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International Journal of Research in Engineering and Science (IJRES)
ISSN (Online): 2320-9364, ISSN (Print): 2320-9356
www.ijres.org Volume 3 Issue 6 ǁ June 2015 ǁ PP.55-65
www.ijres.org 55 | Page
Hot Erosion Experiment on the
Blade Material of Dust Contained Gas Turbine
Huang Xinyou1
, Zheng Lingxiang2
, Sun Chen3
, Zhang Zhiying4
, Lu Jiahua*
1-4
(College of Mechanical Engineering, Shanghai University of Engineering Science, China)
*( College of Mechanical Engineering, Shanghai University of Engineering Science, China)
Abstract: Gas turbine is the main power plant use dusty gas of high temperature and high pressure produced
during the industrial processes. At the same time can effectively bring down nitrogen oxide emissions. High
temperature dust gas will erode the surface of turbine blade, not only aerodynamics characteristics of the
destruction (cause of affection to the blade profile) but also jeopardizes the strength of the safety blade.
Therefore, erosion tests carried out on the blade material at a variety of temperature and angle of attack are
very necessary to provide the basis for optimizing blade material. In simulate real conditions reveal the
resistance to erosion of different materials. In this paper, erosion tests carried out on three different blade
materials(1Cr12Mo、X20Cr13、2Cr12NiMo1W1V)at different angle of attack. Test temperature is 200℃ and
300℃. Experimental results showed that: Accumulate mass loss of materials studied all linearly vary according
to the particle quality; 15 ° ~ 25 °, the erosion rate is the highest; 90 °angle of attack shows the lowest erosion
rate; The erosion rate of material 2Cr12NiMo1W1V is higher than the other two materials at 200 ℃ and 300 ℃,
poor resistance to erosion.
Keywords: erosion rate, gas-solid, gas turbine, hot erosion, turbine blades
I. Introduction
In the industrial areas of energy, metallurgy, oil, chemicals, etc, high temperature and high pressure gas
dust produced during industrial processes has enormous potential, among which the gas turbine is the most
typical case. It could not only effectively bring down nitrogen oxide emissions during energy conversion
processes, but also could be used as energy recycle. However high temperature dust gas in loose small particles
according to certain angle and speed eroding material surface, causing wear and tear. This impact not only
aerodynamics characteristics of the destruction (cause of affection to the blade profile) but also jeopardizes the
strength of the safety blade. This phenomenon is common in electric power, machinery, iron and steel, aviation,
chemical and other industries. This becomes one of the important reasons for material damage or equipment
failure [1,2]
.
The erosion on the blade material has carried out many studies at home and abroad [3-6]
, but as a result of
test conditions, test results is still need further argumentation and exploring stage. In this research, firstly
developed hot erosion wind tunnel system, then test three kinds of commonly used blade materials at different
Angle of attack and temperatures to explore the erosion phenomenon, trying to further reveal the erosion of their
features, so as to provide the basis for optimizing blade material.
II. Composition of Test Device
Hot wind tunnel system designed open loop system is shown in Fig. 2-1, contains electric heater, stable
Hot Erosion Experiment on the Blade Material of Dust Contained Gas Turbine
www.ijres.org 56 | Page
section, test section, heat exchanger, dust collector and induced draft fan. The test bench is designed as a
negative pressure system to avoid test particles cannot be well mixed with the airflow due to the atmospheric
pressure inside the duct is higher than that of outside if a positive pressure system applied [7]
. In positive
pressure system, a bypass channel is needed to balance pressure to make the particles suffered particles into the
flow channel. Negative pressure system also can ensure that the high temperature gas in wind tunnel will not
leaked through the cracks, causing danger.
Firstly, erosion particles into the pipe and mixed with heated air by star-shaped feed valve. And then in the
stable section particles are mixed with air and reach a steady speed. In test section, specimens are eroded. Later,
the airflow is cooled by heat exchanger, the dust particles are filtered out by dust filter. Finally, after the
completion of the airflow into the air, the test is finished. The cross-sectional area of the entire experiment began
to shrink before the stable section. This is to make sure the particle stream into the test section have enough
erosion speed and the contraction ratio is approximately 1: 17.36. In the stable section, pipe length to diameter
ratio is 129:1, to ensure that there is sufficient distance particles mixed with the airflow, at the same temperature
with airflow and reached a steady speed.
1
2
4
5
6
7
8
9
10
3
1.Electric heater 2.Star-shaped feed valve 3.Particle hopper 4.Convergent nozzle 5.Stable section
6.Test section 7.Heat exchanger 8.Cooling water tank 9.Dust filter 10.Induced draft fan
Fig. 2-1 Erosion test wind tunnel system schematic diagram
Wind tunnel use electric heater for heating, and temperature is controlled by automatic control device.
Electric heater has rapid heating and cooling rate, high efficiency, good mechanical, high security, air clean
pollution-free, etc. Wind tunnel using the star-shaped feed valve adding particles to the pipe, particles down to
the airflow only by its own gravity, ensure uniform particle concentration. Test section of the specimen clamp
can rotate 360 degrees, to realize stepless attack angle.
There are thirteen temperature sensors, pressure transmitter ten, a flow meter, a pressure gauge and an
anemometer in the wind tunnel system to collect experimental data, signal acquisition, processing and storage
by computer. The Star-shaped feed valve adjustable speed (control particles flow rate) and the angle of attack to
show experimental conditions simultaneously displayed.
III. The Test Scheme
According to different morphologies, erosion material erosion can be summarized as ductile and brittle erosion
Hot Erosion Experiment on the Blade Material of Dust Contained Gas Turbine
www.ijres.org 57 | Page
modes. Generally, it is called ductility erosion if the erosion sand is micro cutting, shovels and other plastic
deformation of the material loss. Plastic materials generally have this feature. If the loss is the micro-cracks
caused by the impact of stress and extends along the crack caused by the process, it belongs to brittle erosion.
