In this study we prepared high density polyethylene (HDPE)/ clay nanocomposites by melt
compounding in a twin screw extruder with rotational speed of 50rpm and the temperatures of the zones are set
to 180-210°C.Different screw configuration have been used to study the effect of screw elements on the
properties of nanocomposites. screw configuration changed from dispersive to distributive type. Cloisite 15A
was used as the filler and weight percent of clay was fixed to 3wt%. Maleated polyethylene grafted polyolefins
supplied from Reliance ltd. A new combination of maleic anhydride grafted polyethylene prepared in our lab
through grafting also taken as compatibilizer.the samples were then characterized by XRD,FTIR and DSC. The
results showed that PE/clay nanocomposites provide better exfoliation with high dispersive screw
configuration. The addition of clay also increased the dispersion and crystallinity of the composite. The clay
particles helped the nanocomposites to develop toruos path that prevent the leakage of gas through it.
Rheological results indicated an increase in the viscosity with the addition of nano clay to PE. wide angle x-ray
diffraction shows the better exfoliation of nano particle clays in the polymer matrix. The mechanical, thermal
and rheological characteristics were measured by using differential scanning calorimetry (DSC), X-ray
diffraction (XRD). XRD indicates that Compatibilizer –nanoclay ratio plays an important role in the exfoliation
of clay in the polyethylene.
Study on Properties of Fresh and Hardened Self Compacting Concrete with Varie...IOSRJMCE
The objective of this paper is to study the properties of fresh and hardened self compacting concrete with varied percentages of metakaolin as mineral admixture (M40 grade). In this study cement is replaced by metakoalin with varied percentages, 20%, 22%, 24%, 26%, 28%, 30%, 32%, 34%, 36% & 38% with a constant packing factor of 1.14. In the present study, B233 GLENIUM super plasticizer is used. As per the European guidelines for Self-compacting concrete, the workability tests such as slump flow test, V-funnel test and L- box, U-box test were carried out in laboratory. The concrete specimens were cured in the tank for 7 and 28 days and tested for determining the compressive strength and split tensile strength and flexural strength respectively. From the study it is observed that workability and mechanical properties such as Compressive strength, Split tensile strength and Flexural strength test increased with increase in metakoalin up to 30% and decreased from 32% to 38%. Non Destructive Test is also performed to assess the quality of concrete in the hardened state.
Study on Properties of Fresh and Hardened Self Compacting Concrete with Varie...IOSRJMCE
The objective of this paper is to study the properties of fresh and hardened self compacting concrete with varied percentages of metakaolin as mineral admixture (M40 grade). In this study cement is replaced by metakoalin with varied percentages, 20%, 22%, 24%, 26%, 28%, 30%, 32%, 34%, 36% & 38% with a constant packing factor of 1.14. In the present study, B233 GLENIUM super plasticizer is used. As per the European guidelines for Self-compacting concrete, the workability tests such as slump flow test, V-funnel test and L- box, U-box test were carried out in laboratory. The concrete specimens were cured in the tank for 7 and 28 days and tested for determining the compressive strength and split tensile strength and flexural strength respectively. From the study it is observed that workability and mechanical properties such as Compressive strength, Split tensile strength and Flexural strength test increased with increase in metakoalin up to 30% and decreased from 32% to 38%. Non Destructive Test is also performed to assess the quality of concrete in the hardened state.
An Experimental Investigation on Strength Characteristics of Concrete with P...IJMER
One of the approaches in improving the durability of concrete is to use blended cement
materials such as fly ash, silica fume, slag and more recently, metakaolin.. This study presents the results
of different mechanical properties of concrete such as compressive strength, split tensile strength and
flexural concrete by partially replacing cement with metakaolin and silica fume. The replacement of
metakaolin is varied from 10%, 15%, 20% and 25% and silica fume from 6%, 8% and 10%. The property
of concrete in fresh state, that is the workability is also studied during the present investigation.The
optimum doses of silica fume and metakaolin in combination were found to be 6% and 15% (by weight)
respectively, when used as part replacement of ordinary Portland cement.
Packing density is new kind of mix design method used to design different types of concrete. To
optimize the particle packing density of concrete, the particles should be selected to fill up the voids between
large particles with smaller particles and so on, in order to obtain a dense and stiff particle structure.
STUDY ON EFFECT OF HYBRID FRP LAMINATES WRAPPED EXTERNALLY (U-WRAP) ON REINFO...IAEME Publication
Recently fibre reinforced polymer composite material namely glass FRP, carbon FRP, basalt FRP etc, is being used as strengthening material. Each technique has its own merits and limitations. Experimental study have been conducted on Reinforced concrete beams which are externally strengthened with GFRP and CFRP as double layer one above the other and it is referred as Hybrid FRP techniques is attained with epoxy resin as adhesive compound. All the ingredients in the beam specimens were maintained with same consistency. A total six beams were cast for the experimental investigation. Out of that three were kept as control specimens and the remaining three were strengthened with double layer of CFRP and GFRP in the U-Wrap pattern. From the overall experimental investigation it can be observed that there is an appreciable increase in ultimate load carrying capacity of the beams strengthened with hybrid FRP laminates.
