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International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 05 Issue: 11 | Nov 2018 www.irjet.net p-ISSN: 2395-0072
© 2018, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 1181
EXPERIMENTAL STUDY ON RESIDUAL CHARACTERISTICS OF
CONCRETE SUBJECTED TO ELEVATED TEMPERATURE
Mr. V. Niranjan1, Mr. A. Sathya Deva 2
1Assistant professor , Department of Civil Engineering, RVS Technical Campus, Coimbatore-641402, India,
2PG student, Department of Civil Engineering, RVS Technical Campus, Coimbatore-641402, India
---------------------------------------------------------------------***----------------------------------------------------------------------
Abstract - The effect of high temperatures exposed on the
concrete structural members is an important parameter tobe
considered in the design. The residual characteristics of
temperature damaged concrete structural elements, the
strength and stiffness degradation are considered to be very
important in the modern design. The effect of this high
temperature alter the physical, mechanical and
microstructural characteristics of concrete thus the residual
strength andstiffnessbecomesreduced. Experimentalconcrete
cube test specimens were made and will be subjected to
varying high temperatures 250ºC, 500ºC and 750ºC for a
period of two hours and then these were cooled down to room
temperatures before they were subjected to testing for its
physical, mechanical characteristics. The specimens were
cooled suddenly by quenched in water thus the high
temperature is being reduced to room temperature. Theeffect
of this sudden cooling of specimens will be compared and
subjected to high temperatures and cooled normally. The
differences in the mechanical characteristics and stiffness
properties are being experimented and the observation are to
be recorded. From these it would be interpreted the effect of
sudden cooling vs the other types were compared and
analyzed and will be reported as the results of this study
outcomes.
Key Words: Mechanical characteristics, microstructural
characteristics, stiffness properties
1. INTRODUCTION
1.1 General
Construction activityconstitutesnearly45%ofourcountry’s
GDP and one of the key factors contributing for the national
economy. Construction involves building up of roads,
bridges, tunnels, buildings, dams, and other related
infrastructure. In all these construction activity cement and
steel is the most predominant material that is being used to
the extent of 25% cost. Concrete is very widely used andone
of the significant construction materials since more than a
century .Concrete is a rigid material with high compressive
strength and low tensile strength with low resistance to
cracking. Most of the researches have been focused on
strength, stability and stiffness related topics. In addition to
that fibres can make concrete more homogeneous and can
improve the tensile response, compressivestrength,flexural
strength, particular the ductility. A reasonable accuracy and
theory have been developed for the making of concreteto its
fresh concrete properties in addition to its hardened
concrete properties for variousloadingconditions,including
dead load, live load, wind load, earthquake load etc.
However, in the recent few decades a group of researchers
were working on the fire performance of concrete subjected
to high temperatures in the order of about 1000ºC, which
takes place when a concrete structure is getting in to a fire.
The effect of high temperature on concrete completely
changes its physical, chemical and mechanical properties.
When concrete is subjected to high temperatures the basic
properties of the material getting altered and thusthe entire
design validity becomes invalid. Hence it was interesting for
many researchers to study on the different aspects of the
concrete subjected to high temperatures.
2. LITERATURE REVIEW
Adel A. El-Kurdi et.al., (2014) Limestone is normally less
expensive than Portland cement and can cost effectively
replace a part of the powder content in most concretes. For
this suppose, the scope of this work is to provide
experimental data on the residual mechanical and physical
properties of concrete containing limestone powder as a
replacement or additive of cement content by mass
subjected to heat. For this goal, five mixtures were casted,
one as a control mixture and the others were with 10 and
15% limestone fines as a replacement and additive of
cement content by mass. Reductions in both compressive
and flexural strength results along with the extent of weight
loss were examined. The mineralogy in unheated and
preheated concrete at 20, 200, 400 and 600ºCwasidentified
by means of thermo-gravimetric (TGA/DTG). Finally the
scanning electron microscope (SEM) was done to study the
microstructure of the hardened concrete. According to the
results, limestone fines had a considerable effect on the
properties of the concrete. The results indicated that, the
residual compressive and flexural strength of 10 and15 %
limestone fines as additive to cement content by mass are
generally higher than those of convention concrete. In other
words, elevated fire temperature is more damaging to the
traditional concrete compared with additive limestone
concrete. It has been establishedthatlimestonereplacement
causes reduce the compressive and flexural strength due to
the dilution effect. The presence of limestone finesgenerally
reduces the weight loss of heated concrete.TGA/DTGcurves
of unheated and preheated specimens can be used to
estimate the degree of temperature which may the concrete
exposed in accidental building fire as a practical part. Based
on SEM images, no obvious cracks in limestone concrete
whether as limestone replacement or additive up to 600ºC
and the CaCO3 clearly observed without decomposition.
