The study determines the linear absorption coefficients for lead, copper, and aluminum using gamma-rays by measuring the intensity of radiation passing through these materials. Results indicated the coefficients as 0.545 cm-1 for lead, 0.139 cm-1 for copper, and 0.271 cm-1 for aluminum, aligning with standard values. The experimental setup involved various thicknesses of materials and statistical analysis to derive the coefficients through the relationship between radiation intensity and material properties.