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Characterization and Optimization of an Electron
Cyclotron Resonance Ion Source
J.Rabinder Henry
External: Dr. Stefhan Facsko(FZR Rossendorf)
Dip-Ing. Gerald Staats
Professor: Prof. Dr.-Ing. Christian Schäffer
Outlook
• Introduction
Electron Cyclotron Resonance Ion Source (ECRIS)
FZR 14.5 GHz source
• Characterization and Optimization
Plasma –X-ray Spectroscopy
Results
• Beam Emittance
Results
• Summary and outlook
RFce meB ωω == /
Principle of ECRIS
●Electron Cyclotron Resonance Heating
●Electron impact ionization
●Magnetic confinement
Magnetic Field
FZR 14.5 GHz Supernanogan
RF Power
3
RF Power
ECR Zone
Gas Inlet
ECR Source Working Principle
Extraction Electrode
Electron Cyclotron Emission
FC2
Microwave source
BL1
BL2
Target Chamber
BPM2
SL2
FZR 14.5 GHz ECR Source
and Beam Line
4
ECRISSL1BPM1FC1
MD
EL1
EBIT
Multielectrode
extraction
MS1
SL2
RF Power (x)
Pressure (y)
Biased disc (z)
I extracted (Iex)ECRIS
Characterization and Optimization
Max f (Iex) = min (x, y, z)
5
Gas mixing (a)
Plasma Characterization
X-ray Spectroscopy
Ion beam quality
Emittance
Electron Distribution
Charge State Distribution } Source Parameters
x, y, z, a
X-ray Spectroscopy
Electron –Bremsstrahlung Measurement
Ion charge state –Characteristics X-ray Measurement
Germanium Detector Attenuation of Radiation
Be window
Air column
Collimation
Extraction Voltage
6
Analyzing
Magnet
HPGe Detector
ECRIS
Faraday Cup
Beryllium
Window
4000
6000 ElectronicPeak
Counts
Nocollimation
Withcollimation1mm
2000
4000
Counts
US=25KV
US=0V
Bremsstrahlung Measurement
Collimation Extraction Voltage
7
0 50 100 150 200
0
2000
Energy(keV)
0 50 100 150 200
0
2000
E(keV)
0 50 100 150 200
0
2000
4000
6000
8000
10000
25W
50W
75W
100W
125W
175W
200W
250W
Counts
E(keV)
0 50 100 150 200
0
1000
2000
3000
0V
-100V
-200v
-300V
-400V
-600V
Counts
E ( keV)
Photon Distribution Analysis
Power Bias
8
0 50 100 150 200
0
2000
4000
6000
8000
1x10
-5
mbar
2.5x10
-5
mbar
5X10
-5
mbar
4.210
-5
mbar
7.5x10
-5
mbar
1x10
-4
mbar
Counts
E(keV)
0 50 100 150 200
0
2000
4000
6000
8000
Counts
E (keV)
Argon+Oxygen
Argon
Photon Distribution Analysis
Pressure
Gas mixing
Bremsstrahlung Spectra for Varying Power
6000
8000
10000
25W
50W
75W
100W
125W
175W
200W
250W
Counts
Xenon Plasma
Pressure 9.8x10-5mbar
Bias voltage -200 V
9
0 50 100 150 200
0
2000
4000
Counts
E(keV)
4000
6000
8000
1x10
-5
mbar
2.5x10
-5
mbar
5X10
-5
mbar
4.210
-5
mbar
7.5x10
-5
mbar
1x10
-4
mbar
Counts
Bremsstrahlung Spectra for Varying Pressure
Argon Plasma
Power 100 W
Bias voltage -164 V
10
0 50 100 150 200
0
2000