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 05 Issue: 11 | Nov 2018 www.irjet.net p-ISSN: 2395-0072
© 2018, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 1182
Balakrishnaiah et.al., (2013) In their study they studied
the effect of elevated temperature on mechanical properties
and microstructure of silica flour concrete was investigated
and studied using ordinary Portlandcement(OPC)andsilica
flour (SF) in percentages varying from 0,5 to 20% with
water/binder ratio of 0.5. After 28 days of curing, the
specimens were exposed to 100ºC to 800ºc.
Franz-Josef et.al., (1996) They developed a macroscopic
material model for heated concrete. The experimental
determination of all the thermal dehydration function from
in-situ measurements the elastic modulus versus furnace
temperature rise was shown from experimental data
available from concrete.
Gyu-Yong Kim, Young-SunKim,Tae-Gyu Lee,Mechanical
properties of high strength concrete subjected to high
temperature by stressed test [September 2009]: The
present study is aimed to study the effect of elevated
temperatures ranging from 200 to 700 ºC on the material
mechanical properties of high-strength concrete of 40, 60
and 80 MPa grade. During the strength test, the specimens
are subjected to a 25% of ultimate compressive strength at
room temperature and sustained during heating, and when
the target temperature is reached, the specimens are loaded
to failure. The tests were conducted at varioustemperatures
(200 to 700 ºC) for concretes made with W/B ratios of 46%,
32% and 25%, respectively. The results show that the
relative values of compressive strength and elastic modulus
decrease with increasing compressive strength grade of
specimen.
H. G. Mundle, variation in strength of concrete subjected
to high temperature [Feb 2014]: The influence ofelevated
temperatures on mechanical propertiesof concreteisofvery
much important for fire resistance studies and also for
understanding the behavior of containment vessels,
chimneys, nuclear reactor pressure vessels during service
and ultimate conditions structures like storage tanks for
crude oil, hot water, coal gasification, liquefaction vessels
used in petrochemical industries, foundation for blast
furnace and coke industries, furnace walls industrial
chimney, air craft runway etc., will be subjected to elevated
temperatures. So that the variation of compressivestrength,
performance are some of the important parameters to be
investigated when concrete structures are subjected to
temperatures.
Ke-cheng He et.al., (2016) In order to investigate spalling
and the compressive performanceofthe concretetypesafter
exposure to high temperatures, four concrete mixes were
prepared, including normal concrete (NC), lightweight
aggregate concrete(LWAC),modificationmaterial Imodified
lightweight aggregate concrete (PLWAC), and modification
material II modified lightweight aggregate concrete
(GLWAC). After mixing, concrete types were cast into
100mm × 100mm× 300mmprismmould.After de-moulding
concrete specimens were cured in a standardcuringroom at
a temperature of 20 ± 2ºC and relative humidity above 95%
for 28 days. Before the exposure to high temperatures, the
extra water on the surface of the specimens was wiped off
with a damp cloth. Before heating, the specimens in
saturated-surface-dry condition were weighed at room
temperature. Then, the specimens were placed in an electric
furnace under unstressed condition and were heated to
200ºC, 400ºC, 600ºC, 800ºC, 1000ºC, and 1200ºC,
respectively, with an increasing rate of 10 C/min. The
elevation of temperature was controlled by a programming
instrument with precision of 10ºC. When the target
temperatures were achieved, the temperatures were
maintained as constant for 3 h to allow the specimens to
reach a thermal steady state. Then, the heated specimens
were cooled down slowly to room temperature in the
furnace. It can be observed that no Spalling occured for the
concretespecimenswhenthetemperaturewasbelow400ºC.
