SlideShare a Scribd company logo
1 of 8
Download to read offline
P. K. MandalInt. Journal of Engineering Research and Applicationswww.ijera.com
ISSN: 2248-9622, Vol. 6, Issue 1, (Part - 2) January 2016, pp.40-47
www.ijera.com 40|P a g e
A refined energy-based model for friction stir processing of Al-
Zn-Mg alloy
P. K. Mandal
Department of Metallurgy, Amal Jyothi College of Engineering, Kanjirapally, Kerala-686518, INDIA
Abstract
Friction stir processing (FSP) is a promising solid state surface modification technique. Also, considered as an
innovative technique that the FSPwas employed to modify the surface layer of aluminium alloy. The FSP passes
of only two passes were applied on aluminium alloy samples. A rotating tool with a pin and shoulder is inserted
into a single piece of material and results in significant microstructural changes in the processed zone, due to
intense plastic deformation. It has been proved to be an effective way to refine the microstructure of aluminium
alloys, and thereby improve the mechanical properties. In procedural phenomenon there are different parameters
adjustment have been worked out to refine microstructure and several properties characterised to TEM, SEM,
FESEM and mechanical properties. In this study, a refined energy based model that estimates the energy
generated due to friction and plastic deformation is presented with the help ofexperimental and theoretical
results available in many literatures. The model is applied to 7xxx series of aluminium alloys.
Keywords: FSP, solid-state process, processed zone, energy generation, 7xxx series.
I. Introduction
Age-hardening is the prime criteria in 7xxx
series of Al alloy. It has several technological
importances likely to as high strength light metal
with various precipitation phases terminated from the
supersaturated sold solution. There is an inseparable
relationship between their improved combination of
mechanical properties and the large number of fine
precipitates formed during artificial ageing. The alloy
composition, artificial ageing temperature and
thermal history (solution treatment, quenching in
water, natural ageing) are the main parameters
influencing the age hardening response [1-5].
Generally, age hardening response is the increase in
yield strength during artificial ageing than natural
aged condition. A high yield strength implies a high
resistance to dislocation motion [6]. It is also well
known that adding minor scandium in aluminium
alloy can refine grains and increase tensile strength,
which attributed to the presence of coherent, L12-
ordered Al3Sc particles. It can substantially inhibit
recrystallization and pin subgrain boundaries and
dislocations [7-11]. By adapting the concepts of
friction stir welding (FSW), a new processing
technique, friction stir processing (FSP), has been
recently developed. The basic concept of FSP is
remarkably simple. A rotating tool with a pin and
shoulder is inserted into a single piece of material and
results in significant microstructural changes in the
processed zone, due to intense plastic deformation at
elevated temperature resulting in significant grain
refinement [12-15].Therefore, FSP has been proved
to be an effective way to refine the microstructure of
aluminium alloys, and thereby improve the
mechanical properties. The microstructure and
properties of the modified layer depend on the
amount of fractional heat generated by processing.
Actually, heat is generated due to plastic deformation
of the workpiece and the effect of the friction
between the surfaces of the tool and the workpiece.
The process is carried out in solid state at low
temperature, typically around 0.6 to 0.7 of the
aluminium alloy fusion temperature. The processed
zone is deformed and under the thermal effect
recovers and recrystallizes, forming a defect-free
recrystallized fine grain microstructure. During
experimental FSP, it is seen that in aluminium alloy
the action of tool produces different microstructurally
distinct regions; the stir zone (SZ), the thermo-
mechanically affected zone (TMAZ) and the heat
affected zone (HAZ). The stir zone is in centre of
FSP and has undergone the most severe plastic
deformation during processing. The stir zone grains
suggest effective strains together with a
microstructural evolution that occurs by a
combination of hot working and a dynamic recovery
or recrystallization. The temperature reached in the
stir zone is known as being situated in the range of
480 o
C [C.B. Fuller et al., 2010; at 640 rpm, 160
mm/min]for the aluminium alloy. The authors like
Heurtier et al. and [2006] and Hamilton et al. [2008]
have been proposed energy based model for the FSW
during their works [16]. In fact, the energy due to
plastic deformation and friction of the shoulder with
the surface of the workpiece are related and
competing each other. As the heat generated by the
shoulder is low, the flow stress is higher and hence
the resulting plastic deformation energy increases. On
RESEARCH ARTICLE OPEN ACCESS
P. K. MandalInt. Journal of Engineering Research and Applicationswww.ijera.com
ISSN: 2248-9622, Vol. 6, Issue 1, (Part - 2) January 2016, pp.40-47
www.ijera.com 41|P a g e
the other hand, as the heat generated by the shoulder
is high, the flow stress reduces and as a result the
plastic strain contribution decreases. As per
Khandkarโ€™s torque-based model for which the total
torque is the sum of torque contributions from the
tool shoulder against the workpiece, the bottom of the
tool pin against thickness material and the pin
surface against thickness material [17]. There are
several characterizations have been done likely to
FESEM (field emission scanning electron
microscopy), SEM (scanning electron microscopy)
and age hardening phenomena through Vickerโ€™s
hardness testing. The aim of this study is to
investigate the effects of double FSP passes on
microstructural and mechanical properties of
aluminium alloy. Besides, the effects of the plastic
deformation as well as heat energy generation as
compared to the theoretical and experimental results
available in many literatures. In this work, heat is
modelled to be generated by the friction of the
shoulder and plastic deformation.
II. Experimental procedure
The research was conducted on cast plate as well
as different heat treated plates of 7xxx series of
aluminium alloy with the dimension as 150 ร— 90 ร— 8
mm3
, and the chemical composition is presented in
Table-1. Standard metallographic procedures were
followed for the macro and microstructural analysis.
A modified Kellerโ€™s reagent was used for etching of
metallographic samples. The age hardening
characteristics have been identified through Vickerโ€™s
hardness measurements at 10 kg. load with 15 min
dwell time at different time intervals at 120, 140, 180
o
C temperatures, respectively. Obviously, an as-cast
sample first solution treated from 465 o
C for 1h then
immediately water quenching (i.e., T4 heat
treatment), then maintained above artificial ageing
temperatures (i.e., T6 heat treatment) and performed
hardness sequentially upto 16 h ageing time. The cast
plates were subjected to double FSP passes along the
clockwise direction with predetermined rotational
speed and traverse speed. The FSP was conducted on
the base of a conventional vertical milling machine.
The machine was well equipped with appropriate
devices to collection data during working period. The
materials for tensile specimens were produced (i.e.,
pick up along the stir zone) with tool parameters of
720 rpm (tool rotational speed) and 80 mm/min (plate
travel speed) from the different heat treated
conditions (in Fig.-1.a). Used tool dimensions
(shoulder dia. 25 mm, shoulder height 20 mm, pin
root dia. 6 mm, pin tip dia. 3 mm, and pin height 3.5
mm) were selected during experimental FSP.
Similarly, the FSP tool geometry has been referred as
per Hamilton et al. energy model as shown in Fig.-
1(b). It is well know that the material is transported
from advancing side (A) to the retreating side (R)
during rotational phenomena. The plasticized
material may travel many cycles around the tool
before being deposited. Microstructural evolution
was studied using scanning electron microscopy
(SEM) and field emission scanning electron
microscopy (FESEM) and the resultant mechanical
properties were examined with microhardness
measurements and tensile tests. Similarly,
transmission electron microscopy (TEM) and X-ray
diffraction (XRD) methods characterization were
examined for materials intuitive precipitation
phenomena. The tensile test was conducted in Instron
(universal testing machine) UTM(25 KN, H25 K-S,
UK). The tensile samples (flat shape sample
dimensions (mm): full length 58, gauge length 26,
width 4) had collected from stir zone, and tested with
cross head speed 1 mm/min at room temperature.
Table-1: Chemical composition analyzed by ICP-AES (in wt%).
Alloy no. Zn Mg Sc Si Fe Al Zn+Mg Zn/Mg
1 8.24 5.67 0.87 0.88 0.42 Bal. 13.91 1.45
Fig.-1: (a) Schematic illustration of the friction stir processing (FSP) set-up; (b) Geometry of the FSP tool.
(a) (b)
P. K. MandalInt. Journal of Engineering Research and Applicationswww.ijera.com
ISSN: 2248-9622, Vol. 6, Issue 1, (Part - 2) January 2016, pp.40-47
www.ijera.com 42|P a g e
Table-2: Processing parameters of FSP.
FSP parameters (experiment performed through double passes)
Tool rotation speed
ฯ‰ (rpm)
Work piece travel speed
๐œ ๐‘œ (mm/min)
Axial compressive force
F (KN)
Pin angle
(o
)
720 80 15 2.5
III. Results and discussion
The Al-Zn-Mg alloy is age hardening aluminium
alloy. There are several phases transitions have been
occurred during ageing heat treatment. The GP zones
(GP I and GP II) and ฮฎ are the phases that contribute
to the precipitation hardening of this alloy in the
under-ageing and peak-ageing conditions, while ฮท
forms during over-ageing conditions. Moreover, Sc
addition in aluminium alloy consists of a spatial
distribution of Al3Sc particles. These small coherent
particles with nano size were distributed
homogeneously throughout the grains. Also, ample
interaction between a matrix dislocation and an Al3Sc
precipitates at 400o
C [18]. In Fig.-2 shows the of
hardness measurements, with the error bars indicating
the deviations of individual measurements. In fact,
the hardness-ageing curve can be roughly divided
into three regions: region I (i.e., called under-aged)
with a gradual increase in harness for all ageing
curves; region II (i.e., called peak-aged) with peak
hardness accompanied by slight hardness decreases
over a long time ageing duration; region III (i.e.,
called over-aged) with a further hardness decreases.
In present three ageing curves have shown gradually
hardness diminish due to growth of the ฮท (MgZn2)
precursor particles may lead to loss of the lattice
match or coherency between the matrix and the
particles [19,1]. When the ageing temperature is
higher the peak formation earlier than at lower ageing
temperatures. On the other hand, Sc additions in
aluminium alloy ageing peak formation accelerate
with high value but coarsening effect one more
adversely phenomena during ageing. Hardening
effect of Sc useful upto 0.6 wt% beyond this
coarsening effect dominates in our experimental
observation and many literature references. During
ageing, Al3Sc particle coherency is maintained until a
critical size is reached. Above that, heterogeneous
precipitation occurs indicated by the formation of the
new nuclei on dislocations and grain boundaries. As
mention in literature, introduction of dislocation
networks to the Al/Al3Sc interface is most possibly
related to coherency loss, low elastic strain energy
caused by the reduction in the lattice misfit [20, 8].
At 120 0
C ageing shows higher hardening response in
among three ageing temperatures. Stability of GP
zones with high Sc content Al3Sc particles can be
claimed higher hardness value. Also, many literatures
supported at this temperature GP formation and
acceleration by Sc added Al-Zn-Mg alloy. At 140 o
C
ageing shows moderate hardening response although
this temperature regime specially meant for
metastable ฮฎ phase formation region. But due to
higher Sc contents hardening effect diminish
although uniformly decrease hardness with increasing
ageing time. At 180 o
C ageing shows lowest
hardening effect among three studied ageing
temperatures. In this temperature regime hardening
effect arrives earlier but coherency loss at faster rate
due to higher Sc contents mostly dominate factor. On
the other hand, due to higher Sc contents in
aluminium alloy suppress the inherently hardening
effect. In Fig.-3 shows FESEM with EDS analysis in
cast aluminium alloy. The EDS analysis revealed
grain boundary segregation with impurity elements
and grain boundaries broaden prominent in cast
aluminium alloy although Sc transition elements
eliminate grain boundary segregation but probably
high contents this effect decline also EDS result
shows Sc-2.71%, Si-1.30%, and Fe-0.91%,
respectively.Recently, a derivative from FSW, the so
called friction stir processing โ€“ FSP was proved as
being useful for inducing directed, localized, and
controlled materials properties in any arbitrary
location of components. The microstructure of the
processed layer is complex and highly dependent on
the position within the processed zone. This is due to
the large local variations in the plastic flow, and to
the thermal history resulted from the material
interaction with the processing tool. In FSW/FSP, the
processing technique called โ€˜cold workingโ€™ does not
generate the melting of the nugget or stir zone. The
microstructure in stir zone is characterized by refined
grains in a discrete series of bands and some
precipitates mainlydistributed in the matrix with
subgrain boundaries formation.
P. K. MandalInt. Journal of Engineering Research and Applicationswww.ijera.com
ISSN: 2248-9622, Vol. 6, Issue 1, (Part - 2) January 2016, pp.40-47
www.ijera.com 43|P a g e
Fig.-2: The hardness-time curves plotted for a studied alloy aged at different temperatures.
Fig.-3: FESEM with EDS anaysis(as-cast condition) of studied alloy.
The stir zone grains suggest effective strains together
with a microstructural evolution that occurs by a
combination of hot working and a dynamic recovery
or recrystallization.It is likely to that sometimes low
hardness in the stir zone can be attributed to
dissolution of the precipitate during FSP.Generally,
the hardness depends on the precipitate distribution
rather than grain size.The thermo-mechanically
affected zone adjacent to the nugget or stir zone is the
region where the metal is plastically deformed as
well as heated to a temperature, which is not
sufficient to cause recrystallization.Distinct
precipitates and coarsened grains are observed in
HAZ regions, where the grains are severely
coarsened by FSP. There are several assumptions
have been taken as per Hamilton et al. and Heurtier et
al. [2006] that the heat generated due to friction of
the pin shoulder on the workpiece surface is
dominant and the heat generated due to the plastic
deformation within the workpiece and the friction of
the pin of the material is negligible. However, heat
generated mostly from both the friction of the pin
shoulder and plastic flow. It is assumed that the tool
rotates with an angular speed of ฯ‰ (rpm) and
traversely translates along the line of processing with
a speed of ๐œ ๐‘œ (mm/min) and tool is acted upon by a
compressive axial force F as shown in Fig.-1(b).
According to Hamilton et al. energy model, since
I II III
P. K. MandalInt. Journal of Engineering Research and Applicationswww.ijera.com
ISSN: 2248-9622, Vol. 6, Issue 1, (Part - 2) January 2016, pp.40-47
www.ijera.com 44|P a g e
FSP is the metal working technology adapted from
FSW using the same basic principles [16]. Since,
energy generated per unit length during processing as
E is given by Ef = Pf /๐œ ๐‘œโ€ฆโ€ฆ..(1), where P is the total
power generated by friction. Assuming that the total
torque due to friction of the pin, shoulder, and pin
circumference with the work piece surfaces is Tf, the