4000 1x10 mbar
Counts
E(keV)
2000
3000
0V
-100V
-200v
-300V
-400V
-600V
Counts
Bremsstrahlung Spectra for Varying Bias
Xenon Plasma
Pressure 9.8x10-5mbar
Power 100 W
11
0 50 100 150 200
0
1000
Counts
E ( keV)
4000
6000
8000
Counts
Argon+Oxygen
Argon
Bremsstrahlung Spectra for Gas Mixing
Power 50 W
Pressure 3.9x 10-5 mbar
Bias voltage of -200V
12
0 50 100 150 200
0
2000
4000
Counts
E (keV)
0 50 100 150 200
0
1
2
3
4
5
6
7
F(E)(RealtiveCounts)
Energy
50W
100W
200W
40 50 60 70 80 90 100 110 120
0,0
0,2
0,4
0,6
0,8
1,0
F(E)RelativeCounts
Energy (keV)
-200V
-300V
-400V
-500V
-600V
Electron Distribution Analysis
Power Bias
130 50 100 150 200 250
0,0
0,2
0,4
0,6
0,8
1,0
1,2
1,4
1,6
F(E)(RelativeCounts)
Energy (keV)
1x10
-4
mbar
5x10
-5
mbar
1X10
-5
mbar
50 100 150 200
0
1
2
F(E)RelativeCounts
Energy (kev)
Argon
Argon+Oxygen
Electron Distribution Analysis
Pressure
Gas mixing
10000
15000
20000
18054ev
17061ev
16401ev
XeLα14104ev
Counts
Characteristics X-ray Measurements
Xenon
Power 120 W
Pressure 9.7 x 10-5 mbar
Bias -200V
14
0 5000 10000 15000 20000 25000 30000 35000 40000
0
5000
XeKβ133384ev
XeKα129779ev
CuKβ18904ev
CuKα18054ev
FeKβ17061ev
FeKα16401ev
Counts
E(eV)
0 10000 20000 30000 40000
0
5000
10000
15000
20000
60W
200W
20W
60W
80W
100W
120W
140W
160W
180W
200W
Counts
0 10000 20000 30000 40000
0
2000
4000
6000
8000
10000
12000
14000
2.7x10
-6
mbar
1.03X
-4
mbar
Kseries
Lseries
1.03x10
-4
mbar
6.5x10
-5
mbar
4.5x10
-5
mbar
3.9x10
-5
mbar
2.4x10
-5
mbar
1.5x10
-5
mbar
4.1x10
-6
mbar
9.8x10
-6
mbar
2.7x10
-6
mbar
Counts
X-ray Spectra
Power Pressure
15
0 10000 20000 30000 40000
E (eV)
0 10000 20000 30000 40000
E(eV)
0 20 40 60 80 100 120 140 160 180 200
0,02
0,04
0,06
0,08
0,10
IntensityRatio
RF-Power(watts)
0,0 2,0x10
-5
4,0x10
-5
6,0x10
-5
8,0x10
-5
1,0x10
-4
1,2x10
-4
0,00
0,01
0,02
0,03
0,04
0,05
0,06
Ik/ILIntensityratio
Pressure mbar
10000
15000
20000
60W
200W
20W
60W
80W
100W
120W
140W
160W
180W
200W
Counts
X-ray Spectra For Varying Power
Xenon plasma
Pressure1.03 x 10-4 mbar
Bias voltage -200 V
16
0 10000 20000 30000 40000
0
5000
10000
Counts
E (eV)
8000
10000
12000
14000
Lseries
1.03x10
-4
mbar
6.5x10
-5
mbar
4.5x10
-5
mbar
3.9x10
-5
mbar
2.4x10
-5
mbar
1.5x10
-5
mbar
4.1x10
-6
mbar
9.8x10
-6
mbar
2.7x10
-6
mbar
Counts
X-ray Spectra For Varying Pressure
Xenon plasma
Power 100 W
Bias voltage -200 V
17
0 10000 20000 30000 40000
0
2000
4000
6000
2.7x10
-6
mbar
1.03X
-4
mbar
Kseries
2.7x10 mbar
Counts
E(eV)
6000
8000
10000
XeLSeries
Counts
-50V
-250V
-400V
-600V 2000
FeKα
CuKα1,2
XeLα1,2
Counts
Xe27%/O20%
Xe27%/O21.50%
Xe27%/O25.20%
X-ray Spectra
Bias Gas mixing
