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International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 11 | Nov -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 34
A PERFORMANCE EVALUATION OF WARM MIX ASPHALT MIXTURE BY
INCORPORATING SASOBIT ADDITIVE
Uma shanker Gunti1, Javedali M Jalegar2
1. Post graduate Student, Department of Civil Engineering, AVNIET, Ibrahimpatnam, India
2. Assistance Professor, Department of Civil Engineering, AVNIET, Ibrahimpatnam, India
---------------------------------------------------------------------***---------------------------------------------------------------------
Abstract - Around 80% of road system in India comprises
of flexible pavement in which Hot Mix Asphalt (HMA) is used
in the bituminous layer. Warm Mix Asphalt (WMA) is useful
in certain circumstances when the issues related with HMA
might be lessened. Warm Mix Asphalt brings down the
mixing temperatures at which asphalt materials are mixed
and laid on road. The benefits of WMA are reduced emission,
enhanced workability and lessened energy consumption.
Furthermore, it gives simpler compaction in longer pull
separations and outrageous climate conditions. In this
study, experimental investigations have been carried
including a warm mix chemical sasobit additive which is
effectively accessible. To choose the ideal concentration of
sasobit additive substance for DBM mix, warm mix has been
prepared by utilizing sasobit additive substance with VG 30
at different mixing temperatures of 110°C, 120°C, 130°C and
140°C. According to specifications by MORTH, samples of
Marshal test made by the use of Dense Bituminous
Macadam (DBM) grade and a short time later Marshall
properties were studied with ideal mixing temperature and
ideal Binder sasobit additive composite. It was found that
the DBM warm mix with sasobit additive has given high
Indirect Tensile Strength (ITS) and high Marshall Soundness
(stability) with other satisfactory Marshall parameters. The
held stability and tensile strength are observed likely to be
satisfactory in such warm mixes. The resulting warm mixes
are additionally seen to be comparable to the control HMA.
Key Words: Warm Mix Asphalt, Sasobit, Indirect
Tensile Strength, Marshal Properties, Retained
stability
1. INTRODUCTION
Warm mix asphalt is picking up acknowledgment now a
day in light of around 80% of the paved roads in India are
involves flexible pavement, which comprises of aggregate
and asphalt binder which are heated and mixed together.
Generally, the mixing temperatures of warm mix asphalt
limits from 100 to 135°C (Hurley and Prowell, 2005)
compared with the mixing temperatures of 150 to 180°C
(300 to 350°F) for hot mix asphalt. WMA uses Sasobit, a
chemical additive to yield asphalt mix at lower
temperature by decreasing the binder viscosity, which
increase the workability of mix without compromising
performance of asphalt. Energy use, global warming,
oxidative solidifying of asphalt, and overhead cost
expenses of the asphalt industry are lessened in warm mix
asphalt and it makes better working environment too.
Warm mix asphalt is produced, placed and compacted at
temperature10°C to 40°C lesser than the control Hot Mix
Asphalt (D' Angelo et.al, 2008). In any case, the lower
mixing temperatures have raised concerns on the
performance of the mix. Along these lines, it is expected to
completely assess and characterize the WMA mixtures to
ensure sufficient performance.
2. POTENTIAL ADVANTAGES
Warm Mix Asphalt (WMA) deals with the technology which
reduces production and compaction temperatures.
 Environmental- Fumes and emission (bringing
lower discharges of CO2 and other greenhouse
gasses) are lessened on account of the
temperature level is nearly low, air-contamination
is less.
 Production - Ageing of bitumen binder amid the
production and paving process is controlled
significantly, which enhances serviceability of
pavement.
 Paving - Compaction and workability are
enhanced because of reducing bitumen viscosity at
paving temperature. Construction season develops
and furthermore it increases haul distance.
Pavement cooling time is reduced because of low
initial temperature. It is convincing to public near
work and production site as emissions, odour and
fumes are decreased.
As compared with Hot Mix Asphalt, WMA offers a few
advantages mentioned below.
Energy cost is lessened due to lower production and
placement temperatures. During the production of WMA,
aging of binder is controlled considerably which enhances
of pavement service life. Due to decreased temperature, it
causes less wear on Asphalt plant. Because of lower
temperature, it makes decrease in pavement cooling time.
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 11 | Nov -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 35
3. OBJECTIVE OF STUDY
The essential objective of the study is to develop WMA
using Sasobit additive and to assess the effects of additive
on the properties of binder and mixture.
 To investigate the physical properties and
viscosity of the binder modified with different
percentages of Sasobit additive at various
temperatures.
 To choose suitable percentage of Sasobit for
optimum mixing temperature for the mixtures.
 To assess the warm asphalt mix prepared with
different percentages of additive in terms of
Engineering Properties such as indirect tensile
strength and Marshall Characteristics.
 To study performance of mix in terms of their
held tensile strength ratio and retained stability
value.
4. EXPERIMENTAL TESTS TO BE PERFORMED
Based on the literature review, the following experimental
tests were carried out.