Most brittle metals, ceramics, carbides, oxides, etc. have this feature.
Ductility erosion was first proposed by scholars Finnie, when he pointed out that more high-speed impact
surface angular grit, sand protruding corner edge cutting tool will approach the material loss caused by erosion,
strength and impact angle of the erosion, sandy, sand between target shape and nature are closely related. In this
research, brittle and plastic characteristics of blade material can be judged by the conclusion.
3.1 Selection of Test Materials
In this test, there are three different steel are tested. No. for them are 1Cr12Mo, X20Cr13 and 2Cr12NiMo1W.
The main characteristics are shown in Table 3-1.
Table 3-1 Main parameters of the substrate steel
No. Steel brand Main ingredients Application
1 1Cr12Mo
Cr 11.5-13.0 Mo 0.3-0.6
Ni 0.3-0.6 Si<0.5 Cu<0.3
C 0.1-0.15 P<0.04 S<0.03
It’s very commonly used as blades of gas
turbine, compressor guide vanes material,
with high strength, corrosion resistance,
high temperature, and good process
characteristics.
2 X20Cr13
C 0.16-0.25 Si<1 Mn<1
Cr 12-14 S<0.03 P<0.04
It’s a blade steel of turbine imported from
Germany's Siemens, Belong to the
martensitic stainless steel.
3 2Cr12NiMo1W1V
Cr 11-12.5 Mo 0.9-1.25
W0.9-1.25 Ni0.5-1 Si<0.5
Mn0.5-1 Ni0.5-1 C0.2-0.25
It is used for blade, shroud, bolts, valve
stem and so on.
3.2 Selection of Particles
In this test, the test particle selected is quartz sand. Due to coal-bearing is the main working medium of the
gas-solid turbine. Table 3-2 is the analysis to the composition of coal mine in West Virginia Kingston, US [8]
.
Among which the main component is SiO2, so we select quartz sand particles as grains tested representative.
The microscopic observation shows that the appearances of quartz sand are polyhedral particles similar to the
coal-bearing. The diameter of quartz sand is 0.074 mm in this experiment.
Table 3-2 Composition of coal mine in West Virginia Kingston, US [8]
Compound SiO2 Al2O3 Fe2O3 TiO2 CaO MgO Na2O K2O SO3 Undetermined Total
Percentage 54.39 28.58 10.08 0.47 1.28 1.04 0.20 2.09 1.03 0.84 100
3.3 Estimation of Particle Velocity
In the experiment, airflow velocity is easy to get, but the particle velocity needs determined by estimating.
Hot Erosion Experiment on the Blade Material of Dust Contained Gas Turbine
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Among the estimates, assuming that the particles are spherical in shape, and only consider Stokes drag speed
slip between the particles and the gas caused. Under the condition of low particle concentration, ignore
collisions between particles and energy transport between particles and gas (one-way coupling). Based on
multiphase fluid dynamics knowledge [9]
, one dimensional particle momentum equation is obtained:
)(Re
)(
p
p
pgp
f
t
vv
dt
dv 
 3-1
In the formula, pt is particle relaxation time; pv is particle velocity; gv is gas velocity; pRe is
Particles Reynolds; )(Repf is higher Reynolds number, the correction formula of drag coefficient.
Respectively for:
g
pp
p
d
t


18
2
 3-2
g
pgpg
p
vvd

 
Re 3-3
)Re
6
1
1()(Re 3
2
ppf  3-4
Rewritten formula 3-1 into expression of spatial coordinates:
)Re
6
1
1(
)()(
3
2
p
pp
pgp
tv
xvxv
dx
dv



3-5
In the formula, X represents the flow direction of particles in the wind tunnel.
Fig. 3-1 Simplified schematic of the particle flow channel
Simplify the granular flow shape as shown in Fig. 3-1. According to the measured outlet gas velocity, the
size of the pipeline, other related parameters and using the Runge-Kutta method to solve equation 3-1 can
calculate the erosion velocity of particle in the pipe outlet.
Hot Erosion Experiment on the Blade Material of Dust Contained Gas Turbine
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Table 3-3 Particle velocity estimation at the outlet of accelerating straight pipe
Particle type
Particle size
Dp(mm)
Gas velocity
gv (m/s)
Particle velocity
pv (m/s)
pv / gv
Quartz sand 0.074 139 79 0.57
Quartz sand 0.038 139 81 0.58
Quartz sand 0.074 105 62 0.59
Quartz sand 0.038 110 63 0.60
3.4 Effective range of uniform gas-solid flow
There is a great relationship between mass loss of specimen and particle flow rate uniformity. If the erosion area
is too big, particles left nozzle assumes the diffusivity will lead to the edge of the specimen by erosion (that is
mass loss of specimen) assumes the attenuation distribution. However, the erosion area is too small, require
balance a high accuracy to measure the mass loss of specimen. Two cases of the experimental results can not
accurately reflect the erosion characteristics of material. Therefore to determine the area of particle distribution
uniformity is particularly important.
Fig. 3-2 Relationship between particle flow rate uniformity and erosion area
This test bench, nozzle diameter is 2.4 cm, specimens from the nozzle 7 cm. After calibration, particle
flow rate uniformity change with erosion area as shown in Fig. 3-2. The figure shows that erosion area in the
range of 1 square centimeters, the particle flow rate is basically constant, but after the erosion area is more than
1 square centimeters, flow rate decreases with the increasing area. Comprehensive above factors, the specimen
erosion area is 1.5 cm diameter circular (area is 1.76 cm2
). To make erosion experiment results comparable,
calculate the erosion rate divided by area is the erosion rate per unit area.
