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“EVALUATION OF COMPRESSIVE STRENGTH GEO-POLYMER FOAMED CONCRETE”
1.
International Research Journal
of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 09 Issue: 09 | Sep 2022 www.irjet.net p-ISSN: 2395-0072 © 2022, IRJET | Impact Factor value: 7.529 | ISO 9001:2008 Certified Journal | Page 239 “EVALUATION OF COMPRESSIVE STRENGTH GEO-POLYMER FOAMED CONCRETE” ASHUTOSH KHARE1, DR ANUDEEP NEMA2 1PG Student, Department of Civil Engineering Eklavya University, Damoh M. P, India 2Associate Professor, Department of Civil Engineering, Eklavya University, Damoh M. P, India ---------------------------------------------------------------------***--------------------------------------------------------------------- Abstract - Foamed concrete isthefuturecommercial material in construction industry due to its light weight nature The physical and mechanical properties of foamed concrete varies from type of mixture and its composition Fly ash and grounded granulated blast furnace slag are industrial waste and generally used as mineral admixture in concrete blend to enhance the property of hardened concrete. In our work we have used fly ash, grounded granulated blast and alkaline solution which acts as an activator is used to develop foamed geopolymer concrete and parameters effecting compressive strength of the foamed concrete were studied. Fly ash isusedas fine aggregate and grounded granulated blast furnace slag helps in improving strength of concrete. Rice husk ash and micro silica are also used to improvethedensityandstrengthof our concrete Compression strength test wasconductedtostudy the mechanical strength of concrete and water absorption test was also carried out. Trial and error approach is used and every mix proportion of materialand quantityoffoam isvaried. Key Words: Fly ash, Foamed Concrete, GGBS, Compressive strength, Geo-polymer Concrete, Rice Husk. 1. INTRODUCTION 1.1 General After water, concrete is the most widely used material by the community and in the construction world, around 15 billion tonnes of concrete is used annually. Ordinary Portland Cement (OPC) is primarily used binder for production of concrete, there is environmental issue for the production of OPC, we burn CaCO3 in kiln at temperature of about 1400 C0 during this lime (Cao) and CO2 is produced by process called calcination. 5CaCO3+SiO2→(3CaO,SiO2)(2CaO,SiO2)+5CO2 In this process CO2 is emittedin the atmospherewhichisa greenhouse gas. India iscontributing7.1%oftotalgreenhouse gas emission Olivier and peters,2018) [24]. Silica containing material is added to the lime which produces an intermediate product called clinker then clinker is cool and small amount of gypsum is added to produce ordinary Portland cement. For production of OPC, fossil fuel generally coal is used which produces CO2 .1 ton of cement produces around 0.95 tonnes CO2 (Davidov its, 2015) [8]. Development in infrastructure leads to rise in demand of cement concrete. Global production of concrete is approximately 15 Billion tonnes and 1 cubic meterperperson per year is already achieved (Gartner, 2004)[10]. India is second largest manufacturer of cement after China and produces around 330 million tonnes cement (Government of India, 2017)[11].We can reduce the GHGs emission by using supplementary cementitious material such as fly ash, blast furnace slag, silica fume etc In India coal based thermal power plant is used for electricity generation, which produces waste material fly ash as by product of burning coal. Fly ash is effectively used for making cement concrete, by using this waste, reduces environmental impactand increases the technical propertyof concrete .Other waste material like rice husk, Ground Granulated Blast Furnace Slag (GGBFS) by productofironand steel making. It can be blended with Portland cement which increase concrete workability, durability, density, and resistance to alkali silica reaction. 2. OBJECTIVES There are two main constituent of geopolymer concrete source material and alkaline solution .Source materialshould be enrich with Silicon (Si),Aluminium (Al).These can be by- product such as fly ash ,GGBFS, Silica fume, rice husk ash ,red mud etc. and can be natural mineral like clay, kaolinite. Selection of material depends upon the availability, cost, type of application, and specific demand of end user .The most commonly used alkaline solution are sodium hydroxide (NaOH), potassium hydroxide (KOH), and sodium silicate (Na2SiO3),potassium silicate (K2O3Si). Slag based geopolymer concrete: In this concrete,blast furnace slag is usedassecondarybinderandsilicafume as primary binder with alkali activator. Rock based geopolymer concrete: The materials used in this concrete are crushed volcanic tuff (type of volcanic rock ejected from volcanic eruption), and mine tailing (left over material from mines) with silica fume and alkali activator. Fly ash based geopolymer concrete: Fly ash from thermal power plants is used as primary binder with furnace slag as secondary binder is used and alkali activator. Recent studies have shown thatthisconcrete can be made by 100% fly ash as binder.
