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International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 11 | Nov -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 1327
Investigate wear resistance of aluminium 2024 alloy by using pin on
disc tribometer
Ranjeet Aloriya¹, Gaurav Verma2
1 M-Tech student, Department of Mechanical Engineering, ITM University, Gwalior. MP, India.
2 Assistant professor, Department of Mechanical Engineering, ITM University, Gwalior, MP, India.
---------------------------------------------------------------------***---------------------------------------------------------------------
Abstract - The microstructure of a metal may be very
significantly changed by subjecting the material to serve
plastic deformation (SPD) and by using Pin on Disk
Tribometer SPD lead to a substantial refinement in the grain
size to the sub micrometer or even the nanometer range. This
Experiment were conducted on high purity aluminum alloy
2024 investigate the wear resistance of severely plastic
deformed Al 2024 alloy using Pin on Disc Tribometer. In this
initially Al 2024 alloy is solution treated at 520o C and
followed by mechanical testing (such as tensile, micro Vickers
hardness), characterization techniques (such as x ray
diffraction) and then wear testing by the help of pin on disc
tribometer results are described showing this potential for
using this approach in superplastic forming applications at
high strain rates
Key Words: Aluminium Alloy 2024, Solution Heat
Treatment, Pin on Disc, Wear resistance, SPD.
1. INTRODUCTION
Aluminum alloy 2024 is an age hardening and is
strengthened during the heat treatment process.Thealloyis
heated at 493°C (920°F) and then quenched for 10 h at
190°C (370°F) and finally cooled air. The condition is
obtained when this alloy is heated at 493°C followed by cold
water quenched and finallyagingatroomtemperature.After
this process metal to change their micro structure and to
bring out the physical and mechanical characteristics that
make metal more desirable. The size of samples 1cm
diameter and 5 cm long. These samples are obtained rolling
process and optical microscopy and then process of pin on
disc.
1.1 Processes and Equipment’s
The heating of an alloy to a suitable temperature, holding it
at that temperature long enough to cause one or more
constituents to enter into a solid solution. In the case of
Al2024, the major alloy element is copper, and by taking the
part to 520°C for 8 hours. The copper present within the
2024 will dissolve or disperse uniformly throughout the
solid aluminum part.
FIG 1 Phase diagram of Al 2024
After solution treated material were rolled by simple rolling
machine, with rolling speed 8 RPM and roller diameter 110
mm, Rolled sample having 40% thickness reduction. in this
sample performed multiple rolling were done. after rolling
done some testing such as Micro hardness test for
mechanical testing,optical microscopyandX-RAYdiffraction
for microstructural characterization
Micro-vickers hardness test
Micro-vickers hardnesstest wasdoneonQualitestQV-10000
DM hardness machine system, test were done according to
ASTM E384, using diamond indenter with indent diameter
20um. It performed at load of 5 gram and dwell time of 10
sec.
FIG 2 Indent on hardness sample Solution Treated and
40%Room temperature rolling respectively.
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 11 | Nov -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 1328
FIG 3 Micro Hardness Test
Optical microscopy were done Axioskop2 and use Zen
software to make optical image, in this image were taken at
20x, 10x, 5x, to find the grain size by using the image
software.
FIG 4 Optical Microscopy
FIG 5 Optical Microscopy after solution treatment and
after room temperature rolling respectively.
XRD is an analytical technique design to provide more in
depth information about crystalline compounds and
measure thickness of thin filmsandmultilayerstodetermine
atomic arrangement before the XRD analysis we need to
prepare the sample. In this case Sample preparationAl-alloy
is polished with SiC paper uptown 2000 grid size(kerosene)
and then polished with aluminium oxide powder.
After that it is etched by Keller's Reagent
2.5%HNO3 + 1%HF + 95%H2O
1.2 WEAR TESTING OF PIN ON DISC TRIBOMETER
The pin on disc configuration iscommonlyusedforweartest
in laboratories Because of its simple arrangement. However
some phenomena which affect the test results markedly are
always overlooked. The ASTM code for this method is G99.