18
0 10000 20000 30000 40000
0
2000
4000 XeKSeries
Counts
E(eV)
0 10000 20000 30000 40000
0
1000
XeKβ
CuKβ
FeKβ
XeLβ
Counts
E(eV)
X-ray Spectra For Varying Bias
6000
8000
10000
XeLSeries
Counts
-50V
-250V
-400V
-600V
Xenon plasma
Pressure1.03 x 10-4 mbar
Power 100 W
19
0 10000 20000 30000 40000
0
2000
4000
XeKSeries
Counts
E (eV )
200 0
FeKα
CuKα1,2
β
XeLα1,2
Counts
X e 27 % /O 2 0%
X e 27 % /O 2 1.50%
X e 27 % /O 2 5.20%
X-ray Spectra For Gas Mixing
Xenon and Oxygen
Pressure 1.6x 10-6 mbar
Power 100 W
Bias voltage -200 V
20
0 10000 2000 0 300 00 4 0000
0
100 0
XeKβ
CuKβ
FeKβ
XeLβ
Counts
E (eV )
60
80
Ar2+
Ar3+
Ar4+
IextracteduA
40W
60W
80W
100W
Mass Spectra For Varying Power
Argon
Pressure 1x 10-4 mbar
Bias voltage -400 V
21
200 250 300 350 400 450 500
0
20
40
Ar9+
Ar8+
Ar7+
Ar5+
Ar6+
IextracteduA
B mT
200 250 300 350 400 450 500
0
20
40
60
80
Ar9+
Ar8+
Ar7+
Ar6+
Ar5+
Ar4+
Ar3+
Ar2+
IextracteduA
B m T
1x10
-5
m bar
1x10
-4
m bar
5x10
-5
m bar
Mass Spectra For Varying Pressure
Argon
Power 100 W
Bias voltage -400 V
22
B m T
2 3 4 5 6 7 8 9
0
20
40
60
80
IuA
Charge State
1x10
-5
mbar
5x10
-5
mbar
1x10
-4
mbar
Charge State Distribution
200 250 300 350 400 450 500
0
10
20
30
40
50
60
70
80
Ar2+
Ar3+
Ar4+
Ar5+
Ar6+
Ar7+
Ar8+
Ar9+
IextracteduA
0V
-400V
-200V
Mass Spectra For Varying Bias
Argon
Power 100 W
Pressure 1x 10-4 mbar
23
B m T
1 2 3 4 5 6 7 8 9 10
0
10
20
30
40
50
60
70
80
IuA
C harge State
Ar
0V
-200V
-400V
Charge State Distribution
α
σ
z
y
x
Current
Profile
d
Emittance calculation
πε /xx
A=
ασε .2 xx
=
( )d/tan 1
σα −
=
24
FC1
SL1
ECRIS
z
d
Pin hole
Einzel lens
Steerer
Measurement Setup
0 2 4 6 8
0,0
0,2
0,4
0,6
0,8
1,0
1,2
FCCurrentmA
Slit Position mm
Slit +X
Slit -X
Slit +Y
Slit -Y
-x
+x
Z
+y
-y
Emittance Measurement
250 2 4 6 8 10 12 14 16
0,00
0,05
0,10
0,15
0,20
0,25
Peak3
Peak 2
Peak1
M1S1
dI/dx
Current Profile
σ =0.24149
σ =0.40832
σ =0.35993
σ =0.4551
RelativeIntensitymA
Slit position mm
Pea
ks
Peak width
2σ mm
Peak half width
σ mm
Divergenc
e Angle α
Phase
space
area
2σ* α
mmrad
1 0.72 0.36 0.147 0.001
2 0.92 0.46 0.188 0.003
3 0.80 0.40 0.163 0.002
Mea
n = 0.81 = 0.40
=0.166
0.002
Summary
Plasma
Two different population of electrons below 30 keV and 100 keV
Stable plasma at nominal power
Unstable plasma at very low pressure
Charge state distribution
Enhanced with bias voltage but no change in plasma characteristics
Ion current extracted depends on gas mixing ratio
Emittance
26
Emittance
Ion beam emittance depends on extraction and beam line elements
Outlook
Longmuir probe measurements
Better emittance with pin hole and CCD camera
Thank you !