I. Aggregate tests
 Shape Test (Elongation Index)
 Shape Test (Flakiness Index)
 Aggregate Crushing Strength Test
 Aggregate Impact Test
 Los Angeles Abrasion
 Water Absorption Test Of Aggregates
II. Bituminous tests
 Specific gravity
 Softening Point
 Penetration
 Ductility
 Elastic Recovery
 Marshall test
5. TEST RESULTS
Table -1: Physical Properties of Coarse Aggregates
Property Test Method
Test
Result
Elongation Index (%) IS: 2386 (P I) 21.5
Water Absorption (%) IS: 2386 (P III) 0.1
Los Angeles Abrasion
Value (%)
IS: 2386 (P IV) 18
Flakiness Index (%) IS: 2386 (P I) 18.8
Aggregate Impact value IS: 2386 (P IV) 14.3
Aggregate crushing
value
IS: 2386 (P IV) 13
Table -2: Physical Properties of VG 30 bitumen
Property Test Method Value
Specific gravity IS: 1203:1978 1.03
Softening Point, ºC IS: 1203:1978 48.5
Penetration at
25ºC(0.1mm) I
IS: 1203:1978 52
Ductility, mm IS: 1208:1978 80.2
Elastic Recovery, mm IS 15462 76
6. METHODOLOGY
According to the methodology and experimental work, test
results are presented, analyzed and discussed as following
in four sections.
 First section refers to Marshall parameters used
for volumetric analysis of mix.
 Second section deals with choosing optimum
mixing temperature used for warm mix
preparation. This section also gives physical
properties of bitumen with different percentages
of additive.
 Third section deals the Marshall properties of
additive modified DBM warm mix with mixing
temperature of 110°C, 120°C, 130°C or 140°C and
choosing the suitable mixing temperature.
 Fourth section refers the other engineering
properties of additive modified DBM.
7. EXPERIMENTAL TEST RESULTS
7.1 Binder Test results
In this study, it is suggested to prepare warm mix asphalt
with mixing temperature obtained from Brookfield
viscometer by using VG 30 with various percentages of
Sasobit additive. As the mixing temperature plays an
important role for improve the DBM warm mix Marshall
properties. Mixtures prepared with changing mixing
temperatures have been studied. Mixing temperatures of
110°C, 120°C, 130°C and140°C were considered for
preparation of sample and compared without Sasobit
additive at various temperature.
7.1.1 Determination of Mixing Temperature for
warm DBM mix
In this study, the mixing temperature is find out by
conducting viscosity experimental test of binder in
Brookfield viscometer at various temperature for different
percentages of Sasobit. Viscosity of VG-30 with 1%, 2% &
3% percentage of Sasobit is measured at 110°C, 120°C and
130°C to produce WMA. It is Compared without Sasobit
additive at various temperatures.
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 11 | Nov -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 36
Table -3: Rotational viscometer temperature test results
Temperatur
e
(℃)
Torqu
e
(%)
Shea
r
Rate
(
Sec-
1)
Viscosit
y
( cp)
Viscosit
y
(Pa.s)
Average
Viscosit
y
(Pa.s)
110 0.73 6.80 730 0.73
0.73110 0.73 6.80 730 0.73
110 0.73 6.80 730 0.73
120 0.64 6.80 640 0.64
0.61120 0.64 6.80 640 0.64
120 055 6.80 550 0.55
130 0.43 6.80 430 0.43
0.38130 0.37 6.80 370 0.37
130 0.34 6.80 340 0.34
140 0.25 6.80 250 0.25
0.29140 0.33 6.80 330 0.33
140 0.29 6.80 290 0.29
160 0.13 6.80 130 0.13
0.17160 0.22 6.80 220 0.22
160 0.16 6.80 160 0.16
Table -4: Rotational viscometer temperature test results
Temperatur
e
(℃)
Torqu
e
(%)
Shea
r
Rate
( Sec-
1)
Viscosit
y
( cp)
Viscosit
y
(Pa.s)
Average
Viscosit
y
(Pa.s)
110 0.15 6.80 150 0.15
0.70110 0.30 6.80 300 0.30
110 1.65 6.80 165 1.65
120 0.59 6.80 590 0.59
0.58120 0.53 6.80 530 0.53
120 0.62 6.80 620 0.62
130 0.39 6.80 390 0.39
0.34130 0.39 6.80 390 0.39
130 0.62 6.80 620 0.62
140 0.31 6.80 310 0.31
0.26140 0.23 6.80 230 0.23
140 0.24 6.80 240 0.24
Table -5: Rotational viscometer temperature test results
Temperatu
re
(℃)
Torque
(%)
Shea
r
Rate
( Sec-
1)
Viscosit
y
( cp)
Viscosit
y
(Pa.s)
Average
Viscosit
y
(Pa.s)
110 0.78 6.80 780 0.78
0.65110 0.59 6.80 590 0.59
110 0.58 6.80 580 0.58
120 0.63 6.80 630 0.63
0.54
120 0.54 6.80 540 0.54
120 0.45 6.80 450 0.45
130 0.35 6.80 350 0.35
0.32130 0.28 6.80 280 0.28
130 0.35 6.80 350 0.35
140 0.15 6.80 150 0.15
0.20140 0.23 6.80 230 0.23
140 0.23 6.80 230 0.23
Table -6: Rotational viscometer temperature test results
Tempera
ture
(℃)
Torqu
e
(%)
Shear
Rate
( Sec-
1)
Viscos
ity
( cp)
Viscos
ity
(Pa.s)
Average
Viscosity
(Pa.s)
110 0.54 6.80 540 0.54
0.58110 0.51 6.80 510 0.51
110 0.69 6.80 690 0.69
120 0.51 6.80 510 0.51
0.48120 0.46 6.80 460 0.46
120 0.47 6.80 470 0.47
130 0.31 6.80 310 0.31
0.3130 0.21 6.80 210 0.21
130 0.38 6.80 380 0.38
140 0.15 6.80 150 0.15
0.13140 0.09 6.80 90 0.09
140 0.15 6.80 150 0.15
7.1.2 Determination of physical properties of VG
30 with varying percentages of additive
Before using this additive in road construction, it is
important to the test the physical properties of binder. In
this way, subsequent after adding the additive in VG 30, the
physical properties are studied here in terms of
penetration value, softening point, ductility and elastic
recovery.