Wear testing of Pin on disc Tribometer
Test Procedure
Steps to be followed in order to conductthe experimentare:-
 Place the test metal disc on DC motor.
 Place the pin over the disc.
 Run the motor at full speed and ON the rangemeter.
 Place the weights in the pan and observe the wear
pattern on disc made by pin.
 Measure the radius of wear circle made by pin on
the disc.
 Take the highest value of depth of penetration.
2. CALCULATION
Table 1 VHN no. w.r.t. Solution Treatment And Room
Temperature Rolling
Table 2 Crystalline Size of the Al 2024 at both
condition from XRD
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 11 | Nov -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 1329
FIG 6 XRD image of Al 2024 40% room temperature
rolled
FIG 7 XRD at both the conditions
Table 3 Specific wear rate of solution treated
Aluminum
Table 4 Specific wear rate of room temperature rolled
Aluminum
FIG 8 SPECIFIC WEAR RATE VS APPLIED LOAD
FIG 9 DEPTH OF PENETRATION VS APPLIED LOAD
3. CONCLUSIONS
The optical microscopy consideredultra finegrainstructure.
The tensile strength increase. The result was observed that
friction and wear resistance depended on the sliding
velocity. The main evidence was seen by constricting the
wear, friction and dynamic response at 0.25 m/s at this
velocity. The energy level increase with acceleration. The
result is increase hardness, material strength and wear
resistance.
ACKNOWLEDGEMENT
The authors wishes to very thank Asst. Professor Gaurav
Verma Department of mechanical engineer ITM University,
Gwalior MP.
REFERENCES
[1]Yoshinori Iwahashi, Zenji Horita, Minori Nemoti, and
Terence G. Langdon " The process of grain refinement in
equal-channel angular pressing" Acta mater. [46][9] pp.
3317-3331, 1998
[2]Y. Saito, H. Utsunomiya, N. Tsuji and T. Sakai "novel
ultrahigh straining process for bulk materials development
of the accumulative roll bonding process" Acta mater.
[47][2], pp. 579-583, 1999
[3]Yuntian Theodore Zhu *,TerryC.Lowe"Observationsand
issues on mechanisms of grain refinement during ECAP
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 11 | Nov -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 1330
process" Materials ScienceandEngineeringA291(2000)46-
53
[4]Vladimir V. Stolyarov a, Y. Theodore Zhu b,*, Igor V.
Alexandrov a, Terry C. Lowe b Ruslan Z. Valiev a "Influence
of ECAP routes on the microstructure and propertiesofpure
Ti Materials Science and Engineering A299 (2001) 59-67
[5]R.S. Mishra a,*, V.V. Stolyarov b, C. Echer c, R.Z. Valiev b,
A.K. Mukherjee d "Mechanical behavior and superplasticity
of a severe plastic deformation processed nanocrystalline
Ti–6Al–4V alloy Materials Science and Engineering A298
(2001) 44-50
[6]A.P. Zhilyaev a,b,*, B.-K. Kim d, G.V. Nurislamova a, M.D.
