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Industrial Campus UTeM
          December 12, 2012




Research Methodology

 Mohd Khairi Bin Mohamed Nor
  Nona Merry Merpati Mitan
Outline

• Part 1: Research process

• Part 2: Writing a research proposal/report




                                               2
Outline



• Part 1: Research process




                             3
What is research?
Research is systematic, because it follows certain steps that are logical in
order. These steps are:

•Understanding the nature of problem to be studied and identifying the
related area of knowledge.
•Reviewing literature to understand how others have approached or dealt
with the problem.
•Collecting data in an organized and controlled manner so as to arrive at
valid decisions.
•Analyzing data appropriate to the problem.
•Drawing conclusions and making generalizations.




                                                                           4
Which of these can be
       classified as research?
• Encik Samad prepared a paper on
  “computer usage in secondary schools”
  after reviewing literature on the subject
  available in his university library and
  called it a piece of research.




                                          5
Which of these can be
       classified as research?
• Encik Muthu says that he has researched
  and completed a document which gives
  information about the age, of his students,
  their SPM results, their parents income and
  distance of their schools from the District
  Office.


                                            6
Which of these can be
       classified as research?
• Encik Lim participated in a workshop on
  curriculum development and prepared
  what he calls, a research report on the
  curriculum for building technicians. He did
  this through a literature survey on the
  subject and by discussing with the
  participants of the workshop.

                                            7
Consider the following case
 which is an example of research
• A general manager of a car producing
  company was concerned with the
  complaints received from the car users
  that the car they produce have some
  problems with rating sound at the dash
  board and the rear passenger seat after
  few thousand kilometers of driving.

                                        8
• He obtained information from the company workers to
  identify the various factors influencing the problem.
• He then formulated the problem and generated
  guesses (hypotheses).
• He constructed a checklist and obtained requisite
  information from a representative sample of cars.
• He analyzed the data thus collected, interpreted the
  results in the light of his hypotheses and reached
  conclusions.

                                                      9
• You will notice in the example above that
  the researcher went through a sequence of
  steps which were in order and thus
  systematic.
• • Secondly, the researcher did not just jump
  at the conclusions, but used a scientific
  method of inquiry in reaching at conclusions.
• • The two important characteristics of
  research are : it is systematic and secondly it
  follows a scientific method of enquiry.       10
Research concepts
• A way of thinking.

• Hunting for facts or truth about a subject.

• Organized scientific investigation to solve
  problems, test hypotheses, develop or invent
  new products.

                                                 11
Research process

• Phase 1: Deciding what to research

• Phase 2: Planning a research study

• Phase 3: Conducting a research study


                                         12
Research Process
                  THE RESEARCH PROCESS
Phase             PHASE I             PHASE II                PHASE III
Main task         DECIDING           PLANNING            UNDERTAKING




                    WHAT                HOW                  COLLECTING



                  (research     (to gather evidence to       (the required
                 questions to    answer the research         information)
                  answer?)             question)
Operational
steps/research              1    2     3    4      5     6      7       8
journey
                                                                             13
Details Research Process
•   Phase I: Deciding what to research

     Step 1 Formulating a research problem

• Phase II: Planning a research study

     Step 2   Conceptualising a research design
     Step 3   Constructing an instrument for data collection
     Step 4   Selecting a sample
     Step 5   Writing a research proposal

• Phase III: Conducting a research study
   Step 6 Collecting data
   Step 7 Processing and displaying data
   Step 8 Writing a research report                            14
Proses Penyelidikan
                            Kenalpasti
                             masalah


                 Kajian
                Literatur


  Hipotesis,
 Objektif dan                    Experimen
    Skop
                                             Penulisan

         Reka Bentuk           Analisis



                                                     15
Interactions with Supervisors
• Relying heavily on our supervisor
  – step by step supervision
• Relying everything on ourselves
  – no interaction with supervisor
• Supervisor provides the initial basic
  knowledge for the student and student
  continue to develop new ideas on the subject
  – then continue regular discussions with
    supervisor to overcome research problems.
                                                16
Supervisors and Students
Role of Supervisors
•   Determine topic and scope.
                                           Role of Students
•   Confirm the research or project        •   Write a research/project proposal
    proposal.                              •   Get relevant literature on the
•   Specify the correct literature to be       research topic
    read by students.                      •   Study and formulate
•   Provide the necessary hardware or          (mathematical eqns., techniques,
    Laboratory apparatus.                      etc.)
•   Verify whether proposed algorithm      •   Develop simulations (write
    or methodology is correct.             •   programs)
•   Determine the results given are        •   Develop hardware (if relevant)
    enough or not.                         •   Carry out experiments
•   Read students thesis and feedback      •   Write a thesis
    the necessary modifications or
    improvement
•   Give the relevant marks and grades.
                                                                                   17
Outline



Part 2: Writing a research proposal/report




                                             18
Writing report …

• Most crucial step.

