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Separation Processes Lab
Department of Chemical Engineering & Technology Page | 1
Table of Contents
ABSTRACT ................................................................................................................................................3
INTRODUCTION.......................................................................................................................................4
PRACTICAL APPLICATIONS................................................................................................................4
EQUIPMENT & PARTS DESCRIPTION...............................................................................................5
1. Aeration Tank ...............................................................................................................................6
2. DO Meter ........................................................................................................................................6
3. Diaphgram Pump.........................................................................................................................6
4. Flow Meter.....................................................................................................................................7
5. Stirrer Controller.........................................................................................................................7
6. Electrical Unit...............................................................................................................................7
EXPERIMENT No. 01...............................................................................................................................8
EXPERIMENT No. 02.............................................................................................................................12
REFRENCES............................................................................................................................................15
Table of Figures
Figure 1: Aeration Unit (Manual) .........................................................................5
Figure 2: Aeration Tank (Manual) ........................................................................6
Figure 3: DO Meter (Manual) ...............................................................................6
Figure 4: Diaphragm Pump (Manual)...................................................................6
Figure 5: Flow Meter (Manual).............................................................................7
Figure 6: Stirrer Controller (Manual) ...................................................................7
Figure 7: Electrical Cabin (Manual) .....................................................................7
Separation Processes Lab
Department of Chemical Engineering & Technology Page | 2
LAB LAYOUT
Evaluation
Table
Tray DrierChemicals
Cupboard
Rotary Drier Wetted Wall Gas
Absorb. Column
AerationUnit
SolidLiquid
Extraction
Unit
IonExchange
Gas/Liq.
Absorption
Column
Distillation
ColumnUnit
Liq/Liq.
Extraction
Unit
DoorDoor
Separation Processes Lab
Department of Chemical Engineering & Technology Page | 3
ABSTRACT
Aeration is a unit process in which air and water are brought
into intimate contact. The contact time and ratio of air to water must be sufficient
for effective removal of unwanted gas. Following report concisely explicate the
working of an Aeration Unit and major description of equipment. Simple
experiments are added for better understanding of equipment and process of
Aeration. Observatory columns efficiently describe the effect of various factors
upon Aeration. Graphical representations make it easy to judge the trend of effect
of specific factor upon equipment.
Separation Processes Lab
Department of Chemical Engineering & Technology Page | 4
INTRODUCTION
The Aeration Unit allows the study of oxygen transfer
characteristics of diffused air systems, and the physical and chemical parameters,
which influence oxygenation capacity. Aeration Unit demonstrates the water
aeration process which, mainly, eliminates smell and taste from water. Aeration is
also an effective method of bacteria removal.
Two general methods can be used for the aeration of water;
1. Water-fall Aerator
2. Air Diffusion Method
The Water fall aerator works through the use of spray
nozzles, the water droplets are broken into small droplets or a thin film to enhance
counter-current air contact. In the Air Diffusion method, air is diffused into a
receiving vessel containing counter-current flowing water, creating very small air
bubbles. This ensures good water-air contact for ‘‘scrubbing’’ of the undesired
gases from water. (Manual)
PRACTICAL APPLICATIONS
In industrial water conditioning, one of the major
applications of aeration is to remove Carbon Dioxide. Aeration is also used to
oxidize the soluble Iron & Manganese to insoluble precipitates. Aeration I soften
used to reduce the Carbon Dioxide liberated by a treatment process. Air stripping
maybe used to reduce concentrations of volatile organics, such as Chloroform.
Separation Processes Lab
Department of Chemical Engineering & Technology Page | 5
EQUIPMENT & PARTS DESCRIPTION
The Aeration Unit used in experiment is locally fabricated
and contain six major parts. Equipment is used for the measurement of Dissolved
Oxygen in water at normal conditions of temperature & pressure.
Figure 1: Aeration Unit (Manual)
Major parts of the equipment as briefly explained later to
completely understand the working of Aeration Unit. Electrical wires, air pipe and
stirrer motor are not included in thse parts. (ATICO, 2015)
Separation Processes Lab
Department of Chemical Engineering & Technology Page | 6
1. Aeration Tank
The main part of the Aeration tank is
the Aeration Tank with a meschanical stirring paddle in it
to provide turbulence for better mixing of air with water.
Temperature as well as Dissolved Oxygen Meter sensors
are mounted at top of the tank.