Effects of Layered Silicate Fillers and Their Surface Treatments in NR/BIIR B...drboon
In this study, the improvement in mechanical properties and abrasion resistance of natural rubber/bromobutyl rubber (NR/BIIR) blends were investigated when using different types of layered silicates as secondary fillers. Moreover, the effects of organophillic surface treatments and their synergistic effects with ENR compatibilizer were also studied. These fillers include montmorillonite clay, kaolin, bleaching clay, and talcum. We found that the secondary fillers could improve the properties of the rubber composites differently. Bleaching clay contributed to a dramatic increase in crosslink density, which could also increase the modulus and hardness of the composite. Montmorillonite clay could provide dramatic increase in abrasion resistance with low compression set, while kaolin was excellent in terms of tensile strength. With organophillic surface treatments, the silane-treated kaolin led to dramatic improvement in all aspects. Conversely, montmorillonite clay treated with octadecylamine contributed to significantly higher modulus and hardness, while losing its abrasion resistance and resilience. These results were opposite for bleaching clay. In this case, even though the composites of silane-treated kaolin obtained improved abrasion resistance and lower compression set, they suffered the drop in crosslink density, modulus, hardness and tensile strength.
Effect of Different Types of Coarse Aggregates on Physical Properties of Most...IOSRJMCE
Aggregates are inert granular materials such as sand, gravel, or crushed stone that, along with water and binder (cement/blended cement), are an essential ingredient in concrete. For a good concrete mix, aggregates need to be clean, hard, strong particles free of absorbed chemicals or coatings of clay and other fine materials that could cause the deterioration of concrete with required shape and sizeAggregates, which account for 60 to 75 percent of the total volume of concrete, are divided into two distinct categories--fine and coarse. The most important property of concrete is its compressive strength. For the purpose of comparison of such compressive strength, three types of coarse aggregates, quartzite, granite, and river gravel, were used. The fine aggregate is normal sand obtained from a borrow pit. This experimental investigation describes the influence of aggregate type and size on the density, compressive, split tensile strength of concrete. To investigate the effect of type and size of aggregate on the compressive strength, density, split tensile strength of concrete an experimental program shall be carried out in GRIET Laboratory. Three different types with three different sizes of course aggregates shall used for developing mix design. The sizes of coarse aggregate shall be 40mm, 20mm, and 12 mm. Ordinary Portland cement is intended to be used as binding material. Different samples shall be tested for compressive strength, split tensile strength and density of concrete. Cylinders of size 150mmx150mm shall be cast in laboratory and tested in testing machines. For each type of coarse aggregate cubes of 150x150mm size to be cast to allow the compressive strength 7 and 28 days. Based on test results, conclusion shall follow
IJERA (International journal of Engineering Research and Applications) is International online, ... peer reviewed journal. For more detail or submit your article, please visit www.ijera.com
Impact test on geopolymer concrete slabseSAT Journals
Abstract
Geopolymer is an eco-friendly binding material alternative for Ordinary Portland Cement (OPC). Geopolymer concrete is
produced by mixing fly ash, GGBS, alkaline solution, fine aggregate and coarse aggregate. Alkaline solution is composed of
NaOH and Na2SiO3 solution. This paper deals with the study of impact resistance capacity of geopolymer concrete slabs
subjected to impact loading. For this study, ten specimens of size 600 mm (length) × 600 mm (width) × 60 mm (thick) were casted
with nine different combination of geopolymer concrete mix using different molar sodium hydroxide solutions and different
percentages of mineral admixtures and a normal concrete slab as control slab. The molarity of NaOH solution used was 8M, 12M
and 16M. Fly ash and GGBS admixtures were used in three different ratios of 100:0, 75:25 and 50:50.The slabs were oven cured
at 600C for 24 hours. These slabs were subjected to impact loading by drop weight test method. All the slabs were tested under a
drop weight of 75.50 N through a guide pipe from a height of 700mm. The results obtained from this study showed that with the
increase in molarity of NaOH solution, the strength characteristics and the impact resistance capacity of the specimen increases.
Also increase in percentage of GGBS content as replacement for Fly ash content increases the impact resistance and overall
strength characteristics of geopolymer concrete. From the test results, geopolymer concrete slab with 16M NaOH solution using
50:50 Fly ash and GGBS content showed higher impact energy absorption capacity as compared other geopolymer mixes.
Key Words: Geopolymer, Molarity, Impact loading, First crack, Ultimate failure etc…
Properties of Glass Fibre Reinforced Geopolymer ConcreteIJMER
International Journal of Modern Engineering Research (IJMER) is Peer reviewed, online Journal. It serves as an international archival forum of scholarly research related to engineering and science education.
International Journal of Modern Engineering Research (IJMER) covers all the fields of engineering and science: Electrical Engineering, Mechanical Engineering, Civil Engineering, Chemical Engineering, Computer Engineering, Agricultural Engineering, Aerospace Engineering, Thermodynamics, Structural Engineering, Control Engineering, Robotics, Mechatronics, Fluid Mechanics, Nanotechnology, Simulators, Web-based Learning, Remote Laboratories, Engineering Design Methods, Education Research, Students' Satisfaction and Motivation, Global Projects, and Assessment…. And many more.
The Journal of MC Square Scientific Research is published by MC Square Publication on the monthly basis. It aims to publish original research papers devoted to wide areas in various disciplines of science and engineering and their applications in industry. This journal is basically devoted to interdisciplinary research in Science, Engineering and Technology, which can improve the technology being used in industry. The real-life problems involve multi-disciplinary knowledge, and thus strong inter-disciplinary approach is the need of the research.