Table -7: Penetration test results of VG30 bitumen
without Sasobit at 25 ℃
Test No. 1 2 3
Penetration 51 55 50
Average Penetration
(dmm)
52
Table -8: Penetration test results of VG30 bitumen
with 1% Sasobit at 25 ℃
Test No. 1 2 3
Penetration 42.5 38 39
Average Penetration
(dmm)
40
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 11 | Nov -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 37
Table -9: Penetration test results of VG30 bitumen with
1% Sasobit at 25 ℃
Test No. 1 2 3
Penetration 39 36.5 38.5
Average Penetration
(dmm)
38
Table -10: Penetration test results of VG30 bitumen with
1% Sasobit at 25 ℃
Test No. 1 2 3
Penetration 34.5 33.5 37
Average Penetration (dmm) 35
Table – 11: Softening point test results of VG30 bitumen
without Sasobit
Ring No.
Instant
Temperature, ℃
Softening Point,
Average ℃
1 49
49
2 49
Table – 12: Softening point test results of VG30 bitumen
without Sasobit
Ring No. Instant
Temperature, ℃
Softening Point,
Average ℃
1 46 46.5
2 47
Table – 13: Softening point test results of VG30 bitumen
without Sasobit
Ring
No.
Instant
Temperature, ℃
Softening Point,
Average ℃
1 49.5 50
2 50.5
Table – 14: Softening point test results of VG30 bitumen
1% Sasobit
Ring
No.
Instant
Temperature, ℃
Softening Point,
Average ℃
1 56 56
2 56
Table – 15: Softening point test results of VG30 bitumen
1% Sasobit
Ring
No.
Instant
Temperature, ℃
Softening Point,
Average ℃
1 59.5 60
2 60.5
Table – 16: Softening point test results of VG30 bitumen
1% Sasobi
Ring
No.
Instant
Temperature, ℃
Softening Point,
Average ℃
1 58 58
2 58
Table – 17: Softening point test results of VG30 bitumen
2% Sasobit
Ring
No.
Instant
Temperature, ℃
Softening Point,
Average ℃
1 60.5 61
2 61.5
Table – 18: Softening point test results of VG30 bitumen
2% Sasobit
Ring
No.
Instant
Temperature, ℃
Softening Point,
Average ℃
1 61.00 61.15
2 61.30
Table – 19: Softening point test results of VG30 bitumen
2% Sasobit
Ring
No.
Instant
Temperature, ℃
Softening Point,
Average ℃
1 62 62.5
2 63
Table – 20: Softening point test results of VG30 bitumen
3% Sasobit
Ring
No.
Instant
Temperature, ℃
Softening Point,
Average ℃
1 65.60 64.8
2 64
Table – 21: Softening point test results of VG30 bitumen
3% Sasobit
Ring No. Instant
Temperature, ℃
Softening Point,
Average ℃
1 67.40 66.70
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 11 | Nov -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 38
2 66.00
Table – 22: Softening point test results of VG30 bitumen
3% Sasobit
Ring
No.
Instant
Temperature, ℃
Softening Point,
Average ℃
1 65 65
2 65
Fig. 1: Temperature, ℃ v/s Viscosity, Pa.s at 0% Sasobit
Fig. 2: Temperature, ℃ v/s Viscosity, Pa.s at 1% Sasobit
Fig. 3: Temperature, ℃ v/s Viscosity, Pa.s at 2% Sasobit
Fig. 4: Temperature, ℃ v/s Viscosity, Pa.s at 3% Sasobit
Fig. 5: Viscosity, Pa.s v/s % Sasobit at 130 ℃
Fig. 6: Penetration, mm v/s % Sasobit at 25 ℃
Fig. 7: Softening Point, ℃ v/s % Sasobit
110 120 130 140 150
0
100
200
0.73 0.61 0.38 0.29 0.17
Temperature,℃
Viscosity, Pa.s
110 120 130 140
0
50
100
150
0.7 0.58 0.34 0.26
Temperature,℃
Viscosity, Pa.s
110 120 130 140
0
50
100
150
0.65 0.54 0.32 0.2
Temperature,℃
Viscosity, Pa.s
110
120
130 140
0
50
100
150
0.58 0.48 0.3 0.13
Temperature,℃
Viscosity, Pa.s
0.38
0.34 0.32 0.3
0% S 1% S 2% S 3% SViscosity,Pa.s
Percentage of Sasobit
Viscosity, Pa.s
52
40 38 35
0
20
40
60
0% S 1% S 2% S 3% S
Penetration,mm
Percentage of Sasobit
48.5
58 61.55 65.5
0
20
40
60
80
0% S 1% S 2% S 3% S
SofteningPoint,℃
Percentage of Sasobit
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 11 | Nov -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 39
Fig. 8: Ductility, mm v/s % Sasobit at 27 ℃
Fig. 9: Elastic Recovery, mm v/s % Sasobit at 15 ℃
7.2Effect of additive content on Marshall
Properties for DBM warm mix
To evaluate the best combination additive percentages in
mixing temperature and bitumen, warm DBM mixtures are
prepared with VG-30 with various percentages of additive
content at 110°C, 120°C, 130°C and 140°C temperature.
