strength of fabric and seam strength of trousers has
been decreased due to enzyme washing.
Stiffness of denim fabric has been decreased after washing
which results in the increase of denim fabric softness. To hold
the qualities of sewn apparel it is very necessary to observe
the effects of enzyme wash on denim apparels.
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36. Enzyme Inactivation
To prevent any damage of the fabric after the finishing operation
it is very essential that the reaction be terminated at the end of
treatment by enzyme inactivation. If the enzyme is not
inactivated entirely then at the end of the reaction fibres get
damaged and even extreme cases total destruction of the
material may result. The enzyme inactivation is therefore of
great importance from the technical point of view.
There are two distinct process of termination of enzyme:
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1) Hot treatment at 800C for 20 min.
2) By raising the pH to 11–12.
37. Why the industry owner should use Bio-technology
in textile processing?????
It is very useful during waste managing.
Bio-technology helps the quality control.
Used instead of harmful dyestuffs and chemical
treatments.
Prevents the adulteration.
Enhance the low energy type detergents.
Using enzymes in finishing department.
Low temperature operation.
Cost saving.
Eco friendly.
9/25/2014 Bio-processing of Textiles 37
39. References “Bio- Processing Of Textiles” by Abhishek Jadhav & Javed Sheikh.
“Chemistry & Technology of Fabric Preparation & Finishing” by Dr.
Charles Tomasino.
“Applying Enzyme Technology for Sustainable Growth” by Guifang Wu,
Han Kuilderd & Sonja Salmon (Novozymes).
“Bio Polishing of Knit Goods” by Prof. S.K. Laga, Prof. Dr. A.I. Wasif &
Mr. Karan Shah (Textile & Engineering Institute, Ichalkaranji).
“CIRCOT’s Eco-friendly Process for Scouring of Cotton Textile: Bio-scouring”
–Annual article of Central Institute for Research on Cotton
Technology, Mumbai.
“Bio-vision in Textile Wet Processing Industry- Technological
Challenges” by C. Vigneswaran, N. Anbumani and M.
Ananthasubramanian. Journal of Textile & Apperal, Technology &
Management; Volume 7, Issue 1, spring 2011.
“Effects of industrial enzyme wash on denim apparel characteristics” by
M. M. Rahman, Daffodil International University. www.ptj.com.pk ; January
2011.
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40. THANK YOU ALL
9/25/2014 Bio-processing of Textiles 40