frictional power is then given by Pf= Tfฯ‰ โ€ฆโ€ฆโ€ฆ(2),
where ฯ‰ is the pin angular speed. To find an
expression for the total frictional torque Tf, we let Tf
= Ts + Tp โ€ฆโ€ฆโ€ฆ(3), where Ts is the torque
generated by the shoulder and Tp is torque generated
by the pin. Assuming that a uniform shear stress ฮท
occurs during processing, we obtain Tf = 2ฯ€๐‘Ÿ๐‘œ
2
ฮท (
1
3
๐‘Ÿ๐‘œ
+
๐‘Ÿ๐‘–
2
๐‘Ÿ ๐‘œ
2h)โ€ฆ.(4). Assuming a coefficient of friction is ยต,
the total friction force Ff due to the compressive force
F is given by Ff = ยตF โ€ฆโ€ฆโ€ฆ(5). It is noting that ฯ€๐‘Ÿ๐‘œ
2
ฮท
is the total frictional force, then from equ.-(4) Tf =
2ยตF (
1
3
๐‘Ÿ๐‘œ +
๐‘Ÿ๐‘–
2
๐‘Ÿ ๐‘œ
2h)โ€ฆโ€ฆ(6). Now consider from equ.-(1)
and (2), we obtain Ef = Tf ฯ‰ / ๐œ ๐‘œ = 2ยตF (
1
3
๐‘Ÿ๐‘œ +
๐‘Ÿ๐‘–
2
๐‘Ÿ ๐‘œ
2 h)
ฯ‰
๐œ ๐‘œ
.........(7). So, equ.-(7) defines the energy per
unit length of the FSW/FSP due to friction between
the tool and the workpiece. For a given tool
geometry, tool speed, and workpiece material, this
energy can be easily identified. As can be noted from
equ.-(1), the power generated due to friction is given
by Pf = 2ยตF (
1
3
๐‘Ÿ๐‘œ +
๐‘Ÿ๐‘–
2
๐‘Ÿ ๐‘œ
2 h)ฯ‰โ€ฆโ€ฆโ€ฆ(8). As Frigaard
[1998] reported that the coefficient of friction (ยต)
between Al and mild steel should be set as the
average value between 0.5 for sticky friction and 0.25
for dry sliding. However, in this study a coefficient of
friction (ยต) is used 0.5 (as per Hamilton et al.). The
other source of heat is due to the plastic deformation
within the workpiece. Provided that the plastic
deformation within the workpiece is totally
transformed into heat, the heat generated due to
plastic deformation per unit FSP length can be
expressed as follows: Ep = ฮถ ฮต dVโ€ฆโ€ฆ(9), where ฮถ
and ฮต are the stress and strain, respectively, dV = 2๐‘Ÿ๐‘–
h is the volume per unit length of the material. Since
the effect of the energy due to plastic deformation is
much smaller than that due to friction, a simple
model was proposed as follows:Ep = ฮถe ฮตe 2 ๐‘Ÿ๐‘– h
โ€ฆโ€ฆ.(10), where ฮถe is the equivalent (effective)
stress and ฮตe is the effective strain. Using the finite
element method, Heurtier et al. [2006] found that the
effective strain is around 6. The power generated due
to the plastic deformation is given by Pp = ฮถe ฮตe(2๐‘Ÿ๐‘–
h) ๐œ ๐‘œ โ€ฆ..(11). The total eregry generated per unit
length of the FSP is the sum of the energy generated
due to friction between the tool and the workpiece
and the plastic deformation within the workpiece. An
empirical formula developed a proposed energy
model by Hamilton et al.,
๐‘‡ ๐‘š๐‘Ž๐‘ฅ
๐‘‡๐‘ 
= 1.56 ร— 10โˆ’4
๐ธ๐‘’๐‘“๐‘“ +
0.54โ€ฆโ€ฆโ€ฆ..(12), where ๐‘‡ ๐‘š๐‘Ž๐‘ฅ is the maximum
temperature generated within the FSP, ๐‘‡๐‘  is the
solidus temperature in Kelvin, ๐ธ๐‘’๐‘“๐‘“ is the effective
energy generated per unit length of FSP in J/mm. In
this study, one aluminium alloy is considered using
different FSP parameters such as tool geometry and
FSP speed. As per many literatures supported and
Hamilton energy model we can be concluded ๐‘‡๐‘  =
636 o
C [from Al-Zn equilibrium phase diagram]and
๐‘‡ ๐‘š๐‘Ž๐‘ฅ = 480 o
C[C.B. Fuller et al., 2010; at 640 rpm,
160 mm/min] , its can put into equ.-(12) to obtained
๐ธ๐‘’๐‘“๐‘“ =
๐‘‡ ๐‘š๐‘Ž๐‘ฅ
๐‘‡๐‘ 
(
104
1.56
) โ€“ 0.54 (J/mm)โ€ฆโ€ฆ..(13).
Considering equ.-13, we can be obtained ๐ธ๐‘’๐‘“๐‘“ =
5319.97 J/mm. Consequently, as per Khandkarโ€™s
torque-based model for which the total torque, Ttotal ,
is expressed as the sum of torque contributions from
the tool shoulder against the workpiece, the bottom of
the tool pin against thickness material and the pin
surface against thickness material. Therefore, Ttotal =
2ยตF (
1
3
๐‘Ÿ๐‘œ +
๐‘Ÿ๐‘–
2
๐‘Ÿ ๐‘œ
2h)โ€ฆโ€ฆ(14), where, ยต (0.5 value) is the
coefficient of friction between the tool and the
workpiece, F is the applied force, ro is the radius of
the tool shoulder, ri is the radius of the pin, h is the
pin height. The total energy per unit length of FSW,
Etotal is found by dividing the average power, Pavgby
the weld velocity to yield the expression using Etotal =
๐‘ƒ ๐‘Ž๐‘ฃ๐‘”
๐‘ฃ ๐‘ค
= Ttotal
๐œ”
๐‘ฃ ๐‘ค
โ€ฆโ€ฆโ€ฆ(15), where ๐‘ฃ ๐‘ค is the velocity
during FSW and ฯ‰ is the tool angular velocity. As
per C. Hamilton et al. [2009] proposed his paper
during FSW welding temperature is equal to the
solidus temperature of aluminium alloy, i.e.,
๐‘‡ ๐‘š๐‘Ž๐‘ฅ
๐‘‡๐‘ 
= 1.
So, from the equ.-(13) we can easily found out
๐ธ๐‘’๐‘“๐‘“ = 6409.72 J/mm. for the Sc-modified Al-Zn-
Mg-Cu alloy examined in this work, the model
successfully predicts the maximum welding
temperature and temperature distributions over the
energy range investigated by C. Hamilton et al.. The
model, however, shows its greatest potential at higher
energy welds (i.e., (Etotal)eff หƒ1000 J/mm) where heat
generation due to friction dominates. At the lower
energy levels (i.e., (Etotal)eff ห‚1000 J/mm), the
predicted temperature data in terms of magnitude and
shape away from the tool shoulder, but the model
under-predicts the maximum welding temperatures
due to the assumptions/simplifications that were used
in the calculation of the plastic energy. According to
H. Lombard et al., hinted that the basic energy model
based on the external FSW parameters [21, 22]. Heat
input from the tool shoulder per unit length of weld
(J/mm) can be estimated from torque measurements
that remain reasonably constant once thermal
equilibrium is reached and given by Q =
Power
Traverse speed
P. K. MandalInt. Journal of Engineering Research and Applicationswww.ijera.com
ISSN: 2248-9622, Vol. 6, Issue 1, (Part - 2) January 2016, pp.40-47
www.ijera.com 45|P a g e
= ฮท
2๐œ‹๐œ”๐‘‡
๐œ
โ€ฆ..(16), where Q is the heat input (J/mm), ฮท
= efficiency factor = 0.9 (for Al and Cu), ฯ‰ (rpm) is
the rotational speed, T (Nm) is the torque, ๐œ
(mm/min) is the traverse speed. They also hinted on
heat input appears to be dominated by the traverse
speed, suggesting that changes in the rotational
speedare compensated by changes in the torque.In
Fig.-4 shows different FSP
Fig.-4: The illustration of optical micrograph (at T4 + FSP) of different FSP regions of studied alloy.
regions which has created during this processing just
because tool shoulder with workpiece downward
frictional force with predetermined tool geometry and
predetermined FSP parameters, which can be created
three distinct zones likely to stir zone (SZ- centre
zone as equal area of pin diameter), thermo-
mechanically affected zone (TMAZ- nearer to stir
zone), and heat affected zone (HAZ- nearer to
thermo-mechanically affected zone), also identified
in specific regions in optical micrograph. As a result,
stir zone is the most effective region to refine
microstructure to modify material surface
characteristics and enhanced mechanical properties.
Hence, main aim of the investigation is to determine
the relationship between parameters of the process
(rotational speed, traverse speed, downward force,
and type of tool design) and torque (Nm) and
temperature generated in the stir zone [A.N. Solonin
et al., 2010; P. Heurtier et al., 2006]. Torque,
temperature and stress generated by the movement
and friction of materials, decide about heat
generation in the modified material and thus the
changes of microstructure and consequently the
mechanical properties of material. It is evidence that
the torque strongly depends on the rotational speed of
the FSP tool. This is because the rotational speed
stimulates the temperature in the FSP area and thus
the friction coefficient decreases when temperature
increases. The value of torque is influenced by
rotational speed, travelling speed, downward force,
design of tool, and a kind of modified material. Here,
the experimental results are compared with the results
obtained from the theoretical models. In Fig.-5(a-b)
shows tensile fractographs at different conditions, for
Fig.-5(a) has indicated ductile mode of fracture
surface and microcracks are normally originated from
grain boundaries (e.g. generally called intergranular
fracture mode) and fine precipitates are appears
mostly in grain boundary regions in between some
black holes also indicate origin of fracture initiation.
Similarly, in Fig.-5 (b) shows fracture surfaces are
blunt due to may ageing exposed indication and
overall fracture surface indicating uniformly arranged
with some dip black holes observed. These black
holes are possibly indication of stress centre. This
studied alloy has Sc content 0.87%, which can be
SZ
TMAZ
HAZ
P. K. MandalInt. Journal of Engineering Research and Applicationswww.ijera.com
ISSN: 2248-9622, Vol. 6, Issue 1, (Part - 2) January 2016, pp.40-47
www.ijera.com 46|P a g e
deleterious effect of coarsening tendency during post
ageing heat treatment. During age hardening
treatment at 140 o
C ageing hardness dropped
marginally than at lower ageing temperature.
Consequently, during tensile testing also indicated at
this condition overall mechanical properties diminish.
Since, aluminium alloy is prominent for age
hardening ability to response natural ageing and
subsequently artificial ageing tendency at elevated
temperatures. The age hardening kinetics can be
revealed through tensile testing measurement, also
depend on chemical composition, heat treatment
conditions and after all surface modification
technique, so called FSP. In Table-3 shows tensile
results at different FSP conditions in three stages at
as-cast plus FSP condition exhibited higher tensile
properties due to cast condition with FSP hardening
phases (ฮท-Mg2Zn) are homogeneously distributed
with fine grains cause dynamic recrystallization and
presence of coherent Al3Sc particles. But hardness
value (105.8HV) indicated lowest due to higher
ductility. Consequently, T4 heat treatment plus FSP
condition tensile properties are slightly dropped due
to specific solution treatment the hardening phases
are dissolution occurred, possibly. One more
possibility may happen for solution treatment Al3Sc
particles remain in solution, particles have not taken
part hardening activity as like during ageing
phenomena hardening stimulated with time. But
hardness value (153.6HV) is highest due to higher Sc
contents. After T4 plus FSP with post ageing
treatment tensile properties dropped drastically
because material become ovreaged with
predominantly incoherent equilibrium (ฮท) phases,
particle coarsening particularly at grain boundary
regions. Other hand, at FSP with post-heating
specimen often exposed faster precipitates nucleation
(i.e., depends nature of material, time, and
temperature) with facilities of high angle grain
boundaries are main factors. Similarly, hardness
value (128.2HV) dropped drastically due to higher Sc
contents to faster precipitates coarsening effect.
Fig.-5: The tensile fractographs of studied alloy (a) at T4+FSP; (b) at T4+FSP+Ageing at 140 o
C/2h.
Table-3: Results of tensile properties are tabulated through FSP directionof studies alloy.
FSP by double passes at different
conditions
Tensile properties
ฮถ0.2(MPa) ฮถu(MPa) ฮด(%) VHN(10kg.)
AC + FSP 99.4 207.8 5.7 105.8
T4 + FSP 98.9 197.6 4.3 153.6
T4 + FSP + Aged at 140 o
C /2h 79.2 168.5 5.2 128.2
Note: AC= as-cast; T4 = solutionized at 465 o
C/1 h then WQ; yield strength denoted at 0.2% offset from stress-
strain curve. Hardness (at average six values) taken along the stir zone.
IV. Conclusions
1. The Al-Zn-Mg alloy is the best age hardening
performer in all aluminum series.
2. Based on experimental results Sc is best hardener
in cast aluminum alloy within the limit 0.25-0.60
wt%.
3. Adding minor scandium in aluminium alloy can
refine grains and increase tensile strength, which
attributed to the presence of coherent, L12-
ordered Al3Sc particles. It can substantially
inhibit recrystallization and pin subgrain
boundaries and dislocations.
4. At higher Sc contents diminish age hardening
effect and deteriorate overall mechanical
properties.
5. The friction stir processing (FSP) originates from
the technology of friction stir welding (FSW),
yet in comparison with this method, the
phenomena taking place in the interface between
the stirring area and the workpiece will have a
(a) (b)
P. K. MandalInt. Journal of Engineering Research and Applicationswww.ijera.com
ISSN: 2248-9622, Vol. 6, Issue 1, (Part - 2) January 2016, pp.40-47
www.ijera.com 47|P a g e
decisive effect on the functional properties of a
surface layer obtained through this process.
6. The friction stir processing (FSP) is a promising
solid state surface modification technique. Also,
considered as an innovative technique that the
FSPwas employed to modify the surface layer of
aluminium alloy. The FSP process addresses the
industry as surface repairing technique in case of
different types of flows.
7. The proof stress and tensile stress dropped
marginally due to elimination of residual
stresses, dissolution of precipitates (ฮท-MgZn2)
and grains coarsening are main reasons.
8. The goal of presented work is to estimate the
relationship between FSP parameters such as
rotational and travelling speed, downward force,
torque, temperature.
9. There are several theoretical energy-based
models explained for better coincidence with
present experimental data. According to Heurtier
et al. and Hamilton et al. a simply energy-based
model for the FSW/FSP is proposed. The model
aims at estimating the heat generated due to
plastic deformation within the workpieces and
friction between the tool surfaces and the
workpieces. A comparison between the
estimated heat energy and its corresponding
maximum temperature obtained using the
proposed model and the experimental result
shows a good agreement.
10. Here, we have discussed Khandkarโ€™s torque-
based model that is good agreement with heat
energy generated is a function of applied force,
coefficient of friction between the tool and the
workpiece, tool dimensions, and FSW/FSP
parameters. As per Khandkarโ€™s torque-based
model and Hamilton energy-based modelโ€™s
correlation has been found out effective energy
value (Eeff) during our experiment work. The
numerical value is Eeff = 6409.72 J/mm.This is
good agreement with Khandkarโ€™s torque-based
model value. Also, from our experimental data
obtained value is Eeff = 5319.97 J/mm. As per H.
Lombard et al. explained basic energy based
model, also explained amount of heat generation
depends on process parameters.
References
[1] J.Z. Liu et al., Scripta Materialia 63 (2010)
1061-1064.
[2] S. Ahmadi et al., Journal of Alloys and
Compounds 484 (2009) 90-94.
[3] J.K. Park et al., Metallurgical Transactions
A, Vol. 14A, Oct. 1983, 1957-1965.
[4] W.J. Poole et al., Metallurgical and
Materials Transactions A, Vol. 31A, Sept.
2000, 2327-2338.
[5] H. Loffler et al., Journal of Materials
Science 18 (1983) 2215-2240.
[6] E. Hornbogen et al., Acta Metall. Mater.
Vol. 41, No. 1, pp. 1-16, 1993.
[7] B. Li et al., Journal of Alloys and
Compounds 584 (2014) 406-416.
[8] D. Tsivoulas et al., Materials Science
Forum, Vols. 519-521 (2006) pp. 473-478.
[9] Z. Ahmad, Journal of Materials, Feb.2003,
pp. 35-39.
[10] A.L. Berezina et al., Materials Science
Forum, Vols. 396-402 (2002) pp. 741-746.
[11] Y. Deng et al., Journal of Alloys and
Compounds 530(2012) 71-80.
[12] C.G. Rhodes et al., Scripta Materialia 48
(2003) 1451-1455.
[13] S. Soleymani et al., Journal of Surface
Engineering Materials and Advanced
Technology, 2011, 1, 95-100.
[14] C.B. Fuller et al., Materials Science and
Engineering A 527 (2010) 2233-2240.
[15] J-Q. Su et al., Scripta Materialia 52 (2005)
135-140.
[16] S. A. Emam et al., World Academy of
Science, Engineering and Technology 53,
2009, pp. 1016-1022.
[17] C. Hamilton et al., International Journal of
Machine Tools & Manufacturing 49 (2009)
230-238.
[18] B.G. Clark et al., Journal of Materials
Research, Vol. 20, No. 7, July 2005, pp.
1792-1801.
[19] W. Feng et al., Rare Metals, Vol. 26, No. 2,
Apr. 2007, pp. 163-168.
[20] J. Royset et al., International Materials
Reviews, 2005, Vol. 50, No. 1, 19-44.
[21] M.S. Weglowski et al., Key Engineering
Materials, Vols. 554-557 (2013) pp. 1787-
1792.
[22] H. Lombard et al., Materials Science and
Engineering A 501 (2009) 119-124.