27

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Master thesis: Characterization and Optimization of an Electron Cyclotron Resonance Ion Source

  • 1. Characterization and Optimization of an Electron Cyclotron Resonance Ion Source J.Rabinder Henry External: Dr. Stefhan Facsko(FZR Rossendorf) Dip-Ing. Gerald Staats Professor: Prof. Dr.-Ing. Christian Schäffer
  • 2. Outlook • Introduction Electron Cyclotron Resonance Ion Source (ECRIS) FZR 14.5 GHz source • Characterization and Optimization Plasma –X-ray Spectroscopy Results • Beam Emittance Results • Summary and outlook
  • 3. RFce meB ωω == / Principle of ECRIS ●Electron Cyclotron Resonance Heating ●Electron impact ionization ●Magnetic confinement Magnetic Field FZR 14.5 GHz Supernanogan RF Power 3 RF Power ECR Zone Gas Inlet ECR Source Working Principle Extraction Electrode Electron Cyclotron Emission
  • 4. FC2 Microwave source BL1 BL2 Target Chamber BPM2 SL2 FZR 14.5 GHz ECR Source and Beam Line 4 ECRISSL1BPM1FC1 MD EL1 EBIT Multielectrode extraction MS1 SL2
  • 5. RF Power (x) Pressure (y) Biased disc (z) I extracted (Iex)ECRIS Characterization and Optimization Max f (Iex) = min (x, y, z) 5 Gas mixing (a) Plasma Characterization X-ray Spectroscopy Ion beam quality Emittance Electron Distribution Charge State Distribution } Source Parameters x, y, z, a
  • 6. X-ray Spectroscopy Electron –Bremsstrahlung Measurement Ion charge state –Characteristics X-ray Measurement Germanium Detector Attenuation of Radiation Be window Air column Collimation Extraction Voltage 6 Analyzing Magnet HPGe Detector ECRIS Faraday Cup Beryllium Window
  • 7. 4000 6000 ElectronicPeak Counts Nocollimation Withcollimation1mm 2000 4000 Counts US=25KV US=0V Bremsstrahlung Measurement Collimation Extraction Voltage 7 0 50 100 150 200 0 2000 Energy(keV) 0 50 100 150 200 0 2000 E(keV)
  • 8. 0 50 100 150 200 0 2000 4000 6000 8000 10000 25W 50W 75W 100W 125W 175W 200W 250W Counts E(keV) 0 50 100 150 200 0 1000 2000 3000 0V -100V -200v -300V -400V -600V Counts E ( keV) Photon Distribution Analysis Power Bias 8 0 50 100 150 200 0 2000 4000 6000 8000 1x10 -5 mbar 2.5x10 -5 mbar 5X10 -5 mbar 4.210 -5 mbar 7.5x10 -5 mbar 1x10 -4 mbar Counts E(keV) 0 50 100 150 200 0 2000 4000 6000 8000 Counts E (keV) Argon+Oxygen Argon Photon Distribution Analysis Pressure Gas mixing
  • 9. Bremsstrahlung Spectra for Varying Power 6000 8000 10000 25W 50W 75W 100W 125W 175W 200W 250W Counts Xenon Plasma Pressure 9.8x10-5mbar Bias voltage -200 V 9 0 50 100 150 200 0 2000 4000 Counts E(keV)
  • 10. 4000 6000 8000 1x10 -5 mbar 2.5x10 -5 mbar 5X10 -5 mbar 4.210 -5 mbar 7.5x10 -5 mbar 1x10 -4 mbar Counts Bremsstrahlung Spectra for Varying Pressure Argon Plasma Power 100 W Bias voltage -164 V 10 0 50 100 150 200 0 2000 4000 1x10 mbar Counts E(keV)