• Communicate the findings to the readers.

• A badly written report can spoil all your
  hard work you have done.

                                              19
Format umum

  Introduction (Pengenalan)

  Methodology (Kaedah)

  Results (Keputusan)

  Analysis (Analisis)

  Discussion (Perbincangan)

  Conclusion (Kesimpulan)

                              20
Komponen tesis

  1. Awalan
  2. Abstrak dalam bahasa Melayu dan Inggeris
  3. Pendahuluan
     - Pernyataan Masalah
     - Objektif
     - Skop
  4. Kajian Kepustakaan
  5. Metodologi (Bahan dan Kaedah)
  6. Hasil Kajian, Keputusan dan Perbincangan
  7. Kesimpulan
  8. Rujukan
  9. Lampiran


                                                21
Abstract

• Summary highlight of your own research.
• Cover briefly your introduction, objective, methodology
  and conclusion.
• Include implication.
• Passive verbs and past tenses.
• The third person (he, she, they) should not be used.
• No abbreviations.
• Standard nomenclature.
• No citations.

                                                            22
Introduction

• Develop an outline (`chapterisation`).
• Try to make a link for each paragraph.
        • Narrow down your idea.
         • Remember the citation.




                                           23
Objective(s)
• The goals you set out to attain your project.
• Inform a reader of what you want to achieve through your
  project.
• Clearly and specifically.

Objectives should be listed under two headings:
1. Main objectives
2. Subobjectives



                                                       24
A Script for Writing Qualitative Objective(s)




The purpose of this (strategy of inquiry, such as ethnography, case study, or
other type) study is (was? will be?) to (understand? describe? develop?
discover?) the (central phenomenon being studied) for (the participants, such
as the individual, groups, organization) at (research site). At this stage in the
research, the (central phenomenon being studied) will be generally defined
as (provide a general definition).




                                                                               25
A Script for Writing Quantitative Objective(s)



The purpose of this (experiment? survey?) study is (was? will be?) to test
the theory of (theory name) that (compares? relates?) the (independent
variable) to (dependent variable), controlling for (control variables) for
(participants) at (the research site). The independent variable(s) will be
defined as (provide a definition). The dependent variable(s) will be defined
as (provide a definition), and the control and intervening variable(s) will be
defined as (provide a definition).




                                                                            26
Literature Review
• Integral part of the research process and
  make valuable contribution to almost every
  operational step.

•   Time consuming
•   Daunting
•   Frustrating
•   Rewarding
                                               27
Literature Review (2)
  •Functions:
  a. It provides a theoretical background to your study.
  b. It helps you to establish the links between what you are proposing to
  examine and what has already been studied.
  c. It enable you to show how your findings have contributed to the existing
  body of knowledge in your profession. It helps you to integrate you research
  findings into the existing body of knowledge.




                                                                            28
Literature Review (3)
  Help in four ways:
  1.Bring clarity and focus to your research
  problem.
  2.Improving your research methodology.
  3.Broadening your knowledge base in your
  research area.
  4.Enabling you to contextualize your findings.



                                               29
How to review the literature? (4)
  1. Searching the existing literatures in your area
     of study.
  2. Define your idea in as general terms as
     possible by using general sources.
  3. Search through the secondary sources.
  4. Search through the primary sources.
  5. Organize your notes.