Baro b, J.A. Szpunar c, T.G. Langdon d "Orientation imaging
microscopy of ultrafine-grained nickel" Scripta materialia46
(2002) 575-580
[7]Minoru Furukawa a, Zenji Horita b, Minoru Nemoto c,
Terence G. Langdon d,* "The use of severe plastic
deformation for micro structural control" Materials Science
and Engineering A324 (2002) 82-89
[8]Georgy J. Raab a, Ruslan Z. Valiev a, Terry C. Lowe b,
Yuntian T. Zhu b,∗ "Continuous processing of ultrafine
grained Al by ECAP–Conform" Materials Science and
Engineering A 382 (2004) 30-34
[9]M.T. Pe´rez-Prado *,J.A. del Valle,O.A. Ruano "Grain
refinement of Mg–Al–Zn alloys via accumulative roll
bonding" Scripta Materialia 51 (2004) 1093-1097
[10]H.B. Bhaskar, Abdul Sharief "Dry slidingwearbehaviour
of Al 2024 Alloy-Beryl particulate metal matrix composites"
ICCOMIM 2012

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Investigate Wear Resistance of Aluminium 2024 Alloy by using Pin on Disc Tribometer

  • 1. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 11 | Nov -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 1327 Investigate wear resistance of aluminium 2024 alloy by using pin on disc tribometer Ranjeet Aloriya¹, Gaurav Verma2 1 M-Tech student, Department of Mechanical Engineering, ITM University, Gwalior. MP, India. 2 Assistant professor, Department of Mechanical Engineering, ITM University, Gwalior, MP, India. ---------------------------------------------------------------------***--------------------------------------------------------------------- Abstract - The microstructure of a metal may be very significantly changed by subjecting the material to serve plastic deformation (SPD) and by using Pin on Disk Tribometer SPD lead to a substantial refinement in the grain size to the sub micrometer or even the nanometer range. This Experiment were conducted on high purity aluminum alloy 2024 investigate the wear resistance of severely plastic deformed Al 2024 alloy using Pin on Disc Tribometer. In this initially Al 2024 alloy is solution treated at 520o C and followed by mechanical testing (such as tensile, micro Vickers hardness), characterization techniques (such as x ray diffraction) and then wear testing by the help of pin on disc tribometer results are described showing this potential for using this approach in superplastic forming applications at high strain rates Key Words: Aluminium Alloy 2024, Solution Heat Treatment, Pin on Disc, Wear resistance, SPD. 1. INTRODUCTION Aluminum alloy 2024 is an age hardening and is strengthened during the heat treatment process.Thealloyis heated at 493°C (920°F) and then quenched for 10 h at 190°C (370°F) and finally cooled air. The condition is obtained when this alloy is heated at 493°C followed by cold water quenched and finallyagingatroomtemperature.After this process metal to change their micro structure and to bring out the physical and mechanical characteristics that make metal more desirable. The size of samples 1cm diameter and 5 cm long. These samples are obtained rolling process and optical microscopy and then process of pin on disc. 1.1 Processes and Equipment’s The heating of an alloy to a suitable temperature, holding it at that temperature long enough to cause one or more constituents to enter into a solid solution. In the case of Al2024, the major alloy element is copper, and by taking the part to 520°C for 8 hours. The copper present within the 2024 will dissolve or disperse uniformly throughout the solid aluminum part. FIG 1 Phase diagram of Al 2024 After solution treated material were rolled by simple rolling machine, with rolling speed 8 RPM and roller diameter 110 mm, Rolled sample having 40% thickness reduction. in this sample performed multiple rolling were done. after rolling done some testing such as Micro hardness test for mechanical testing,optical microscopyandX-RAYdiffraction for microstructural characterization Micro-vickers hardness test Micro-vickers hardnesstest wasdoneonQualitestQV-10000 DM hardness machine system, test were done according to ASTM E384, using diamond indenter with indent diameter 20um. It performed at load of 5 gram and dwell time of 10 sec. FIG 2 Indent on hardness sample Solution Treated and 40%Room temperature rolling respectively.