0.00
1.00
2.00
3.00
4.00
5.00
6.00
7.00
0.00 0.25 0.50 0.75 1.00 1.25 1.50 1.75 2.00
Particleflowrate(g/cm2*min)
Erosion area(cm2)
Hot Erosion Experiment on the Blade Material of Dust Contained Gas Turbine
www.ijres.org 60 | Page
3.5 Relative Quality of Particles and Relative Mass Loss of Specimen
Fig. 3-3 Location diagram of test piece
As shown in Fig. 3-3, when the specimen fixture adjustment to the angle of attack is less than 90°the projection
area in the vertical plan of the erosive area of specimens is reduced. The decrease in the number of particles that
the actual erosion to the specimen. The mass loss of material is not comparable. There are two ways to solve this
contradiction:
The first one is the conception of relative quality of particles [10]
. Refer to figure 3-2, when the Angle of
attack is 90°and the quality of particles is M g, however when the Angle of attack is  degree the quality of
the particles actually impact onto the specimen is only sinM  g. So,when the angle of attack is 90°and the
quality of particles in each test is M g, the quality of particles at the other Angle of attack should be M/sin
g.
The second one is the conception of relative mass loss of specimen [10]
. Scilicet, when the Angle of attack
is less than 90°, each test does not increase the quality of particles, but will be reduced mass loss of specimen.
When the Angle of attack is  degree and the mass loss of specimen is N g that the relative gravity of
specimen is N/ sin g. Scilicet, Compare N/ sin with the mass loss of specimen when the Angle of
attack is 90°.
The method of this experiment is relative gravity of specimen. Its advantage is that use less grain quality
and less test time. Different angles of erosion test finished at the same time have a higher comparability.
3.6 Calculating Erosion Rate
Firstly, clean the processed specimens with ultrasonic cleaning machine in acetone solution. Secondly,
measuring the initial specimen quality in electronic balance which precision is 0.01mg after dying, denoted as
0M .Thirdly, put the test specimen into specimen clamp which can rotate 360 degrees. Fourthly, choose an
angle between 0°and 90°and then do the erosion test. Fifthly, each completed an erosion test, repeat the cleaning,
drying, weighing process. Measuring the specimen quality in electronic balance, denoted as 1M .
Mass loss of specimen: 0 1m=M M  3-6
Relative Mass loss:
m
X=
sin

3-7
Angle of attack
Specime
n
Particles
Hot Erosion Experiment on the Blade Material of Dust Contained Gas Turbine
www.ijres.org 61 | Page
Mass loss of specimen per unit area:
1
Y
X
S
 3-8
In the formula,  is the angle of attack, 1S is the erosive area of specimen.
The analysis on the result of the erosion of the specimens test particles mainly reflected in the change of
specimen quality before and after erosion as well as the ratio of the changes and erosion particle quality, and the
ratio is defined as the erosion rate:
Mass loss of specimen per unit area
Erosion rate =
Quality of particles M
(Y)
( Z)
( )
3-9
IV. Test Results and Analysis
In order to guarantee the reliability of the test data and explore the relationship between the mass loss of
specimen and the accumulate quality of particles, at the same time. In every angle of attack accumulated for six
tests under the same conditions. After each test, measure the quality of specimen and records, calculated the
mass loss of specimen per unit area. Data smoothing and least squares fitting are studied and used to modify the
test data.
4. 1 Accumulate Particle Quality Impact on Mass Loss of Specimen
Fig. 4-1 Accumulate mass loss of Fig. 4-2 Accumulate mass loss of
material 1Cr12Mo at 200 ℃ material 1Cr12Mo at 300 ℃
0
5
10
15
20
25
40 80 120 160 200 240
Y(mg*cm-2)
M(g)
10°
20°
30°
40°
50°
60°
70°
80°
90°
0
5
10
15
20
25
40 80 120 160 200 240
Y(mg*cm-2)
M(g)
10°
20°
30°
40°
50°
60°
70°
80°
90°
Hot Erosion Experiment on the Blade Material of Dust Contained Gas Turbine
www.ijres.org 62 | Page
Fig. 4-3 Accumulate mass loss of Fig. 4-4 Accumulate mass loss of
material X20Cr13 at 200 ℃ material X20Cr13 at 300 ℃
Fig. 4-5 Accumulate mass loss of Fig. 4-6 Accumulate mass loss of
material 2Cr12NiMo1W1V at 200 ℃ material 2Cr12NiMo1W1V at 300 ℃
Fig.4-1 to Fig. 4-6 shows that the three kinds of materials under test conditions, there is linear relationship
between accumulate mass loss of specimen and the quality of particles. The mass loss of specimen is most at
20°the angle of attack. Mass loss of specimen is least at 90°. Usually first mass loss of specimen is more
significant, the main reason is the loose material on surface are more likely to be erosion. Another reason is at
the particle erosion process, the hard particle has cold work hardening on the surface of the specimen like a
cutting tool that improved the erosion resistance of the specimen.
Not only reflects the relationship between mass loss and particle mass, but also based on this linear
relationship, it is possible to measure the relationship between accumulate mass loss and time. It is also possible
to implanted a change factor into predict the blade natural frequency of vibration changes, thus explore the
influence factors of blade life more objectively.
4.2 Influence of Temperature on Erosion Rate
0
5
10
15
20
40 80 120 160 200 240
Y(mg*cm-2)
M(g)
10°
20°
30°
40°
50°
60°
70°
80°
90°
0
5
10
15
20
40 80 120 160 200 240
Y(mg*cm-2)
M(g)
10°
20°
30°
40°
50°
60°
70°
80°
90°
0
5
10
15
20
25
40 80 120 160 200 240
Y(mg*cm-2)
M(g)
10°
20°
30°
40°
50°
60°
70°
80°
90°
0
5
10
15
20
25
40 80 120 160 200 240
Y(mg*cm-2)
M(g)
10°
20°
30°
40°
50°
60°
70°
80°
90°
Hot Erosion Experiment on the Blade Material of Dust Contained Gas Turbine
www.ijres.org 63 | Page
Fig.4-7 Erosion rate comparison of material X20Cr13 Fig.4-8 Erosion rate comparison of material 1Cr12Mo
Fig. 4-9 Erosion rate comparison of material 2Cr12NiMo1W1V
Fig. 4-7 to Fig. 4-9 shows that the maximum erosion rate appeared between 15 ° and 25 ° the minimum erosion
rate at 90 ° angle of attack. The influence of temperature change on the mass loss of material X20Cr13 is
minimal. The most influence is on material 2Cr12NiMo1W1V. The erosion rate of three kinds of materials at
300℃is higher than that at 200 ℃. This phenomenon has certain rationality, because existing studies have shown
that the erosion rate of plastic material along with the change of temperature in general can be divided into three
categories [11]
:(1) Erosion rate decreases with temperature increase and then increases with temperature rise
when achieve the minimum. (2) Below the threshold temperature erosion rate were similar, after more than the
temperature, erosion rate increases with temperature increase rapidly. (3)Erosion rate always increases with
temperature rise. In this experiment proved that the first kind of phenomenon under the condition of the test, and
at what temperature erosion rate will appear the opposite trend change, need more test to verify.