More Related Content

What's hot

SELECTION OF THE DISC BRAKE MATERIAL USING PIN ON DISC APPARATUS
SELECTION OF THE DISC BRAKE MATERIAL USING PIN ON DISC APPARATUSSELECTION OF THE DISC BRAKE MATERIAL USING PIN ON DISC APPARATUS
SELECTION OF THE DISC BRAKE MATERIAL USING PIN ON DISC APPARATUSijiert bestjournal
ย 
Weightage Allocation to influential parameters in FSW for Yield Strength Eval...
Weightage Allocation to influential parameters in FSW for Yield Strength Eval...Weightage Allocation to influential parameters in FSW for Yield Strength Eval...
Weightage Allocation to influential parameters in FSW for Yield Strength Eval...IJERA Editor
ย 
INFLUENCE MECHANISM OF THICKNESS AND VISCOSITY OF FLAT ENERGY DIRECTOR TO THE...
INFLUENCE MECHANISM OF THICKNESS AND VISCOSITY OF FLAT ENERGY DIRECTOR TO THE...INFLUENCE MECHANISM OF THICKNESS AND VISCOSITY OF FLAT ENERGY DIRECTOR TO THE...
INFLUENCE MECHANISM OF THICKNESS AND VISCOSITY OF FLAT ENERGY DIRECTOR TO THE...adeij1
ย 
Thermo-Mechanical Analysis of Automotive Disc Brake Composite Rotor
Thermo-Mechanical Analysis of Automotive Disc Brake Composite RotorThermo-Mechanical Analysis of Automotive Disc Brake Composite Rotor
Thermo-Mechanical Analysis of Automotive Disc Brake Composite Rotorinventionjournals
ย 
STUDY ON PREDICTION OF MECHANICAL PROPERTIES OF LARGE RING-SHAPED FORGING DEP...
STUDY ON PREDICTION OF MECHANICAL PROPERTIES OF LARGE RING-SHAPED FORGING DEP...STUDY ON PREDICTION OF MECHANICAL PROPERTIES OF LARGE RING-SHAPED FORGING DEP...
STUDY ON PREDICTION OF MECHANICAL PROPERTIES OF LARGE RING-SHAPED FORGING DEP...IAEME Publication
ย 
Verification of johnson cook material model constants of aa2024-t3 for use in...
Verification of johnson cook material model constants of aa2024-t3 for use in...Verification of johnson cook material model constants of aa2024-t3 for use in...
Verification of johnson cook material model constants of aa2024-t3 for use in...eSAT Publishing House
ย 
solid state recycling . ECAP
solid state recycling . ECAP solid state recycling . ECAP
solid state recycling . ECAP sami alalimi
ย 
FE Simulation Modelling and Exergy Analysis of Conventional Forging Deformati...
FE Simulation Modelling and Exergy Analysis of Conventional Forging Deformati...FE Simulation Modelling and Exergy Analysis of Conventional Forging Deformati...
FE Simulation Modelling and Exergy Analysis of Conventional Forging Deformati...IJERA Editor
ย 
Thickness optimization of thick walled circular cylinder by heat treatment
Thickness optimization of thick walled circular cylinder by heat treatmentThickness optimization of thick walled circular cylinder by heat treatment
Thickness optimization of thick walled circular cylinder by heat treatmentIRJET Journal
ย 
Design &Analysis of Pure Iron Casting with Different Moulds
Design &Analysis of Pure Iron Casting with Different MouldsDesign &Analysis of Pure Iron Casting with Different Moulds
Design &Analysis of Pure Iron Casting with Different MouldsIJMER
ย 
Application of Taguchi Method to Study the Effect of Saw Parameters on Nickel...
Application of Taguchi Method to Study the Effect of Saw Parameters on Nickel...Application of Taguchi Method to Study the Effect of Saw Parameters on Nickel...
Application of Taguchi Method to Study the Effect of Saw Parameters on Nickel...IJERA Editor
ย 
Verification of johnson cook material model by sanjeev n k
Verification of johnson cook material model by sanjeev n kVerification of johnson cook material model by sanjeev n k
Verification of johnson cook material model by sanjeev n ksanjeevnks
ย 
F021202058066
F021202058066F021202058066
F021202058066theijes
ย 
A New Surface Modification Technique and Their Characterisation: Friction Sti...
A New Surface Modification Technique and Their Characterisation: Friction Sti...A New Surface Modification Technique and Their Characterisation: Friction Sti...
A New Surface Modification Technique and Their Characterisation: Friction Sti...IJERA Editor
ย 
STRESS DISTRIBUTION IN GRINDING BY FINITE ELEMENT ANALYSIS
STRESS DISTRIBUTION IN GRINDING BY FINITE ELEMENT ANALYSISSTRESS DISTRIBUTION IN GRINDING BY FINITE ELEMENT ANALYSIS
STRESS DISTRIBUTION IN GRINDING BY FINITE ELEMENT ANALYSISBijoy Das
ย 
Ac04405162169
Ac04405162169Ac04405162169
Ac04405162169IJERA Editor
ย 