Polymer Concrete Made With Recycled Glass Aggregates, Flyash and MetakaolinIOSR Journals
A novel polymer concrete (PC) was synthesized by mixing epoxy resins and waste glass as
aggregates. In this study, metakaolin (MK) and fly ash (FA) were used as filler and compositions with 0%, 10%
and 15% by weight of recycled glass sand (<2.36 mm) were prepared to investigate the mechanical and
durability properties of the PC. The results indicated that all compositions assessed in this study display high
strength and modulus of elasticity values. MK and FA have a significant effect on the compressive strength, the
flexural strength and the modulus of elasticity of the PC. Moreover, the PC made with recycled glass aggregate,
MK and FA has good chemical resistance for 20% Na2CO3, 10% NaOH, tap water, and sea water. Besides the acceptable chemical resistance, the prepared waste glass PC shows low apparent porosity and low water
absorption
An Experimental Investigation on Strength Characteristics of Concrete with P...IJMER
One of the approaches in improving the durability of concrete is to use blended cement
materials such as fly ash, silica fume, slag and more recently, metakaolin.. This study presents the results
of different mechanical properties of concrete such as compressive strength, split tensile strength and
flexural concrete by partially replacing cement with metakaolin and silica fume. The replacement of
metakaolin is varied from 10%, 15%, 20% and 25% and silica fume from 6%, 8% and 10%. The property
of concrete in fresh state, that is the workability is also studied during the present investigation.The
optimum doses of silica fume and metakaolin in combination were found to be 6% and 15% (by weight)
respectively, when used as part replacement of ordinary Portland cement.
Packing density is new kind of mix design method used to design different types of concrete. To
optimize the particle packing density of concrete, the particles should be selected to fill up the voids between
large particles with smaller particles and so on, in order to obtain a dense and stiff particle structure.
STUDY ON EFFECT OF HYBRID FRP LAMINATES WRAPPED EXTERNALLY (U-WRAP) ON REINFO...IAEME Publication
Recently fibre reinforced polymer composite material namely glass FRP, carbon FRP, basalt FRP etc, is being used as strengthening material. Each technique has its own merits and limitations. Experimental study have been conducted on Reinforced concrete beams which are externally strengthened with GFRP and CFRP as double layer one above the other and it is referred as Hybrid FRP techniques is attained with epoxy resin as adhesive compound. All the ingredients in the beam specimens were maintained with same consistency. A total six beams were cast for the experimental investigation. Out of that three were kept as control specimens and the remaining three were strengthened with double layer of CFRP and GFRP in the U-Wrap pattern. From the overall experimental investigation it can be observed that there is an appreciable increase in ultimate load carrying capacity of the beams strengthened with hybrid FRP laminates.
Effects of Layered Silicate Fillers and Their Surface Treatments in NR/BIIR B...drboon
In this study, the improvement in mechanical properties and abrasion resistance of natural rubber/bromobutyl rubber (NR/BIIR) blends were investigated when using different types of layered silicates as secondary fillers. Moreover, the effects of organophillic surface treatments and their synergistic effects with ENR compatibilizer were also studied. These fillers include montmorillonite clay, kaolin, bleaching clay, and talcum. We found that the secondary fillers could improve the properties of the rubber composites differently. Bleaching clay contributed to a dramatic increase in crosslink density, which could also increase the modulus and hardness of the composite. Montmorillonite clay could provide dramatic increase in abrasion resistance with low compression set, while kaolin was excellent in terms of tensile strength. With organophillic surface treatments, the silane-treated kaolin led to dramatic improvement in all aspects. Conversely, montmorillonite clay treated with octadecylamine contributed to significantly higher modulus and hardness, while losing its abrasion resistance and resilience. These results were opposite for bleaching clay. In this case, even though the composites of silane-treated kaolin obtained improved abrasion resistance and lower compression set, they suffered the drop in crosslink density, modulus, hardness and tensile strength.