4.3 Erosion Rate Comparison of Different Materials
20
30
40
50
60
70
80
90
10 20 30 40 50 60 70 80 90
Z(mg*cm-2*g-1)
Angle of attack(°)
200℃
300℃
20
30
40
50
60
70
80
90
10 20 30 40 50 60 70 80 90
Z(mg*cm-2*g-1)
Angle of attack(°)
200℃
300℃
20
30
40
50
60
70
80
90
100
110
10 20 30 40 50 60 70 80 90
Z(mg*cm-2*g-1)
Angle of attack(°)
200℃
300℃
Hot Erosion Experiment on the Blade Material of Dust Contained Gas Turbine
www.ijres.org 64 | Page
Fig. 4-10 Erosion rate comparison of three materials Fig. 4-11 Erosion rate comparison of three materials
at 200℃ at 300℃
Fig.4-10 and Fig. 4-11 shows that the erosion rate of material 2Cr12NiMo1W1V is higher than the other two
materials at 200 ℃ and 300 ℃, poor resistance to erosion. The erosion rate of material 1Cr12Mo is higher than
X20Cr13 at small angle of attack but lower at big angle of attack. This provides assistance to gas turbine blade
materials selection under the experimental conditions.
V. Conclusion
In his research first developed hot erosion wind tunnel system, then test three kinds of commonly used
blade materials(1Cr12Mo、X20Cr13、2Cr12NiMo1W1V)at different Angle of attack and temperature, to
explore the erosion of their features. The following conclusions: (1) There is linear relationship between
accumulate mass loss of specimen and the quality of particles at the different angle of attack and temperature. (2)
The maximum erosion rate appeared between 15 ° and 25 ° the minimum erosion rate at 90 ° angle of attack. (3)
The erosion rate of material 2Cr12NiMo1W1V is higher than the other two materials at 200 ℃ and 300 ℃, poor
resistance to erosion. (4) Erosion rate decreases with temperature increase under the condition of test
temperature. At what temperature erosion rate will appear the opposite trend change, need more test to verify.
References
[1] Allen C, Ball A, A review of the perfomance of engineering materials under prevalent tribological and wear situations in South
Africa industries, Tribo Inter,1996,(29):105-116.
[2] Ma Ying, Ren Jun, Li Yuandong, Research Progress of Erosion, Journal of Lanzhou University of Technology,2005,31(1):21-25.
[3] Shun-sen Wang, Guan-wei Liu, Jing-ru Mao, Effects of Coating Thickness, Test Temperature, and Coating Hardness on the
Erosion Resistance of Steam Turbine Blades, Journal of Engineering for Gas Turbines and Power. 2010,2.
[4] Zhao Xianping, Sun Rongjian, Experimental Research of 15CrMo Alloy Steel’s Erosion Resistance at Constant and
HighTemperature, Shanghai Electric Power College Journal,2006,22(1).
[5] Tabakoff, W., and Shanov, V., Erosion Rate Testing at High Temperature for Turbomachinery Use, Surf. Coat. Technol.,
76–77(1–3):75–80.
[6] Wang, S. S., Liu, G. W., Mao, J. R., and Feng, Z. P., 2007, Experimental Investigation on the Solid Particle Erosion in the Control
Stage Nozzles of Steam Turbine, Proceedings of the ASME Turbo Expo 2007, Vol. 6:713–721.
20
30
40
50
60
70
80
90
100
110
10 20 30 40 50 60 70 80 90
Z(mg*cm-2*g-1)
Angle of attack(°)
1Cr12Mo
2Cr12NiMo1W1V
X20Cr13
20
30
40
50
60
70
80
90
100
10 20 30 40 50 60 70 80 90
Z(mg*cm-2*g-1)
Angle of attack(°)
1Cr12Mo
2Cr12NiMo1W1V
X20Cr13
Hot Erosion Experiment on the Blade Material of Dust Contained Gas Turbine
www.ijres.org 65 | Page
[7] Lu Jiahua, Ling Zhiguang, The Gas-solid Two-phase Turbine Blade Erosion Characteristics of the Pneumatic Test Research, Fluid
Mechanics Experiment and Measurement,2003,2.
[8] Tabakoff, W, Metwally, M., Coating effect on particle trajectories and turbine blade erosion, J. of Eng. for Gas Turbines and
Power. 1992, 114(2): 250~ 257.
[9] Shu Chaohui, Wu Keqi, Advanced Fluid Mechanics, China electric power press,2009.
[10] Lu Jiahua, The Viscous Flow Field of Turbine Blade Erosion Numerical Simulation and Experimental Research, Ph.D. Thesis.,
Shanghai University of Science and Technology, 2002.
[11] Nahum Gat, Widen Tabakoff, Some effects of temperature on the erosion of metals, Wear,1978, 50(1):85–94.