What's hot (17)

SELECTION OF THE DISC BRAKE MATERIAL USING PIN ON DISC APPARATUS
SELECTION OF THE DISC BRAKE MATERIAL USING PIN ON DISC APPARATUSSELECTION OF THE DISC BRAKE MATERIAL USING PIN ON DISC APPARATUS
SELECTION OF THE DISC BRAKE MATERIAL USING PIN ON DISC APPARATUS
ย 
Weightage Allocation to influential parameters in FSW for Yield Strength Eval...
Weightage Allocation to influential parameters in FSW for Yield Strength Eval...Weightage Allocation to influential parameters in FSW for Yield Strength Eval...
Weightage Allocation to influential parameters in FSW for Yield Strength Eval...
ย 
INFLUENCE MECHANISM OF THICKNESS AND VISCOSITY OF FLAT ENERGY DIRECTOR TO THE...
INFLUENCE MECHANISM OF THICKNESS AND VISCOSITY OF FLAT ENERGY DIRECTOR TO THE...INFLUENCE MECHANISM OF THICKNESS AND VISCOSITY OF FLAT ENERGY DIRECTOR TO THE...
INFLUENCE MECHANISM OF THICKNESS AND VISCOSITY OF FLAT ENERGY DIRECTOR TO THE...
ย 
Thermo-Mechanical Analysis of Automotive Disc Brake Composite Rotor
Thermo-Mechanical Analysis of Automotive Disc Brake Composite RotorThermo-Mechanical Analysis of Automotive Disc Brake Composite Rotor
Thermo-Mechanical Analysis of Automotive Disc Brake Composite Rotor
ย 
STUDY ON PREDICTION OF MECHANICAL PROPERTIES OF LARGE RING-SHAPED FORGING DEP...
STUDY ON PREDICTION OF MECHANICAL PROPERTIES OF LARGE RING-SHAPED FORGING DEP...STUDY ON PREDICTION OF MECHANICAL PROPERTIES OF LARGE RING-SHAPED FORGING DEP...
STUDY ON PREDICTION OF MECHANICAL PROPERTIES OF LARGE RING-SHAPED FORGING DEP...
ย 
Verification of johnson cook material model constants of aa2024-t3 for use in...
Verification of johnson cook material model constants of aa2024-t3 for use in...Verification of johnson cook material model constants of aa2024-t3 for use in...
Verification of johnson cook material model constants of aa2024-t3 for use in...
ย 
solid state recycling . ECAP
solid state recycling . ECAP solid state recycling . ECAP
solid state recycling . ECAP
ย 
FE Simulation Modelling and Exergy Analysis of Conventional Forging Deformati...
FE Simulation Modelling and Exergy Analysis of Conventional Forging Deformati...FE Simulation Modelling and Exergy Analysis of Conventional Forging Deformati...
FE Simulation Modelling and Exergy Analysis of Conventional Forging Deformati...
ย 
Thickness optimization of thick walled circular cylinder by heat treatment
Thickness optimization of thick walled circular cylinder by heat treatmentThickness optimization of thick walled circular cylinder by heat treatment
Thickness optimization of thick walled circular cylinder by heat treatment
ย 
Design &Analysis of Pure Iron Casting with Different Moulds
Design &Analysis of Pure Iron Casting with Different MouldsDesign &Analysis of Pure Iron Casting with Different Moulds
Design &Analysis of Pure Iron Casting with Different Moulds
ย 
Application of Taguchi Method to Study the Effect of Saw Parameters on Nickel...
Application of Taguchi Method to Study the Effect of Saw Parameters on Nickel...Application of Taguchi Method to Study the Effect of Saw Parameters on Nickel...
Application of Taguchi Method to Study the Effect of Saw Parameters on Nickel...
ย 
Verification of johnson cook material model by sanjeev n k
Verification of johnson cook material model by sanjeev n kVerification of johnson cook material model by sanjeev n k
Verification of johnson cook material model by sanjeev n k
ย 
F021202058066
F021202058066F021202058066
F021202058066
ย 
A New Surface Modification Technique and Their Characterisation: Friction Sti...
A New Surface Modification Technique and Their Characterisation: Friction Sti...A New Surface Modification Technique and Their Characterisation: Friction Sti...
A New Surface Modification Technique and Their Characterisation: Friction Sti...
ย 
STRESS DISTRIBUTION IN GRINDING BY FINITE ELEMENT ANALYSIS
STRESS DISTRIBUTION IN GRINDING BY FINITE ELEMENT ANALYSISSTRESS DISTRIBUTION IN GRINDING BY FINITE ELEMENT ANALYSIS
STRESS DISTRIBUTION IN GRINDING BY FINITE ELEMENT ANALYSIS
ย 
REVIEW ON THERMAL, THERMO-MECHANICAL AND THERMAL STRESS DISTRIBUTION DURING F...
REVIEW ON THERMAL, THERMO-MECHANICAL AND THERMAL STRESS DISTRIBUTION DURING F...REVIEW ON THERMAL, THERMO-MECHANICAL AND THERMAL STRESS DISTRIBUTION DURING F...
REVIEW ON THERMAL, THERMO-MECHANICAL AND THERMAL STRESS DISTRIBUTION DURING F...
ย 
Ac04405162169
Ac04405162169Ac04405162169
Ac04405162169
ย 

Viewers also liked

Influence of Zirconium on the Grain Refinement of Al 6063 alloy
Influence of Zirconium on the Grain Refinement of Al 6063 alloyInfluence of Zirconium on the Grain Refinement of Al 6063 alloy
Influence of Zirconium on the Grain Refinement of Al 6063 alloyIJERA Editor
ย 
Calculation and comparison of circuit breaker parameters in Power World Simul...
Calculation and comparison of circuit breaker parameters in Power World Simul...Calculation and comparison of circuit breaker parameters in Power World Simul...
Calculation and comparison of circuit breaker parameters in Power World Simul...IJERA Editor
ย 
Travel essentials for women
Travel essentials for womenTravel essentials for women
Travel essentials for womenCelestine Celestine
ย 
How to Buy Stocks
How to Buy StocksHow to Buy Stocks
How to Buy StocksJames Tenney
ย 
No.246 japanese
No.246 japaneseNo.246 japanese
No.246 japanesehuldahministry
ย 
Accelerating Capital - Final Report - April 24 2014
Accelerating Capital - Final Report - April 24 2014Accelerating Capital - Final Report - April 24 2014
Accelerating Capital - Final Report - April 24 2014David Kort
ย 
Tic
TicTic
Ticbeapb3
ย 
Contexto internacional neoliberalismo en educaciรณn mao zuรฑiga
Contexto internacional  neoliberalismo en educaciรณn mao zuรฑigaContexto internacional  neoliberalismo en educaciรณn mao zuรฑiga
Contexto internacional neoliberalismo en educaciรณn mao zuรฑigaJesus Villa
ย 
CV Croatian( Hrvatski)
CV  Croatian( Hrvatski)CV  Croatian( Hrvatski)
CV Croatian( Hrvatski)Kenan Kuloviฤ‡
ย 

Viewers also liked (14)

Influence of Zirconium on the Grain Refinement of Al 6063 alloy
Influence of Zirconium on the Grain Refinement of Al 6063 alloyInfluence of Zirconium on the Grain Refinement of Al 6063 alloy
Influence of Zirconium on the Grain Refinement of Al 6063 alloy
ย 
Calculation and comparison of circuit breaker parameters in Power World Simul...
Calculation and comparison of circuit breaker parameters in Power World Simul...Calculation and comparison of circuit breaker parameters in Power World Simul...
Calculation and comparison of circuit breaker parameters in Power World Simul...
ย 
Java titles 2015 2016
Java titles 2015 2016Java titles 2015 2016
Java titles 2015 2016
ย 
Travel essentials for women
Travel essentials for womenTravel essentials for women
Travel essentials for women
ย 
How to Buy Stocks
How to Buy StocksHow to Buy Stocks
How to Buy Stocks
ย 
Pahuatlรกn
PahuatlรกnPahuatlรกn
Pahuatlรกn
ย 
No.246 japanese
No.246 japaneseNo.246 japanese
No.246 japanese
ย 
Accelerating Capital - Final Report - April 24 2014
Accelerating Capital - Final Report - April 24 2014Accelerating Capital - Final Report - April 24 2014
Accelerating Capital - Final Report - April 24 2014
ย 
youth today presentation
youth today presentationyouth today presentation
youth today presentation
ย 
Equinoterapia
EquinoterapiaEquinoterapia
Equinoterapia
ย 
Tic
TicTic
Tic
ย 
9883
98839883
9883
ย 
Contexto internacional neoliberalismo en educaciรณn mao zuรฑiga
Contexto internacional  neoliberalismo en educaciรณn mao zuรฑigaContexto internacional  neoliberalismo en educaciรณn mao zuรฑiga
Contexto internacional neoliberalismo en educaciรณn mao zuรฑiga
ย 
CV Croatian( Hrvatski)
CV  Croatian( Hrvatski)CV  Croatian( Hrvatski)
CV Croatian( Hrvatski)
ย 

Similar to A refined energy-based model for friction stir processing of Al- Zn-Mg alloy

Mechanism of Fracture in Friction Stir Processed Aluminium Alloy
Mechanism of Fracture in Friction Stir Processed Aluminium AlloyMechanism of Fracture in Friction Stir Processed Aluminium Alloy
Mechanism of Fracture in Friction Stir Processed Aluminium AlloyDr. Amarjeet Singh
ย 
Study on hardening mechanisms in aluminium alloys
Study on hardening mechanisms in aluminium alloysStudy on hardening mechanisms in aluminium alloys
Study on hardening mechanisms in aluminium alloysIJERA Editor
ย 
Study on hardening mechanisms in aluminium alloys
Study on hardening mechanisms in aluminium alloysStudy on hardening mechanisms in aluminium alloys
Study on hardening mechanisms in aluminium alloysIJERA Editor
ย 
Experimental Investigations on Tribiological Properties of 6061-T6 Al Alloy b...
Experimental Investigations on Tribiological Properties of 6061-T6 Al Alloy b...Experimental Investigations on Tribiological Properties of 6061-T6 Al Alloy b...
Experimental Investigations on Tribiological Properties of 6061-T6 Al Alloy b...IJAEMSJORNAL
ย 
AN APPROACH FOR ENERGY CONSERVATION ON PARTIALLY LATERISED KHONDALITE ROCKS U...
AN APPROACH FOR ENERGY CONSERVATION ON PARTIALLY LATERISED KHONDALITE ROCKS U...AN APPROACH FOR ENERGY CONSERVATION ON PARTIALLY LATERISED KHONDALITE ROCKS U...
AN APPROACH FOR ENERGY CONSERVATION ON PARTIALLY LATERISED KHONDALITE ROCKS U...IAEME Publication
ย 
Effect of broaching on high temperature fatigue behavior
Effect of broaching on high temperature fatigue behaviorEffect of broaching on high temperature fatigue behavior
Effect of broaching on high temperature fatigue behaviorPhuong Dx
ย 
15136-17380-1-PB.pdf
15136-17380-1-PB.pdf15136-17380-1-PB.pdf
15136-17380-1-PB.pdfvijayasarathi17
ย 
A. i. selmy , 2016
A. i. selmy , 2016A. i. selmy , 2016
A. i. selmy , 2016sami alalimi
ย 
Microhardness of Friction Stir Processed Aluminium-6063
Microhardness of Friction Stir Processed Aluminium-6063Microhardness of Friction Stir Processed Aluminium-6063
Microhardness of Friction Stir Processed Aluminium-6063ijsrd.com
ย 
Bhale2016
Bhale2016Bhale2016
Bhale2016dream2nasa
ย 
Solid state recycling of light metal reinforced-sami icme2017-00013
Solid state recycling of light metal reinforced-sami icme2017-00013Solid state recycling of light metal reinforced-sami icme2017-00013
Solid state recycling of light metal reinforced-sami icme2017-00013sami alalimi
ย 
Annealing Response of Aluminum Alloy AA6014 Processed By Severe Plastic Defor...
Annealing Response of Aluminum Alloy AA6014 Processed By Severe Plastic Defor...Annealing Response of Aluminum Alloy AA6014 Processed By Severe Plastic Defor...
Annealing Response of Aluminum Alloy AA6014 Processed By Severe Plastic Defor...IRJESJOURNAL
ย 
EFFECT OF THERMAL EXPOSURE ON THE MECHANICAL AND WEAR PROPERTIES OF AEROSPACE...
EFFECT OF THERMAL EXPOSURE ON THE MECHANICAL AND WEAR PROPERTIES OF AEROSPACE...EFFECT OF THERMAL EXPOSURE ON THE MECHANICAL AND WEAR PROPERTIES OF AEROSPACE...
EFFECT OF THERMAL EXPOSURE ON THE MECHANICAL AND WEAR PROPERTIES OF AEROSPACE...Journal For Research
ย 
Improving Mechanical Properties of AL 7075 alloy by Equal Channel Angular Ext...
Improving Mechanical Properties of AL 7075 alloy by Equal Channel Angular Ext...Improving Mechanical Properties of AL 7075 alloy by Equal Channel Angular Ext...
Improving Mechanical Properties of AL 7075 alloy by Equal Channel Angular Ext...IJMER
ย 
STRUCTURE PROPERTY CORRELATION OF MODIFIED Al-Mg ALLOYS FOR AEROSPACE APPLICA...
STRUCTURE PROPERTY CORRELATION OF MODIFIED Al-Mg ALLOYS FOR AEROSPACE APPLICA...STRUCTURE PROPERTY CORRELATION OF MODIFIED Al-Mg ALLOYS FOR AEROSPACE APPLICA...
STRUCTURE PROPERTY CORRELATION OF MODIFIED Al-Mg ALLOYS FOR AEROSPACE APPLICA...sivanagaraju chittelu
ย 
Study on Influence of heat treatment on Tribological properties of mild steel
Study on Influence of heat treatment on Tribological properties of mild steelStudy on Influence of heat treatment on Tribological properties of mild steel
Study on Influence of heat treatment on Tribological properties of mild steeldbpublications
ย 
3 dimensional nonlinear finite element analysis of both thermal and mechanica...
3 dimensional nonlinear finite element analysis of both thermal and mechanica...3 dimensional nonlinear finite element analysis of both thermal and mechanica...
3 dimensional nonlinear finite element analysis of both thermal and mechanica...Alexander Decker
ย 