Effect of Different Types of Coarse Aggregates on Physical Properties of Most...IOSRJMCE
Aggregates are inert granular materials such as sand, gravel, or crushed stone that, along with water and binder (cement/blended cement), are an essential ingredient in concrete. For a good concrete mix, aggregates need to be clean, hard, strong particles free of absorbed chemicals or coatings of clay and other fine materials that could cause the deterioration of concrete with required shape and sizeAggregates, which account for 60 to 75 percent of the total volume of concrete, are divided into two distinct categories--fine and coarse. The most important property of concrete is its compressive strength. For the purpose of comparison of such compressive strength, three types of coarse aggregates, quartzite, granite, and river gravel, were used. The fine aggregate is normal sand obtained from a borrow pit. This experimental investigation describes the influence of aggregate type and size on the density, compressive, split tensile strength of concrete. To investigate the effect of type and size of aggregate on the compressive strength, density, split tensile strength of concrete an experimental program shall be carried out in GRIET Laboratory. Three different types with three different sizes of course aggregates shall used for developing mix design. The sizes of coarse aggregate shall be 40mm, 20mm, and 12 mm. Ordinary Portland cement is intended to be used as binding material. Different samples shall be tested for compressive strength, split tensile strength and density of concrete. Cylinders of size 150mmx150mm shall be cast in laboratory and tested in testing machines. For each type of coarse aggregate cubes of 150x150mm size to be cast to allow the compressive strength 7 and 28 days. Based on test results, conclusion shall follow
IJERA (International journal of Engineering Research and Applications) is International online, ... peer reviewed journal. For more detail or submit your article, please visit www.ijera.com
Impact test on geopolymer concrete slabseSAT Journals
Abstract
Geopolymer is an eco-friendly binding material alternative for Ordinary Portland Cement (OPC). Geopolymer concrete is
produced by mixing fly ash, GGBS, alkaline solution, fine aggregate and coarse aggregate. Alkaline solution is composed of
NaOH and Na2SiO3 solution. This paper deals with the study of impact resistance capacity of geopolymer concrete slabs
subjected to impact loading. For this study, ten specimens of size 600 mm (length) × 600 mm (width) × 60 mm (thick) were casted
with nine different combination of geopolymer concrete mix using different molar sodium hydroxide solutions and different
percentages of mineral admixtures and a normal concrete slab as control slab. The molarity of NaOH solution used was 8M, 12M
and 16M. Fly ash and GGBS admixtures were used in three different ratios of 100:0, 75:25 and 50:50.The slabs were oven cured
at 600C for 24 hours. These slabs were subjected to impact loading by drop weight test method. All the slabs were tested under a
drop weight of 75.50 N through a guide pipe from a height of 700mm. The results obtained from this study showed that with the
increase in molarity of NaOH solution, the strength characteristics and the impact resistance capacity of the specimen increases.
Also increase in percentage of GGBS content as replacement for Fly ash content increases the impact resistance and overall
strength characteristics of geopolymer concrete. From the test results, geopolymer concrete slab with 16M NaOH solution using
50:50 Fly ash and GGBS content showed higher impact energy absorption capacity as compared other geopolymer mixes.
Key Words: Geopolymer, Molarity, Impact loading, First crack, Ultimate failure etc…
Properties of Glass Fibre Reinforced Geopolymer ConcreteIJMER
International Journal of Modern Engineering Research (IJMER) is Peer reviewed, online Journal. It serves as an international archival forum of scholarly research related to engineering and science education.
International Journal of Modern Engineering Research (IJMER) covers all the fields of engineering and science: Electrical Engineering, Mechanical Engineering, Civil Engineering, Chemical Engineering, Computer Engineering, Agricultural Engineering, Aerospace Engineering, Thermodynamics, Structural Engineering, Control Engineering, Robotics, Mechatronics, Fluid Mechanics, Nanotechnology, Simulators, Web-based Learning, Remote Laboratories, Engineering Design Methods, Education Research, Students' Satisfaction and Motivation, Global Projects, and Assessment…. And many more.
The Journal of MC Square Scientific Research is published by MC Square Publication on the monthly basis. It aims to publish original research papers devoted to wide areas in various disciplines of science and engineering and their applications in industry. This journal is basically devoted to interdisciplinary research in Science, Engineering and Technology, which can improve the technology being used in industry. The real-life problems involve multi-disciplinary knowledge, and thus strong inter-disciplinary approach is the need of the research.
Polymer Concrete Made With Recycled Glass Aggregates, Flyash and MetakaolinIOSR Journals
A novel polymer concrete (PC) was synthesized by mixing epoxy resins and waste glass as
aggregates. In this study, metakaolin (MK) and fly ash (FA) were used as filler and compositions with 0%, 10%
and 15% by weight of recycled glass sand (<2.36 mm) were prepared to investigate the mechanical and
durability properties of the PC. The results indicated that all compositions assessed in this study display high
strength and modulus of elasticity values. MK and FA have a significant effect on the compressive strength, the
flexural strength and the modulus of elasticity of the PC. Moreover, the PC made with recycled glass aggregate,
MK and FA has good chemical resistance for 20% Na2CO3, 10% NaOH, tap water, and sea water. Besides the acceptable chemical resistance, the prepared waste glass PC shows low apparent porosity and low water
absorption
The roles of process parameters on structures and mechanical properties of po...Bambang Afrinaldi
Process parameters are crucial to produce targeted qualities in polypropylene (PP)/clay nanocomposites, due to their roles on the generation of shear and diffusion. Thus, this research aims to observe their effects on structures and properties of PP/clay nanocomposites. Samples were produced by mixing PP, PP grafting maleic anhydride (PP-gMA), and Cloisite 20A at fixed compositions, 88/9/3 wt%, respectively, in an internal mixer with variations on temperatures (210, 220, 230 °C) and speeds (60, 80, 100 rpm). Effect of mixing parameters on nanocomposite structures and properties were investigated from XRD, SEM and flexural properties. The results showed that all samples had intercalated as well as agglomerated structures. Further analysis on XRD and SEM showed that samples produced at
high conditions (230C or 100 rpm) had similar structures. In contrast, low setting sample (210C and 60 rpm), despite its similarity on dispersion level, had longer agglomerates than that of mixed at high settings. Correlated both increase of d-spacing and agglomerates length to flexural properties suggested that modulus was more influenced by dispersion level, while strength
was affected by agglomerates. However, it was worth to note that improvement on dspacing, with availability of long agglomerates might not guarantee modulus and strength improvement due to low interfacial bonding.