Fund project:Shanghai municipal education commission 085 engineering projects (JR0901)
Author: Huang Xinyou(1989-), male, Qingdao China, master, The main research direction is the turbine thermal
state aerodynamic experiment. Tel: 18201751263; E-mail:huangxinyou37@163.com
Corresponding author: Lu Jiahua(1960-), male, Shanghai China, doctor, The main research direction is
multiphase fluid dynamics numerical analysis and experiment research. Tel: 021-67791007; E-mail:
lujiahua@sues.edu.cn

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Hot Erosion Experiment on the Blade Material of Dust Contained Gas Turbine

  • 1. International Journal of Research in Engineering and Science (IJRES) ISSN (Online): 2320-9364, ISSN (Print): 2320-9356 www.ijres.org Volume 3 Issue 6 ǁ June 2015 ǁ PP.55-65 www.ijres.org 55 | Page Hot Erosion Experiment on the Blade Material of Dust Contained Gas Turbine Huang Xinyou1 , Zheng Lingxiang2 , Sun Chen3 , Zhang Zhiying4 , Lu Jiahua* 1-4 (College of Mechanical Engineering, Shanghai University of Engineering Science, China) *( College of Mechanical Engineering, Shanghai University of Engineering Science, China) Abstract: Gas turbine is the main power plant use dusty gas of high temperature and high pressure produced during the industrial processes. At the same time can effectively bring down nitrogen oxide emissions. High temperature dust gas will erode the surface of turbine blade, not only aerodynamics characteristics of the destruction (cause of affection to the blade profile) but also jeopardizes the strength of the safety blade. Therefore, erosion tests carried out on the blade material at a variety of temperature and angle of attack are very necessary to provide the basis for optimizing blade material. In simulate real conditions reveal the resistance to erosion of different materials. In this paper, erosion tests carried out on three different blade materials(1Cr12Mo、X20Cr13、2Cr12NiMo1W1V)at different angle of attack. Test temperature is 200℃ and 300℃. Experimental results showed that: Accumulate mass loss of materials studied all linearly vary according to the particle quality; 15 ° ~ 25 °, the erosion rate is the highest; 90 °angle of attack shows the lowest erosion rate; The erosion rate of material 2Cr12NiMo1W1V is higher than the other two materials at 200 ℃ and 300 ℃, poor resistance to erosion. Keywords: erosion rate, gas-solid, gas turbine, hot erosion, turbine blades I. Introduction In the industrial areas of energy, metallurgy, oil, chemicals, etc, high temperature and high pressure gas dust produced during industrial processes has enormous potential, among which the gas turbine is the most typical case. It could not only effectively bring down nitrogen oxide emissions during energy conversion processes, but also could be used as energy recycle. However high temperature dust gas in loose small particles according to certain angle and speed eroding material surface, causing wear and tear. This impact not only aerodynamics characteristics of the destruction (cause of affection to the blade profile) but also jeopardizes the strength of the safety blade. This phenomenon is common in electric power, machinery, iron and steel, aviation, chemical and other industries. This becomes one of the important reasons for material damage or equipment failure [1,2] . The erosion on the blade material has carried out many studies at home and abroad [3-6] , but as a result of test conditions, test results is still need further argumentation and exploring stage. In this research, firstly developed hot erosion wind tunnel system, then test three kinds of commonly used blade materials at different Angle of attack and temperatures to explore the erosion phenomenon, trying to further reveal the erosion of their features, so as to provide the basis for optimizing blade material. II. Composition of Test Device Hot wind tunnel system designed open loop system is shown in Fig. 2-1, contains electric heater, stable
  • 2. Hot Erosion Experiment on the Blade Material of Dust Contained Gas Turbine www.ijres.org 56 | Page section, test section, heat exchanger, dust collector and induced draft fan. The test bench is designed as a negative pressure system to avoid test particles cannot be well mixed with the airflow due to the atmospheric pressure inside the duct is higher than that of outside if a positive pressure system applied [7] . In positive pressure system, a bypass channel is needed to balance pressure to make the particles suffered particles into the flow channel. Negative pressure system also can ensure that the high temperature gas in wind tunnel will not leaked through the cracks, causing danger. Firstly, erosion particles into the pipe and mixed with heated air by star-shaped feed valve. And then in the stable section particles are mixed with air and reach a steady speed. In test section, specimens are eroded. Later, the airflow is cooled by heat exchanger, the dust particles are filtered out by dust filter. Finally, after the completion of the airflow into the air, the test is finished. The cross-sectional area of the entire experiment began to shrink before the stable section. This is to make sure the particle stream into the test section have enough erosion speed and the contraction ratio is approximately 1: 17.36. In the stable section, pipe length to diameter ratio is 129:1, to ensure that there is sufficient distance particles mixed with the airflow, at the same temperature with airflow and reached a steady speed. 1 2 4 5 6 7 8 9 10 3 1.Electric heater 2.Star-shaped feed valve 3.Particle hopper 4.Convergent nozzle 5.Stable section 6.Test section 7.Heat exchanger 8.Cooling water tank 9.Dust filter 10.Induced draft fan Fig. 2-1 Erosion test wind tunnel system schematic diagram Wind tunnel use electric heater for heating, and temperature is controlled by automatic control device. Electric heater has rapid heating and cooling rate, high efficiency, good mechanical, high security, air clean pollution-free, etc. Wind tunnel using the star-shaped feed valve adding particles to the pipe, particles down to the airflow only by its own gravity, ensure uniform particle concentration. Test section of the specimen clamp can rotate 360 degrees, to realize stepless attack angle. There are thirteen temperature sensors, pressure transmitter ten, a flow meter, a pressure gauge and an anemometer in the wind tunnel system to collect experimental data, signal acquisition, processing and storage by computer. The Star-shaped feed valve adjustable speed (control particles flow rate) and the angle of attack to show experimental conditions simultaneously displayed. III. The Test Scheme According to different morphologies, erosion material erosion can be summarized as ductile and brittle erosion