Figure 2: Aeration Tank (Manual)
2. DO Meter
DO stands for Dissolved Oxygen
Meter and it gives the reading of amount of oxygen
dissolved in the tank at normal temperature.
Figure 3: DO Meter (Manual)
3. Diaphgram Pump
A Diaphram Pump of small duty is
also installed with the equipment. A small button is set up
on the pump to manually set the flow rate to High or Low.
Figure 4: Diaphragm Pump (Manual)
Separation Processes Lab
Department of Chemical Engineering & Technology Page | 7
4. Flow Meter
A flow meter in parallel to Diaphgram Pump is attached
to the euipment board to measure the flow rate of air. Scale of
the flow meter is pretty high as compared to the duty of the
pump, so it need to be replaced.
Figure 5: Flow Meter (Manual)
5. Stirrer Controller
In order to control the speed of the
stirrer a controller setup is used with high low &
moderate speeds of the stirrer.
Figure 6: Stirrer Controller (Manual)
6. Electrical Unit
An Electrical Cabnit is installed at
the top of the euipment board to control the stirrer motor
and diaphgram motor.
Figure 7: Electrical Cabin (Manual)
Separation Processes Lab
Department of Chemical Engineering & Technology Page | 8
EXPERIMENT No. 01
Objective
To observe the absorption of Oxygen in water at various RPM of stirrer.
Apparatus
 Aeration Tank
 DO Meter
 Stopwatch
Reagents
 Water
 Air
Procedure
 Setup the procedure as shown in the Figure 1.
 Filled the tank with distilled water.
 Inserted the probe of DO meter in the tank.
 Made sure that DO meter was properly caliberated and in working
condition.
 Switched on the air blower & adjusted the flow rate of Air .
 Switched the stirrer on & adjusted the RPM.
 Noted the readings of Dissolved Oxygen in water after regular intervals
of one minute.
Separation Processes Lab
Department of Chemical Engineering & Technology Page | 9
 After that changed the RPM of stirrer & again noted the Dissolved
Oxygen in water.
 Repeated the above step for High , Medium & Low speeds of the stirrer.
 Plotted the graph & compared the results. (Manual)
Observations & Calculations
Air Flow Rate = 1.75
Stirrer RPM = Low , Medium , High
Table 1: Amount of DO change w.r.t time
Sr.
No
Time (min) Dissolved Oxygen (mg/L)
1
0 8.4
2
2 8.8
3
4 9.5
4
7 11
5
8 11.5
6
10 12.3
7
12 13.1
8
15 13.9
9
16 13.9
Separation Processes Lab
Department of Chemical Engineering & Technology Page | 10
8
9
10
11
12
13
14
15
16
0 5 10 15 20 25
DissolvedOxygen
Time (min)
Low RPM
Medium RPM
High RPM
Graphical Representation
The following graph shows the cahnge in amount of dissolved oxygen as the time
increases.
Graph 1: DO vs Time Representation (Stirrer Speed Variation)
Separation Processes Lab
Department of Chemical Engineering & Technology Page | 11
Results
The Graph 1 based on the values by Table 1 shows variation
in dissolved oxygen as the time and stirrer speed changes. Dissolved oxygen shows
a significant change after 15 minutes and at high stirrer speed.
Conclusion
The results depict that Dissolved Oxygen is directly proportional to time.
𝑫𝑶 ∝ 𝑻𝒊𝒎𝒆
From the results of experiments we can also conclude that Dissolved Oxygen is
also proportional to stirrer speed. (Joseph A. Salvato, 2006)
𝑫𝑶 ∝ 𝑺𝒕𝒊𝒓𝒓𝒆𝒓 𝑺𝒑𝒆𝒆𝒅
Separation Processes Lab
Department of Chemical Engineering & Technology Page | 12
EXPERIMENT No. 02
Objective
To observe the absorption of Oxygen in water at various flow rates of Air.
Apparatus
 Aeration Tank
 DO Meter
 Stopwatch
Reagents
 Water
 Air
Procedure
 Setup the procedure as shown in the Figure 1.
 Filled the tank with distilled water.
 Inserted the probe of DO meter in the tank.
 Made sure that DO meter was properly caliberated and in working
condition.
 Switched on the air blower & adjusted the flow rate of Air.
 Switched the stirrer on & adjusted the RPM.
 Noted the readings of Dissolved Oxygen in water after regular intervals
of one minute.