When the temperature increased to approximately 450ºC,
Spalling occurred for the concrete specimens to different
extents. After 1200ºC,thePLWACandtheGLWACspecimens
still had 26% and 38% of the compressive strengthretained,
respectively, exhibiting superior resistance to high
temperature.
R V Balendran, et.al., (2013) A great deal of research has
been conducted on the fire resistancepropertiesofconcrete.
With the advent of use of HSC in 1970's, the researchers are
trying to establish the body of knowledge concerning
different aspects, for example, differences with normal
strength concrete, effects of various ingredients on the
overall performance of High Strength Concrete etc. Such
knowledge established so far is considerable but when it
comes to the fire properties of HSC it becomes scarce,
showing this area is still under researched. It has been
observed that HSC has certain shortcomings in the form of
increased brittleness and decreased fire resistance. High
strength concrete (HSC) becomes more brittle with the
increase in strength and silica fume content. The strength of
HPC degenerated more sharply than the conventional
concrete with the increase of exposed temperature but it
was found that HPC had higher residual strength. With low
water/cementitious material ratios and addition of silica
fume, HSC becomes denser and it is more difficult for the
vapour to escape in the case of fire. Therefore, the risk of
spalling is increased for HSC. This paper forms the part of
research project undertaken to establish and evaluate fire
properties of HSC and is specifically relatedtoseek theeffect
of 'Cooling Method', if any, at two curing ages tofurtheralign
and refine the research methodology. The paper illustrates
an investigation undertaken to demonstrate the effect of
quick and slow cooling on residual compressive strengths of
various high strength concrete grades (60, 90, 110, 130
MPA) cured for 28 days and 180 days and heated to the
temperatures of 200°C and 400°C. It was found that cooling
method has a significant effect on the residual compressive
strength. The strength loss Pattern produced by quick
cooling at 200°C and 400°C is almost similar for all the
concrete grades tested. It was also found true for slow
cooling. However the strength loss was found to be higher at
400°C than at 200°C under both cooling conditions. The
specimens lost the strength in the range of 30-45% of the
original when quick cooled in water and 2-20% when slow
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 05 Issue: 11 | Nov 2018 www.irjet.net p-ISSN: 2395-0072
© 2018, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 1183
cooled in air. In addition, specimens cured for 180 days
exhibited more loss in strength than those curedfora period
of 28days, under both cooling conditions.Itisconcludedthat
the critical condition may occurs when a concrete cured for
an age of 180 days or more is subjected to an elevated
temperature of 400°C and quick cooled later, causing a loss
of 40-45% of its original compressive strength.
R. Sri Ravindrarajahet.al.,(2015)High-strengthconcreteis
a material often used in the construction of high rise
buildings. In the case of unexpected fire, the building
concrete elements such as columns, slab and walls will be
subjected to extreme temperatures. In order to assess the
performance of high-rise reinforced concrete members it is
important to understand the changes in the concrete
properties due to extreme temperature exposure. Since the
high-strengthconcreteproducedmaycontainvariousbinder
materials in addition to cement, it is also becoming
necessary to investigate the influence of the binder material
type on the concrete properties under elevatedtemperature
exposure. This paper summarizes and discusses the
degradation of the strengths and stiffness of high-strength
concrete in relation to the binder material type. The results
showed that the binder material type has a significant
influence on the performance of high-strength concrete
particularly at temperatures below 800ºC. The influence of
the binder material type is significantly decreased at
temperature of 1000ºC. The strengths and stiffness of high-
strength concrete are reduced with the increase in
temperature without any threshold temperature level. The
strengths are susceptible to the elevated temperatures
compared to stiffness of concrete. High-strength concrete
containing silica fume seems tobe moresensitivetoelevated
temperature.
3. PROPERTIES AND MATERIAL USED
3.1 Cement
IS-8112, 43 Grade OPC was used in this work with specific
gravity of 3.15 and standard consistency 26%.
3.2 Fine aggregate
Sand used in his work confirming to Zone-II, with fineness
modulus of 2.81 and specific gravity as 2.63.