Similar to A refined energy-based model for friction stir processing of Al- Zn-Mg alloy (20)

Mechanism of Fracture in Friction Stir Processed Aluminium Alloy
Mechanism of Fracture in Friction Stir Processed Aluminium AlloyMechanism of Fracture in Friction Stir Processed Aluminium Alloy
Mechanism of Fracture in Friction Stir Processed Aluminium Alloy
ย 
Study on hardening mechanisms in aluminium alloys
Study on hardening mechanisms in aluminium alloysStudy on hardening mechanisms in aluminium alloys
Study on hardening mechanisms in aluminium alloys
ย 
Study on hardening mechanisms in aluminium alloys
Study on hardening mechanisms in aluminium alloysStudy on hardening mechanisms in aluminium alloys
Study on hardening mechanisms in aluminium alloys
ย 
Experimental Investigations on Tribiological Properties of 6061-T6 Al Alloy b...
Experimental Investigations on Tribiological Properties of 6061-T6 Al Alloy b...Experimental Investigations on Tribiological Properties of 6061-T6 Al Alloy b...
Experimental Investigations on Tribiological Properties of 6061-T6 Al Alloy b...
ย 
30120140505008
3012014050500830120140505008
30120140505008
ย 
AN APPROACH FOR ENERGY CONSERVATION ON PARTIALLY LATERISED KHONDALITE ROCKS U...
AN APPROACH FOR ENERGY CONSERVATION ON PARTIALLY LATERISED KHONDALITE ROCKS U...AN APPROACH FOR ENERGY CONSERVATION ON PARTIALLY LATERISED KHONDALITE ROCKS U...
AN APPROACH FOR ENERGY CONSERVATION ON PARTIALLY LATERISED KHONDALITE ROCKS U...
ย 
30720130101006
3072013010100630720130101006
30720130101006
ย 
Effect of broaching on high temperature fatigue behavior
Effect of broaching on high temperature fatigue behaviorEffect of broaching on high temperature fatigue behavior
Effect of broaching on high temperature fatigue behavior
ย 
15136-17380-1-PB.pdf
15136-17380-1-PB.pdf15136-17380-1-PB.pdf
15136-17380-1-PB.pdf
ย 
A. i. selmy , 2016
A. i. selmy , 2016A. i. selmy , 2016
A. i. selmy , 2016
ย 
Microhardness of Friction Stir Processed Aluminium-6063
Microhardness of Friction Stir Processed Aluminium-6063Microhardness of Friction Stir Processed Aluminium-6063
Microhardness of Friction Stir Processed Aluminium-6063
ย 
Bhale2016
Bhale2016Bhale2016
Bhale2016
ย 
Solid state recycling of light metal reinforced-sami icme2017-00013
Solid state recycling of light metal reinforced-sami icme2017-00013Solid state recycling of light metal reinforced-sami icme2017-00013
Solid state recycling of light metal reinforced-sami icme2017-00013
ย 
Annealing Response of Aluminum Alloy AA6014 Processed By Severe Plastic Defor...
Annealing Response of Aluminum Alloy AA6014 Processed By Severe Plastic Defor...Annealing Response of Aluminum Alloy AA6014 Processed By Severe Plastic Defor...
Annealing Response of Aluminum Alloy AA6014 Processed By Severe Plastic Defor...
ย 
EFFECT OF THERMAL EXPOSURE ON THE MECHANICAL AND WEAR PROPERTIES OF AEROSPACE...
EFFECT OF THERMAL EXPOSURE ON THE MECHANICAL AND WEAR PROPERTIES OF AEROSPACE...EFFECT OF THERMAL EXPOSURE ON THE MECHANICAL AND WEAR PROPERTIES OF AEROSPACE...
EFFECT OF THERMAL EXPOSURE ON THE MECHANICAL AND WEAR PROPERTIES OF AEROSPACE...
ย 
Improving Mechanical Properties of AL 7075 alloy by Equal Channel Angular Ext...
Improving Mechanical Properties of AL 7075 alloy by Equal Channel Angular Ext...Improving Mechanical Properties of AL 7075 alloy by Equal Channel Angular Ext...
Improving Mechanical Properties of AL 7075 alloy by Equal Channel Angular Ext...
ย 
STRUCTURE PROPERTY CORRELATION OF MODIFIED Al-Mg ALLOYS FOR AEROSPACE APPLICA...
STRUCTURE PROPERTY CORRELATION OF MODIFIED Al-Mg ALLOYS FOR AEROSPACE APPLICA...STRUCTURE PROPERTY CORRELATION OF MODIFIED Al-Mg ALLOYS FOR AEROSPACE APPLICA...
STRUCTURE PROPERTY CORRELATION OF MODIFIED Al-Mg ALLOYS FOR AEROSPACE APPLICA...
ย 
Study on Influence of heat treatment on Tribological properties of mild steel
Study on Influence of heat treatment on Tribological properties of mild steelStudy on Influence of heat treatment on Tribological properties of mild steel
Study on Influence of heat treatment on Tribological properties of mild steel
ย 
20320140501018
2032014050101820320140501018
20320140501018
ย 
3 dimensional nonlinear finite element analysis of both thermal and mechanica...
3 dimensional nonlinear finite element analysis of both thermal and mechanica...3 dimensional nonlinear finite element analysis of both thermal and mechanica...
3 dimensional nonlinear finite element analysis of both thermal and mechanica...
ย 

Recently uploaded

Decoding Kotlin - Your guide to solving the mysterious in Kotlin.pptx
Decoding Kotlin - Your guide to solving the mysterious in Kotlin.pptxDecoding Kotlin - Your guide to solving the mysterious in Kotlin.pptx
Decoding Kotlin - Your guide to solving the mysterious in Kotlin.pptxJoรฃo Esperancinha
ย 
main PPT.pptx of girls hostel security using rfid
main PPT.pptx of girls hostel security using rfidmain PPT.pptx of girls hostel security using rfid
main PPT.pptx of girls hostel security using rfidNikhilNagaraju
ย 
POWER SYSTEMS-1 Complete notes examples
POWER SYSTEMS-1 Complete notes  examplesPOWER SYSTEMS-1 Complete notes  examples
POWER SYSTEMS-1 Complete notes examplesDr. Gudipudi Nageswara Rao
ย 
Application of Residue Theorem to evaluate real integrations.pptx
Application of Residue Theorem to evaluate real integrations.pptxApplication of Residue Theorem to evaluate real integrations.pptx
Application of Residue Theorem to evaluate real integrations.pptx959SahilShah
ย 
power system scada applications and uses
power system scada applications and usespower system scada applications and uses
power system scada applications and usesDevarapalliHaritha
ย 
Current Transformer Drawing and GTP for MSETCL
Current Transformer Drawing and GTP for MSETCLCurrent Transformer Drawing and GTP for MSETCL
Current Transformer Drawing and GTP for MSETCLDeelipZope
ย 
Introduction-To-Agricultural-Surveillance-Rover.pptx
Introduction-To-Agricultural-Surveillance-Rover.pptxIntroduction-To-Agricultural-Surveillance-Rover.pptx
Introduction-To-Agricultural-Surveillance-Rover.pptxk795866
ย 
Call Girls Narol 7397865700 Independent Call Girls
Call Girls Narol 7397865700 Independent Call GirlsCall Girls Narol 7397865700 Independent Call Girls
Call Girls Narol 7397865700 Independent Call Girlsssuser7cb4ff
ย 
SPICE PARK APR2024 ( 6,793 SPICE Models )
SPICE PARK APR2024 ( 6,793 SPICE Models )SPICE PARK APR2024 ( 6,793 SPICE Models )
SPICE PARK APR2024 ( 6,793 SPICE Models )Tsuyoshi Horigome
ย 
Artificial-Intelligence-in-Electronics (K).pptx
Artificial-Intelligence-in-Electronics (K).pptxArtificial-Intelligence-in-Electronics (K).pptx
Artificial-Intelligence-in-Electronics (K).pptxbritheesh05
ย 
GDSC ASEB Gen AI study jams presentation
GDSC ASEB Gen AI study jams presentationGDSC ASEB Gen AI study jams presentation
GDSC ASEB Gen AI study jams presentationGDSCAESB
ย 
Concrete Mix Design - IS 10262-2019 - .pptx
Concrete Mix Design - IS 10262-2019 - .pptxConcrete Mix Design - IS 10262-2019 - .pptx
Concrete Mix Design - IS 10262-2019 - .pptxKartikeyaDwivedi3
ย 
CCS355 Neural Network & Deep Learning Unit II Notes with Question bank .pdf
CCS355 Neural Network & Deep Learning Unit II Notes with Question bank .pdfCCS355 Neural Network & Deep Learning Unit II Notes with Question bank .pdf
CCS355 Neural Network & Deep Learning Unit II Notes with Question bank .pdfAsst.prof M.Gokilavani
ย 
Microscopic Analysis of Ceramic Materials.pptx
Microscopic Analysis of Ceramic Materials.pptxMicroscopic Analysis of Ceramic Materials.pptx
Microscopic Analysis of Ceramic Materials.pptxpurnimasatapathy1234
ย 
Architect Hassan Khalil Portfolio for 2024
Architect Hassan Khalil Portfolio for 2024Architect Hassan Khalil Portfolio for 2024
Architect Hassan Khalil Portfolio for 2024hassan khalil
ย 
Study on Air-Water & Water-Water Heat Exchange in a Finned ๏ปฟTube Exchanger
Study on Air-Water & Water-Water Heat Exchange in a Finned ๏ปฟTube ExchangerStudy on Air-Water & Water-Water Heat Exchange in a Finned ๏ปฟTube Exchanger
Study on Air-Water & Water-Water Heat Exchange in a Finned ๏ปฟTube ExchangerAnamika Sarkar
ย 
HARMONY IN THE NATURE AND EXISTENCE - Unit-IV
HARMONY IN THE NATURE AND EXISTENCE - Unit-IVHARMONY IN THE NATURE AND EXISTENCE - Unit-IV
HARMONY IN THE NATURE AND EXISTENCE - Unit-IVRajaP95
ย 
๐Ÿ”9953056974๐Ÿ”!!-YOUNG call girls in Rajendra Nagar Escort rvice Shot 2000 nigh...
๐Ÿ”9953056974๐Ÿ”!!-YOUNG call girls in Rajendra Nagar Escort rvice Shot 2000 nigh...๐Ÿ”9953056974๐Ÿ”!!-YOUNG call girls in Rajendra Nagar Escort rvice Shot 2000 nigh...
๐Ÿ”9953056974๐Ÿ”!!-YOUNG call girls in Rajendra Nagar Escort rvice Shot 2000 nigh...9953056974 Low Rate Call Girls In Saket, Delhi NCR
ย 

