The document discusses the analysis of phenolic compounds in whisky using HPLC with fluorescence detection. Ten phenolic compounds were separated within 10 minutes using a C18 column and acetonitrile/water mobile phase. Calibration curves for the standards showed good linearity with R2 > 0.999. Three whisky samples were analyzed and showed differences in their phenolic profiles. The method demonstrated effective separation and quantitation of most phenolic compounds in whisky.