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255,Techno 2-ro,Yuseong-gu, Daejeon, Korea (Daedeok techno valley) Tel: +82-42-931-6100 Fax: +82-42-935-6103 Homepage: www.suflux.com E-mail: webmaster@suflux.com
HIGH PRESSURE REACTOR
Magnedrive
Seal type
(O-ring/gasket)
Port(Inlet/Outlet)
Thermocouple
Pressure Vessel
Liner
Hydrothermal Synthesis of Zeolite (ZSM-5) Hydrothermal Synthesis of ZrO2 Nanoparticles
Hydrothermal Synthesis of Amorphous SiO2 Hydrothermal Synthesis of MnO2 Nanorod
BET Surface Area: 186 m2
∙g-1
SEM (Size & Morphology) XRD (Crystal Structure)
Zirconia NanoparticlesH S
NH4OH Solution
10 20 30 40 50 60 70 80 90
Intensity(arb.unit)
2 Theta (degree)
KMnO4
Solution
Mn(CH3COOH)2
Solution
XRD (Crystal Structure)SEM (Size & Morphology)
Cal. 300-500 ℃ for 2h
10 20 30 40 50 60
Intensity(arb.unit)
2 Theta (degree)
M
SIO2
A12O2
H20
MOH(F)
SI-O, AI-O boundsMordenite(MOR) Rho(RHO) UZM-5(UFI) SSZ-13, SAPO-34(CHA)
200
150
100
50
0
0.0 0.2 0.4 0.6 0.8 1.0
P/P0
Adsorption
Desorption
VolumeAdsorbed(cm3
g-1
,STP)
PoreVolume(cm
3
g
-1
nm
-1
)
0.60
0.45
0.30
0.15
0.00
1 10010
Pore Width / nm
BET Surface Area TEM (Size & Morphology)
Ref. Journal of Colloid and Interface Science 350 (2010) 290–294
Hydrothermal
XRD (Crystal Structure)
Amorphous SiO2
M OR HOH ROHOH
Hydrolysis
Reesterification
M+ +
M OH OH HOHO
Water
Condensation
Hydrolysis
M M M+ +
M OH OR ROHO
Alcohol
Condensation
Alcoholysis
M M M+ +
10 20 30 40 50 60 70 80 90
Intesity(arb.unit)
2 Theta (degree)
AFM (Size & Morphology)
The reactor systems by high pressure & temperature have application of synthesis, decomposition, sublimation, extraction,
any other industries as customized engineering service
Pressure(㎏/㎠)
Volume(ℓ)
Temperature(℃
)

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High pressure oven Inforgrapfic - ilshinautoclave

  • 1. 255,Techno 2-ro,Yuseong-gu, Daejeon, Korea (Daedeok techno valley) Tel: +82-42-931-6100 Fax: +82-42-935-6103 Homepage: www.suflux.com E-mail: webmaster@suflux.com HIGH PRESSURE REACTOR Magnedrive Seal type (O-ring/gasket) Port(Inlet/Outlet) Thermocouple Pressure Vessel Liner Hydrothermal Synthesis of Zeolite (ZSM-5) Hydrothermal Synthesis of ZrO2 Nanoparticles Hydrothermal Synthesis of Amorphous SiO2 Hydrothermal Synthesis of MnO2 Nanorod BET Surface Area: 186 m2 ∙g-1 SEM (Size & Morphology) XRD (Crystal Structure) Zirconia NanoparticlesH S NH4OH Solution 10 20 30 40 50 60 70 80 90 Intensity(arb.unit) 2 Theta (degree) KMnO4 Solution Mn(CH3COOH)2 Solution XRD (Crystal Structure)SEM (Size & Morphology) Cal. 300-500 ℃ for 2h 10 20 30 40 50 60 Intensity(arb.unit) 2 Theta (degree) M SIO2 A12O2 H20 MOH(F) SI-O, AI-O boundsMordenite(MOR) Rho(RHO) UZM-5(UFI) SSZ-13, SAPO-34(CHA) 200 150 100 50 0 0.0 0.2 0.4 0.6 0.8 1.0 P/P0 Adsorption Desorption VolumeAdsorbed(cm3 g-1 ,STP) PoreVolume(cm 3 g -1 nm -1 ) 0.60 0.45 0.30 0.15 0.00 1 10010 Pore Width / nm BET Surface Area TEM (Size & Morphology) Ref. Journal of Colloid and Interface Science 350 (2010) 290–294 Hydrothermal XRD (Crystal Structure) Amorphous SiO2 M OR HOH ROHOH Hydrolysis Reesterification M+ + M OH OH HOHO Water Condensation Hydrolysis M M M+ + M OH OR ROHO Alcohol Condensation Alcoholysis M M M+ + 10 20 30 40 50 60 70 80 90 Intesity(arb.unit) 2 Theta (degree) AFM (Size & Morphology) The reactor systems by high pressure & temperature have application of synthesis, decomposition, sublimation, extraction, any other industries as customized engineering service Pressure(㎏/㎠) Volume(ℓ) Temperature(℃ )