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Prof. M.R.Ezhilkumar
Assistant Professor
Department of Civil Engineering
Sri Krishna College of Engineering and Technology
Coimbatore
ezhilkumar@skcet.ac.in
I only feel angry when I see waste.
When I see people throwing away things
we could use. – Mother Teresa
1
17CE413
SOLID AND HAZARDOUS
WASTE MANAGEMENT
1.4 – Sampling Protocols
SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 2
 Purpose of sampling
 Sampling methods
 Characteristics of sampling
 Factors affecting the sampling characterization
1.4 – Sampling Protocols
Learning Outcomes
SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 3
Video Session 1
SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 4
Video Session 2
SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 5
Purpose of sampling
Sampling is Regarded as representative
if the actual substance relations are evaluated,
Correct: The estimation is given with the demanded
accuracy and no systematic errors have been committed.
Reproducible: The statement guarantees for equivalent
results under comparable conditions.
Reliable: The targets are achieved at an acceptable risk
(for instance economic efforts, probability the required
accuracy of the results, consequences of wrong
decisions).
SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 6
Sampling methods
Sampling Protocols
MSW consists of a range of materials that vary in composition depending on,
1. The community and its consumers’ income and lifestyle
2. Degree of industrialization
3. Institutionalization
4. Commercialism
 Based on these variables, several protocols can be adopted to estimate the
MSW composition for location.
SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 7
Sampling methods
Sampling Protocols
In order to compile accurate data, several issues must be addressed,
How to obtain the representative samples of the MSW?
What is the desired sample size?
How many samples are needed to achieve a desired
level of accuracy?
SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 8
Sampling methods
Sampling Protocols
1. Direct sampling
2. Material flow
3. Surveys
4. Multipliers for projecting waste quantities
SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 9
Sampling methods
Sampling Protocols
1. Direct sampling
 Useful on a small scale data collection about MSW composition
 Involves physical sampling and sorting of MSW at the source of generation
 One of the more accurate characterisation method
 To achieve accuracy, samples must be collected randomly from several locations
within the community
 Sampling from Single & Multifamily homes, Commercial and institutional
establishments is encouraged as they act as a local variant inputs to the MSW.
SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 10
Sampling methods
Sampling Protocols
1. Direct sampling
 Other way of direct sampling is studying its characteristics after the MSW arrives
the central collection point (Transfer station or Disposal facility)
 ASTM D5231-92 recommends the sample size of 91-136kg from manual sorting
 One drawback about this methods is due to the occurrence of unexpected
circumstances mislead to the data error
 Delivery of infrequent and exotic waste
 Combined wet & dry waste
 Error in sampling methods
 Expensive when adopted for estimating on a national scale
SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 11
Sampling methods
Sampling Protocols
2. Material Flow
 Another approach of estimation on the waste composition
 Useful for estimating waste stream composition and trends on a regional basis
 EPA uses for the data compilation on waste data for the USA
 The methodology is based on material production data and products in the waste
stream
 For a municipality, the material input and output is recorded and compared
 This is an over simplified method unless proper database is made available in all
process
SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 12
Sampling methods
Sampling Protocols
3. Surveys
 Through this method, questionnaires are distributed to generators of waste
 Most applicable to generators of commercial and industrial wastes and not for
domestic sources
 The questionnaire contains an explicit details concerning the quantity and
composition of waste generated
 But still this method is difficult due to the concerns over the release of company
and proprietary information
SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 13
Sampling methods
Components of a sampling program
The Following defines the Overall objective of the sampling,
1) Selection of parameters
2) Selection of sampling location
3) Time & Frequency of sampling
4) Mode of sampling
5) Selection of sampling equipment
6) Sample Handling & Preservation
SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 14
Characteristics of sampling
Sampling process
 Have Representative samples
 Greater the number of samples more the accuracy
 Greater the variation, more should be the samples
 Continue Sample for a week (8 days)
 Sampling location: Mostly at MSW Facility and not at the Place of generation
(expensive and less valid)
 Cover as many different sectors of the target area as possible
 Selecting samples : Every nth truck/every nth ton of waste /a truck every nth
minutes; Random sampling (crew may be idle/work over time)
SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 15
Characteristics of sampling
Sampling procedure
 Vehicle Unloading
 Sample Selection and Retrieval
 Container Preparation
 Sample Placement
 Sorting
SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 16
Characteristics of sampling
Sampling Collection
► Sample size (100 kg)
► Sampling method
o Coning and quartering
• Reduces variation among samples
• More Sampling time/space
• Need for a front end loader
• Increases sorting time and promotes loss of moisture
• Waste stratification
• Random Grab sample & Composite sample
► Number of samples
SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 17
Characteristics of sampling
Sorting and Weighing
© Sorting areas
© Sorting containers
© Container labelling
© Sorting process
© Weighing samples
© Disposal of samples
© Visual Characterisation of bulky waste
SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 18
Factors influencing the waste characters during sampling
Variability affecting waste sampling
1. Seasonal
2. Regional
3. Household
4. National Economy
SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 19
Factors influencing the waste characters during sampling
Variability affecting waste sampling
1. Seasonal
SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 20
Factors influencing the waste characters during sampling
Variability affecting waste sampling
2. Regional
SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 21
Factors influencing the waste characters during sampling
Variability affecting waste sampling
3. Household
SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 22
Factors influencing the waste characters during sampling
Variability affecting waste sampling
4. National Economy
SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 23
Assessment Time
Review
Question Suggest a sampling protocol for a bio-medical waste for a
proper estimation and quantification of waste composition.