3.3 Coarse aggregate
Coarse aggregate consisting of crushed granite (angular),
conforming to IS 383-1970 was used. The specific gravity of
coarse aggregate was 2.84.
3.4 Mineral Admixture
Table 3.1-Properties of silica fume
3.5 Fly Ash
Class C fly ash produced from lignite coals was used. The fly
ash is rich in Silicon and low in Calcium Oxide content.
3.6Chemical Admixture
Conplast SP 430 , Ceraplast 300 ,Naphthalene sulphonate
based superplasticizer have been used to improve
workability and strength of concrete.
3.6.1Ceraplast 300
Supply Form : Liquid
Specific Gravity : 1.2
Color : Brown
Chloride content : Nil
Recommended Dosage by :0.4% to 1% by
weight of cement.
3.6.2 Conplast SP 430
Specific Gravity : 1.22 to 1.22
Chloride content : Nil
Air Entrainment :1%(approximately)
Compatibility :canbeusedwithall
types of cement
4. MIX DESIGN
Table 4.1 Mix Proportion
MATERIALS NSC HSC HPC
Cement(kg/m3) 477 500 522.5
Fine
aggregate(kg/m3)
701 640 638
Coarse
aggregate(kg/m3)
1078 1170 1166
Water(1/m3) 203 160 160
Fly ash(kg/m3) - 50 -
Silica fume(kg/m3) - - 27.5
Super
plasticizers(1/m3)
- 3.2 3.2
Parameters Specification Analysis
SiO2 Min 85.0% 89.2
Loss of ignition Max 3.0% 0.7
Carbon Max 6.0% 1.7
Specific surface Max 15% 21.4
Bulk density 500-700 Kg/m3 620
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 05 Issue: 11 | Nov 2018 www.irjet.net p-ISSN: 2395-0072
© 2018, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 1184
5. CONCLUSION
The study have examine heat generation in the concrete
which undergoes changeinphysical andchemical properties
when subjected to high temperatures. The respective
specimens in the furnace heated to 250C, 500C, 750C till
reaches the steady state and maintained for a period 2hours
in the respective temperatures. The weight loss must be
observed significantly more in NSC concrete at 250C
compared to others. This may be due to the loss of moisture
at these lower level temperature. The concrete mix design is
designed and the grade of concrete, mix proportion was
found out. Materials like chemical admixtures and mineral
admixtures were used to increase the compressive strength
of concrete by reducing theamountofwaterin watercement
ratio. The effect ofhightemperaturesonconcretecompletely
modifies its physical, chemical and mechanical
characteristics. The three types of concrete like high
performance concrete, high strength concrete and normal
concrete were designed and standardized in this study. The
temperature and its intensity, the distribution pattern,
sustaining duration, exposed duration, mode of cooling etc.,
were of important sub factors associated with the
temperatures. The mechanical properties of concretevizthe
strength, tensile, compressive and shearstrengthapartfrom
the Young’s modulus and other residual engineering
parameters were undergo reductions and these were
attempted for quantification through this research work.
Concrete is inherently fire resistant, virtually fire proof. The
fire resistance and thermal properties of concrete depends
on mineral constitutes of aggregates used.
REFERENCES
[1] Adel A. El-Kurdi, Ali Abdel-Hakam, Mohamed M. El-
Gohary (2014), ‘ Impact of Elevated Temperature on
Properties of Limestone Concrete’,International Journal
of Innovative Technology and Exploring Engineering
(IJITEE) , Volume-4 Issue-4.
[2] Balakrishnaiah D, Balaji K.V.G.D, Srinivasa Rao.P,(2013)
‘Study of mechanical properties of concrete at elevated
temperatures’, International Journal of Research in
Engineering and Technology (IJRET), Volume: 02
Issue:08.
[3] Ke-cheng He, Rong-xin Guo, Qian-minMa,FengYan,Zhi-
wei Lin, and Yan-Lin Sun (2016), ‘Experimental
Research on High Temperature Resistance of Modified
Lightweight Concrete after Exposure to Elevated
Temperatures,’ Advances in Materials Science and
Engineering, Volume 2016.