                                                   30
Sources (5)

  1. Books
  2. Journals
  3. Internet




                31
Sources (6)

Journals




              32
Internet resources (7)
Online journal
Internet resources (8)

Web Search Engine



Others
Literature Review (Previous studies)
 Table 1-2 The previous studies on the pyrolysis of bromine containing plastics
Samples                           Types of brominated flame retardants            Techniques                            Results                     References

ABS                     Decabromobiphenyl and tetrabromobisphenol-A      Macro pyrolysis                10 ppb of Br dibenzofuran at 400 oC in      R. Luijk and H. A. J.
                                                                                                                nitrogen atmosphere                         Govers (1992)
                                                                                                                                                            [49]

Printed circuit board   Unknown                                          Fixed bed reactor              72.3% of Br in product gas and mainly as    Y. C. Chien, et al.
         wastes                                                                                                HBr and bromobenzene                         (2000) [53]

ABS                     Epoxy type flame retardant                       Pyrolysis at 450 oC with PP    FeC removed bromine compounds in oil.       T. Bhaskar et al.
                                                                                 and ironoxide-carbon                                                       (2002) [54]
                                                                                 composite catalyst


Electronic scrap        Epoxy resin and brominated polystyrene           Pyrolysis GC-MS at 450 oC      1.4-5.2% Br-methane, 0.8-5% Br-             M. Blaszó, et al.
                                                                                 and 600 oC                     phenols, 0.1-1.6 Br2-phenols. 29-          (2002) [55]
                                                                                                                70 (peak area/mass sample) of
                                                                                                                Br2 styrene, 21-106 (peak
                                                                                                                area/sample mass) of Br3 styrene.


ABS                     Epoxy type flame retardant                       Pyrolysis at 450 oC            7120 ppm and 6150 ppm in oil                T. Bhaskar, et al.
                                                                                                                                                            (2003) [56]

ABS                     Epoxy type flame retardant                       Pyrolysis at 450 oC with PE,   1000-4000 ppm bromine in oil                M. Brebu, et al. (2004)
                                                                                 PP, PS, PVC and/or                                                        [21]
                                                                                 PET

HIPS                    DDO-Sb(5)                                        Pyrolysis with calcium         1410 ppm decreased to 490 and 190 ppm       T. Bhaskar et al.
                                                                                 hydroxide-carbon              (or 7 mg to 3 mg and 1 mg)                   (2006) [57]
                                                                                 composite sorbent
                                                                                 with PE, PP, PS,
                                                                                 PVDC and PET

HIPS                    DDO-Sb(5), DDO-Sb(0), DDE-Sb(5)                  Pyrolysis with ammonia         More than 90 wt% of initial bromine in      M. Brebu et al. (2007)
                        And DDE-Sb(0)                                                                          samples could be recovered.                 [45]

                                                                                                                                                                          35
Previous studies
The presence of brominated compounds in the liquid products of pyrolysis is
highly undesirable. Some efforts to debromination of plastics have been done
by Fe-C catalyst [54] and Ca-C sorbent [57] and atmosphere modification with
ammonia [45].

There are a lot of investigations of diantimony trioxide in brominated flame
retardants [44-51] but no report exist on synergistic effect of diantimony trioxide
in bromine containing high impact polystyrene with presence of polyolefins
such as PE, PP and PS.




                                                                                 36
Methodology
• Procedures:
  Clear and concise.
• Equipment/Tools:
  Specification, manufacturer series, capacity
  and software.
• Materials:
  Specify all materials involved in your
  research, amount (if necessary with the
  manufacturer series).                      37
Example of Experimental
       setup
                                      Temperature program

                                               450 0C

                                           5 0C/min
          Materials :
    - Polycarbonate (PC)
     - CD and DVD disks              RT
- Vegetable cooking oil (VCO)




                    Residue: XRD

                                             Gas: GC-TCD
     Liquid: GC-FID,GC-AED, GC-MSD


                                                            38
Example of design process


 Product     Project    Product     Conceptual     Product
Discovery   Planning   Definition     Design     Development



                                                  Product
                                                  Support




                                                               39
Results and Discussion

Methods of communicating and displaying analyzed
data:
1. Text
2. Tables
3. Graphs
4. Statistical measures

• Never fabricate data.
• Validity and reliability of data.
• Consistent (uniform) – Units: measurements; numbering: section/sub-
  sections; referencing.
• All Figures & Tables must be referred to as close as possible in Text.
                                                                           40
Discussion (Text)

  • Should be thematic;

  • follow a logical progression of thought; in order to your methodology.

  • written around various themes of your report;

  • findings should be integrated into the literature citing references – using an
  acceptable system of citation;

  • layout should be attractive and please to the eye.