  • 3. Hot Erosion Experiment on the Blade Material of Dust Contained Gas Turbine www.ijres.org 57 | Page modes. Generally, it is called ductility erosion if the erosion sand is micro cutting, shovels and other plastic deformation of the material loss. Plastic materials generally have this feature. If the loss is the micro-cracks caused by the impact of stress and extends along the crack caused by the process, it belongs to brittle erosion. Most brittle metals, ceramics, carbides, oxides, etc. have this feature. Ductility erosion was first proposed by scholars Finnie, when he pointed out that more high-speed impact surface angular grit, sand protruding corner edge cutting tool will approach the material loss caused by erosion, strength and impact angle of the erosion, sandy, sand between target shape and nature are closely related. In this research, brittle and plastic characteristics of blade material can be judged by the conclusion. 3.1 Selection of Test Materials In this test, there are three different steel are tested. No. for them are 1Cr12Mo, X20Cr13 and 2Cr12NiMo1W. The main characteristics are shown in Table 3-1. Table 3-1 Main parameters of the substrate steel No. Steel brand Main ingredients Application 1 1Cr12Mo Cr 11.5-13.0 Mo 0.3-0.6 Ni 0.3-0.6 Si<0.5 Cu<0.3 C 0.1-0.15 P<0.04 S<0.03 It’s very commonly used as blades of gas turbine, compressor guide vanes material, with high strength, corrosion resistance, high temperature, and good process characteristics. 2 X20Cr13 C 0.16-0.25 Si<1 Mn<1 Cr 12-14 S<0.03 P<0.04 It’s a blade steel of turbine imported from Germany's Siemens, Belong to the martensitic stainless steel. 3 2Cr12NiMo1W1V Cr 11-12.5 Mo 0.9-1.25 W0.9-1.25 Ni0.5-1 Si<0.5 Mn0.5-1 Ni0.5-1 C0.2-0.25 It is used for blade, shroud, bolts, valve stem and so on. 3.2 Selection of Particles In this test, the test particle selected is quartz sand. Due to coal-bearing is the main working medium of the gas-solid turbine. Table 3-2 is the analysis to the composition of coal mine in West Virginia Kingston, US [8] . Among which the main component is SiO2, so we select quartz sand particles as grains tested representative. The microscopic observation shows that the appearances of quartz sand are polyhedral particles similar to the coal-bearing. The diameter of quartz sand is 0.074 mm in this experiment. Table 3-2 Composition of coal mine in West Virginia Kingston, US [8] Compound SiO2 Al2O3 Fe2O3 TiO2 CaO MgO Na2O K2O SO3 Undetermined Total Percentage 54.39 28.58 10.08 0.47 1.28 1.04 0.20 2.09 1.03 0.84 100 3.3 Estimation of Particle Velocity In the experiment, airflow velocity is easy to get, but the particle velocity needs determined by estimating.
  • 4. Hot Erosion Experiment on the Blade Material of Dust Contained Gas Turbine www.ijres.org 58 | Page Among the estimates, assuming that the particles are spherical in shape, and only consider Stokes drag speed slip between the particles and the gas caused. Under the condition of low particle concentration, ignore collisions between particles and energy transport between particles and gas (one-way coupling). Based on multiphase fluid dynamics knowledge [9] , one dimensional particle momentum equation is obtained: )(Re )( p p pgp f t vv dt dv   3-1 In the formula, pt is particle relaxation time; pv is particle velocity; gv is gas velocity; pRe is Particles Reynolds; )(Repf is higher Reynolds number, the correction formula of drag coefficient. Respectively for: g pp p d t   18 2  3-2 g pgpg p vvd    Re 3-3 )Re 6 1 1()(Re 3 2 ppf  3-4 Rewritten formula 3-1 into expression of spatial coordinates: )Re 6 1 1( )()( 3 2 p pp pgp tv xvxv dx dv    3-5 In the formula, X represents the flow direction of particles in the wind tunnel. Fig. 3-1 Simplified schematic of the particle flow channel Simplify the granular flow shape as shown in Fig. 3-1. According to the measured outlet gas velocity, the size of the pipeline, other related parameters and using the Runge-Kutta method to solve equation 3-1 can calculate the erosion velocity of particle in the pipe outlet.
  • 5. Hot Erosion Experiment on the Blade Material of Dust Contained Gas Turbine www.ijres.org 59 | Page Table 3-3 Particle velocity estimation at the outlet of accelerating straight pipe Particle type Particle size Dp(mm) Gas velocity gv (m/s) Particle velocity pv (m/s) pv / gv Quartz sand 0.074 139 79 0.57 Quartz sand 0.038 139 81 0.58 Quartz sand 0.074 105 62 0.59 Quartz sand 0.038 110 63 0.60 3.4 Effective range of uniform gas-solid flow There is a great relationship between mass loss of specimen and particle flow rate uniformity. If the erosion area is too big, particles left nozzle assumes the diffusivity will lead to the edge of the specimen by erosion (that is mass loss of specimen) assumes the attenuation distribution. However, the erosion area is too small, require balance a high accuracy to measure the mass loss of specimen. Two cases of the experimental results can not accurately reflect the erosion characteristics of material. Therefore to determine the area of particle distribution uniformity is particularly important. Fig. 3-2 Relationship between particle flow rate uniformity and erosion area This test bench, nozzle diameter is 2.4 cm, specimens from the nozzle 7 cm. After calibration, particle flow rate uniformity change with erosion area as shown in Fig. 3-2. The figure shows that erosion area in the range of 1 square centimeters, the particle flow rate is basically constant, but after the erosion area is more than 1 square centimeters, flow rate decreases with the increasing area. Comprehensive above factors, the specimen erosion area is 1.5 cm diameter circular (area is 1.76 cm2 ). To make erosion experiment results comparable, calculate the erosion rate divided by area is the erosion rate per unit area. 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 0.00 0.25 0.50 0.75 1.00 1.25 1.50 1.75 2.00 Particleflowrate(g/cm2*min) Erosion area(cm2)