Separation Processes Lab
Department of Chemical Engineering & Technology Page | 13
 After that changed the flow rate of Air & again noted the Dissolved
Oxygen in water.
 Repeated the above step for various flow rates of Air.
 Plotted the graph & compared the results. (Manual)
Observations & Calculations
Air Flow Rate = 1.75 & 2.75
Stirrer RPM = Medium
Table 2: Amount of DO change w.r.t time
Sr.
No
Time (min) Dissolved Oxygen (mg/L)
1
0 13.9
2
2 14.4
3
4 14.8
4
6 15.3
5
8 16
6
10 16.4
7
12 17.1
8
14 17.6
9
17 17.9
Separation Processes Lab
Department of Chemical Engineering & Technology Page | 14
8
10
12
14
16
18
20
0 2 4 6 8 10 12 14 16 18
DissolvedOxygen
Time (min)
FlowRate 1
Flow Rate 2
Graphical Representation
The following graph based on the values by Table 2 shows
the cahnge in amount of dissolved oxygen as the time increases.
Graph 2: DO vs Time Representation (Flow Rate Variation)
Separation Processes Lab
Department of Chemical Engineering & Technology Page | 15
Results
The Graph 2 shows variation in dissolved oxygen as the time
and stirrer speed changes. Dissolved oxygen shows a significant change after
sufficient time and at high fllow rate.
Conclusion
The results depict that Dissolved Oxygen is directly proportional to time.
𝑫𝑶 ∝ 𝑻𝒊𝒎𝒆
From the results of experiments we can also conclude that Dissolved Oxygen is
also proportional to flow rate of Air. (Joseph A. Salvato, 2006)
𝑫𝑶 ∝ 𝑭𝒍𝒐𝒘 𝑹𝒂𝒕𝒆
REFRENCES
 ATICO, 2. (2015). Retrieved Feb 2018, from Lab Manual for ATICO
Aeration Unit: https://www.aticoexport.com/product.aeration-
unit/manual.pdf
 Joseph A. Salvato, P. D. (2006). Introduction to Envoirnmental
Engineering,5th Edition. New York State Department of Health Albani, N.Y.
 Manual, A. (n.d.). Retrieved Feb 21, 2018, from Lab Manual for Aeration
Unit: https://ocw.tudelft.nl/wp-content/uploads/Aerationto.pdf

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Aeration unit Lab Report(Separation Lab)

  • 1.
  • 2. Separation Processes Lab Department of Chemical Engineering & Technology Page | 1 Table of Contents ABSTRACT ................................................................................................................................................3 INTRODUCTION.......................................................................................................................................4 PRACTICAL APPLICATIONS................................................................................................................4 EQUIPMENT & PARTS DESCRIPTION...............................................................................................5 1. Aeration Tank ...............................................................................................................................6 2. DO Meter ........................................................................................................................................6 3. Diaphgram Pump.........................................................................................................................6 4. Flow Meter.....................................................................................................................................7 5. Stirrer Controller.........................................................................................................................7 6. Electrical Unit...............................................................................................................................7 EXPERIMENT No. 01...............................................................................................................................8 EXPERIMENT No. 02.............................................................................................................................12 REFRENCES............................................................................................................................................15 Table of Figures Figure 1: Aeration Unit (Manual) .........................................................................5 Figure 2: Aeration Tank (Manual) ........................................................................6 Figure 3: DO Meter (Manual) ...............................................................................6 Figure 4: Diaphragm Pump (Manual)...................................................................6 Figure 5: Flow Meter (Manual).............................................................................7 Figure 6: Stirrer Controller (Manual) ...................................................................7 Figure 7: Electrical Cabin (Manual) .....................................................................7
  • 3. Separation Processes Lab Department of Chemical Engineering & Technology Page | 2 LAB LAYOUT Evaluation Table Tray DrierChemicals Cupboard Rotary Drier Wetted Wall Gas Absorb. Column AerationUnit SolidLiquid Extraction Unit IonExchange Gas/Liq. Absorption Column Distillation ColumnUnit Liq/Liq. Extraction Unit DoorDoor
  • 4. Separation Processes Lab Department of Chemical Engineering & Technology Page | 3 ABSTRACT Aeration is a unit process in which air and water are brought into intimate contact. The contact time and ratio of air to water must be sufficient for effective removal of unwanted gas. Following report concisely explicate the working of an Aeration Unit and major description of equipment. Simple experiments are added for better understanding of equipment and process of Aeration. Observatory columns efficiently describe the effect of various factors upon Aeration. Graphical representations make it easy to judge the trend of effect of specific factor upon equipment.