                                                                                41
Discussion (Tables)
  Tables present large amounts of detailed information in a small space*.
  A table has five parts:
                 Table X.Y: Attitudes towards uranium mining by age

Attitude towards                                    Age of respondent
                                                                                      Total
uranium mining          < 25          25-34             35-44           45-54   55+
Strongly
favourable
Favourable

Uncertain

Unfavourable

Strongly
unfavourable
Total
Source: ……Hypothetical data                    Supplementary notes
                                                                                              42
  The Chicago Manual of Style (1993:21) in Ranjit Kumar, 2011.
Graph
                                10
Volume of liquid product , mL




                                8


                                6


                                4
                                                                                     DVD
                                                                                     VCO
                                2                                                    DVD/VCO exp
                                                                                     DVD/VCO average

                                0
                                     60         120           180              240             300
                                                         Degradation time , min

                                     Figure X.Y. Cumulative volume of liquid product from DVD          43
Statistical measures

  • Use of statistical measures is dependent upon
     the type of data collected,
     your knowledge of statistics,
     the purpose of communicating the findings, and
     the knowledge base in statistics of your readership.




                                                            44
Discussion (Figures)

  - Clear, following the sequencing.
  - Related to text (proper location).




                                         45
Ethical Issue

• Personal disclosure.

• Authenticity.

• Credibility.




                                  46
References

       Consistent (uniform).
       Follow the standard.
      For internet sources, do not forget to put retrieve date.

Four referencing system according to Butcher*:
1.     The short-title system;
2.     The author-date system;
3.     The reference by number system;
4.     The author-number system.




* Butcher in Ranjit Kumar, 2011

                                                                   47
Tips to use grammatical tenses*

Present tense when referring to previously published work.

Past tense when referring to your present results (Normally, we go back & forth
between the Present & Past tenses).

ABSTRACT
Past tense because you described what you did & what you found.

INTRODUCTION/DISCUSSION/CONCLUSION
Present tense if you refer to previously published work.

RESULTS
Past tense if refer to Tabs & Figs (Ideas should be presented in Present tense).


*Kamaruzaman Jusoff, 2012
                                                                                   48
References:

  1.Mohd Noor, M. Jailani. , Mohd Nopiah, Z. and Mohd Ihsan. A. K. A.,
  2004, Kaedah Penyelidikan Kejuruteraan, Malaysia, Thomson.

  2.Kumar, R., 2011, Research Methodology: A step-by-step guide for
  beginners, Singapore, Sage.

  3.Creswell, J. W., Research Design: Qualitative, Quantitative, and Mixed
  Methods Approaches (3rd edn), 2009, USA, Sage.

  4.Jusoff, K., High Impact/IF Journal Writing Workshop: Made Easy.
  AKEPT-KPT/UTHM Writing High Impact Journal Workshop, 26-27
  September 2012, Johor, Malaysia.

  5.Khalid, M. B., Kursus Kaedah Penyelidikan UTM, 26 March 2003,
  UTM, Malaysia.
                                                                        49
50
Problem statement
Objective




                    51
52
Thank you



            53
Types of tables




  test




                  54
Jadual
  Jadual X.X: Peratus Ketumpatan,  untuk sampel

       No. Sampel                           Peratus  (%)




                                                             55
Research
1.   Research: a way of thinking
2.   Research process
3.   Reviewing literature
4.   Formulating research problem
5.   Identifying variable
6.   Constructing hypothesis
7.   Writing a research report

                                    56

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research methodology (fyp)