7.2.1 Effect of additive content on Marshall
Properties for DBM warm mix samples prepared
at 110°C, 120°C, 130°C and 140°C.
For DBM warm mix having in different dosages of
additives, the Marshall properties, such as air voids, flow
value, unit weight, air voids, voids filled with mineral
aggregates (VMA), stability, and voids filled with bitumen
(VFB). It has been seen that pattern of variation in Marshall
Properties with binder content are like normal HMA and
furthermore denoted that stability and unit weight
increases with binder content and there after decreases.
The maximum unit weight and stability values obtained at
their optimum binder content. Moreover, the flow value
and air voids accordingly decrease and increase with
increase in binder content. It has been observed that with
increment in bitumen concentration in mix VMA reduce up
certain binder content and after that increases sharply and
furthermore observed that VFB increases sharply with
increase in binder content.
7.3 Other Engineering properties of warm mixes
are
7.3.1 Indirect tensile strength of DBM mixes
Indirect elasticity of the mix decides the resistance against
thermal cracking. These tests have been conducted on DBM
mixes with modified binder at their respective mix
temperatures and binder content having changing additive
contents. The effects of additive concentration and
temperature in DBM mixes are studied.
Table 23: Test reults of Indirect tensile strength and
Ductility experiments
Percentage of
Sasobit
Ductility at 27°C
Elastic Recovery
at 15°C
0 80.2 76
1 68 68
2 66 64
3 60.1 60.1
7.3.2 Tensile strength ratio of warm mix
Moisture susceptibility is main cause of distress in
pavement. The evaluation of moisture sensitivity of DBM
warm mix has mostly conducted using a standard method,
AASHTO T283.
7.3.3 Retained stability for DBM warm mix.
Another way of assessing the resistance to moisture
damage of mix is find out by conducting retained stability
test. For this additive modified DBM warm mix, retained
stability and additive modified DBM has been measured at
their respective optimum mixing temperatures.
8. CONCLUSION
Performance evaluation of WMA using Sasobit additive
with different percentages and test temperatures are
done. The following conclusions were obtained.
 Penetration values are found to decrease with the
addition of Sasobit additive. The reduction in
penetration value with 1% of Sasobit is found to
higher than 2 and 3 percentages of Sasobit.
 Addition of Sasobit additive has increased the
softening point of WMA. 1% of Sasobit has higher
increment of softening point value than2 and 3
percentages of Sasobit.
80.2
68 66
60.1
0
20
40
60
80
100
0% S 1% S 2% S 3% S
Ductility,mm
Percentage of Sasobit
76 68
64
60.1
0
20
40
60
80
0% S 1% S 2% S 3% S
ElasticRecovery,mm
Percentage of Sasobit
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 04 Issue: 11 | Nov -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 40
 Viscosity of WMA has reduced with the addition of
Sasobit additive. There found higher value
reduction of viscosity by 1% Sasobit at 130 ℃.
 Addition of Sasobit additive has reduced the
elastic recovery values.
 Ductility values increased with addition of Sasobit
additive and it is found to be higher in increment
at 1% than 2 and 3 percentages.
REFERENCES
[1] Bonaquist, R. (2009). “NCHRP 9-43 Mix Design
Practices for Warm Mix Asphalt.” Interim Report-
National Cooperative Highway Research Program
Project 943.
[2] Chowdhury, A. and Button, J. (2008). “A Review of
Warm Mix Asphalt.” Technicalreport, National
Technical Information Service, Texas Transportation
Institute Springfield, Virginia, USA.
[3] Goh, S.W. and You, Z. (2008a). “Mechanical properties
of warm mix asphalt using aspha-min.” Proc.,
Transportation Research Board 87th Annual Meeting.
Washington, DC, USA.
[4] IS: 1203 (1978), “Methods for Testing Tar and
Bituminous Materials: “Determinationof Penetration.”
Bureau of Indian Standards, New Delhi.
[5] Button, J. W., Estakhri, C. and Wimsatt, A. (2007).
“Evaluation of Warm-Mix Asphalt New Technology.”
Technical Report, Texas Transportation Institute, the
Texas A&M University System College Station, Texas
77843-3135, USA.
[6] Harrison, T., and Christodulaki, L. (2000). "Innovative
processes in asphalt production and application -
strengthening asphalt's position in helping build a
better world." First International Conference of
Asphalt Pavement, Sydney, Australia.
[7] Buss, A., Rashwan, M., Breakah, T., Williams, R.C. and
Kvasnak, A. (2009). “Investigation of Warm-Mix
Asphalt Using the Mechanistic-Empirical
PavementDesign Guide.” Mid Continent
Transportation research Symposium, Ames, Iowa,
USA.
[8] Blanco, (2004a). “Maintenance of Porous Wearing
Courses by Using Warm Open- Graded Mixes with
Polymer-Modified Medium Setting Emulsions.”
Proceedings, 3rdEuroasphalt&Eurobitume Congress,
Vienna, Austria, pp. 560-567.