2.
International Research Journal
of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 09 Issue: 09 | Sep 2022 www.irjet.net p-ISSN: 2395-0072 © 2022, IRJET | Impact Factor value: 7.529 | ISO 9001:2008 Certified Journal | Page 240 Ferro-isolatebasedgeopolymerconcrete:Thisconcrete is similar to rock based concrete, but the rocks used have higher iron oxide content. Thus polymer formed in this concrete have iron (Fe) atoms. 3. LITERATURE REVIEW Mohd & Samidi, 1997 Aerated concrete can be classified based on curing method andbasedonporeformationmethod. So based on curing method aerated concrete can be classified as autoclaved aerated concrete (AAC) and non-autoclaved aerated concrete (NAAC). similarly based on pore formation method it can be classified as “gas concrete” and “foamed concrete” Zhang, Liu, Yan, Qin, 2016Weproducedgeopolymerfoamed concrete by entraining air into it. When the air content varies 2 to 6 % the number closed micro pores in the hardened concrete increases space between air void and diameter of void decreases so providing good frost resistance property Rashad, A. (2014) The development of new binders, as an alternative to Portlandcement (PC),byalkalineactivation,isa current researchers interest. Alkali-activated fly ash (AAFA) binder is obtained by a manufacturing process less energy- intensive than PC and involves lower greenhouse gasses emission. Utilizing AAFA system as binder material can limit the consumption of virgin materials (limestone and sand) required in PC manufacture. AAFA belongs to be prospective material in the field of Civil Engineering where it can resist aggressive acids, resist sulfate attacks, resist aggregate alkali reaction, and resist elevated temperatures. Researchers have employed different fibers, chemical admixtures, mineral admixtures, additives and other materials in AAFA system aiming to modify special properties of this system Ali Hansberger et al (2012) Globally, the cement industry accounts for approximately 5 percent of current anthropogenic carbondioxide(CO2)emissions.Worldcement demand and productionareincreasingsignificantly,leadingto an increase in this industry’s absolute energy use and CO2 emissions. Development of new energy-efficiency and CO2 emission- reduction technologies and their deploymentinthe market will be key for the cement industry’s mid- and long- term climate change mitigation strategies. 3. MATERIAL AND METHODS 3.1 Ordinary Portland Cement (OPC) Ordinary Portland cement (OPC) of “ULTRATECH”brandedof grade 53 confirming to IS:12269 was used for our study. It was kept in a dry environment with proper storage facility 53 grade of OPC is used because of its optimum particle size distributionand superiorcrystallizedstructureoffersastrong and durability of structure. It has high early strength as compared to any other grade of cement but because of early strength it does not increase much after 28 days. 3.2 Fly Ash Low Calcium Class F fly ash used for our work. fly ash was obtained from the Spat Thermal power plantat BilaspurIndia and it is used as basic material for making concrete. The physical properties of fly ash are according to IS 1727 (1967). 3.3 Micro silica Micro silica used for this study has been obtained from Nagpur. It is known to be extremely pozzalanic in nature and is used as concrete additive .Addition of micro silica to concrete and geopolymer have shown better packing ability and improve the strength . It is also known as silica fume and is obtained as by product of silicon or ferro-silicon alloy development from electrical arc furnace (EAF). 3.4 Grounded Granulated Blast Furnace Slag GGBFS used in our work was obtained from Uttam Galva,Wardha . It is used in combination with standard Portland cement or other pozzolanic materials to produce durable concretestructures. GGBS based concretesetsslower than concrete made of ordinary Portland cement It reduces hydration and lower temperatures making it easier to avoid cold joints but also effects building schedules where fast setting is required. It also reduces the risk of alkali-silica reaction offers higher chloride intrusion resistance and reduces the risk of corrosion reinforcements and offers greater resistance to sulphate and other chemical attacks 3.5 Rice Husk Ash (RHA) Rice husk ash used in this project is obtained from Nagpur. It is produced from rice milling industry as agro-industrial waste. Burning process and temperature affect the chemical composition of RHA. The amount of silica increases when temperature is increased. RHA contains amorphous and very cellular silica with asurface area of 50-1000 m2/g.Ithasbeen observed that use of RHA reduces heat development, thermal cracking and plastic shrinkage also increases strength of hydrated cement paste which modifies pore structures and blocking the large voids in the pozzolanic reaction. Indian standard IS 456:2000 recommends the useofRHAinconcrete and reinforced concrete but does not specify the quantity which can be used in mixed design. 4. METHODOLOGY 4.1 Preliminary Laboratory Work There is no standard available for making geopolymer foamed concrete, so trial and error method is adopted and numerous sample were made. Identifying the appropriate quantity of foamed, proportion of various filler material and their effect on fresh and hardened properties, air void characteristics of foamed concrete were dealt. There is very few study available on use of geopolymer foamed concrete so