Recently uploaded (20)

Decoding Kotlin - Your guide to solving the mysterious in Kotlin.pptx
Decoding Kotlin - Your guide to solving the mysterious in Kotlin.pptxDecoding Kotlin - Your guide to solving the mysterious in Kotlin.pptx
Decoding Kotlin - Your guide to solving the mysterious in Kotlin.pptx
ย 
main PPT.pptx of girls hostel security using rfid
main PPT.pptx of girls hostel security using rfidmain PPT.pptx of girls hostel security using rfid
main PPT.pptx of girls hostel security using rfid
ย 
POWER SYSTEMS-1 Complete notes examples
POWER SYSTEMS-1 Complete notes  examplesPOWER SYSTEMS-1 Complete notes  examples
POWER SYSTEMS-1 Complete notes examples
ย 
Application of Residue Theorem to evaluate real integrations.pptx
Application of Residue Theorem to evaluate real integrations.pptxApplication of Residue Theorem to evaluate real integrations.pptx
Application of Residue Theorem to evaluate real integrations.pptx
ย 
power system scada applications and uses
power system scada applications and usespower system scada applications and uses
power system scada applications and uses
ย 
Current Transformer Drawing and GTP for MSETCL
Current Transformer Drawing and GTP for MSETCLCurrent Transformer Drawing and GTP for MSETCL
Current Transformer Drawing and GTP for MSETCL
ย 
Introduction-To-Agricultural-Surveillance-Rover.pptx
Introduction-To-Agricultural-Surveillance-Rover.pptxIntroduction-To-Agricultural-Surveillance-Rover.pptx
Introduction-To-Agricultural-Surveillance-Rover.pptx
ย 
young call girls in Green Park๐Ÿ” 9953056974 ๐Ÿ” escort Service
young call girls in Green Park๐Ÿ” 9953056974 ๐Ÿ” escort Serviceyoung call girls in Green Park๐Ÿ” 9953056974 ๐Ÿ” escort Service
young call girls in Green Park๐Ÿ” 9953056974 ๐Ÿ” escort Service
ย 
Call Girls Narol 7397865700 Independent Call Girls
Call Girls Narol 7397865700 Independent Call GirlsCall Girls Narol 7397865700 Independent Call Girls
Call Girls Narol 7397865700 Independent Call Girls
ย 
SPICE PARK APR2024 ( 6,793 SPICE Models )
SPICE PARK APR2024 ( 6,793 SPICE Models )SPICE PARK APR2024 ( 6,793 SPICE Models )
SPICE PARK APR2024 ( 6,793 SPICE Models )
ย 
Artificial-Intelligence-in-Electronics (K).pptx
Artificial-Intelligence-in-Electronics (K).pptxArtificial-Intelligence-in-Electronics (K).pptx
Artificial-Intelligence-in-Electronics (K).pptx
ย 
GDSC ASEB Gen AI study jams presentation
GDSC ASEB Gen AI study jams presentationGDSC ASEB Gen AI study jams presentation
GDSC ASEB Gen AI study jams presentation
ย 
Concrete Mix Design - IS 10262-2019 - .pptx
Concrete Mix Design - IS 10262-2019 - .pptxConcrete Mix Design - IS 10262-2019 - .pptx
Concrete Mix Design - IS 10262-2019 - .pptx
ย 
CCS355 Neural Network & Deep Learning Unit II Notes with Question bank .pdf
CCS355 Neural Network & Deep Learning Unit II Notes with Question bank .pdfCCS355 Neural Network & Deep Learning Unit II Notes with Question bank .pdf
CCS355 Neural Network & Deep Learning Unit II Notes with Question bank .pdf
ย 
Microscopic Analysis of Ceramic Materials.pptx
Microscopic Analysis of Ceramic Materials.pptxMicroscopic Analysis of Ceramic Materials.pptx
Microscopic Analysis of Ceramic Materials.pptx
ย 
Design and analysis of solar grass cutter.pdf
Design and analysis of solar grass cutter.pdfDesign and analysis of solar grass cutter.pdf
Design and analysis of solar grass cutter.pdf
ย 
Architect Hassan Khalil Portfolio for 2024
Architect Hassan Khalil Portfolio for 2024Architect Hassan Khalil Portfolio for 2024
Architect Hassan Khalil Portfolio for 2024
ย 
Study on Air-Water & Water-Water Heat Exchange in a Finned ๏ปฟTube Exchanger
Study on Air-Water & Water-Water Heat Exchange in a Finned ๏ปฟTube ExchangerStudy on Air-Water & Water-Water Heat Exchange in a Finned ๏ปฟTube Exchanger
Study on Air-Water & Water-Water Heat Exchange in a Finned ๏ปฟTube Exchanger
ย 
HARMONY IN THE NATURE AND EXISTENCE - Unit-IV
HARMONY IN THE NATURE AND EXISTENCE - Unit-IVHARMONY IN THE NATURE AND EXISTENCE - Unit-IV
HARMONY IN THE NATURE AND EXISTENCE - Unit-IV
ย 
๐Ÿ”9953056974๐Ÿ”!!-YOUNG call girls in Rajendra Nagar Escort rvice Shot 2000 nigh...
๐Ÿ”9953056974๐Ÿ”!!-YOUNG call girls in Rajendra Nagar Escort rvice Shot 2000 nigh...๐Ÿ”9953056974๐Ÿ”!!-YOUNG call girls in Rajendra Nagar Escort rvice Shot 2000 nigh...
๐Ÿ”9953056974๐Ÿ”!!-YOUNG call girls in Rajendra Nagar Escort rvice Shot 2000 nigh...
ย 