Preparation and Characterization of Rubber Composites using Sawdust as Fillerijtsrd
The research work aims to prepare, characterize and apply the vulcanized rubber composites by using sawdust as filler. Sawdust was used as filler in the process of preparation of vulcanized rubber composites. The composite of natural rubber sawdust NR SD was prepared by being replaced the percent ratio 100 0 75 25 50 50 and 25 75 parts weight of natural rubber NR with SD vulcanized for rubbery goods. The surface morphology, elemental analysis and thermal degradation of the prepared NR SD composites were determined by SEM, EDXRF and TG DTA, respectively. The physic mechanical properties such as tensile strength tear strength, elongation at break, hardness and abrasive resistance of NR SD composites were determined by standard rubber testing methods. It was observed that the vulcanized NR SD composites were again determined by soaking in the selected organic solvents and oils ethanol, gasoline, diesel, engine oil, and used engine oil . Being used the sawdust as filler, it not only reduces the cost of production for appliances but also it is likely the supply of the maintenance for Green. Dr. Htoon Nay Oo ""Preparation and Characterization of Rubber Composites using Sawdust as Filler"" Published in International Journal of Trend in Scientific Research and Development (ijtsrd), ISSN: 2456-6470, Volume-3 | Issue-4 , June 2019, URL: https://www.ijtsrd.com/papers/ijtsrd23683.pdf
Paper URL: https://www.ijtsrd.com/chemistry/other/23683/preparation-and-characterization-of--rubber-composites-using-sawdust-as-filler/dr-htoon-nay-oo
Experimental Studies on Sugar Cane Bagasse Ash based GeomaterialsDr. Amarjeet Singh
Use of conventional materials is increasing day by day due to rapid infrastructural growth which increases the cost of materials and increases the cost of construction. Hence utilization of Sugar cane bagasse ash waste materials without causing threat to environment solves the problems of disposal and also can provide economical materials. In this study glass fiber, sugarcane bagasse ash and blast furnace slag were used and cement used for binding purpose. Different mix ratio was prepared to understand the effect of addition of glass fibre on sugar cane bagasse ash based materials under compressive loading. The mix ratio was taken 0.2 to 1.0% for the research work. Blast furnace slag was added 10% to weight of sugar cane bagasse ash. The sample were tested for compressive loading for 7, 14, 28 days respectively. The density is most important parameter of materials. It was observed that the density of materials significantly influences with addition of glass fibre. The density of materials decreases with percentage of glass fiber increase. The density of materials varies between 901.1 kg/m3 to 741.10kg/m3The compressive strength also significantly affected by percentages of glass fibre. The compressive strength ranging 82 kPa to 798 kPa.The compressive strength increases up to certain mix ratio then decrease continuously. The stiffness of sugar cane bagasse ash specimens reinforced with glass fiber at cement 20% more than 15% and 10%.The stiffness also increase with the curing period. The maximum load was observed at 0.6% mix ratio. The stress strain behavior was observed to be nonlinear.
An Examination of Effectuation Dimension as Financing Practice of Small and M...iosrjce
IOSR Journal of Business and Management (IOSR-JBM) is a double blind peer reviewed International Journal that provides rapid publication (within a month) of articles in all areas of business and managemant and its applications. The journal welcomes publications of high quality papers on theoretical developments and practical applications inbusiness and management. Original research papers, state-of-the-art reviews, and high quality technical notes are invited for publications.
Does Goods and Services Tax (GST) Leads to Indian Economic Development?iosrjce
IOSR Journal of Business and Management (IOSR-JBM) is a double blind peer reviewed International Journal that provides rapid publication (within a month) of articles in all areas of business and managemant and its applications. The journal welcomes publications of high quality papers on theoretical developments and practical applications inbusiness and management. Original research papers, state-of-the-art reviews, and high quality technical notes are invited for publications.
Childhood Factors that influence success in later lifeiosrjce
IOSR Journal of Business and Management (IOSR-JBM) is a double blind peer reviewed International Journal that provides rapid publication (within a month) of articles in all areas of business and managemant and its applications. The journal welcomes publications of high quality papers on theoretical developments and practical applications inbusiness and management. Original research papers, state-of-the-art reviews, and high quality technical notes are invited for publications.
Emotional Intelligence and Work Performance Relationship: A Study on Sales Pe...iosrjce
IOSR Journal of Business and Management (IOSR-JBM) is a double blind peer reviewed International Journal that provides rapid publication (within a month) of articles in all areas of business and managemant and its applications. The journal welcomes publications of high quality papers on theoretical developments and practical applications inbusiness and management. Original research papers, state-of-the-art reviews, and high quality technical notes are invited for publications.
Customer’s Acceptance of Internet Banking in Dubaiiosrjce
IOSR Journal of Business and Management (IOSR-JBM) is a double blind peer reviewed International Journal that provides rapid publication (within a month) of articles in all areas of business and managemant and its applications. The journal welcomes publications of high quality papers on theoretical developments and practical applications inbusiness and management. Original research papers, state-of-the-art reviews, and high quality technical notes are invited for publications.
A Study of Employee Satisfaction relating to Job Security & Working Hours amo...iosrjce
IOSR Journal of Business and Management (IOSR-JBM) is a double blind peer reviewed International Journal that provides rapid publication (within a month) of articles in all areas of business and managemant and its applications. The journal welcomes publications of high quality papers on theoretical developments and practical applications inbusiness and management. Original research papers, state-of-the-art reviews, and high quality technical notes are invited for publications.