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International Research Journal
of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 09 Issue: 09 | Sep 2022 www.irjet.net p-ISSN: 2395-0072 © 2022, IRJET | Impact Factor value: 7.529 | ISO 9001:2008 Certified Journal | Page 241 present study was focusedonthis.Preliminaryworkwasdone to know the effect of foaming agent on geopolymer foamed concrete as there is very less study available with foam and geopolymer. Proportion of various constituents material like flyash, GGBFS,lime, ricehuskweredeterminedandbehaviour with geopolymersolutionwerestudiedformakingthevarious trial mixes. 4.2 Mixing of Geopolymer Solution At beginning geopolymer solution was prepared 1 day before to give maturity of 24 hour. NaOH is used in pallets form. According to the molarity of geopolymer solution mass of NaOH is selectedand massof Na2SiO3 is selectedaccording to ratio of NaOH: Na2SiO3. Then NaOH and Na2SiO3 is added in water. This solution is kept for one day and next day used for preparation offoamedconcrete.Forsometrialfoamedwas generated in water and added into the solution and for some trial foamed is generated in geopolymer solution. Foam is generated by using hand mixer with rpm ( Revolution per Minute ) 1000 as foam generatormachinewas not available in laboratory. Then foaming agent quantity was selected according to volume of geopolymer solution. Consistency of foam get changed if mixing time is vary, so to get a proper consistency of foam, it is mixed for a specified time so that every time we get same consistency. If we mixed the foam for more time air induced in it will increases, however longer mixing lead to air loss by lowering the air content. After sometrial maturityperiodgiventosolutionwas removed insist of it after adding the constituents solutionwas mixed by hand mixer until it get turned brownish. 4.3 Specimen Preparation Hand mixer was used to produce geopolymer foamed concretein laboratoryas thevolume is less but in commercial practice volume will be high for that rotary drum can be used for production, both the cases mixing procedure will be same. For preparation of specimen first all the dry constituents like fly ash, GGBFS, lime, rice husk, cement and other fine material is collected. Then according to required proportion each is mixed in a container. For getting homogeneous mixed of this dry constituent, it is mixed by hand mixer for 1-2 minute. Geopolymer solution is prepared according to point and according to volume of it foaming agent quantity is mixed in solution. To get required consistency foaming agent is mixed for 10-15 minutes. If foam is generated in water, then it is mixed in dry constituent andmixed for2-3minutesuntilfoam get uniformly distributed, incorporated, which we can notice during mixing. To increase the workability of concretewecan use superplasticizer. After that in dry constituentthisprepare solution is mixed until we get required consistency then concrete mix is poured in moulds of 100*100*100. After 24- hour demoulding was done and concrete cube is kept for curing either oven curing or water curing. 5. EXPERIMENTAL WORK The test results are presented and discussed in this chapter. Each data point for the compressive strength test shown in different graphs or in differenttablescorrespondstothemean compression value. the effect of different parameters on the compressive strength of geopolymer foamed concrete is discussed. Alongwithcompressivestrength,otherparameters like water absorption,andefflorescencevaluesoftheconcrete are also discussed. The parameters considered are as follows: Ratio of sodium hydroxide solution to sodium silicate solution Curing time (oven heating) Molarity of the alkaline solution Mixing time Concentration of foam in mix Effect of GGBS in compressive strength Variation of compressive strength with dry density 6. RESULTS 6.1 Variation of compressive strength with molarity It is observed that compressive strength of geopolymer NAAC is proportional to the molarity of solution and it can be ascertained that molarity is the function of compressive strength. Higher the molarity higher will be the compressive strength. On higher molarity free Si molecules are produced which increasesC-S-H gel is produced which givesstrengthto the concrete. Also workability of concrete decreases as more C-S-H gel is produced. Trials of higher molarity which were cured in oven showed increase in compressive strength after one day ofdemoulding.Insteadoftakingcompressivestrength directly, compressive strength to weight of the cube is taken because strength is directly proportional to weight.