  • 11. 2000 3000 0V -100V -200v -300V -400V -600V Counts Bremsstrahlung Spectra for Varying Bias Xenon Plasma Pressure 9.8x10-5mbar Power 100 W 11 0 50 100 150 200 0 1000 Counts E ( keV)
  • 12. 4000 6000 8000 Counts Argon+Oxygen Argon Bremsstrahlung Spectra for Gas Mixing Power 50 W Pressure 3.9x 10-5 mbar Bias voltage of -200V 12 0 50 100 150 200 0 2000 4000 Counts E (keV)
  • 13. 0 50 100 150 200 0 1 2 3 4 5 6 7 F(E)(RealtiveCounts) Energy 50W 100W 200W 40 50 60 70 80 90 100 110 120 0,0 0,2 0,4 0,6 0,8 1,0 F(E)RelativeCounts Energy (keV) -200V -300V -400V -500V -600V Electron Distribution Analysis Power Bias 130 50 100 150 200 250 0,0 0,2 0,4 0,6 0,8 1,0 1,2 1,4 1,6 F(E)(RelativeCounts) Energy (keV) 1x10 -4 mbar 5x10 -5 mbar 1X10 -5 mbar 50 100 150 200 0 1 2 F(E)RelativeCounts Energy (kev) Argon Argon+Oxygen Electron Distribution Analysis Pressure Gas mixing
  • 14. 10000 15000 20000 18054ev 17061ev 16401ev XeLα14104ev Counts Characteristics X-ray Measurements Xenon Power 120 W Pressure 9.7 x 10-5 mbar Bias -200V 14 0 5000 10000 15000 20000 25000 30000 35000 40000 0 5000 XeKβ133384ev XeKα129779ev CuKβ18904ev CuKα18054ev FeKβ17061ev FeKα16401ev Counts E(eV)
  • 15. 0 10000 20000 30000 40000 0 5000 10000 15000 20000 60W 200W 20W 60W 80W 100W 120W 140W 160W 180W 200W Counts 0 10000 20000 30000 40000 0 2000 4000 6000 8000 10000 12000 14000 2.7x10 -6 mbar 1.03X -4 mbar Kseries Lseries 1.03x10 -4 mbar 6.5x10 -5 mbar 4.5x10 -5 mbar 3.9x10 -5 mbar 2.4x10 -5 mbar 1.5x10 -5 mbar 4.1x10 -6 mbar 9.8x10 -6 mbar 2.7x10 -6 mbar Counts X-ray Spectra Power Pressure 15 0 10000 20000 30000 40000 E (eV) 0 10000 20000 30000 40000 E(eV) 0 20 40 60 80 100 120 140 160 180 200 0,02 0,04 0,06 0,08 0,10 IntensityRatio RF-Power(watts) 0,0 2,0x10 -5 4,0x10 -5 6,0x10 -5 8,0x10 -5 1,0x10 -4 1,2x10 -4 0,00 0,01 0,02 0,03 0,04 0,05 0,06 Ik/ILIntensityratio Pressure mbar
  • 16. 10000 15000 20000 60W 200W 20W 60W 80W 100W 120W 140W 160W 180W 200W Counts X-ray Spectra For Varying Power Xenon plasma Pressure1.03 x 10-4 mbar Bias voltage -200 V 16 0 10000 20000 30000 40000 0 5000 10000 Counts E (eV)
  • 17. 8000 10000 12000 14000 Lseries 1.03x10 -4 mbar 6.5x10 -5 mbar 4.5x10 -5 mbar 3.9x10 -5 mbar 2.4x10 -5 mbar 1.5x10 -5 mbar 4.1x10 -6 mbar 9.8x10 -6 mbar 2.7x10 -6 mbar Counts X-ray Spectra For Varying Pressure Xenon plasma Power 100 W Bias voltage -200 V 17 0 10000 20000 30000 40000 0 2000 4000 6000 2.7x10 -6 mbar 1.03X -4 mbar Kseries 2.7x10 mbar Counts E(eV)