[9] Els,H.,(2004). “Cold/Warm Processes and Recycling
Moderator’s.” Report, Part 2A,”Proceedings (CD), 3rd
Eurasphalt&Eurobitume Congress, Vienna, Austria.
[10] IS: 1205 (1978). “Methods for Testing Tar and
Bituminous Materials: “Determination of Softening
Point.” Bureau of Indian Standards, New Delhi.

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A Performance Evaluation of Warm Mix Asphalt Mixture by Incorporating Sasobit Additive

  • 1. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 11 | Nov -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 34 A PERFORMANCE EVALUATION OF WARM MIX ASPHALT MIXTURE BY INCORPORATING SASOBIT ADDITIVE Uma shanker Gunti1, Javedali M Jalegar2 1. Post graduate Student, Department of Civil Engineering, AVNIET, Ibrahimpatnam, India 2. Assistance Professor, Department of Civil Engineering, AVNIET, Ibrahimpatnam, India ---------------------------------------------------------------------***--------------------------------------------------------------------- Abstract - Around 80% of road system in India comprises of flexible pavement in which Hot Mix Asphalt (HMA) is used in the bituminous layer. Warm Mix Asphalt (WMA) is useful in certain circumstances when the issues related with HMA might be lessened. Warm Mix Asphalt brings down the mixing temperatures at which asphalt materials are mixed and laid on road. The benefits of WMA are reduced emission, enhanced workability and lessened energy consumption. Furthermore, it gives simpler compaction in longer pull separations and outrageous climate conditions. In this study, experimental investigations have been carried including a warm mix chemical sasobit additive which is effectively accessible. To choose the ideal concentration of sasobit additive substance for DBM mix, warm mix has been prepared by utilizing sasobit additive substance with VG 30 at different mixing temperatures of 110°C, 120°C, 130°C and 140°C. According to specifications by MORTH, samples of Marshal test made by the use of Dense Bituminous Macadam (DBM) grade and a short time later Marshall properties were studied with ideal mixing temperature and ideal Binder sasobit additive composite. It was found that the DBM warm mix with sasobit additive has given high Indirect Tensile Strength (ITS) and high Marshall Soundness (stability) with other satisfactory Marshall parameters. The held stability and tensile strength are observed likely to be satisfactory in such warm mixes. The resulting warm mixes are additionally seen to be comparable to the control HMA. Key Words: Warm Mix Asphalt, Sasobit, Indirect Tensile Strength, Marshal Properties, Retained stability 1. INTRODUCTION Warm mix asphalt is picking up acknowledgment now a day in light of around 80% of the paved roads in India are involves flexible pavement, which comprises of aggregate and asphalt binder which are heated and mixed together. Generally, the mixing temperatures of warm mix asphalt limits from 100 to 135°C (Hurley and Prowell, 2005) compared with the mixing temperatures of 150 to 180°C (300 to 350°F) for hot mix asphalt. WMA uses Sasobit, a chemical additive to yield asphalt mix at lower temperature by decreasing the binder viscosity, which increase the workability of mix without compromising performance of asphalt. Energy use, global warming, oxidative solidifying of asphalt, and overhead cost expenses of the asphalt industry are lessened in warm mix asphalt and it makes better working environment too. Warm mix asphalt is produced, placed and compacted at temperature10°C to 40°C lesser than the control Hot Mix Asphalt (D' Angelo et.al, 2008). In any case, the lower mixing temperatures have raised concerns on the performance of the mix. Along these lines, it is expected to completely assess and characterize the WMA mixtures to ensure sufficient performance. 2. POTENTIAL ADVANTAGES Warm Mix Asphalt (WMA) deals with the technology which reduces production and compaction temperatures.  Environmental- Fumes and emission (bringing lower discharges of CO2 and other greenhouse gasses) are lessened on account of the temperature level is nearly low, air-contamination is less.  Production - Ageing of bitumen binder amid the production and paving process is controlled significantly, which enhances serviceability of pavement.  Paving - Compaction and workability are enhanced because of reducing bitumen viscosity at paving temperature. Construction season develops and furthermore it increases haul distance. Pavement cooling time is reduced because of low initial temperature. It is convincing to public near work and production site as emissions, odour and fumes are decreased. As compared with Hot Mix Asphalt, WMA offers a few advantages mentioned below. Energy cost is lessened due to lower production and placement temperatures. During the production of WMA, aging of binder is controlled considerably which enhances of pavement service life. Due to decreased temperature, it causes less wear on Asphalt plant. Because of lower temperature, it makes decrease in pavement cooling time.