[4] Franz-Josef Ulm Oliver Coussy and Zdenek
P.BaxankEvaluated (1996), ‘The effect of thermal
damage and thermal de cohesion up on the stress state
and cracking at structural level’.
[5] Gyu-Yong Kim, Young-Sun Kim, Tae-Gyu Lee (2009),
‘Mechanical properties of high strength concrete
subjected to high temperature by stressed test’
Transaction of Nonferrous Metal Society of
China,Volume 19, Supplement 1.
[6] H. G. Mundle (2014), ‘Variation in strength of concrete
subjected to high temperature’, International Journal of
Research in Engineering & Technology’, Vol. 2, Issue 2.
[7] R. Sri Ravindrarajah, R. Lopez and H. Reslan (2015),
‘Effect of Variation of Elevated Temperature on
Compressive Strength of Metakaolin Concrete’,
Literature Study International Journal of Current
Engineering and Technology,Vol.5, No.8.
[8] R V Balendran, T Maqsood, A Nadeem[2013], ‘The fire
resistance properties of concrete’.

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IRJET- Experimental Study on Residual Characteristics of Concrete Subjected to Elevated Temperature

  • 1. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 05 Issue: 11 | Nov 2018 www.irjet.net p-ISSN: 2395-0072 © 2018, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 1181 EXPERIMENTAL STUDY ON RESIDUAL CHARACTERISTICS OF CONCRETE SUBJECTED TO ELEVATED TEMPERATURE Mr. V. Niranjan1, Mr. A. Sathya Deva 2 1Assistant professor , Department of Civil Engineering, RVS Technical Campus, Coimbatore-641402, India, 2PG student, Department of Civil Engineering, RVS Technical Campus, Coimbatore-641402, India ---------------------------------------------------------------------***---------------------------------------------------------------------- Abstract - The effect of high temperatures exposed on the concrete structural members is an important parameter tobe considered in the design. The residual characteristics of temperature damaged concrete structural elements, the strength and stiffness degradation are considered to be very important in the modern design. The effect of this high temperature alter the physical, mechanical and microstructural characteristics of concrete thus the residual strength andstiffnessbecomesreduced. Experimentalconcrete cube test specimens were made and will be subjected to varying high temperatures 250ºC, 500ºC and 750ºC for a period of two hours and then these were cooled down to room temperatures before they were subjected to testing for its physical, mechanical characteristics. The specimens were cooled suddenly by quenched in water thus the high temperature is being reduced to room temperature. Theeffect of this sudden cooling of specimens will be compared and subjected to high temperatures and cooled normally. The differences in the mechanical characteristics and stiffness properties are being experimented and the observation are to be recorded. From these it would be interpreted the effect of sudden cooling vs the other types were compared and analyzed and will be reported as the results of this study outcomes. Key Words: Mechanical characteristics, microstructural characteristics, stiffness properties 1. INTRODUCTION 1.1 General Construction activityconstitutesnearly45%ofourcountry’s GDP and one of the key factors contributing for the national economy. Construction involves building up of roads, bridges, tunnels, buildings, dams, and other related infrastructure. In all these construction activity cement and steel is the most predominant material that is being used to the extent of 25% cost. Concrete is very widely used andone of the significant construction materials since more than a century .Concrete is a rigid material with high compressive strength and low tensile strength with low resistance to cracking. Most of the researches have been focused on strength, stability and stiffness related topics. In addition to that fibres can make concrete more homogeneous and can improve the tensile response, compressivestrength,flexural strength, particular the ductility. A reasonable accuracy and theory have been developed for the making of concreteto its fresh concrete properties in addition to its hardened concrete properties for variousloadingconditions,including dead load, live load, wind load, earthquake load etc. However, in the recent few decades a group of researchers were working on the fire performance of concrete subjected to high temperatures in the order of about 1000ºC, which takes place when a concrete structure is getting in to a fire. The effect of high temperature on concrete completely changes its physical, chemical and mechanical properties. When concrete is subjected to high temperatures the basic properties of the material getting altered and thusthe entire design validity becomes invalid. Hence it was interesting for many researchers to study on the different aspects of the concrete subjected to high temperatures. 