This document summarizes a study on solvent recovery using a rotary vacuum evaporator-condenser. The study examined the effect of various operating conditions on the flow rate of condensed solvents recovered. Higher initial volumes, temperatures of the crude mixture, cooling water flow rates, and rotational speeds of the evaporator increased the condensate flow rate. The composition of the initial mixture also impacted the recovery rate when compared to distilled water. Operating conditions that increased heat transfer and evaporation rates, such as higher temperatures and turbulence, improved the solvent recovery performance of the rotary evaporator system.