  • 2. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 11 | Nov -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 35 3. OBJECTIVE OF STUDY The essential objective of the study is to develop WMA using Sasobit additive and to assess the effects of additive on the properties of binder and mixture.  To investigate the physical properties and viscosity of the binder modified with different percentages of Sasobit additive at various temperatures.  To choose suitable percentage of Sasobit for optimum mixing temperature for the mixtures.  To assess the warm asphalt mix prepared with different percentages of additive in terms of Engineering Properties such as indirect tensile strength and Marshall Characteristics.  To study performance of mix in terms of their held tensile strength ratio and retained stability value. 4. EXPERIMENTAL TESTS TO BE PERFORMED Based on the literature review, the following experimental tests were carried out. I. Aggregate tests  Shape Test (Elongation Index)  Shape Test (Flakiness Index)  Aggregate Crushing Strength Test  Aggregate Impact Test  Los Angeles Abrasion  Water Absorption Test Of Aggregates II. Bituminous tests  Specific gravity  Softening Point  Penetration  Ductility  Elastic Recovery  Marshall test 5. TEST RESULTS Table -1: Physical Properties of Coarse Aggregates Property Test Method Test Result Elongation Index (%) IS: 2386 (P I) 21.5 Water Absorption (%) IS: 2386 (P III) 0.1 Los Angeles Abrasion Value (%) IS: 2386 (P IV) 18 Flakiness Index (%) IS: 2386 (P I) 18.8 Aggregate Impact value IS: 2386 (P IV) 14.3 Aggregate crushing value IS: 2386 (P IV) 13 Table -2: Physical Properties of VG 30 bitumen Property Test Method Value Specific gravity IS: 1203:1978 1.03 Softening Point, ºC IS: 1203:1978 48.5 Penetration at 25ºC(0.1mm) I IS: 1203:1978 52 Ductility, mm IS: 1208:1978 80.2 Elastic Recovery, mm IS 15462 76 6. METHODOLOGY According to the methodology and experimental work, test results are presented, analyzed and discussed as following in four sections.  First section refers to Marshall parameters used for volumetric analysis of mix.  Second section deals with choosing optimum mixing temperature used for warm mix preparation. This section also gives physical properties of bitumen with different percentages of additive.  Third section deals the Marshall properties of additive modified DBM warm mix with mixing temperature of 110°C, 120°C, 130°C or 140°C and choosing the suitable mixing temperature.  Fourth section refers the other engineering properties of additive modified DBM. 7. EXPERIMENTAL TEST RESULTS 7.1 Binder Test results In this study, it is suggested to prepare warm mix asphalt with mixing temperature obtained from Brookfield viscometer by using VG 30 with various percentages of Sasobit additive. As the mixing temperature plays an important role for improve the DBM warm mix Marshall properties. Mixtures prepared with changing mixing temperatures have been studied. Mixing temperatures of 110°C, 120°C, 130°C and140°C were considered for preparation of sample and compared without Sasobit additive at various temperature. 7.1.1 Determination of Mixing Temperature for warm DBM mix In this study, the mixing temperature is find out by conducting viscosity experimental test of binder in Brookfield viscometer at various temperature for different percentages of Sasobit. Viscosity of VG-30 with 1%, 2% & 3% percentage of Sasobit is measured at 110°C, 120°C and 130°C to produce WMA. It is Compared without Sasobit additive at various temperatures.
  • 3. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 11 | Nov -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 36 Table -3: Rotational viscometer temperature test results Temperatur e (℃) Torqu e (%) Shea r Rate ( Sec- 1) Viscosit y ( cp) Viscosit y (Pa.s) Average Viscosit y (Pa.s) 110 0.73 6.80 730 0.73 0.73110 0.73 6.80 730 0.73 110 0.73 6.80 730 0.73 120 0.64 6.80 640 0.64 0.61120 0.64 6.80 640 0.64 120 055 6.80 550 0.55 130 0.43 6.80 430 0.43 0.38130 0.37 6.80 370 0.37 130 0.34 6.80 340 0.34 140 0.25 6.80 250 0.25 0.29140 0.33 6.80 330 0.33 140 0.29 6.80 290 0.29 160 0.13 6.80 130 0.13 0.17160 0.22 6.80 220 0.22 160 0.16 6.80 160 0.16 Table -4: Rotational viscometer temperature test results Temperatur e (℃) Torqu e (%) Shea r Rate ( Sec- 1) Viscosit y ( cp) Viscosit y (Pa.s) Average Viscosit y (Pa.s) 110 0.15 6.80 150 0.15 0.70110 0.30 6.80 300 0.30 110 1.65 6.80 165 1.65 120 0.59 6.80 590 0.59 0.58120 0.53 6.80 530 0.53 120 0.62 6.80 620 0.62 130 0.39 6.80 390 0.39 0.34130 0.39 6.80 390 0.39 130 0.62 6.80 620 0.62 140 0.31 6.80 310 0.31 0.26140 0.23 6.80 230 0.23 140 0.24 6.80 240 0.24 Table -5: Rotational viscometer temperature test results Temperatu re (℃) Torque (%) Shea r Rate ( Sec- 1) Viscosit y ( cp) Viscosit y (Pa.s) Average Viscosit y (Pa.s) 110 0.78 6.80 780 0.78 0.65110 0.59 6.80 590 0.59 110 0.58 6.80 580 0.58 120 0.63 6.80 630 0.63 0.54 120 0.54 6.80 540 0.54 120 0.45 6.80 450 0.45 130 0.35 6.80 350 0.35 0.32130 0.28 6.80 280 0.28 130 0.35 6.80 350 0.35 140 0.15 6.80 150 0.15 