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Career skills and experience
 Solid State Chemistry
 Colour Chemistry
 Encapsulation
 Polymer Synthesis
 Applications Testing
 Quality Control
 Highly reactive low molecular weight
compound.
 Functional group R-N=C=O
 Common synthesis route is to react amines
with phosgene.
 Used in foams, rubbers and coatings, such as
paints and varnishes to protect wood, cement
etc.
 Global market in 2000 was 4.4m tonnes
 of which 61% methylene diphenyl diisocyanate
(MDI)
 34% toluene diisocyanate
 Isocyanate exposure can affect respiration
 Can also have sensitising effect.
 Residual isocyante is possible within
polyurethane foams
 Nucleophilic reaction with alcohol forms
urethane
 Di-isocyanates can react with diols to form
polyurethane
 Reaction with water forms primary amine and
releases CO2
 Combining these two produces foams with the gas
acting as a blowing agent
 Reaction with an amine forms a urea
 One year industrial placement from university
 First industrial experience
 Learnt business focus
 Focus on converting blue to violet
 Learnt colour terminologies
 Ion exchange process
 Solid State process
 Learnt limitations of solid state chemistry
 Sought consistent quality
 Improved product delivered
 Business decision not to take to pilot plant
 Pigment used in paint formulations
 First position at Ciba/BASF
 Laboratory-based role
 Additional responsibility for EHS
 Included Risk, COSHH, MH Assessments
 Encapsulation of dye lakes
 Colour chemistry
 Lab process
 Cosmetic application
 Scale-up to, and commissioning of, pilot plant
 Material used by customer; product sold in stores
 Dealings with other departments/countries
 Different Global regulations dealt with
 Process creates solid coloured particle
 Involves film forming chemistry and curing of polymer
Phase Change Materials
 Umbrella for several projects
 In-fibre
 Dealings with sales team
 Improved process scaled to full plant scale
 Aminoplast process
 Requires curing of synthesised polymer
 Larger capsules (coating fibres)
 Process scaled to pilot plant
 Teamwork/communication – deliver liquid wax on
time
Phase Change Materials
 Treating fibreboards/insulation
 Acrylic mPCM with replenishable waxes
 Modified conventional process for new active
 Looking to use Green Chemistry
 Inorganic PCM (salt hydrates)
 Encapsulated with natural polymers
 Aminoplast encapsulation of Smartlight
 First project I had overall responsibility for
 Customer was agricultural
 Dealing with different departments/countries
 Lead candidate product approved by customer
 Process scaled to pilot plant
 Laboratory Development Document written
and handed to Process Development
Department
 Design and development of Liquid Dispersion
Polymers for Personal Care
 Polymerisation of acrylic monomers to produce
target polymer properties
 Applications testing of above polymers in hair
care and skin care formulations
 Sensorial testing on hair swatches
 Combing studies on hair swatches
 Testing on skin of HPC department personnel
 Working in a fast paced environment
 Right result first time was essential
 Time critical work
 Limited amount of sample
 Working shifts and overtime
 Supervisor responsibility
 Managing day-to-day work of testers
 Responsibility for performance reviews
 Strong background in business-focussed R&D
 Years of experience in R&D laboratory
 Experience commissioning and operating a
pilot plant facility, scaling up processes
 Experience of working in QC laboratory
 Strong track record of meeting tight deadlines
 Strong focus on EHS, safe running of
laboratories
 Interdepartmental and interdisciplinary
communication is a strength

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Paul Dymond Summary

  • 1. Career skills and experience
  • 2.  Solid State Chemistry  Colour Chemistry  Encapsulation  Polymer Synthesis  Applications Testing  Quality Control
  • 3.  Highly reactive low molecular weight compound.  Functional group R-N=C=O  Common synthesis route is to react amines with phosgene.  Used in foams, rubbers and coatings, such as paints and varnishes to protect wood, cement etc.
  • 4.  Global market in 2000 was 4.4m tonnes  of which 61% methylene diphenyl diisocyanate (MDI)  34% toluene diisocyanate  Isocyanate exposure can affect respiration  Can also have sensitising effect.  Residual isocyante is possible within polyurethane foams
  • 5.  Nucleophilic reaction with alcohol forms urethane  Di-isocyanates can react with diols to form polyurethane  Reaction with water forms primary amine and releases CO2  Combining these two produces foams with the gas acting as a blowing agent  Reaction with an amine forms a urea
  • 6.  One year industrial placement from university  First industrial experience  Learnt business focus  Focus on converting blue to violet  Learnt colour terminologies  Ion exchange process  Solid State process  Learnt limitations of solid state chemistry  Sought consistent quality  Improved product delivered  Business decision not to take to pilot plant  Pigment used in paint formulations
  • 7.  First position at Ciba/BASF  Laboratory-based role  Additional responsibility for EHS  Included Risk, COSHH, MH Assessments
  • 8.  Encapsulation of dye lakes  Colour chemistry  Lab process  Cosmetic application  Scale-up to, and commissioning of, pilot plant  Material used by customer; product sold in stores  Dealings with other departments/countries  Different Global regulations dealt with  Process creates solid coloured particle  Involves film forming chemistry and curing of polymer
  • 9. Phase Change Materials  Umbrella for several projects  In-fibre  Dealings with sales team  Improved process scaled to full plant scale  Aminoplast process  Requires curing of synthesised polymer  Larger capsules (coating fibres)  Process scaled to pilot plant  Teamwork/communication – deliver liquid wax on time
  • 10. Phase Change Materials  Treating fibreboards/insulation  Acrylic mPCM with replenishable waxes  Modified conventional process for new active  Looking to use Green Chemistry  Inorganic PCM (salt hydrates)  Encapsulated with natural polymers
  • 11.  Aminoplast encapsulation of Smartlight  First project I had overall responsibility for  Customer was agricultural  Dealing with different departments/countries  Lead candidate product approved by customer  Process scaled to pilot plant  Laboratory Development Document written and handed to Process Development Department
  • 12.  Design and development of Liquid Dispersion Polymers for Personal Care  Polymerisation of acrylic monomers to produce target polymer properties  Applications testing of above polymers in hair care and skin care formulations  Sensorial testing on hair swatches  Combing studies on hair swatches  Testing on skin of HPC department personnel
  • 13.  Working in a fast paced environment  Right result first time was essential  Time critical work  Limited amount of sample  Working shifts and overtime  Supervisor responsibility  Managing day-to-day work of testers  Responsibility for performance reviews
  • 14.  Strong background in business-focussed R&D  Years of experience in R&D laboratory  Experience commissioning and operating a pilot plant facility, scaling up processes  Experience of working in QC laboratory  Strong track record of meeting tight deadlines  Strong focus on EHS, safe running of laboratories  Interdepartmental and interdisciplinary communication is a strength