  • 6. Hot Erosion Experiment on the Blade Material of Dust Contained Gas Turbine www.ijres.org 60 | Page 3.5 Relative Quality of Particles and Relative Mass Loss of Specimen Fig. 3-3 Location diagram of test piece As shown in Fig. 3-3, when the specimen fixture adjustment to the angle of attack is less than 90°the projection area in the vertical plan of the erosive area of specimens is reduced. The decrease in the number of particles that the actual erosion to the specimen. The mass loss of material is not comparable. There are two ways to solve this contradiction: The first one is the conception of relative quality of particles [10] . Refer to figure 3-2, when the Angle of attack is 90°and the quality of particles is M g, however when the Angle of attack is  degree the quality of the particles actually impact onto the specimen is only sinM  g. So,when the angle of attack is 90°and the quality of particles in each test is M g, the quality of particles at the other Angle of attack should be M/sin g. The second one is the conception of relative mass loss of specimen [10] . Scilicet, when the Angle of attack is less than 90°, each test does not increase the quality of particles, but will be reduced mass loss of specimen. When the Angle of attack is  degree and the mass loss of specimen is N g that the relative gravity of specimen is N/ sin g. Scilicet, Compare N/ sin with the mass loss of specimen when the Angle of attack is 90°. The method of this experiment is relative gravity of specimen. Its advantage is that use less grain quality and less test time. Different angles of erosion test finished at the same time have a higher comparability. 3.6 Calculating Erosion Rate Firstly, clean the processed specimens with ultrasonic cleaning machine in acetone solution. Secondly, measuring the initial specimen quality in electronic balance which precision is 0.01mg after dying, denoted as 0M .Thirdly, put the test specimen into specimen clamp which can rotate 360 degrees. Fourthly, choose an angle between 0°and 90°and then do the erosion test. Fifthly, each completed an erosion test, repeat the cleaning, drying, weighing process. Measuring the specimen quality in electronic balance, denoted as 1M . Mass loss of specimen: 0 1m=M M  3-6 Relative Mass loss: m X= sin  3-7 Angle of attack Specime n Particles
  • 7. Hot Erosion Experiment on the Blade Material of Dust Contained Gas Turbine www.ijres.org 61 | Page Mass loss of specimen per unit area: 1 Y X S  3-8 In the formula,  is the angle of attack, 1S is the erosive area of specimen. The analysis on the result of the erosion of the specimens test particles mainly reflected in the change of specimen quality before and after erosion as well as the ratio of the changes and erosion particle quality, and the ratio is defined as the erosion rate: Mass loss of specimen per unit area Erosion rate = Quality of particles M (Y) ( Z) ( ) 3-9 IV. Test Results and Analysis In order to guarantee the reliability of the test data and explore the relationship between the mass loss of specimen and the accumulate quality of particles, at the same time. In every angle of attack accumulated for six tests under the same conditions. After each test, measure the quality of specimen and records, calculated the mass loss of specimen per unit area. Data smoothing and least squares fitting are studied and used to modify the test data. 4. 1 Accumulate Particle Quality Impact on Mass Loss of Specimen Fig. 4-1 Accumulate mass loss of Fig. 4-2 Accumulate mass loss of material 1Cr12Mo at 200 ℃ material 1Cr12Mo at 300 ℃ 0 5 10 15 20 25 40 80 120 160 200 240 Y(mg*cm-2) M(g) 10° 20° 30° 40° 50° 60° 70° 80° 90° 0 5 10 15 20 25 40 80 120 160 200 240 Y(mg*cm-2) M(g) 10° 20° 30° 40° 50° 60° 70° 80° 90°
  • 8. Hot Erosion Experiment on the Blade Material of Dust Contained Gas Turbine www.ijres.org 62 | Page Fig. 4-3 Accumulate mass loss of Fig. 4-4 Accumulate mass loss of material X20Cr13 at 200 ℃ material X20Cr13 at 300 ℃ Fig. 4-5 Accumulate mass loss of Fig. 4-6 Accumulate mass loss of material 2Cr12NiMo1W1V at 200 ℃ material 2Cr12NiMo1W1V at 300 ℃ Fig.4-1 to Fig. 4-6 shows that the three kinds of materials under test conditions, there is linear relationship between accumulate mass loss of specimen and the quality of particles. The mass loss of specimen is most at 20°the angle of attack. Mass loss of specimen is least at 90°. Usually first mass loss of specimen is more significant, the main reason is the loose material on surface are more likely to be erosion. Another reason is at the particle erosion process, the hard particle has cold work hardening on the surface of the specimen like a cutting tool that improved the erosion resistance of the specimen. Not only reflects the relationship between mass loss and particle mass, but also based on this linear relationship, it is possible to measure the relationship between accumulate mass loss and time. It is also possible to implanted a change factor into predict the blade natural frequency of vibration changes, thus explore the influence factors of blade life more objectively. 4.2 Influence of Temperature on Erosion Rate 0 5 10 15 20 40 80 120 160 200 240 Y(mg*cm-2) M(g) 10° 20° 30° 40° 50° 60° 70° 80° 90° 0 5 10 15 20 40 80 120 160 200 240 Y(mg*cm-2) M(g) 10° 20° 30° 40° 50° 60° 70° 80° 90° 0 5 10 15 20 25 40 80 120 160 200 240 Y(mg*cm-2) M(g) 10° 20° 30° 40° 50° 60° 70° 80° 90° 0 5 10 15 20 25 40 80 120 160 200 240 Y(mg*cm-2) M(g) 10° 20° 30° 40° 50° 60° 70° 80° 90°