  • 1. Industrial Campus UTeM December 12, 2012 Research Methodology Mohd Khairi Bin Mohamed Nor Nona Merry Merpati Mitan
  • 2. Outline • Part 1: Research process • Part 2: Writing a research proposal/report 2
  • 3. Outline • Part 1: Research process 3
  • 4. What is research? Research is systematic, because it follows certain steps that are logical in order. These steps are: •Understanding the nature of problem to be studied and identifying the related area of knowledge. •Reviewing literature to understand how others have approached or dealt with the problem. •Collecting data in an organized and controlled manner so as to arrive at valid decisions. •Analyzing data appropriate to the problem. •Drawing conclusions and making generalizations. 4
  • 5. Which of these can be classified as research? • Encik Samad prepared a paper on “computer usage in secondary schools” after reviewing literature on the subject available in his university library and called it a piece of research. 5
  • 6. Which of these can be classified as research? • Encik Muthu says that he has researched and completed a document which gives information about the age, of his students, their SPM results, their parents income and distance of their schools from the District Office. 6
  • 7. Which of these can be classified as research? • Encik Lim participated in a workshop on curriculum development and prepared what he calls, a research report on the curriculum for building technicians. He did this through a literature survey on the subject and by discussing with the participants of the workshop. 7
  • 8. Consider the following case which is an example of research • A general manager of a car producing company was concerned with the complaints received from the car users that the car they produce have some problems with rating sound at the dash board and the rear passenger seat after few thousand kilometers of driving. 8
  • 9. • He obtained information from the company workers to identify the various factors influencing the problem. • He then formulated the problem and generated guesses (hypotheses). • He constructed a checklist and obtained requisite information from a representative sample of cars. • He analyzed the data thus collected, interpreted the results in the light of his hypotheses and reached conclusions. 9
  • 10. • You will notice in the example above that the researcher went through a sequence of steps which were in order and thus systematic. • • Secondly, the researcher did not just jump at the conclusions, but used a scientific method of inquiry in reaching at conclusions. • • The two important characteristics of research are : it is systematic and secondly it follows a scientific method of enquiry. 10
  • 11. Research concepts • A way of thinking. • Hunting for facts or truth about a subject. • Organized scientific investigation to solve problems, test hypotheses, develop or invent new products. 11
  • 12. Research process • Phase 1: Deciding what to research • Phase 2: Planning a research study • Phase 3: Conducting a research study 12
  • 13. Research Process THE RESEARCH PROCESS Phase PHASE I PHASE II PHASE III Main task DECIDING PLANNING UNDERTAKING WHAT HOW COLLECTING (research (to gather evidence to (the required questions to answer the research information) answer?) question) Operational steps/research 1 2 3 4 5 6 7 8 journey 13
  • 14. Details Research Process • Phase I: Deciding what to research Step 1 Formulating a research problem • Phase II: Planning a research study Step 2 Conceptualising a research design Step 3 Constructing an instrument for data collection Step 4 Selecting a sample Step 5 Writing a research proposal • Phase III: Conducting a research study Step 6 Collecting data Step 7 Processing and displaying data Step 8 Writing a research report 14
  • 15. Proses Penyelidikan Kenalpasti masalah Kajian Literatur Hipotesis, Objektif dan Experimen Skop Penulisan Reka Bentuk Analisis 15
  • 16. Interactions with Supervisors • Relying heavily on our supervisor – step by step supervision • Relying everything on ourselves – no interaction with supervisor • Supervisor provides the initial basic knowledge for the student and student continue to develop new ideas on the subject – then continue regular discussions with supervisor to overcome research problems. 16
  • 17. Supervisors and Students Role of Supervisors • Determine topic and scope. Role of Students • Confirm the research or project • Write a research/project proposal proposal. • Get relevant literature on the • Specify the correct literature to be research topic read by students. • Study and formulate • Provide the necessary hardware or (mathematical eqns., techniques, Laboratory apparatus. etc.) • Verify whether proposed algorithm • Develop simulations (write or methodology is correct. • programs) • Determine the results given are • Develop hardware (if relevant) enough or not. • Carry out experiments • Read students thesis and feedback • Write a thesis the necessary modifications or improvement • Give the relevant marks and grades. 17