A refined energy-based model for friction stir processing of Al- Zn-Mg alloy

  • 1. P. K. MandalInt. Journal of Engineering Research and Applicationswww.ijera.com ISSN: 2248-9622, Vol. 6, Issue 1, (Part - 2) January 2016, pp.40-47 www.ijera.com 40|P a g e A refined energy-based model for friction stir processing of Al- Zn-Mg alloy P. K. Mandal Department of Metallurgy, Amal Jyothi College of Engineering, Kanjirapally, Kerala-686518, INDIA Abstract Friction stir processing (FSP) is a promising solid state surface modification technique. Also, considered as an innovative technique that the FSPwas employed to modify the surface layer of aluminium alloy. The FSP passes of only two passes were applied on aluminium alloy samples. A rotating tool with a pin and shoulder is inserted into a single piece of material and results in significant microstructural changes in the processed zone, due to intense plastic deformation. It has been proved to be an effective way to refine the microstructure of aluminium alloys, and thereby improve the mechanical properties. In procedural phenomenon there are different parameters adjustment have been worked out to refine microstructure and several properties characterised to TEM, SEM, FESEM and mechanical properties. In this study, a refined energy based model that estimates the energy generated due to friction and plastic deformation is presented with the help ofexperimental and theoretical results available in many literatures. The model is applied to 7xxx series of aluminium alloys. Keywords: FSP, solid-state process, processed zone, energy generation, 7xxx series. I. Introduction Age-hardening is the prime criteria in 7xxx series of Al alloy. It has several technological importances likely to as high strength light metal with various precipitation phases terminated from the supersaturated sold solution. There is an inseparable relationship between their improved combination of mechanical properties and the large number of fine precipitates formed during artificial ageing. The alloy composition, artificial ageing temperature and thermal history (solution treatment, quenching in water, natural ageing) are the main parameters influencing the age hardening response [1-5]. Generally, age hardening response is the increase in yield strength during artificial ageing than natural aged condition. A high yield strength implies a high resistance to dislocation motion [6]. It is also well known that adding minor scandium in aluminium alloy can refine grains and increase tensile strength, which attributed to the presence of coherent, L12- ordered Al3Sc particles. It can substantially inhibit recrystallization and pin subgrain boundaries and dislocations [7-11]. By adapting the concepts of friction stir welding (FSW), a new processing technique, friction stir processing (FSP), has been recently developed. The basic concept of FSP is remarkably simple. A rotating tool with a pin and shoulder is inserted into a single piece of material and results in significant microstructural changes in the processed zone, due to intense plastic deformation at elevated temperature resulting in significant grain refinement [12-15].Therefore, FSP has been proved to be an effective way to refine the microstructure of aluminium alloys, and thereby improve the mechanical properties. The microstructure and properties of the modified layer depend on the amount of fractional heat generated by processing. Actually, heat is generated due to plastic deformation of the workpiece and the effect of the friction between the surfaces of the tool and the workpiece. The process is carried out in solid state at low temperature, typically around 0.6 to 0.7 of the aluminium alloy fusion temperature. The processed zone is deformed and under the thermal effect recovers and recrystallizes, forming a defect-free recrystallized fine grain microstructure. During experimental FSP, it is seen that in aluminium alloy the action of tool produces different microstructurally distinct regions; the stir zone (SZ), the thermo- mechanically affected zone (TMAZ) and the heat affected zone (HAZ). The stir zone is in centre of FSP and has undergone the most severe plastic deformation during processing. The stir zone grains suggest effective strains together with a microstructural evolution that occurs by a combination of hot working and a dynamic recovery or recrystallization. The temperature reached in the stir zone is known as being situated in the range of 480 o C [C.B. Fuller et al., 2010; at 640 rpm, 160 mm/min]for the aluminium alloy. The authors like Heurtier et al. and [2006] and Hamilton et al. [2008] have been proposed energy based model for the FSW during their works [16]. In fact, the energy due to plastic deformation and friction of the shoulder with the surface of the workpiece are related and competing each other. As the heat generated by the shoulder is low, the flow stress is higher and hence the resulting plastic deformation energy increases. On RESEARCH ARTICLE OPEN ACCESS
  • 2. P. K. MandalInt. Journal of Engineering Research and Applicationswww.ijera.com ISSN: 2248-9622, Vol. 6, Issue 1, (Part - 2) January 2016, pp.40-47 www.ijera.com 41|P a g e the other hand, as the heat generated by the shoulder is high, the flow stress reduces and as a result the plastic strain contribution decreases. As per Khandkarโ€™s torque-based model for which the total torque is the sum of torque contributions from the tool shoulder against the workpiece, the bottom of the tool pin against thickness material and the pin surface against thickness material [17]. There are several characterizations have been done likely to FESEM (field emission scanning electron microscopy), SEM (scanning electron microscopy) and age hardening phenomena through Vickerโ€™s hardness testing. The aim of this study is to investigate the effects of double FSP passes on microstructural and mechanical properties of aluminium alloy. Besides, the effects of the plastic deformation as well as heat energy generation as compared to the theoretical and experimental results available in many literatures. In this work, heat is modelled to be generated by the friction of the shoulder and plastic deformation. II. Experimental procedure The research was conducted on cast plate as well as different heat treated plates of 7xxx series of aluminium alloy with the dimension as 150 ร— 90 ร— 8 mm3 , and the chemical composition is presented in Table-1. Standard metallographic procedures were followed for the macro and microstructural analysis. A modified Kellerโ€™s reagent was used for etching of metallographic samples. The age hardening characteristics have been identified through Vickerโ€™s hardness measurements at 10 kg. load with 15 min dwell time at different time intervals at 120, 140, 180 o C temperatures, respectively. Obviously, an as-cast sample first solution treated from 465 o C for 1h then immediately water quenching (i.e., T4 heat treatment), then maintained above artificial ageing temperatures (i.e., T6 heat treatment) and performed hardness sequentially upto 16 h ageing time. The cast plates were subjected to double FSP passes along the clockwise direction with predetermined rotational speed and traverse speed. The FSP was conducted on the base of a conventional vertical milling machine. The machine was well equipped with appropriate devices to collection data during working period. The materials for tensile specimens were produced (i.e., pick up along the stir zone) with tool parameters of 720 rpm (tool rotational speed) and 80 mm/min (plate travel speed) from the different heat treated conditions (in Fig.-1.a). Used tool dimensions (shoulder dia. 25 mm, shoulder height 20 mm, pin root dia. 6 mm, pin tip dia. 3 mm, and pin height 3.5 mm) were selected during experimental FSP. Similarly, the FSP tool geometry has been referred as per Hamilton et al. energy model as shown in Fig.- 1(b). It is well know that the material is transported from advancing side (A) to the retreating side (R) during rotational phenomena. The plasticized material may travel many cycles around the tool before being deposited. Microstructural evolution was studied using scanning electron microscopy (SEM) and field emission scanning electron microscopy (FESEM) and the resultant mechanical properties were examined with microhardness measurements and tensile tests. Similarly, transmission electron microscopy (TEM) and X-ray diffraction (XRD) methods characterization were examined for materials intuitive precipitation phenomena. The tensile test was conducted in Instron (universal testing machine) UTM(25 KN, H25 K-S, UK). The tensile samples (flat shape sample dimensions (mm): full length 58, gauge length 26, width 4) had collected from stir zone, and tested with cross head speed 1 mm/min at room temperature. Table-1: Chemical composition analyzed by ICP-AES (in wt%). Alloy no. Zn Mg Sc Si Fe Al Zn+Mg Zn/Mg 1 8.24 5.67 0.87 0.88 0.42 Bal. 13.91 1.45 Fig.-1: (a) Schematic illustration of the friction stir processing (FSP) set-up; (b) Geometry of the FSP tool. (a) (b)
  • 3. P. K. MandalInt. Journal of Engineering Research and Applicationswww.ijera.com ISSN: 2248-9622, Vol. 6, Issue 1, (Part - 2) January 2016, pp.40-47 www.ijera.com 42|P a g e Table-2: Processing parameters of FSP. FSP parameters (experiment performed through double passes) Tool rotation speed ฯ‰ (rpm) Work piece travel speed ๐œ ๐‘œ (mm/min) Axial compressive force F (KN) Pin angle (o ) 720 80 15 2.5 III. Results and discussion The Al-Zn-Mg alloy is age hardening aluminium alloy. There are several phases transitions have been occurred during ageing heat treatment. The GP zones (GP I and GP II) and ฮฎ are the phases that contribute to the precipitation hardening of this alloy in the under-ageing and peak-ageing conditions, while ฮท forms during over-ageing conditions. Moreover, Sc addition in aluminium alloy consists of a spatial distribution of Al3Sc particles. These small coherent particles with nano size were distributed homogeneously throughout the grains. Also, ample interaction between a matrix dislocation and an Al3Sc precipitates at 400o C [18]. In Fig.-2 shows the of hardness measurements, with the error bars indicating the deviations of individual measurements. In fact, the hardness-ageing curve can be roughly divided into three regions: region I (i.e., called under-aged) with a gradual increase in harness for all ageing curves; region II (i.e., called peak-aged) with peak hardness accompanied by slight hardness decreases over a long time ageing duration; region III (i.e., called over-aged) with a further hardness decreases. In present three ageing curves have shown gradually hardness diminish due to growth of the ฮท (MgZn2) precursor particles may lead to loss of the lattice match or coherency between the matrix and the particles [19,1]. When the ageing temperature is higher the peak formation earlier than at lower ageing temperatures. On the other hand, Sc additions in aluminium alloy ageing peak formation accelerate with high value but coarsening effect one more adversely phenomena during ageing. Hardening effect of Sc useful upto 0.6 wt% beyond this coarsening effect dominates in our experimental observation and many literature references. During ageing, Al3Sc particle coherency is maintained until a critical size is reached. Above that, heterogeneous precipitation occurs indicated by the formation of the new nuclei on dislocations and grain boundaries. As mention in literature, introduction of dislocation networks to the Al/Al3Sc interface is most possibly related to coherency loss, low elastic strain energy caused by the reduction in the lattice misfit [20, 8]. At 120 0 C ageing shows higher hardening response in among three ageing temperatures. Stability of GP zones with high Sc content Al3Sc particles can be claimed higher hardness value. Also, many literatures supported at this temperature GP formation and acceleration by Sc added Al-Zn-Mg alloy. At 140 o C ageing shows moderate hardening response although this temperature regime specially meant for metastable ฮฎ phase formation region. But due to higher Sc contents hardening effect diminish although uniformly decrease hardness with increasing ageing time. At 180 o C ageing shows lowest hardening effect among three studied ageing temperatures. In this temperature regime hardening effect arrives earlier but coherency loss at faster rate due to higher Sc contents mostly dominate factor. On the other hand, due to higher Sc contents in aluminium alloy suppress the inherently hardening effect. In Fig.-3 shows FESEM with EDS analysis in cast aluminium alloy. The EDS analysis revealed grain boundary segregation with impurity elements and grain boundaries broaden prominent in cast aluminium alloy although Sc transition elements eliminate grain boundary segregation but probably high contents this effect decline also EDS result shows Sc-2.71%, Si-1.30%, and Fe-0.91%, respectively.Recently, a derivative from FSW, the so called friction stir processing โ€“ FSP was proved as being useful for inducing directed, localized, and controlled materials properties in any arbitrary location of components. The microstructure of the processed layer is complex and highly dependent on the position within the processed zone. This is due to the large local variations in the plastic flow, and to the thermal history resulted from the material interaction with the processing tool. In FSW/FSP, the processing technique called โ€˜cold workingโ€™ does not generate the melting of the nugget or stir zone. The microstructure in stir zone is characterized by refined grains in a discrete series of bands and some precipitates mainlydistributed in the matrix with subgrain boundaries formation.
  • 4. P. K. MandalInt. Journal of Engineering Research and Applicationswww.ijera.com ISSN: 2248-9622, Vol. 6, Issue 1, (Part - 2) January 2016, pp.40-47 www.ijera.com 43|P a g e Fig.-2: The hardness-time curves plotted for a studied alloy aged at different temperatures. Fig.-3: FESEM with EDS anaysis(as-cast condition) of studied alloy. The stir zone grains suggest effective strains together with a microstructural evolution that occurs by a combination of hot working and a dynamic recovery or recrystallization.It is likely to that sometimes low hardness in the stir zone can be attributed to dissolution of the precipitate during FSP.Generally, the hardness depends on the precipitate distribution rather than grain size.The thermo-mechanically affected zone adjacent to the nugget or stir zone is the region where the metal is plastically deformed as well as heated to a temperature, which is not sufficient to cause recrystallization.Distinct precipitates and coarsened grains are observed in HAZ regions, where the grains are severely coarsened by FSP. There are several assumptions have been taken as per Hamilton et al. and Heurtier et al. [2006] that the heat generated due to friction of the pin shoulder on the workpiece surface is dominant and the heat generated due to the plastic deformation within the workpiece and the friction of the pin of the material is negligible. However, heat generated mostly from both the friction of the pin shoulder and plastic flow. It is assumed that the tool rotates with an angular speed of ฯ‰ (rpm) and traversely translates along the line of processing with a speed of ๐œ ๐‘œ (mm/min) and tool is acted upon by a compressive axial force F as shown in Fig.-1(b). According to Hamilton et al. energy model, since I II III