  • 5. Separation Processes Lab Department of Chemical Engineering & Technology Page | 4 INTRODUCTION The Aeration Unit allows the study of oxygen transfer characteristics of diffused air systems, and the physical and chemical parameters, which influence oxygenation capacity. Aeration Unit demonstrates the water aeration process which, mainly, eliminates smell and taste from water. Aeration is also an effective method of bacteria removal. Two general methods can be used for the aeration of water; 1. Water-fall Aerator 2. Air Diffusion Method The Water fall aerator works through the use of spray nozzles, the water droplets are broken into small droplets or a thin film to enhance counter-current air contact. In the Air Diffusion method, air is diffused into a receiving vessel containing counter-current flowing water, creating very small air bubbles. This ensures good water-air contact for ‘‘scrubbing’’ of the undesired gases from water. (Manual) PRACTICAL APPLICATIONS In industrial water conditioning, one of the major applications of aeration is to remove Carbon Dioxide. Aeration is also used to oxidize the soluble Iron & Manganese to insoluble precipitates. Aeration I soften used to reduce the Carbon Dioxide liberated by a treatment process. Air stripping maybe used to reduce concentrations of volatile organics, such as Chloroform.
  • 6. Separation Processes Lab Department of Chemical Engineering & Technology Page | 5 EQUIPMENT & PARTS DESCRIPTION The Aeration Unit used in experiment is locally fabricated and contain six major parts. Equipment is used for the measurement of Dissolved Oxygen in water at normal conditions of temperature & pressure. Figure 1: Aeration Unit (Manual) Major parts of the equipment as briefly explained later to completely understand the working of Aeration Unit. Electrical wires, air pipe and stirrer motor are not included in thse parts. (ATICO, 2015)
  • 7. Separation Processes Lab Department of Chemical Engineering & Technology Page | 6 1. Aeration Tank The main part of the Aeration tank is the Aeration Tank with a meschanical stirring paddle in it to provide turbulence for better mixing of air with water. Temperature as well as Dissolved Oxygen Meter sensors are mounted at top of the tank. Figure 2: Aeration Tank (Manual) 2. DO Meter DO stands for Dissolved Oxygen Meter and it gives the reading of amount of oxygen dissolved in the tank at normal temperature. Figure 3: DO Meter (Manual) 3. Diaphgram Pump A Diaphram Pump of small duty is also installed with the equipment. A small button is set up on the pump to manually set the flow rate to High or Low. Figure 4: Diaphragm Pump (Manual)
  • 8. Separation Processes Lab Department of Chemical Engineering & Technology Page | 7 4. Flow Meter A flow meter in parallel to Diaphgram Pump is attached to the euipment board to measure the flow rate of air. Scale of the flow meter is pretty high as compared to the duty of the pump, so it need to be replaced. Figure 5: Flow Meter (Manual) 5. Stirrer Controller In order to control the speed of the stirrer a controller setup is used with high low & moderate speeds of the stirrer. Figure 6: Stirrer Controller (Manual) 6. Electrical Unit An Electrical Cabnit is installed at the top of the euipment board to control the stirrer motor and diaphgram motor. Figure 7: Electrical Cabin (Manual)
  • 9. Separation Processes Lab Department of Chemical Engineering & Technology Page | 8 EXPERIMENT No. 01 Objective To observe the absorption of Oxygen in water at various RPM of stirrer. Apparatus  Aeration Tank  DO Meter  Stopwatch Reagents  Water  Air Procedure  Setup the procedure as shown in the Figure 1.  Filled the tank with distilled water.  Inserted the probe of DO meter in the tank.  Made sure that DO meter was properly caliberated and in working condition.  Switched on the air blower & adjusted the flow rate of Air .  Switched the stirrer on & adjusted the RPM.  Noted the readings of Dissolved Oxygen in water after regular intervals of one minute.