  • 18. Outline Part 2: Writing a research proposal/report 18
  • 19. Writing report … • Most crucial step. • Communicate the findings to the readers. • A badly written report can spoil all your hard work you have done. 19
  • 20. Format umum Introduction (Pengenalan) Methodology (Kaedah) Results (Keputusan) Analysis (Analisis) Discussion (Perbincangan) Conclusion (Kesimpulan) 20
  • 21. Komponen tesis 1. Awalan 2. Abstrak dalam bahasa Melayu dan Inggeris 3. Pendahuluan - Pernyataan Masalah - Objektif - Skop 4. Kajian Kepustakaan 5. Metodologi (Bahan dan Kaedah) 6. Hasil Kajian, Keputusan dan Perbincangan 7. Kesimpulan 8. Rujukan 9. Lampiran 21
  • 22. Abstract • Summary highlight of your own research. • Cover briefly your introduction, objective, methodology and conclusion. • Include implication. • Passive verbs and past tenses. • The third person (he, she, they) should not be used. • No abbreviations. • Standard nomenclature. • No citations. 22
  • 23. Introduction • Develop an outline (`chapterisation`). • Try to make a link for each paragraph. • Narrow down your idea. • Remember the citation. 23
  • 24. Objective(s) • The goals you set out to attain your project. • Inform a reader of what you want to achieve through your project. • Clearly and specifically. Objectives should be listed under two headings: 1. Main objectives 2. Subobjectives 24
  • 25. A Script for Writing Qualitative Objective(s) The purpose of this (strategy of inquiry, such as ethnography, case study, or other type) study is (was? will be?) to (understand? describe? develop? discover?) the (central phenomenon being studied) for (the participants, such as the individual, groups, organization) at (research site). At this stage in the research, the (central phenomenon being studied) will be generally defined as (provide a general definition). 25
  • 26. A Script for Writing Quantitative Objective(s) The purpose of this (experiment? survey?) study is (was? will be?) to test the theory of (theory name) that (compares? relates?) the (independent variable) to (dependent variable), controlling for (control variables) for (participants) at (the research site). The independent variable(s) will be defined as (provide a definition). The dependent variable(s) will be defined as (provide a definition), and the control and intervening variable(s) will be defined as (provide a definition). 26
  • 27. Literature Review • Integral part of the research process and make valuable contribution to almost every operational step. • Time consuming • Daunting • Frustrating • Rewarding 27
  • 28. Literature Review (2) •Functions: a. It provides a theoretical background to your study. b. It helps you to establish the links between what you are proposing to examine and what has already been studied. c. It enable you to show how your findings have contributed to the existing body of knowledge in your profession. It helps you to integrate you research findings into the existing body of knowledge. 28
  • 29. Literature Review (3) Help in four ways: 1.Bring clarity and focus to your research problem. 2.Improving your research methodology. 3.Broadening your knowledge base in your research area. 4.Enabling you to contextualize your findings. 29
  • 30. How to review the literature? (4) 1. Searching the existing literatures in your area of study. 2. Define your idea in as general terms as possible by using general sources. 3. Search through the secondary sources. 4. Search through the primary sources. 5. Organize your notes. 30
  • 31. Sources (5) 1. Books 2. Journals 3. Internet 31
  • 34. Internet resources (8) Web Search Engine Others
  • 35. Literature Review (Previous studies) Table 1-2 The previous studies on the pyrolysis of bromine containing plastics Samples Types of brominated flame retardants Techniques Results References ABS Decabromobiphenyl and tetrabromobisphenol-A Macro pyrolysis 10 ppb of Br dibenzofuran at 400 oC in R. Luijk and H. A. J. nitrogen atmosphere Govers (1992) [49] Printed circuit board Unknown Fixed bed reactor 72.3% of Br in product gas and mainly as Y. C. Chien, et al. wastes HBr and bromobenzene (2000) [53] ABS Epoxy type flame retardant Pyrolysis at 450 oC with PP FeC removed bromine compounds in oil. T. Bhaskar et al. and ironoxide-carbon (2002) [54] composite catalyst Electronic scrap Epoxy resin and brominated polystyrene Pyrolysis GC-MS at 450 oC 1.4-5.2% Br-methane, 0.8-5% Br- M. Blaszó, et al. and 600 oC phenols, 0.1-1.6 Br2-phenols. 29- (2002) [55] 70 (peak area/mass sample) of Br2 styrene, 21-106 (peak area/sample mass) of Br3 styrene. ABS Epoxy type flame retardant Pyrolysis at 450 oC 7120 ppm and 6150 ppm in oil T. Bhaskar, et al. (2003) [56] ABS Epoxy type flame retardant Pyrolysis at 450 oC with PE, 1000-4000 ppm bromine in oil M. Brebu, et al. (2004) PP, PS, PVC and/or [21] PET HIPS DDO-Sb(5) Pyrolysis with calcium 1410 ppm decreased to 490 and 190 ppm T. Bhaskar et al. hydroxide-carbon (or 7 mg to 3 mg and 1 mg) (2006) [57] composite sorbent with PE, PP, PS, PVDC and PET HIPS DDO-Sb(5), DDO-Sb(0), DDE-Sb(5) Pyrolysis with ammonia More than 90 wt% of initial bromine in M. Brebu et al. (2007) And DDE-Sb(0) samples could be recovered. [45] 35