2. LITERATURE REVIEW Adel A. El-Kurdi et.al., (2014) Limestone is normally less expensive than Portland cement and can cost effectively replace a part of the powder content in most concretes. For this suppose, the scope of this work is to provide experimental data on the residual mechanical and physical properties of concrete containing limestone powder as a replacement or additive of cement content by mass subjected to heat. For this goal, five mixtures were casted, one as a control mixture and the others were with 10 and 15% limestone fines as a replacement and additive of cement content by mass. Reductions in both compressive and flexural strength results along with the extent of weight loss were examined. The mineralogy in unheated and preheated concrete at 20, 200, 400 and 600ºCwasidentified by means of thermo-gravimetric (TGA/DTG). Finally the scanning electron microscope (SEM) was done to study the microstructure of the hardened concrete. According to the results, limestone fines had a considerable effect on the properties of the concrete. The results indicated that, the residual compressive and flexural strength of 10 and15 % limestone fines as additive to cement content by mass are generally higher than those of convention concrete. In other words, elevated fire temperature is more damaging to the traditional concrete compared with additive limestone concrete. It has been establishedthatlimestonereplacement causes reduce the compressive and flexural strength due to the dilution effect. The presence of limestone finesgenerally reduces the weight loss of heated concrete.TGA/DTGcurves of unheated and preheated specimens can be used to estimate the degree of temperature which may the concrete exposed in accidental building fire as a practical part. Based on SEM images, no obvious cracks in limestone concrete whether as limestone replacement or additive up to 600ºC and the CaCO3 clearly observed without decomposition.
  • 2. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 05 Issue: 11 | Nov 2018 www.irjet.net p-ISSN: 2395-0072 © 2018, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 1182 Balakrishnaiah et.al., (2013) In their study they studied the effect of elevated temperature on mechanical properties and microstructure of silica flour concrete was investigated and studied using ordinary Portlandcement(OPC)andsilica flour (SF) in percentages varying from 0,5 to 20% with water/binder ratio of 0.5. After 28 days of curing, the specimens were exposed to 100ºC to 800ºc. Franz-Josef et.al., (1996) They developed a macroscopic material model for heated concrete. The experimental determination of all the thermal dehydration function from in-situ measurements the elastic modulus versus furnace temperature rise was shown from experimental data available from concrete. Gyu-Yong Kim, Young-SunKim,Tae-Gyu Lee,Mechanical properties of high strength concrete subjected to high temperature by stressed test [September 2009]: The present study is aimed to study the effect of elevated temperatures ranging from 200 to 700 ºC on the material mechanical properties of high-strength concrete of 40, 60 and 80 MPa grade. During the strength test, the specimens are subjected to a 25% of ultimate compressive strength at room temperature and sustained during heating, and when the target temperature is reached, the specimens are loaded to failure. The tests were conducted at varioustemperatures (200 to 700 ºC) for concretes made with W/B ratios of 46%, 32% and 25%, respectively. The results show that the relative values of compressive strength and elastic modulus decrease with increasing compressive strength grade of specimen. H. G. Mundle, variation in strength of concrete subjected to high temperature [Feb 2014]: The influence ofelevated temperatures on mechanical propertiesof concreteisofvery much important for fire resistance studies and also for understanding the behavior of containment vessels, chimneys, nuclear reactor pressure vessels during service and ultimate conditions structures like storage tanks for crude oil, hot water, coal gasification, liquefaction vessels used in petrochemical industries, foundation for blast furnace and coke industries, furnace walls industrial chimney, air craft runway etc., will be subjected to elevated temperatures. So that the variation of compressivestrength, performance are some of the important parameters to be investigated when concrete structures are subjected to temperatures. Ke-cheng He et.al., (2016) In order to investigate spalling and the compressive performanceofthe concretetypesafter exposure to high temperatures, four concrete mixes were prepared, including