  • 10. Separation Processes Lab Department of Chemical Engineering & Technology Page | 9  After that changed the RPM of stirrer & again noted the Dissolved Oxygen in water.  Repeated the above step for High , Medium & Low speeds of the stirrer.  Plotted the graph & compared the results. (Manual) Observations & Calculations Air Flow Rate = 1.75 Stirrer RPM = Low , Medium , High Table 1: Amount of DO change w.r.t time Sr. No Time (min) Dissolved Oxygen (mg/L) 1 0 8.4 2 2 8.8 3 4 9.5 4 7 11 5 8 11.5 6 10 12.3 7 12 13.1 8 15 13.9 9 16 13.9
  • 11. Separation Processes Lab Department of Chemical Engineering & Technology Page | 10 8 9 10 11 12 13 14 15 16 0 5 10 15 20 25 DissolvedOxygen Time (min) Low RPM Medium RPM High RPM Graphical Representation The following graph shows the cahnge in amount of dissolved oxygen as the time increases. Graph 1: DO vs Time Representation (Stirrer Speed Variation)
  • 12. Separation Processes Lab Department of Chemical Engineering & Technology Page | 11 Results The Graph 1 based on the values by Table 1 shows variation in dissolved oxygen as the time and stirrer speed changes. Dissolved oxygen shows a significant change after 15 minutes and at high stirrer speed. Conclusion The results depict that Dissolved Oxygen is directly proportional to time. 𝑫𝑶 ∝ 𝑻𝒊𝒎𝒆 From the results of experiments we can also conclude that Dissolved Oxygen is also proportional to stirrer speed. (Joseph A. Salvato, 2006) 𝑫𝑶 ∝ 𝑺𝒕𝒊𝒓𝒓𝒆𝒓 𝑺𝒑𝒆𝒆𝒅
  • 13. Separation Processes Lab Department of Chemical Engineering & Technology Page | 12 EXPERIMENT No. 02 Objective To observe the absorption of Oxygen in water at various flow rates of Air. Apparatus  Aeration Tank  DO Meter  Stopwatch Reagents  Water  Air Procedure  Setup the procedure as shown in the Figure 1.  Filled the tank with distilled water.  Inserted the probe of DO meter in the tank.  Made sure that DO meter was properly caliberated and in working condition.  Switched on the air blower & adjusted the flow rate of Air.  Switched the stirrer on & adjusted the RPM.  Noted the readings of Dissolved Oxygen in water after regular intervals of one minute.
  • 14. Separation Processes Lab Department of Chemical Engineering & Technology Page | 13  After that changed the flow rate of Air & again noted the Dissolved Oxygen in water.  Repeated the above step for various flow rates of Air.  Plotted the graph & compared the results. (Manual) Observations & Calculations Air Flow Rate = 1.75 & 2.75 Stirrer RPM = Medium Table 2: Amount of DO change w.r.t time Sr. No Time (min) Dissolved Oxygen (mg/L) 1 0 13.9 2 2 14.4 3 4 14.8 4 6 15.3 5 8 16 6 10 16.4 7 12 17.1 8 14 17.6 9 17 17.9
  • 15. Separation Processes Lab Department of Chemical Engineering & Technology Page | 14 8 10 12 14 16 18 20 0 2 4 6 8 10 12 14 16 18 DissolvedOxygen Time (min) FlowRate 1 Flow Rate 2 Graphical Representation The following graph based on the values by Table 2 shows the cahnge in amount of dissolved oxygen as the time increases. Graph 2: DO vs Time Representation (Flow Rate Variation)
  • 16. Separation Processes Lab Department of Chemical Engineering & Technology Page | 15 Results The Graph 2 shows variation in dissolved oxygen as the time and stirrer speed changes. Dissolved oxygen shows a significant change after sufficient time and at high fllow rate. Conclusion The results depict that Dissolved Oxygen is directly proportional to time. 𝑫𝑶 ∝ 𝑻𝒊𝒎𝒆 From the results of experiments we can also conclude that Dissolved Oxygen is also proportional to flow rate of Air. (Joseph A. Salvato, 2006) 𝑫𝑶 ∝ 𝑭𝒍𝒐𝒘 𝑹𝒂𝒕𝒆 REFRENCES  ATICO, 2. (2015). Retrieved Feb 2018, from Lab Manual for ATICO Aeration Unit: https://www.aticoexport.com/product.aeration- unit/manual.pdf  Joseph A. Salvato, P. D. (2006). Introduction to Envoirnmental Engineering,5th Edition. New York State Department of Health Albani, N.Y.  Manual, A. (n.d.). Retrieved Feb 21, 2018, from Lab Manual for Aeration Unit: https://ocw.tudelft.nl/wp-content/uploads/Aerationto.pdf