  • 18. 6000 8000 10000 XeLSeries Counts -50V -250V -400V -600V 2000 FeKα CuKα1,2 XeLα1,2 Counts Xe27%/O20% Xe27%/O21.50% Xe27%/O25.20% X-ray Spectra Bias Gas mixing 18 0 10000 20000 30000 40000 0 2000 4000 XeKSeries Counts E(eV) 0 10000 20000 30000 40000 0 1000 XeKβ CuKβ FeKβ XeLβ Counts E(eV)
  • 19. X-ray Spectra For Varying Bias 6000 8000 10000 XeLSeries Counts -50V -250V -400V -600V Xenon plasma Pressure1.03 x 10-4 mbar Power 100 W 19 0 10000 20000 30000 40000 0 2000 4000 XeKSeries Counts E (eV )
  • 20. 200 0 FeKα CuKα1,2 β XeLα1,2 Counts X e 27 % /O 2 0% X e 27 % /O 2 1.50% X e 27 % /O 2 5.20% X-ray Spectra For Gas Mixing Xenon and Oxygen Pressure 1.6x 10-6 mbar Power 100 W Bias voltage -200 V 20 0 10000 2000 0 300 00 4 0000 0 100 0 XeKβ CuKβ FeKβ XeLβ Counts E (eV )
  • 21. 60 80 Ar2+ Ar3+ Ar4+ IextracteduA 40W 60W 80W 100W Mass Spectra For Varying Power Argon Pressure 1x 10-4 mbar Bias voltage -400 V 21 200 250 300 350 400 450 500 0 20 40 Ar9+ Ar8+ Ar7+ Ar5+ Ar6+ IextracteduA B mT
  • 22. 200 250 300 350 400 450 500 0 20 40 60 80 Ar9+ Ar8+ Ar7+ Ar6+ Ar5+ Ar4+ Ar3+ Ar2+ IextracteduA B m T 1x10 -5 m bar 1x10 -4 m bar 5x10 -5 m bar Mass Spectra For Varying Pressure Argon Power 100 W Bias voltage -400 V 22 B m T 2 3 4 5 6 7 8 9 0 20 40 60 80 IuA Charge State 1x10 -5 mbar 5x10 -5 mbar 1x10 -4 mbar Charge State Distribution
  • 23. 200 250 300 350 400 450 500 0 10 20 30 40 50 60 70 80 Ar2+ Ar3+ Ar4+ Ar5+ Ar6+ Ar7+ Ar8+ Ar9+ IextracteduA 0V -400V -200V Mass Spectra For Varying Bias Argon Power 100 W Pressure 1x 10-4 mbar 23 B m T 1 2 3 4 5 6 7 8 9 10 0 10 20 30 40 50 60 70 80 IuA C harge State Ar 0V -200V -400V Charge State Distribution
  • 24. α σ z y x Current Profile d Emittance calculation πε /xx A= ασε .2 xx = ( )d/tan 1 σα − = 24 FC1 SL1 ECRIS z d Pin hole Einzel lens Steerer Measurement Setup
  • 25. 0 2 4 6 8 0,0 0,2 0,4 0,6 0,8 1,0 1,2 FCCurrentmA Slit Position mm Slit +X Slit -X Slit +Y Slit -Y -x +x Z +y -y Emittance Measurement 250 2 4 6 8 10 12 14 16 0,00 0,05 0,10 0,15 0,20 0,25 Peak3 Peak 2 Peak1 M1S1 dI/dx Current Profile σ =0.24149 σ =0.40832 σ =0.35993 σ =0.4551 RelativeIntensitymA Slit position mm Pea ks Peak width 2σ mm Peak half width σ mm Divergenc e Angle α Phase space area 2σ* α mmrad 1 0.72 0.36 0.147 0.001 2 0.92 0.46 0.188 0.003 3 0.80 0.40 0.163 0.002 Mea n = 0.81 = 0.40 =0.166 0.002
  • 26. Summary Plasma Two different population of electrons below 30 keV and 100 keV Stable plasma at nominal power Unstable plasma at very low pressure Charge state distribution Enhanced with bias voltage but no change in plasma characteristics Ion current extracted depends on gas mixing ratio Emittance 26 Emittance Ion beam emittance depends on extraction and beam line elements Outlook Longmuir probe measurements Better emittance with pin hole and CCD camera