Consumer Perspectives on Brand Preference: A Choice Based Model Approachiosrjce
IOSR Journal of Business and Management (IOSR-JBM) is a double blind peer reviewed International Journal that provides rapid publication (within a month) of articles in all areas of business and managemant and its applications. The journal welcomes publications of high quality papers on theoretical developments and practical applications inbusiness and management. Original research papers, state-of-the-art reviews, and high quality technical notes are invited for publications.
Student`S Approach towards Social Network Sitesiosrjce
IOSR Journal of Business and Management (IOSR-JBM) is a double blind peer reviewed International Journal that provides rapid publication (within a month) of articles in all areas of business and managemant and its applications. The journal welcomes publications of high quality papers on theoretical developments and practical applications inbusiness and management. Original research papers, state-of-the-art reviews, and high quality technical notes are invited for publications.
Broadcast Management in Nigeria: The systems approach as an imperativeiosrjce
IOSR Journal of Business and Management (IOSR-JBM) is a double blind peer reviewed International Journal that provides rapid publication (within a month) of articles in all areas of business and managemant and its applications. The journal welcomes publications of high quality papers on theoretical developments and practical applications inbusiness and management. Original research papers, state-of-the-art reviews, and high quality technical notes are invited for publications.
A Study on Retailer’s Perception on Soya Products with Special Reference to T...iosrjce
IOSR Journal of Business and Management (IOSR-JBM) is a double blind peer reviewed International Journal that provides rapid publication (within a month) of articles in all areas of business and managemant and its applications. The journal welcomes publications of high quality papers on theoretical developments and practical applications inbusiness and management. Original research papers, state-of-the-art reviews, and high quality technical notes are invited for publications.
A Study Factors Influence on Organisation Citizenship Behaviour in Corporate ...iosrjce
IOSR Journal of Business and Management (IOSR-JBM) is a double blind peer reviewed International Journal that provides rapid publication (within a month) of articles in all areas of business and managemant and its applications. The journal welcomes publications of high quality papers on theoretical developments and practical applications inbusiness and management. Original research papers, state-of-the-art reviews, and high quality technical notes are invited for publications.
Consumers’ Behaviour on Sony Xperia: A Case Study on Bangladeshiosrjce
IOSR Journal of Business and Management (IOSR-JBM) is a double blind peer reviewed International Journal that provides rapid publication (within a month) of articles in all areas of business and managemant and its applications. The journal welcomes publications of high quality papers on theoretical developments and practical applications inbusiness and management. Original research papers, state-of-the-art reviews, and high quality technical notes are invited for publications.
Design of a Balanced Scorecard on Nonprofit Organizations (Study on Yayasan P...iosrjce
IOSR Journal of Business and Management (IOSR-JBM) is a double blind peer reviewed International Journal that provides rapid publication (within a month) of articles in all areas of business and managemant and its applications. The journal welcomes publications of high quality papers on theoretical developments and practical applications inbusiness and management. Original research papers, state-of-the-art reviews, and high quality technical notes are invited for publications.
Public Sector Reforms and Outsourcing Services in Nigeria: An Empirical Evalu...iosrjce
IOSR Journal of Business and Management (IOSR-JBM) is a double blind peer reviewed International Journal that provides rapid publication (within a month) of articles in all areas of business and managemant and its applications. The journal welcomes publications of high quality papers on theoretical developments and practical applications inbusiness and management. Original research papers, state-of-the-art reviews, and high quality technical notes are invited for publications.
Media Innovations and its Impact on Brand awareness & Considerationiosrjce
IOSR Journal of Business and Management (IOSR-JBM) is a double blind peer reviewed International Journal that provides rapid publication (within a month) of articles in all areas of business and managemant and its applications. The journal welcomes publications of high quality papers on theoretical developments and practical applications inbusiness and management. Original research papers, state-of-the-art reviews, and high quality technical notes are invited for publications.
Customer experience in supermarkets and hypermarkets – A comparative studyiosrjce
IOSR Journal of Business and Management (IOSR-JBM) is a double blind peer reviewed International Journal that provides rapid publication (within a month) of articles in all areas of business and managemant and its applications. The journal welcomes publications of high quality papers on theoretical developments and practical applications inbusiness and management. Original research papers, state-of-the-art reviews, and high quality technical notes are invited for publications.
Social Media and Small Businesses: A Combinational Strategic Approach under t...iosrjce
IOSR Journal of Business and Management (IOSR-JBM) is a double blind peer reviewed International Journal that provides rapid publication (within a month) of articles in all areas of business and managemant and its applications. The journal welcomes publications of high quality papers on theoretical developments and practical applications inbusiness and management. Original research papers, state-of-the-art reviews, and high quality technical notes are invited for publications.
Secretarial Performance and the Gender Question (A Study of Selected Tertiary...iosrjce
IOSR Journal of Business and Management (IOSR-JBM) is a double blind peer reviewed International Journal that provides rapid publication (within a month) of articles in all areas of business and managemant and its applications. The journal welcomes publications of high quality papers on theoretical developments and practical applications inbusiness and management. Original research papers, state-of-the-art reviews, and high quality technical notes are invited for publications.