normal concrete (NC), lightweight aggregate concrete(LWAC),modificationmaterial Imodified lightweight aggregate concrete (PLWAC), and modification material II modified lightweight aggregate concrete (GLWAC). After mixing, concrete types were cast into 100mm × 100mm× 300mmprismmould.After de-moulding concrete specimens were cured in a standardcuringroom at a temperature of 20 ± 2ºC and relative humidity above 95% for 28 days. Before the exposure to high temperatures, the extra water on the surface of the specimens was wiped off with a damp cloth. Before heating, the specimens in saturated-surface-dry condition were weighed at room temperature. Then, the specimens were placed in an electric furnace under unstressed condition and were heated to 200ºC, 400ºC, 600ºC, 800ºC, 1000ºC, and 1200ºC, respectively, with an increasing rate of 10 C/min. The elevation of temperature was controlled by a programming instrument with precision of 10ºC. When the target temperatures were achieved, the temperatures were maintained as constant for 3 h to allow the specimens to reach a thermal steady state. Then, the heated specimens were cooled down slowly to room temperature in the furnace. It can be observed that no Spalling occured for the concretespecimenswhenthetemperaturewasbelow400ºC. When the temperature increased to approximately 450ºC, Spalling occurred for the concrete specimens to different extents. After 1200ºC,thePLWACandtheGLWACspecimens still had 26% and 38% of the compressive strengthretained, respectively, exhibiting superior resistance to high temperature. R V Balendran, et.al., (2013) A great deal of research has been conducted on the fire resistancepropertiesofconcrete. With the advent of use of HSC in 1970's, the researchers are trying to establish the body of knowledge concerning different aspects, for example, differences with normal strength concrete, effects of various ingredients on the overall performance of High Strength Concrete etc. Such knowledge established so far is considerable but when it comes to the fire properties of HSC it becomes scarce, showing this area is still under researched. It has been observed that HSC has certain shortcomings in the form of increased brittleness and decreased fire resistance. High strength concrete (HSC) becomes more brittle with the increase in strength and silica fume content. The strength of HPC degenerated more sharply than the conventional concrete with the increase of exposed temperature but it was found that HPC had higher residual strength. With low water/cementitious material ratios and addition of silica fume, HSC becomes denser and it is more difficult for the vapour to escape in the case of fire. Therefore, the risk of spalling is increased for HSC. This paper forms the part of research project undertaken to establish and evaluate fire properties of HSC and is specifically relatedtoseek theeffect of 'Cooling Method', if any, at two curing ages tofurtheralign and refine the research methodology. The paper illustrates an investigation undertaken to demonstrate the effect of quick and slow cooling on residual compressive strengths of various high strength concrete grades (60, 90, 110, 130 MPA) cured for 28 days and 180 days and heated to the temperatures of 200°C and 400°C. It was found that cooling method has a significant effect on the residual compressive strength. The strength loss Pattern produced by quick cooling at 200°C and 400°C is almost similar for all the concrete grades tested. It was also found true for slow cooling. However the strength loss was found to be higher at 400°C than at 200°C under both cooling conditions. The specimens lost the strength in the range of 30-45% of the original when quick cooled in water and 2-20% when slow
  • 3. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 05 Issue: 11 | Nov 2018 www.irjet.net p-ISSN: 2395-0072 © 2018, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 1183 cooled in air. In addition, specimens cured for 180 days exhibited more loss in strength than those curedfora period of 28days, under both cooling conditions.Itisconcludedthat the critical condition may occurs when a concrete cured for an age of 180 days or more is subjected to an elevated temperature of 400°C and quick cooled later, causing a loss of 40-45% of its original compressive strength. R. Sri Ravindrarajahet.al.,(2015)High-strengthconcreteis a material often used in the construction of high rise buildings. In the case of unexpected fire, the building concrete elements such as columns, slab and walls will be subjected to extreme temperatures. In order to assess the performance of high-rise reinforced concrete members it is important to understand the changes in the concrete properties due to extreme temperature exposure. Since