0.20140 0.23 6.80 230 0.23 140 0.23 6.80 230 0.23 Table -6: Rotational viscometer temperature test results Tempera ture (℃) Torqu e (%) Shear Rate ( Sec- 1) Viscos ity ( cp) Viscos ity (Pa.s) Average Viscosity (Pa.s) 110 0.54 6.80 540 0.54 0.58110 0.51 6.80 510 0.51 110 0.69 6.80 690 0.69 120 0.51 6.80 510 0.51 0.48120 0.46 6.80 460 0.46 120 0.47 6.80 470 0.47 130 0.31 6.80 310 0.31 0.3130 0.21 6.80 210 0.21 130 0.38 6.80 380 0.38 140 0.15 6.80 150 0.15 0.13140 0.09 6.80 90 0.09 140 0.15 6.80 150 0.15 7.1.2 Determination of physical properties of VG 30 with varying percentages of additive Before using this additive in road construction, it is important to the test the physical properties of binder. In this way, subsequent after adding the additive in VG 30, the physical properties are studied here in terms of penetration value, softening point, ductility and elastic recovery. Table -7: Penetration test results of VG30 bitumen without Sasobit at 25 ℃ Test No. 1 2 3 Penetration 51 55 50 Average Penetration (dmm) 52 Table -8: Penetration test results of VG30 bitumen with 1% Sasobit at 25 ℃ Test No. 1 2 3 Penetration 42.5 38 39 Average Penetration (dmm) 40
  • 4. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 11 | Nov -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 37 Table -9: Penetration test results of VG30 bitumen with 1% Sasobit at 25 ℃ Test No. 1 2 3 Penetration 39 36.5 38.5 Average Penetration (dmm) 38 Table -10: Penetration test results of VG30 bitumen with 1% Sasobit at 25 ℃ Test No. 1 2 3 Penetration 34.5 33.5 37 Average Penetration (dmm) 35 Table – 11: Softening point test results of VG30 bitumen without Sasobit Ring No. Instant Temperature, ℃ Softening Point, Average ℃ 1 49 49 2 49 Table – 12: Softening point test results of VG30 bitumen without Sasobit Ring No. Instant Temperature, ℃ Softening Point, Average ℃ 1 46 46.5 2 47 Table – 13: Softening point test results of VG30 bitumen without Sasobit Ring No. Instant Temperature, ℃ Softening Point, Average ℃ 1 49.5 50 2 50.5 Table – 14: Softening point test results of VG30 bitumen 1% Sasobit Ring No. Instant Temperature, ℃ Softening Point, Average ℃ 1 56 56 2 56 Table – 15: Softening point test results of VG30 bitumen 1% Sasobit Ring No. Instant Temperature, ℃ Softening Point, Average ℃ 1 59.5 60 2 60.5 Table – 16: Softening point test results of VG30 bitumen 1% Sasobi Ring No. Instant Temperature, ℃ Softening Point, Average ℃ 1 58 58 2 58 Table – 17: Softening point test results of VG30 bitumen 2% Sasobit Ring No. Instant Temperature, ℃ Softening Point, Average ℃ 1 60.5 61 2 61.5 Table – 18: Softening point test results of VG30 bitumen 2% Sasobit Ring No. Instant Temperature, ℃ Softening Point, Average ℃ 1 61.00 61.15 2 61.30 Table – 19: Softening point test results of VG30 bitumen 2% Sasobit Ring No. Instant Temperature, ℃ Softening Point, Average ℃ 1 62 62.5 2 63 Table – 20: Softening point test results of VG30 bitumen 3% Sasobit Ring No. Instant Temperature, ℃ Softening Point, Average ℃ 1 65.60 64.8 2 64 Table – 21: Softening point test results of VG30 bitumen 3% Sasobit Ring No. Instant Temperature, ℃ Softening Point, Average ℃ 1 67.40 66.70
  • 5. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 11 | Nov -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 38 2 66.00 Table – 22: Softening point test results of VG30 bitumen 3% Sasobit Ring No. Instant Temperature, ℃ Softening Point, Average ℃ 1 65 65 2 65 Fig. 1: Temperature, ℃ v/s Viscosity, Pa.s at 0% Sasobit Fig. 2: Temperature, ℃ v/s Viscosity, Pa.s at 1% Sasobit Fig. 3: Temperature, ℃ v/s Viscosity, Pa.s at 2% Sasobit Fig. 4: Temperature, ℃ v/s Viscosity, Pa.s at 3% Sasobit Fig. 5: Viscosity, Pa.s v/s % Sasobit at 130 ℃ Fig. 6: Penetration, mm v/s % Sasobit at 25 ℃ Fig. 7: Softening Point, ℃ v/s % Sasobit 110 120 130 140 150 0 100 200 0.73 0.61 0.38 0.29 0.17 Temperature,℃ Viscosity, Pa.s 110 120 130 140 0 50 100 150 0.7 0.58 0.34 0.26 Temperature,℃ Viscosity, Pa.s 110 120 130 140 0 50 100 150 0.65 0.54 0.32 0.2 Temperature,℃ Viscosity, Pa.s 110 120 130 140 0 50 100 150 0.58 0.48 0.3 0.13 Temperature,℃ Viscosity, Pa.s 0.38 0.34 0.32 0.3 0% S 1% S 2% S 3% SViscosity,Pa.s Percentage of Sasobit Viscosity, Pa.s 52 40 38 35 0 20 40 60 0% S 1% S 2% S 3% S Penetration,mm Percentage of Sasobit 48.5 58 61.55 65.5 0 20 40 60 80 0% S 1% S 2% S 3% S SofteningPoint,℃ Percentage of Sasobit