Implementation of Quality Management principles at Zimbabwe Open University (...iosrjce
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Effect of Nanoclay on the Structure and Properties of High Density Polyethylene Composites
1. IOSR Journal of Polymer and Textile Engineering (IOSR-JPTE)
e-ISSN: 2348-019X, p-ISSN: 2348-0181, Volume 2, Issue 3 (May - Jun. 2015), PP 06-11
www.iosrjournals.org
DOI: 10.9790/019X-0230511 www.iosrjournals.org 6 | Page
Effect of Nanoclay on the Structure and Properties of High
Density Polyethylene Composites
Vineesh Vishnu1
, R.S.Rajeev2
, M.A.Joseph1
1. Department of Mechanical Engineering, National Institute of Technology Calicut, India
2. Department of Space, Vikram Sarabhai Space Centre, Trivandrum, India.
Abstract: In this study we prepared high density polyethylene (HDPE)/ clay nanocomposites by melt
compounding in a twin screw extruder with rotational speed of 50rpm and the temperatures of the zones are set
to 180-210°C.Different screw configuration have been used to study the effect of screw elements on the
properties of nanocomposites. screw configuration changed from dispersive to distributive type. Cloisite 15A
was used as the filler and weight percent of clay was fixed to 3wt%. Maleated polyethylene grafted polyolefins
supplied from Reliance ltd. A new combination of maleic anhydride grafted polyethylene prepared in our lab
through grafting also taken as compatibilizer.the samples were then characterized by XRD,FTIR and DSC. The
results showed that PE/clay nanocomposites provide better exfoliation with high dispersive screw
configuration. The addition of clay also increased the dispersion and crystallinity of the composite. The clay
particles helped the nanocomposites to develop toruos path that prevent the leakage of gas through it.
Rheological results indicated an increase in the viscosity with the addition of nano clay to PE. wide angle x-ray
diffraction shows the better exfoliation of nano particle clays in the polymer matrix. The mechanical, thermal
and rheological characteristics were measured by using differential scanning calorimetry (DSC), X-ray
diffraction (XRD). XRD indicates that Compatibilizer –nanoclay ratio plays an important role in the exfoliation
of clay in the polyethylene.
Keywords – nanocomposites, Cloisite 15A, Maleated polyethylene grafted polyolefins, HDPE.
I. Introduction
Nanocomposites of polyolefin (PO) with nanoscale layered silicates have been studied by many researchers,
scientifically and technologically, because these materials offer markedly improved properties as compared to
the conventional polymer composites(1-7). Polymer–clay nanocomposites are emerging as a class of advanced
engineering materials. Several key properties, such as strength and permeation, can be improved by adding a
small amount of clay into the polymeric matrix [8,9]. The properties of polymer–clay nanocomposites depend
on the degree of clay dispersion or on the extent of delamination of the individual clay layers in the polymeric
matrix [10]. The clay layer is hydrophilic in nature and can be converted to organoclay to promote the wetting
of the polymermolecule onto the clay surface [11,12]. By properly controlling the surface properties of the
organoclay, various degrees of organoclay dispersion can be achieved to give: (a) conventional composites, (b)
intercalated nanocomposites, (c) intercalated-exfoliated nanocomposites and (d) exfoliated nanocomposites [12].
The clay’s surface properties can be modified in various ways. One can use clay with a different layer charge
density, control the surfactant surface coverage or vary the kind of intercalated surfactant [13–15].
The packaging industry plays a significant role in a nation economic development; thus, its improvement can
help the economic growth by increasing the efficiency of food marketing and other products, and by adding
value to exports, for example. In this context, nanocomposites, a new class of materials, have a fundamental role
in this improvement, because they have better mechanical, thermal and barrier properties than the pure polymer.
The nanocomposites are characterized by the use of a reinforcement agent with nano dimensions, which is
added in small quantities compared to the traditional composites.
II. Materials and Methods
2.1 Screw Elements and Configuration
The screw configuration used for the extrusion of nanoclay reinforced HDPE composites are shown in
figure1. Two types of screw configurations were used one was dispersive and changed to distributive.
2. Effect Of Nanoclay On The Structure And Properties Of High Density Polyethylene Composites
DOI: 10.9790/019X-0230511 www.iosrjournals.org 7 | Page
Fig.1.Screw Configuration
2.1 Materials
A HDPE (film blowing grade), L60075 from Reliance pvt.ltd. with melt flow index of 8 g/10 min (190 °C,
2.16 kg), weight average molecular weight, Mw, of 420,907 g/mol and molecular weight distribution of 20.89
was chosen as matrix. Two grade of HDPE grafted with maleic anhydride (1%), PEMA, trade name Polybond
3009,Optim,and Fusabond Dupont from Reliance, with melt flow index of 2 g/10 min and 1.5g/10min (190 °C,
2.16 kg) and melting temperature of 127°C was used as compatibility agent. The nanoclay was montmorillonite,
MMT, trade name Cloisite15A from Southern Clay, with less than 2% of moisture.
2.2 Mixing Of Materials
The polymer with compatibilizer and nanoclay in the powder form were mixed according to the
combination as follows. Nanoclay in each combination was fixed as 3wt%. the blends were mixed with 5kg
each in an internal mixer with rotational speed of 1500rpm for 10min.all the batches were preheated @100°C
for 8hrs under vacuum condition.