  • 9. Hot Erosion Experiment on the Blade Material of Dust Contained Gas Turbine www.ijres.org 63 | Page Fig.4-7 Erosion rate comparison of material X20Cr13 Fig.4-8 Erosion rate comparison of material 1Cr12Mo Fig. 4-9 Erosion rate comparison of material 2Cr12NiMo1W1V Fig. 4-7 to Fig. 4-9 shows that the maximum erosion rate appeared between 15 ° and 25 ° the minimum erosion rate at 90 ° angle of attack. The influence of temperature change on the mass loss of material X20Cr13 is minimal. The most influence is on material 2Cr12NiMo1W1V. The erosion rate of three kinds of materials at 300℃is higher than that at 200 ℃. This phenomenon has certain rationality, because existing studies have shown that the erosion rate of plastic material along with the change of temperature in general can be divided into three categories [11] :(1) Erosion rate decreases with temperature increase and then increases with temperature rise when achieve the minimum. (2) Below the threshold temperature erosion rate were similar, after more than the temperature, erosion rate increases with temperature increase rapidly. (3)Erosion rate always increases with temperature rise. In this experiment proved that the first kind of phenomenon under the condition of the test, and at what temperature erosion rate will appear the opposite trend change, need more test to verify. 4.3 Erosion Rate Comparison of Different Materials 20 30 40 50 60 70 80 90 10 20 30 40 50 60 70 80 90 Z(mg*cm-2*g-1) Angle of attack(°) 200℃ 300℃ 20 30 40 50 60 70 80 90 10 20 30 40 50 60 70 80 90 Z(mg*cm-2*g-1) Angle of attack(°) 200℃ 300℃ 20 30 40 50 60 70 80 90 100 110 10 20 30 40 50 60 70 80 90 Z(mg*cm-2*g-1) Angle of attack(°) 200℃ 300℃
  • 10. Hot Erosion Experiment on the Blade Material of Dust Contained Gas Turbine www.ijres.org 64 | Page Fig. 4-10 Erosion rate comparison of three materials Fig. 4-11 Erosion rate comparison of three materials at 200℃ at 300℃ Fig.4-10 and Fig. 4-11 shows that the erosion rate of material 2Cr12NiMo1W1V is higher than the other two materials at 200 ℃ and 300 ℃, poor resistance to erosion. The erosion rate of material 1Cr12Mo is higher than X20Cr13 at small angle of attack but lower at big angle of attack. This provides assistance to gas turbine blade materials selection under the experimental conditions. V. Conclusion In his research first developed hot erosion wind tunnel system, then test three kinds of commonly used blade materials(1Cr12Mo、X20Cr13、2Cr12NiMo1W1V)at different Angle of attack and temperature, to explore the erosion of their features. The following conclusions: (1) There is linear relationship between accumulate mass loss of specimen and the quality of particles at the different angle of attack and temperature. (2) The maximum erosion rate appeared between 15 ° and 25 ° the minimum erosion rate at 90 ° angle of attack. (3) The erosion rate of material 2Cr12NiMo1W1V is higher than the other two materials at 200 ℃ and 300 ℃, poor resistance to erosion. (4) Erosion rate decreases with temperature increase under the condition of test temperature. At what temperature erosion rate will appear the opposite trend change, need more test to verify. References [1] Allen C, Ball A, A review of the perfomance of engineering materials under prevalent tribological and wear situations in South Africa industries, Tribo Inter,1996,(29):105-116. [2] Ma Ying, Ren Jun, Li Yuandong, Research Progress of Erosion, Journal of Lanzhou University of Technology,2005,31(1):21-25. [3] Shun-sen Wang, Guan-wei Liu, Jing-ru Mao, Effects of Coating Thickness, Test Temperature, and Coating Hardness on the Erosion Resistance of Steam Turbine Blades, Journal of Engineering for Gas Turbines and Power. 2010,2. [4] Zhao Xianping, Sun Rongjian, Experimental Research of 15CrMo Alloy Steel’s Erosion Resistance at Constant and HighTemperature, Shanghai Electric Power College Journal,2006,22(1). [5] Tabakoff, W., and Shanov, V., Erosion Rate Testing at High Temperature for Turbomachinery Use, Surf. Coat. Technol., 76–77(1–3):75–80. [6] Wang, S. S., Liu, G. W., Mao, J. R., and Feng, Z. P., 2007, Experimental Investigation on the Solid Particle Erosion in the Control Stage Nozzles of Steam Turbine, Proceedings of the ASME Turbo Expo 2007, Vol. 6:713–721. 20 30 40 50 60 70 80 90 100 110 10 20 30 40 50 60 70 80 90 Z(mg*cm-2*g-1) Angle of attack(°) 1Cr12Mo 2Cr12NiMo1W1V X20Cr13 20 30 40 50 60 70 80 90 100 10 20 30 40 50 60 70 80 90 Z(mg*cm-2*g-1) Angle of attack(°) 1Cr12Mo 2Cr12NiMo1W1V X20Cr13
  • 11. Hot Erosion Experiment on the Blade Material of Dust Contained Gas Turbine www.ijres.org 65 | Page [7] Lu Jiahua, Ling Zhiguang, The Gas-solid Two-phase Turbine Blade Erosion Characteristics of the Pneumatic Test Research, Fluid Mechanics Experiment and Measurement,2003,2. [8] Tabakoff, W, Metwally, M., Coating effect on particle trajectories and turbine blade erosion, J. of Eng. for Gas Turbines and Power. 1992, 114(2): 250~ 257. [9] Shu Chaohui, Wu Keqi, Advanced Fluid Mechanics, China electric power press,2009. [10] Lu Jiahua, The Viscous Flow Field of Turbine Blade Erosion Numerical Simulation and Experimental Research, Ph.D. Thesis., Shanghai University of Science and Technology, 2002. [11] Nahum Gat, Widen Tabakoff, Some effects of temperature on the erosion of metals, Wear,1978, 50(1):85–94. Fund project:Shanghai municipal education commission 085 engineering projects (JR0901) Author: Huang Xinyou(1989-), male, Qingdao China, master, The main research direction is the turbine thermal state aerodynamic experiment. Tel: 18201751263; E-mail:huangxinyou37@163.com Corresponding author: Lu Jiahua(1960-), male, Shanghai China, doctor, The main research direction is multiphase fluid dynamics numerical analysis and experiment research. Tel: 021-67791007; E-mail: lujiahua@sues.edu.cn