  • 5. P. K. MandalInt. Journal of Engineering Research and Applicationswww.ijera.com ISSN: 2248-9622, Vol. 6, Issue 1, (Part - 2) January 2016, pp.40-47 www.ijera.com 44|P a g e FSP is the metal working technology adapted from FSW using the same basic principles [16]. Since, energy generated per unit length during processing as E is given by Ef = Pf /๐œ ๐‘œโ€ฆโ€ฆ..(1), where P is the total power generated by friction. Assuming that the total torque due to friction of the pin, shoulder, and pin circumference with the work piece surfaces is Tf, the frictional power is then given by Pf= Tfฯ‰ โ€ฆโ€ฆโ€ฆ(2), where ฯ‰ is the pin angular speed. To find an expression for the total frictional torque Tf, we let Tf = Ts + Tp โ€ฆโ€ฆโ€ฆ(3), where Ts is the torque generated by the shoulder and Tp is torque generated by the pin. Assuming that a uniform shear stress ฮท occurs during processing, we obtain Tf = 2ฯ€๐‘Ÿ๐‘œ 2 ฮท ( 1 3 ๐‘Ÿ๐‘œ + ๐‘Ÿ๐‘– 2 ๐‘Ÿ ๐‘œ 2h)โ€ฆ.(4). Assuming a coefficient of friction is ยต, the total friction force Ff due to the compressive force F is given by Ff = ยตF โ€ฆโ€ฆโ€ฆ(5). It is noting that ฯ€๐‘Ÿ๐‘œ 2 ฮท is the total frictional force, then from equ.-(4) Tf = 2ยตF ( 1 3 ๐‘Ÿ๐‘œ + ๐‘Ÿ๐‘– 2 ๐‘Ÿ ๐‘œ 2h)โ€ฆโ€ฆ(6). Now consider from equ.-(1) and (2), we obtain Ef = Tf ฯ‰ / ๐œ ๐‘œ = 2ยตF ( 1 3 ๐‘Ÿ๐‘œ + ๐‘Ÿ๐‘– 2 ๐‘Ÿ ๐‘œ 2 h) ฯ‰ ๐œ ๐‘œ .........(7). So, equ.-(7) defines the energy per unit length of the FSW/FSP due to friction between the tool and the workpiece. For a given tool geometry, tool speed, and workpiece material, this energy can be easily identified. As can be noted from equ.-(1), the power generated due to friction is given by Pf = 2ยตF ( 1 3 ๐‘Ÿ๐‘œ + ๐‘Ÿ๐‘– 2 ๐‘Ÿ ๐‘œ 2 h)ฯ‰โ€ฆโ€ฆโ€ฆ(8). As Frigaard [1998] reported that the coefficient of friction (ยต) between Al and mild steel should be set as the average value between 0.5 for sticky friction and 0.25 for dry sliding. However, in this study a coefficient of friction (ยต) is used 0.5 (as per Hamilton et al.). The other source of heat is due to the plastic deformation within the workpiece. Provided that the plastic deformation within the workpiece is totally transformed into heat, the heat generated due to plastic deformation per unit FSP length can be expressed as follows: Ep = ฮถ ฮต dVโ€ฆโ€ฆ(9), where ฮถ and ฮต are the stress and strain, respectively, dV = 2๐‘Ÿ๐‘– h is the volume per unit length of the material. Since the effect of the energy due to plastic deformation is much smaller than that due to friction, a simple model was proposed as follows:Ep = ฮถe ฮตe 2 ๐‘Ÿ๐‘– h โ€ฆโ€ฆ.(10), where ฮถe is the equivalent (effective) stress and ฮตe is the effective strain. Using the finite element method, Heurtier et al. [2006] found that the effective strain is around 6. The power generated due to the plastic deformation is given by Pp = ฮถe ฮตe(2๐‘Ÿ๐‘– h) ๐œ ๐‘œ โ€ฆ..(11). The total eregry generated per unit length of the FSP is the sum of the energy generated due to friction between the tool and the workpiece and the plastic deformation within the workpiece. An empirical formula developed a proposed energy model by Hamilton et al., ๐‘‡ ๐‘š๐‘Ž๐‘ฅ ๐‘‡๐‘  = 1.56 ร— 10โˆ’4 ๐ธ๐‘’๐‘“๐‘“ + 0.54โ€ฆโ€ฆโ€ฆ..(12), where ๐‘‡ ๐‘š๐‘Ž๐‘ฅ is the maximum temperature generated within the FSP, ๐‘‡๐‘  is the solidus temperature in Kelvin, ๐ธ๐‘’๐‘“๐‘“ is the effective energy generated per unit length of FSP in J/mm. In this study, one aluminium alloy is considered using different FSP parameters such as tool geometry and FSP speed. As per many literatures supported and Hamilton energy model we can be concluded ๐‘‡๐‘  = 636 o C [from Al-Zn equilibrium phase diagram]and ๐‘‡ ๐‘š๐‘Ž๐‘ฅ = 480 o C[C.B. Fuller et al., 2010; at 640 rpm, 160 mm/min] , its can put into equ.-(12) to obtained ๐ธ๐‘’๐‘“๐‘“ = ๐‘‡ ๐‘š๐‘Ž๐‘ฅ ๐‘‡๐‘  ( 104 1.56 ) โ€“ 0.54 (J/mm)โ€ฆโ€ฆ..(13). Considering equ.-13, we can be obtained ๐ธ๐‘’๐‘“๐‘“ = 5319.97 J/mm. Consequently, as per Khandkarโ€™s torque-based model for which the total torque, Ttotal , is expressed as the sum of torque contributions from the tool shoulder against the workpiece, the bottom of the tool pin against thickness material and the pin surface against thickness material. Therefore, Ttotal = 2ยตF ( 1 3 ๐‘Ÿ๐‘œ + ๐‘Ÿ๐‘– 2 ๐‘Ÿ ๐‘œ 2h)โ€ฆโ€ฆ(14), where, ยต (0.5 value) is the coefficient of friction between the tool and the workpiece, F is the applied force, ro is the radius of the tool shoulder, ri is the radius of the pin, h is the pin height. The total energy per unit length of FSW, Etotal is found by dividing the average power, Pavgby the weld velocity to yield the expression using Etotal = ๐‘ƒ ๐‘Ž๐‘ฃ๐‘” ๐‘ฃ ๐‘ค = Ttotal ๐œ” ๐‘ฃ ๐‘ค โ€ฆโ€ฆโ€ฆ(15), where ๐‘ฃ ๐‘ค is the velocity during FSW and ฯ‰ is the tool angular velocity. As per C. Hamilton et al. [2009] proposed his paper during FSW welding temperature is equal to the solidus temperature of aluminium alloy, i.e., ๐‘‡ ๐‘š๐‘Ž๐‘ฅ ๐‘‡๐‘  = 1. So, from the equ.-(13) we can easily found out ๐ธ๐‘’๐‘“๐‘“ = 6409.72 J/mm. for the Sc-modified Al-Zn- Mg-Cu alloy examined in this work, the model successfully predicts the maximum welding temperature and temperature distributions over the energy range investigated by C. Hamilton et al.. The model, however, shows its greatest potential at higher energy welds (i.e., (Etotal)eff หƒ1000 J/mm) where heat generation due to friction dominates. At the lower energy levels (i.e., (Etotal)eff ห‚1000 J/mm), the predicted temperature data in terms of magnitude and shape away from the tool shoulder, but the model under-predicts the maximum welding temperatures due to the assumptions/simplifications that were used in the calculation of the plastic energy. According to H. Lombard et al., hinted that the basic energy model based on the external FSW parameters [21, 22]. Heat input from the tool shoulder per unit length of weld (J/mm) can be estimated from torque measurements that remain reasonably constant once thermal equilibrium is reached and given by Q = Power Traverse speed
  • 6. P. K. MandalInt. Journal of Engineering Research and Applicationswww.ijera.com ISSN: 2248-9622, Vol. 6, Issue 1, (Part - 2) January 2016, pp.40-47 www.ijera.com 45|P a g e = ฮท 2๐œ‹๐œ”๐‘‡ ๐œ โ€ฆ..(16), where Q is the heat input (J/mm), ฮท = efficiency factor = 0.9 (for Al and Cu), ฯ‰ (rpm) is the rotational speed, T (Nm) is the torque, ๐œ (mm/min) is the traverse speed. They also hinted on heat input appears to be dominated by the traverse speed, suggesting that changes in the rotational speedare compensated by changes in the torque.In Fig.-4 shows different FSP Fig.-4: The illustration of optical micrograph (at T4 + FSP) of different FSP regions of studied alloy. regions which has created during this processing just because tool shoulder with workpiece downward frictional force with predetermined tool geometry and predetermined FSP parameters, which can be created three distinct zones likely to stir zone (SZ- centre zone as equal area of pin diameter), thermo- mechanically affected zone (TMAZ- nearer to stir zone), and heat affected zone (HAZ- nearer to thermo-mechanically affected zone), also identified in specific regions in optical micrograph. As a result, stir zone is the most effective region to refine microstructure to modify material surface characteristics and enhanced mechanical properties. Hence, main aim of the investigation is to determine the relationship between parameters of the process (rotational speed, traverse speed, downward force, and type of tool design) and torque (Nm) and temperature generated in the stir zone [A.N. Solonin et al., 2010; P. Heurtier et al., 2006]. Torque, temperature and stress generated by the movement and friction of materials, decide about heat generation in the modified material and thus the changes of microstructure and consequently the mechanical properties of material. It is evidence that the torque strongly depends on the rotational speed of the FSP tool. This is because the rotational speed stimulates the temperature in the FSP area and thus the friction coefficient decreases when temperature increases. The value of torque is influenced by rotational speed, travelling speed, downward force, design of tool, and a kind of modified material. Here, the experimental results are compared with the results obtained from the theoretical models. In Fig.-5(a-b) shows tensile fractographs at different conditions, for Fig.-5(a) has indicated ductile mode of fracture surface and microcracks are normally originated from grain boundaries (e.g. generally called intergranular fracture mode) and fine precipitates are appears mostly in grain boundary regions in between some black holes also indicate origin of fracture initiation. Similarly, in Fig.-5 (b) shows fracture surfaces are blunt due to may ageing exposed indication and overall fracture surface indicating uniformly arranged with some dip black holes observed. These black holes are possibly indication of stress centre. This studied alloy has Sc content 0.87%, which can be SZ TMAZ HAZ
  • 7. P. K. MandalInt. Journal of Engineering Research and Applicationswww.ijera.com ISSN: 2248-9622, Vol. 6, Issue 1, (Part - 2) January 2016, pp.40-47 www.ijera.com 46|P a g e deleterious effect of coarsening tendency during post ageing heat treatment. During age hardening treatment at 140 o C ageing hardness dropped marginally than at lower ageing temperature. Consequently, during tensile testing also indicated at this condition overall mechanical properties diminish. Since, aluminium alloy is prominent for age hardening ability to response natural ageing and subsequently artificial ageing tendency at elevated temperatures. The age hardening kinetics can be revealed through tensile testing measurement, also depend on chemical composition, heat treatment conditions and after all surface modification technique, so called FSP. In Table-3 shows tensile results at different FSP conditions in three stages at as-cast plus FSP condition exhibited higher tensile properties due to cast condition with FSP hardening phases (ฮท-Mg2Zn) are homogeneously distributed with fine grains cause dynamic recrystallization and presence of coherent Al3Sc particles. But hardness value (105.8HV) indicated lowest due to higher ductility. Consequently, T4 heat treatment plus FSP condition tensile properties are slightly dropped due to specific solution treatment the hardening phases are dissolution occurred, possibly. One more possibility may happen for solution treatment Al3Sc particles remain in solution, particles have not taken part hardening activity as like during ageing phenomena hardening stimulated with time. But hardness value (153.6HV) is highest due to higher Sc contents. After T4 plus FSP with post ageing treatment tensile properties dropped drastically because material become ovreaged with predominantly incoherent equilibrium (ฮท) phases, particle coarsening particularly at grain boundary regions. Other hand, at FSP with post-heating specimen often exposed faster precipitates nucleation (i.e., depends nature of material, time, and temperature) with facilities of high angle grain boundaries are main factors. Similarly, hardness value (128.2HV) dropped drastically due to higher Sc contents to faster precipitates coarsening effect. Fig.-5: The tensile fractographs of studied alloy (a) at T4+FSP; (b) at T4+FSP+Ageing at 140 o C/2h. Table-3: Results of tensile properties are tabulated through FSP directionof studies alloy. FSP by double passes at different conditions Tensile properties ฮถ0.2(MPa) ฮถu(MPa) ฮด(%) VHN(10kg.) AC + FSP 99.4 207.8 5.7 105.8 T4 + FSP 98.9 197.6 4.3 153.6 T4 + FSP + Aged at 140 o C /2h 79.2 168.5 5.2 128.2 Note: AC= as-cast; T4 = solutionized at 465 o C/1 h then WQ; yield strength denoted at 0.2% offset from stress- strain curve. Hardness (at average six values) taken along the stir zone. IV. Conclusions 1. The Al-Zn-Mg alloy is the best age hardening performer in all aluminum series. 2. Based on experimental results Sc is best hardener in cast aluminum alloy within the limit 0.25-0.60 wt%. 3. Adding minor scandium in aluminium alloy can refine grains and increase tensile strength, which attributed to the presence of coherent, L12- ordered Al3Sc particles. It can substantially inhibit recrystallization and pin subgrain boundaries and dislocations. 4. At higher Sc contents diminish age hardening effect and deteriorate overall mechanical properties. 5. The friction stir processing (FSP) originates from the technology of friction stir welding (FSW), yet in comparison with this method, the phenomena taking place in the interface between the stirring area and the workpiece will have a (a) (b)
  • 8. P. K. MandalInt. Journal of Engineering Research and Applicationswww.ijera.com ISSN: 2248-9622, Vol. 6, Issue 1, (Part - 2) January 2016, pp.40-47 www.ijera.com 47|P a g e decisive effect on the functional properties of a surface layer obtained through this process. 6. The friction stir processing (FSP) is a promising solid state surface modification technique. Also, considered as an innovative technique that the FSPwas employed to modify the surface layer of aluminium alloy. The FSP process addresses the industry as surface repairing technique in case of different types of flows. 7. The proof stress and tensile stress dropped marginally due to elimination of residual stresses, dissolution of precipitates (ฮท-MgZn2) and grains coarsening are main reasons. 8. The goal of presented work is to estimate the relationship between FSP parameters such as rotational and travelling speed, downward force, torque, temperature. 9. There are several theoretical energy-based models explained for better coincidence with present experimental data. According to Heurtier et al. and Hamilton et al. a simply energy-based model for the FSW/FSP is proposed. The model aims at estimating the heat generated due to plastic deformation within the workpieces and friction between the tool surfaces and the workpieces. A comparison between the estimated heat energy and its corresponding maximum temperature obtained using the proposed model and the experimental result shows a good agreement. 10. Here, we have discussed Khandkarโ€™s torque- based model that is good agreement with heat energy generated is a function of applied force, coefficient of friction between the tool and the workpiece, tool dimensions, and FSW/FSP parameters. As per Khandkarโ€™s torque-based model and Hamilton energy-based modelโ€™s correlation has been found out effective energy value (Eeff) during our experiment work. The numerical value is Eeff = 6409.72 J/mm.This is good agreement with Khandkarโ€™s torque-based model value. Also, from our experimental data obtained value is Eeff = 5319.97 J/mm. As per H. Lombard et al. explained basic energy based model, also explained amount of heat generation depends on process parameters. References [1] J.Z. Liu et al., Scripta Materialia 63 (2010) 1061-1064. [2] S. Ahmadi et al., Journal of Alloys and Compounds 484 (2009) 90-94. [3] J.K. Park et al., Metallurgical Transactions A, Vol. 14A, Oct. 1983, 1957-1965. [4] W.J. Poole et al., Metallurgical and Materials Transactions A, Vol. 31A, Sept. 2000, 2327-2338. [5] H. Loffler et al., Journal of Materials Science 18 (1983) 2215-2240. [6] E. Hornbogen et al., Acta Metall. Mater. Vol. 41, No. 1, pp. 1-16, 1993. [7] B. Li et al., Journal of Alloys and Compounds 584 (2014) 406-416. [8] D. Tsivoulas et al., Materials Science Forum, Vols. 519-521 (2006) pp. 473-478. [9] Z. Ahmad, Journal of Materials, Feb.2003, pp. 35-39. [10] A.L. Berezina et al., Materials Science Forum, Vols. 396-402 (2002) pp. 741-746. [11] Y. Deng et al., Journal of Alloys and Compounds 530(2012) 71-80. [12] C.G. Rhodes et al., Scripta Materialia 48 (2003) 1451-1455. [13] S. Soleymani et al., Journal of Surface Engineering Materials and Advanced Technology, 2011, 1, 95-100. [14] C.B. Fuller et al., Materials Science and Engineering A 527 (2010) 2233-2240. [15] J-Q. Su et al., Scripta Materialia 52 (2005) 135-140. [16] S. A. Emam et al., World Academy of Science, Engineering and Technology 53, 2009, pp. 1016-1022. [17] C. Hamilton et al., International Journal of Machine Tools & Manufacturing 49 (2009) 230-238. [18] B.G. Clark et al., Journal of Materials Research, Vol. 20, No. 7, July 2005, pp. 1792-1801. [19] W. Feng et al., Rare Metals, Vol. 26, No. 2, Apr. 2007, pp. 163-168. [20] J. Royset et al., International Materials Reviews, 2005, Vol. 50, No. 1, 19-44. [21] M.S. Weglowski et al., Key Engineering Materials, Vols. 554-557 (2013) pp. 1787- 1792. [22] H. Lombard et al., Materials Science and Engineering A 501 (2009) 119-124.