  • 36. Previous studies The presence of brominated compounds in the liquid products of pyrolysis is highly undesirable. Some efforts to debromination of plastics have been done by Fe-C catalyst [54] and Ca-C sorbent [57] and atmosphere modification with ammonia [45]. There are a lot of investigations of diantimony trioxide in brominated flame retardants [44-51] but no report exist on synergistic effect of diantimony trioxide in bromine containing high impact polystyrene with presence of polyolefins such as PE, PP and PS. 36
  • 37. Methodology • Procedures: Clear and concise. • Equipment/Tools: Specification, manufacturer series, capacity and software. • Materials: Specify all materials involved in your research, amount (if necessary with the manufacturer series). 37
  • 38. Example of Experimental setup Temperature program 450 0C 5 0C/min Materials : - Polycarbonate (PC) - CD and DVD disks RT - Vegetable cooking oil (VCO) Residue: XRD Gas: GC-TCD Liquid: GC-FID,GC-AED, GC-MSD 38
  • 39. Example of design process Product Project Product Conceptual Product Discovery Planning Definition Design Development Product Support 39
  • 40. Results and Discussion Methods of communicating and displaying analyzed data: 1. Text 2. Tables 3. Graphs 4. Statistical measures • Never fabricate data. • Validity and reliability of data. • Consistent (uniform) – Units: measurements; numbering: section/sub- sections; referencing. • All Figures & Tables must be referred to as close as possible in Text. 40
  • 41. Discussion (Text) • Should be thematic; • follow a logical progression of thought; in order to your methodology. • written around various themes of your report; • findings should be integrated into the literature citing references – using an acceptable system of citation; • layout should be attractive and please to the eye. 41
  • 42. Discussion (Tables) Tables present large amounts of detailed information in a small space*. A table has five parts: Table X.Y: Attitudes towards uranium mining by age Attitude towards Age of respondent Total uranium mining < 25 25-34 35-44 45-54 55+ Strongly favourable Favourable Uncertain Unfavourable Strongly unfavourable Total Source: ……Hypothetical data Supplementary notes 42 The Chicago Manual of Style (1993:21) in Ranjit Kumar, 2011.
  • 43. Graph 10 Volume of liquid product , mL 8 6 4 DVD VCO 2 DVD/VCO exp DVD/VCO average 0 60 120 180 240 300 Degradation time , min Figure X.Y. Cumulative volume of liquid product from DVD 43
  • 44. Statistical measures • Use of statistical measures is dependent upon the type of data collected, your knowledge of statistics, the purpose of communicating the findings, and the knowledge base in statistics of your readership. 44
  • 45. Discussion (Figures) - Clear, following the sequencing. - Related to text (proper location). 45
  • 46. Ethical Issue • Personal disclosure. • Authenticity. • Credibility. 46
  • 47. References  Consistent (uniform).  Follow the standard.  For internet sources, do not forget to put retrieve date. Four referencing system according to Butcher*: 1. The short-title system; 2. The author-date system; 3. The reference by number system; 4. The author-number system. * Butcher in Ranjit Kumar, 2011 47
  • 48. Tips to use grammatical tenses* Present tense when referring to previously published work. Past tense when referring to your present results (Normally, we go back & forth between the Present & Past tenses). ABSTRACT Past tense because you described what you did & what you found. INTRODUCTION/DISCUSSION/CONCLUSION Present tense if you refer to previously published work. RESULTS Past tense if refer to Tabs & Figs (Ideas should be presented in Present tense). *Kamaruzaman Jusoff, 2012 48
  • 49. References: 1.Mohd Noor, M. Jailani. , Mohd Nopiah, Z. and Mohd Ihsan. A. K. A., 2004, Kaedah Penyelidikan Kejuruteraan, Malaysia, Thomson. 2.Kumar, R., 2011, Research Methodology: A step-by-step guide for beginners, Singapore, Sage. 3.Creswell, J. W., Research Design: Qualitative, Quantitative, and Mixed Methods Approaches (3rd edn), 2009, USA, Sage. 4.Jusoff, K., High Impact/IF Journal Writing Workshop: Made Easy. AKEPT-KPT/UTHM Writing High Impact Journal Workshop, 26-27 September 2012, Johor, Malaysia. 5.Khalid, M. B., Kursus Kaedah Penyelidikan UTM, 26 March 2003, UTM, Malaysia. 49
  • 50. 50
  • 52. 52
  • 53. Thank you 53
  • 54. Types of tables test 54
  • 55. Jadual Jadual X.X: Peratus Ketumpatan,  untuk sampel No. Sampel  Peratus  (%) 55
  • 56. Research 1. Research: a way of thinking 2. Research process 3. Reviewing literature 4. Formulating research problem 5. Identifying variable 6. Constructing hypothesis 7. Writing a research report 56