2.3 Grafting of Maleic Anhydride onto Polyethylene
The grafting reaction was carried out in a twin-screw extruder. Before extruding, MAH and DCP were
dissolved in acetone and then mixed with HDPE granules. After volatilizing the acetone, MAH and DCP
adhered onto the granules homogeneously. The temperature profile of the extruder was 140 °C, 160 °C, 180 °C
and 200 °C, and the rotation speed of the screws was 60 rpm. The strips from the extruder were cut into granules
about 4 mm long after cooling in a water bath.
III. Melt Compounding
For each type of nanocomposite, as well as for the neat polymer, the same processing procedure was
applied so that the thermomechanical history of the nanocomposites and that of neat polymers remain similar.
The powders were dry blended and fed in a co-rotating twin-screw extruder, Brabender,Germany.The mixing
was carried out at a temperature distribution of 180– 200 °C, and speed of 100 rpm. The extruded
nanocomposites were pelletized at the die exit. Nanocomposites containing 3wt% clay and different
combination compatibilizer have been prepared.
Table.1 Combination of composites
No Designation Combination Clay (wt%)
1 HDPE 100/0/0 0
2 HDPE-CLAY 97/3 3
3 HDPE-FB-CLAY 94/3/3,82/15/3,88/9/3 3
4 HDPE-OPT-CLAY 94/3/3,82/15/3,88/9/3 3
5 HDPE-FB 1:1,1:5 0
6 HDPE-OPT 1:1,1:5 0
3. Effect Of Nanoclay On The Structure And Properties Of High Density Polyethylene Composites
DOI: 10.9790/019X-0230511 www.iosrjournals.org 8 | Page
IV. Characterization
4.1 FTIR Analysis of Maleic Anhydride
Fig.2 FTIR Peaks of Maleic Anhydride
4.2 XRD Analysis.
Fig.3 shows the XRD patterns (in the range <10˚) of neat 15A and the 15A-included composites. The
primary (001) diffraction of neat 15A was evident, indicating an interlayer spacing of 3.15 nm For the
PENC1:3 and PENC1:5 composites, the (001) diffraction position of 15A hardly changed, while the PENC1:1
exhibited a weaker diffraction. These results suggest that, PNC1:1 gives better exfoliation. The 15A’s (001)
diffraction was still discernible but became much weaker with the inclusion of the two maleated polyolefins.
Fig.3 XRD Pattern
4. Effect Of Nanoclay On The Structure And Properties Of High Density Polyethylene Composites
DOI: 10.9790/019X-0230511 www.iosrjournals.org 9 | Page
4.3 Crystallization Behaviour of Nanocomposites
133.22°C
126.14°C
154.6J/g
-4
-2
0
2
4
6
HeatFlow(W/g)
20 40 60 80 100 120 140 160
Temperature (°C)
Sample: HDPE-NC/FB, 1:1
Size: 4.3000 mg
Method: H-C-Hl
Comment: TACS /31343, N2 atm
DSC
File: C:TADataDSCHDPE-31343-1-1 FB.001
Operator: PBS/PVA
Run Date: 04-Dec-2013 13:36
Instrument: DSC Q20 V24.9 Build 121
Exo Up Universal V4.7A TA Instruments
Fig.4.DSC Curves
133.22°C
126.14°C
154.6J/g
-4
-2
0
2
4
6
HeatFlow(W/g)
20 40 60 80 100 120 140 160
Temperature (°C)
Sample: HDPE-NC/FB, 1:1
Size: 4.3000 mg
Method: H-C-Hl
Comment: TACS /31343, N2 atm
DSC
File: C:TADataDSCHDPE-31343-1-1 FB.001
Operator: PBS/PVA
Run Date: 04-Dec-2013 13:36
Instrument: DSC Q20 V24.9 Build 121
Exo Up Universal V4.7A TA Instruments
Fig.5. DSC Curves
5. Effect Of Nanoclay On The Structure And Properties Of High Density Polyethylene Composites
DOI: 10.9790/019X-0230511 www.iosrjournals.org 10 | Page
DSC measures the crystallinity of the sample and melting point.
Degree of Crystallinity Xc =
∆H=melting enthalpy of the sample
∆Hm= melting enthalpy of 100% crystalline form of PE, value is 293J/g.
X= weight fraction of HDPE in the sample.
For 1:1, Xc=52.7%
For 1:5, Xc= 49%
Increase in crystalinity increases the gas barrier properties.
V. Torque During The Extrusion of Polymer Nanocomposites
Torque developed during the extrusion increased first and decreased with improvement of exfoliation. The
torque remains constant when the clays are sterted to disperse in the polymer matrix.
VI. Conclusion
The XRD analysis ensures the dispersion of clay in the polymer composites. The effect of compatibilizers
and clay ratio is clear from the chart.1:1 ratio gives the most improvement in exfoliation.Crystallinity increses
with addition of nanclay into HDPE DSC curves validates the result. Intercalation or dispersion of HDPE
between the gallery improves the thermal stability and mechanical strength with compatibilizers.
6. Effect Of Nanoclay On The Structure And Properties Of High Density Polyethylene Composites
DOI: 10.9790/019X-0230511 www.iosrjournals.org 11 | Page
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