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Characteristics - Municipal Solid Wastes

  • 1. Prof. M.R.Ezhilkumar Assistant Professor Department of Civil Engineering Sri Krishna College of Engineering and Technology Coimbatore ezhilkumar@skcet.ac.in I only feel angry when I see waste. When I see people throwing away things we could use. – Mother Teresa 1 17CE413 SOLID AND HAZARDOUS WASTE MANAGEMENT 1.4 – Sampling Protocols
  • 2. SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 2  Purpose of sampling  Sampling methods  Characteristics of sampling  Factors affecting the sampling characterization 1.4 – Sampling Protocols Learning Outcomes
  • 3. SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 3 Video Session 1
  • 4. SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 4 Video Session 2
  • 5. SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 5 Purpose of sampling Sampling is Regarded as representative if the actual substance relations are evaluated, Correct: The estimation is given with the demanded accuracy and no systematic errors have been committed. Reproducible: The statement guarantees for equivalent results under comparable conditions. Reliable: The targets are achieved at an acceptable risk (for instance economic efforts, probability the required accuracy of the results, consequences of wrong decisions).
  • 6. SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 6 Sampling methods Sampling Protocols MSW consists of a range of materials that vary in composition depending on, 1. The community and its consumers’ income and lifestyle 2. Degree of industrialization 3. Institutionalization 4. Commercialism  Based on these variables, several protocols can be adopted to estimate the MSW composition for location.
  • 7. SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 7 Sampling methods Sampling Protocols In order to compile accurate data, several issues must be addressed, How to obtain the representative samples of the MSW? What is the desired sample size? How many samples are needed to achieve a desired level of accuracy?
  • 8. SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 8 Sampling methods Sampling Protocols 1. Direct sampling 2. Material flow 3. Surveys 4. Multipliers for projecting waste quantities
  • 9. SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 9 Sampling methods Sampling Protocols 1. Direct sampling  Useful on a small scale data collection about MSW composition  Involves physical sampling and sorting of MSW at the source of generation  One of the more accurate characterisation method  To achieve accuracy, samples must be collected randomly from several locations within the community  Sampling from Single & Multifamily homes, Commercial and institutional establishments is encouraged as they act as a local variant inputs to the MSW.
  • 10. SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 10 Sampling methods Sampling Protocols 1. Direct sampling  Other way of direct sampling is studying its characteristics after the MSW arrives the central collection point (Transfer station or Disposal facility)  ASTM D5231-92 recommends the sample size of 91-136kg from manual sorting  One drawback about this methods is due to the occurrence of unexpected circumstances mislead to the data error  Delivery of infrequent and exotic waste  Combined wet & dry waste  Error in sampling methods  Expensive when adopted for estimating on a national scale
  • 11. SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 11 Sampling methods Sampling Protocols 2. Material Flow  Another approach of estimation on the waste composition  Useful for estimating waste stream composition and trends on a regional basis  EPA uses for the data compilation on waste data for the USA  The methodology is based on material production data and products in the waste stream  For a municipality, the material input and output is recorded and compared  This is an over simplified method unless proper database is made available in all process
  • 12. SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 12 Sampling methods Sampling Protocols 3. Surveys  Through this method, questionnaires are distributed to generators of waste  Most applicable to generators of commercial and industrial wastes and not for domestic sources  The questionnaire contains an explicit details concerning the quantity and composition of waste generated  But still this method is difficult due to the concerns over the release of company and proprietary information
  • 13. SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 13 Sampling methods Components of a sampling program The Following defines the Overall objective of the sampling, 1) Selection of parameters 2) Selection of sampling location 3) Time & Frequency of sampling 4) Mode of sampling 5) Selection of sampling equipment 6) Sample Handling & Preservation
  • 14. SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 14 Characteristics of sampling Sampling process  Have Representative samples  Greater the number of samples more the accuracy  Greater the variation, more should be the samples  Continue Sample for a week (8 days)  Sampling location: Mostly at MSW Facility and not at the Place of generation (expensive and less valid)  Cover as many different sectors of the target area as possible  Selecting samples : Every nth truck/every nth ton of waste /a truck every nth minutes; Random sampling (crew may be idle/work over time)
  • 15. SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 15 Characteristics of sampling Sampling procedure  Vehicle Unloading  Sample Selection and Retrieval  Container Preparation  Sample Placement  Sorting
  • 16. SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 16 Characteristics of sampling Sampling Collection ► Sample size (100 kg) ► Sampling method o Coning and quartering • Reduces variation among samples • More Sampling time/space • Need for a front end loader • Increases sorting time and promotes loss of moisture • Waste stratification • Random Grab sample & Composite sample ► Number of samples
  • 17. SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 17 Characteristics of sampling Sorting and Weighing © Sorting areas © Sorting containers © Container labelling © Sorting process © Weighing samples © Disposal of samples © Visual Characterisation of bulky waste
  • 18. SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 18 Factors influencing the waste characters during sampling Variability affecting waste sampling 1. Seasonal 2. Regional 3. Household 4. National Economy
  • 19. SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 19 Factors influencing the waste characters during sampling Variability affecting waste sampling 1. Seasonal
  • 20. SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 20 Factors influencing the waste characters during sampling Variability affecting waste sampling 2. Regional
  • 21. SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 21 Factors influencing the waste characters during sampling Variability affecting waste sampling 3. Household
  • 22. SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 22 Factors influencing the waste characters during sampling Variability affecting waste sampling 4. National Economy
  • 23. SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 23 Assessment Time Review Question Suggest a sampling protocol for a bio-medical waste for a proper estimation and quantification of waste composition.
  • 24. SHWM – Module 1 – Characteristics and Sources of Municipal Solid Wastes  Mr.M.R.Ezhilkumar 24