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International Research Journal
of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 09 Issue: 09 | Sep 2022 www.irjet.net p-ISSN: 2395-0072 © 2022, IRJET | Impact Factor value: 7.529 | ISO 9001:2008 Certified Journal | Page 242 6.2 Variation of compressive strength with foamcontent. It is observed from the graphinitially compressive strengthof foam concrete increases uptoa certain point and then decreases the strength of block so optimum content is chosen which is shown in graph 6.3 Trial mixes and compressive strength TRIAL 1 Samp l e no. Ceme nt GGB S Flyas h Foa m Aura+T E A+SP5 0 0+ Molar i ty Age at test Compr es sive strengt h dry dens i ty mea n dens i ty (gm) (gm)(gm)(ml)HVF (ml) (M) (day) (Mpa) (kg/ m3) (kg/ m3) 1 600 600 180015 3+3+3 +3 1 After demou ld ing 1.8 1087 1029 2 3 3.1 1040 3 7 3.8 962 7. FUTURE SCOPE OF WORK In this chapter future scope of work is discussed in line with present work. As we know that cement industry contributes more in greenhouse gas emission, so in present work cement should be completely remove from the GFC As we know that density of GFC depend on quantity of foam content and properties of foam content, in this work protein based foaming agent is used in future work different type of foaming agent with different quantity should be try, this area needs to be explored more. Strength of foamed content depends on GGBFS content so more investigation should be done to find out the optimum quantity of GGBFS and also investigate the potential use of fibre in aerated concrete to overcome the problem of reinforcement. To confirm the long term use of foamed concrete, in future work more test should be done to test the durability. 8. CONCLUSION Aim of this project was to create a geopolymer lightweight foamed concrete alkaline solution as an activator that will address environmental issues and retain their structural properties. Maximum compressive strength 9 MPa was noted at density 1324 Kg/M3 at following percentage of content 10% cement, 20% GGBFS, 60% fly ash, 5% rice husk 5% lime, 2M alkaline solution Efflorescence test was also conduct on GFC, result of this test was Nil. The production process of GFC differ from production process of bricks, blocks in which controlling factor is water/cement ratio whereas GFC is divided into several sub-tasks, main controlling factor was mean target density therefore so there is need to develop design mix strategy for aerated block with air entraining agent. Certain consistency in terms of water content is required for air-entraining otherwise bubbles of foam will reach the surface and escape out or it can be broken during mix phase. The main controlling factor that influences the design mix are GGBFS, Fly ash, foam content, and plasticizers Due to complex nature of air entrainment trial and error method was adopted foamcontentwaschosensuchthatitwill give target density, during trial-and-error procedure it was found that if we generate foam in water it does not give good consistency but when it is mixed with alkaline solution good consistency was found and compressive strength results was also good. Mixing time of foaming agent plays an important role more time mixing produces more foam content so in this test mixing time was kept constant as for as possible It was found that compressive strength of GFC is function of alkaline solution (NaOH) higher the molarity higher compressive strength was observed. Secondaimofwastoanalysetheeffect of properties GGBFS, lime and rice husk on density and compressive strength of GFC. REFERENCES [1] Alaa M. Rashad, A comprehensive overview about the influence of different admixtures and additives on the properties of alkali-activated fly ash, Materials and Design 53 (2014) 1005-1025. [2] Ali Hasanbeigia,n, Lynn Price a, Elina Lin, Emerging energy-efficiency and CO2 emission-reductiontechnologies for ceent and concrete production: A technical review, Renewable and Sustainable Energy Reviews 16 (2012) 6220-6238. [3] Amer Hassan , Mohammed Arif , M. Shariq, Use of geopolymer concrete for a cleaner and sustainable environment- A review of mechanical properties and microstructure, Journal of Cleaner Production223(2019). [4] Curan, Ma.A., 1996. Environmental life cycle assessment. The international journal of Life Cycle Assessment.