  • 2. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 11 | Nov -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 1328 FIG 3 Micro Hardness Test Optical microscopy were done Axioskop2 and use Zen software to make optical image, in this image were taken at 20x, 10x, 5x, to find the grain size by using the image software. FIG 4 Optical Microscopy FIG 5 Optical Microscopy after solution treatment and after room temperature rolling respectively. XRD is an analytical technique design to provide more in depth information about crystalline compounds and measure thickness of thin filmsandmultilayerstodetermine atomic arrangement before the XRD analysis we need to prepare the sample. In this case Sample preparationAl-alloy is polished with SiC paper uptown 2000 grid size(kerosene) and then polished with aluminium oxide powder. After that it is etched by Keller's Reagent 2.5%HNO3 + 1%HF + 95%H2O 1.2 WEAR TESTING OF PIN ON DISC TRIBOMETER The pin on disc configuration iscommonlyusedforweartest in laboratories Because of its simple arrangement. However some phenomena which affect the test results markedly are always overlooked. The ASTM code for this method is G99. Wear testing of Pin on disc Tribometer Test Procedure Steps to be followed in order to conductthe experimentare:-  Place the test metal disc on DC motor.  Place the pin over the disc.  Run the motor at full speed and ON the rangemeter.  Place the weights in the pan and observe the wear pattern on disc made by pin.  Measure the radius of wear circle made by pin on the disc.  Take the highest value of depth of penetration. 2. CALCULATION Table 1 VHN no. w.r.t. Solution Treatment And Room Temperature Rolling Table 2 Crystalline Size of the Al 2024 at both condition from XRD
  • 3. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 11 | Nov -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 1329 FIG 6 XRD image of Al 2024 40% room temperature rolled FIG 7 XRD at both the conditions Table 3 Specific wear rate of solution treated Aluminum Table 4 Specific wear rate of room temperature rolled Aluminum FIG 8 SPECIFIC WEAR RATE VS APPLIED LOAD FIG 9 DEPTH OF PENETRATION VS APPLIED LOAD 3. CONCLUSIONS The optical microscopy consideredultra finegrainstructure. The tensile strength increase. The result was observed that friction and wear resistance depended on the sliding velocity. The main evidence was seen by constricting the wear, friction and dynamic response at 0.25 m/s at this velocity. The energy level increase with acceleration. The result is increase hardness, material strength and wear resistance. ACKNOWLEDGEMENT The authors wishes to very thank Asst. Professor Gaurav Verma Department of mechanical engineer ITM University, Gwalior MP. REFERENCES [1]Yoshinori Iwahashi, Zenji Horita, Minori Nemoti, and Terence G. Langdon " The process of grain refinement in equal-channel angular pressing" Acta mater. [46][9] pp. 3317-3331, 1998 [2]Y. Saito, H. Utsunomiya, N. Tsuji and T. Sakai "novel ultrahigh straining process for bulk materials development of the accumulative roll bonding process" Acta mater. [47][2], pp. 579-583, 1999 [3]Yuntian Theodore Zhu *,TerryC.Lowe"Observationsand issues on mechanisms of grain refinement during ECAP
  • 4. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 11 | Nov -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 1330 process" Materials ScienceandEngineeringA291(2000)46- 53 [4]Vladimir V. Stolyarov a, Y. Theodore Zhu b,*, Igor V. Alexandrov a, Terry C. Lowe b Ruslan Z. Valiev a "Influence of ECAP routes on the microstructure and propertiesofpure Ti Materials Science and Engineering A299 (2001) 59-67 [5]R.S. Mishra a,*, V.V. Stolyarov b, C. Echer c, R.Z. Valiev b, A.K. Mukherjee d "Mechanical behavior and superplasticity of a severe plastic deformation processed nanocrystalline Ti–6Al–4V alloy Materials Science and Engineering A298 (2001) 44-50 [6]A.P. Zhilyaev a,b,*, B.-K. Kim d, G.V. Nurislamova a, M.D. Baro b, J.A. Szpunar c, T.G. Langdon d "Orientation imaging microscopy of ultrafine-grained nickel" Scripta materialia46 (2002) 575-580 [7]Minoru Furukawa a, Zenji Horita b, Minoru Nemoto c, Terence G. Langdon d,* "The use of severe plastic deformation for micro structural control" Materials Science and Engineering A324 (2002) 82-89 [8]Georgy J. Raab a, Ruslan Z. Valiev a, Terry C. Lowe b, Yuntian T. Zhu b,∗ "Continuous processing of ultrafine grained Al by ECAP–Conform" Materials Science and Engineering A 382 (2004) 30-34 [9]M.T. Pe´rez-Prado *,J.A. del Valle,O.A. Ruano "Grain refinement of Mg–Al–Zn alloys via accumulative roll bonding" Scripta Materialia 51 (2004) 1093-1097 [10]H.B. Bhaskar, Abdul Sharief "Dry slidingwearbehaviour of Al 2024 Alloy-Beryl particulate metal matrix composites" ICCOMIM 2012