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It is also known as JACOBSON KATSUKI EPOXIDATION
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Jacobson katsuki named rxn
1.
Presented By: •Gandham Malasree •Regd
no: 620209502002 •Dept of Pharmaceutical Chemistry AU COLLEGE OF PHARMACEUTICAL SCIENCES, VISAKHAPATNAM Jacobson Asymmetric Epoxidation
2.
CONTENTS Introduction History Catalysts Synthesis of catalyst Mechanism
approach Mechanism Applications
3.
INTRODUCTION • It is
also known as JACOBSON KATSUKI EPOXIDATION What is epoxidation?
4.
HISTORY
5.
CATALYST • Manganese (III)
salen catalyst R= alkyl, trialkyl etc., R= tertiary butyl is the most effective
6.
Active species in
catalytic cycle: Oxo – managanese (V) salen
7.
8.
Synthesis of manganese
salen complex
9.
Jacobson and katsuki
individually reported the catalysts Katsuki catalyst
10.
Mechanism approach
11.
Mechanism there are 3
major pathways 1. Concerted pathway 2. Free radical pathway 3. Metallo oxetane pathway
12.
Mechanism
13.
Applications 1
14.
Application in process
chemistry 2 Indene
15.
• Forming a
chiral epoxide is the key step for the synthesis of pharmaceutical drugs. • Cyclic and acyclic cis -1,2- disubstituted alkenes are epoxidized with 100% enantiopurity.
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