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International Research Journal
of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 09 Issue: 09 | Sep 2022 www.irjet.net p-ISSN: 2395-0072 © 2022, IRJET | Impact Factor value: 7.529 | ISO 9001:2008 Certified Journal | Page 243 [5] D.Aldridge (2005) Introduction to foamed concrete: What, Why, How ? [6] D.Falliano, D. De Domenico, G. Ricciardi,E.Gugliandolo, Experimental investigation on the compressivestrengthof foamed concrete: effect of curing conditions, cement type, foaming agent and dry density, Constr. Build. Mater. 165 (2018) 735–749. [7] Davidovits J. Geopolymers, Inorganic polymeric new materials, Journal of Thermal analysis ,Vol 37 (1991), 1633-1656. [8] Davidovits J. 2015, GEOPOLYMER: Chemistry and Application 4th ed. Institute Geopolymer. [9] E.P. Kearsleya, P.J. Wainwright,Theeffectofhighflyash content on the compressive strength offoamed concrete, Cement and Concrete Research 31 (2001)105-112. [10] Gartner E., 2004 Industrially interesting approaches to “low-CO2” cements’. Con. Res. 34,1489-1498 [11] Government of India, 2017. Report on Fly Ash Generation at Coal / Lignite base Power Station and its Utilization in India for Year 2016-2017. [12] Gunasekara, C., Law,D.W.,Setunge,S.,2016.Longterm permeation properties of different fly ash geopolymer concretes. Constr. Build. Mater. 124, 352-362. [13] HuaXu and Jannie S.J. van Deventer , Effect of source materials on geo-polymeirzation,ACSPublicationInd.Eng. Chem. Res. (2003), 42, 8, 1698–1706. [14] HuaXu, J.S.J. Van Deventer, The repolymerization of alumina-silicate minerals, International Journal Mineral . Process.59 _2000.247–266. [15] Klopffer, W., 1997. Life Cycle Assessment: From the beginning to the current state. Environ. Sci. Pollut. Res. 4, 223-228 [16] Kumar, S., Kumar, R. &Mehrotra, S.P. Influence of granulated blast furnace slag on the reaction,structureand properties of fly ash based geopolymer. J Mater Sci45,607– 615(2010). [17] M R Jones, A MaCarthy, Behavior and assessment of foamed concrete for construction application (2005). [18] McCaffrey, R.,2002. Climate Change and Cement Industry. Global Cement and Lime Magazine (Environmental Special Issue): 15-19. [19] McLellan, B.C., Williams, R.P., Lay,bJ., Van Riessen, A., Corder, G.D., 2011. Costs and carbon emission for geopolymer paste in comparison to ordinary Portland Cement. J. Clean. Prod. 19,1080-1090. [20] Mehta, P.K., 2002. Greening of the Concrete Industry for Sustainable Development. ACIConcrete International, 24(7):23-28 [21] MohdRojiSamadi,(1997).Firstreportresearchproject on lightweight concrete, UniversitiTeknologi Malaysia, Skudai, Johor Bahru. [22] N A Lloyd and B V Rangan ,Geopolymer concrete with fly ash , Second international conference on sustainable construction material and technologies , 2010. [23] Nisbet, M.A., Marceau , M.L., Vangeem, M.G., 2002. Environmental Life Cycle Inventory of Portland Cement Concrete, Report 2137a. [24] Olivier JGJ, Schure KM, Peters J,2018Trendsinglobal CO2 and total greenhouse gas emission; 2018 Report. [25] Panesar, D.K., Seto, K. E., Churchill, C. J., 2017. Impact of the selection of functional unit on the life cycle assessment of green concrete. Int. J. Life Cycle Assess. 22,1969-1986
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