  • 6. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 11 | Nov -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 39 Fig. 8: Ductility, mm v/s % Sasobit at 27 ℃ Fig. 9: Elastic Recovery, mm v/s % Sasobit at 15 ℃ 7.2Effect of additive content on Marshall Properties for DBM warm mix To evaluate the best combination additive percentages in mixing temperature and bitumen, warm DBM mixtures are prepared with VG-30 with various percentages of additive content at 110°C, 120°C, 130°C and 140°C temperature. 7.2.1 Effect of additive content on Marshall Properties for DBM warm mix samples prepared at 110°C, 120°C, 130°C and 140°C. For DBM warm mix having in different dosages of additives, the Marshall properties, such as air voids, flow value, unit weight, air voids, voids filled with mineral aggregates (VMA), stability, and voids filled with bitumen (VFB). It has been seen that pattern of variation in Marshall Properties with binder content are like normal HMA and furthermore denoted that stability and unit weight increases with binder content and there after decreases. The maximum unit weight and stability values obtained at their optimum binder content. Moreover, the flow value and air voids accordingly decrease and increase with increase in binder content. It has been observed that with increment in bitumen concentration in mix VMA reduce up certain binder content and after that increases sharply and furthermore observed that VFB increases sharply with increase in binder content. 7.3 Other Engineering properties of warm mixes are 7.3.1 Indirect tensile strength of DBM mixes Indirect elasticity of the mix decides the resistance against thermal cracking. These tests have been conducted on DBM mixes with modified binder at their respective mix temperatures and binder content having changing additive contents. The effects of additive concentration and temperature in DBM mixes are studied. Table 23: Test reults of Indirect tensile strength and Ductility experiments Percentage of Sasobit Ductility at 27°C Elastic Recovery at 15°C 0 80.2 76 1 68 68 2 66 64 3 60.1 60.1 7.3.2 Tensile strength ratio of warm mix Moisture susceptibility is main cause of distress in pavement. The evaluation of moisture sensitivity of DBM warm mix has mostly conducted using a standard method, AASHTO T283. 7.3.3 Retained stability for DBM warm mix. Another way of assessing the resistance to moisture damage of mix is find out by conducting retained stability test. For this additive modified DBM warm mix, retained stability and additive modified DBM has been measured at their respective optimum mixing temperatures. 8. CONCLUSION Performance evaluation of WMA using Sasobit additive with different percentages and test temperatures are done. The following conclusions were obtained.  Penetration values are found to decrease with the addition of Sasobit additive. The reduction in penetration value with 1% of Sasobit is found to higher than 2 and 3 percentages of Sasobit.  Addition of Sasobit additive has increased the softening point of WMA. 1% of Sasobit has higher increment of softening point value than2 and 3 percentages of Sasobit. 80.2 68 66 60.1 0 20 40 60 80 100 0% S 1% S 2% S 3% S Ductility,mm Percentage of Sasobit 76 68 64 60.1 0 20 40 60 80 0% S 1% S 2% S 3% S ElasticRecovery,mm Percentage of Sasobit
  • 7. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 04 Issue: 11 | Nov -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 6.171 | ISO 9001:2008 Certified Journal | Page 40  Viscosity of WMA has reduced with the addition of Sasobit additive. There found higher value reduction of viscosity by 1% Sasobit at 130 ℃.  Addition of Sasobit additive has reduced the elastic recovery values.  Ductility values increased with addition of Sasobit additive and it is found to be higher in increment at 1% than 2 and 3 percentages. REFERENCES [1] Bonaquist, R. (2009). “NCHRP 9-43 Mix Design Practices for Warm Mix Asphalt.” Interim Report- National Cooperative Highway Research Program Project 943. [2] Chowdhury, A. and Button, J. (2008). “A Review of Warm Mix Asphalt.” Technicalreport, National Technical Information Service, Texas Transportation Institute Springfield, Virginia, USA. [3] Goh, S.W. and You, Z. (2008a). “Mechanical properties of warm mix asphalt using aspha-min.” Proc., Transportation Research Board 87th Annual Meeting. Washington, DC, USA. [4] IS: 1203 (1978), “Methods for Testing Tar and Bituminous Materials: “Determinationof Penetration.” Bureau of Indian Standards, New Delhi. [5] Button, J. W., Estakhri, C. and Wimsatt, A. (2007). “Evaluation of Warm-Mix Asphalt New Technology.” Technical Report, Texas Transportation Institute, the Texas A&M University System College Station, Texas 77843-3135, USA. [6] Harrison, T., and Christodulaki, L. (2000). "Innovative processes in asphalt production and application - strengthening asphalt's position in helping build a better world." First International Conference of Asphalt Pavement, Sydney, Australia. [7] Buss, A., Rashwan, M., Breakah, T., Williams, R.C. and Kvasnak, A. (2009). “Investigation of Warm-Mix Asphalt Using the Mechanistic-Empirical PavementDesign Guide.” Mid Continent Transportation research Symposium, Ames, Iowa, USA. [8] Blanco, (2004a). “Maintenance of Porous Wearing Courses by Using Warm Open- Graded Mixes with Polymer-Modified Medium Setting Emulsions.” Proceedings, 3rdEuroasphalt&Eurobitume Congress, Vienna, Austria, pp. 560-567. [9] Els,H.,(2004). “Cold/Warm Processes and Recycling Moderator’s.” Report, Part 2A,”Proceedings (CD), 3rd Eurasphalt&Eurobitume Congress, Vienna, Austria. [10] IS: 1205 (1978). “Methods for Testing Tar and Bituminous Materials: “Determination of Softening Point.” Bureau of Indian Standards, New Delhi.