the high-strengthconcreteproducedmaycontainvariousbinder materials in addition to cement, it is also becoming necessary to investigate the influence of the binder material type on the concrete properties under elevatedtemperature exposure. This paper summarizes and discusses the degradation of the strengths and stiffness of high-strength concrete in relation to the binder material type. The results showed that the binder material type has a significant influence on the performance of high-strength concrete particularly at temperatures below 800ºC. The influence of the binder material type is significantly decreased at temperature of 1000ºC. The strengths and stiffness of high- strength concrete are reduced with the increase in temperature without any threshold temperature level. The strengths are susceptible to the elevated temperatures compared to stiffness of concrete. High-strength concrete containing silica fume seems tobe moresensitivetoelevated temperature. 3. PROPERTIES AND MATERIAL USED 3.1 Cement IS-8112, 43 Grade OPC was used in this work with specific gravity of 3.15 and standard consistency 26%. 3.2 Fine aggregate Sand used in his work confirming to Zone-II, with fineness modulus of 2.81 and specific gravity as 2.63. 3.3 Coarse aggregate Coarse aggregate consisting of crushed granite (angular), conforming to IS 383-1970 was used. The specific gravity of coarse aggregate was 2.84. 3.4 Mineral Admixture Table 3.1-Properties of silica fume 3.5 Fly Ash Class C fly ash produced from lignite coals was used. The fly ash is rich in Silicon and low in Calcium Oxide content. 3.6Chemical Admixture Conplast SP 430 , Ceraplast 300 ,Naphthalene sulphonate based superplasticizer have been used to improve workability and strength of concrete. 3.6.1Ceraplast 300 Supply Form : Liquid Specific Gravity : 1.2 Color : Brown Chloride content : Nil Recommended Dosage by :0.4% to 1% by weight of cement. 3.6.2 Conplast SP 430 Specific Gravity : 1.22 to 1.22 Chloride content : Nil Air Entrainment :1%(approximately) Compatibility :canbeusedwithall types of cement 4. MIX DESIGN Table 4.1 Mix Proportion MATERIALS NSC HSC HPC Cement(kg/m3) 477 500 522.5 Fine aggregate(kg/m3) 701 640 638 Coarse aggregate(kg/m3) 1078 1170 1166 Water(1/m3) 203 160 160 Fly ash(kg/m3) - 50 - Silica fume(kg/m3) - - 27.5 Super plasticizers(1/m3) - 3.2 3.2 Parameters Specification Analysis SiO2 Min 85.0% 89.2 Loss of ignition Max 3.0% 0.7 Carbon Max 6.0% 1.7 Specific surface Max 15% 21.4 Bulk density 500-700 Kg/m3 620
  • 4. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 05 Issue: 11 | Nov 2018 www.irjet.net p-ISSN: 2395-0072 © 2018, IRJET | Impact Factor value: 7.211 | ISO 9001:2008 Certified Journal | Page 1184 5. CONCLUSION The study have examine heat generation in the concrete which undergoes changeinphysical andchemical properties when subjected to high temperatures. The respective specimens in the furnace heated to 250C, 500C, 750C till reaches the steady state and maintained for a period 2hours in the respective temperatures. The weight loss must be observed significantly more in NSC concrete at 250C compared to others. This may be due to the loss of moisture at these lower level temperature. The concrete mix design is designed and the grade of concrete, mix proportion was found out. Materials like chemical admixtures and mineral admixtures were used to increase the compressive strength of concrete by reducing theamountofwaterin watercement ratio. The effect ofhightemperaturesonconcretecompletely modifies its physical, chemical and mechanical characteristics. The three types of concrete like high performance concrete, high strength concrete and normal concrete were designed and standardized in this study. The temperature and its intensity, the distribution pattern, sustaining duration, exposed duration, mode of cooling etc., were of important sub factors associated with the temperatures. The mechanical properties of concretevizthe strength, tensile, compressive and shearstrengthapartfrom the Young’s modulus and other residual engineering parameters were undergo reductions and these were attempted for quantification through this research work. Concrete is inherently fire resistant, virtually fire proof. The fire resistance and thermal properties of concrete depends on mineral constitutes of aggregates used. REFERENCES [1] Adel A. El-Kurdi, Ali Abdel-Hakam, Mohamed M. El- Gohary (2014), ‘ Impact of Elevated Temperature on Properties of Limestone Concrete’,International Journal of Innovative Technology and Exploring Engineering (IJITEE) , Volume-4 Issue-4. [2] Balakrishnaiah D, Balaji K.V.G.D, Srinivasa Rao.P,(2013) ‘Study of mechanical properties of concrete at elevated temperatures’, International Journal of Research in Engineering and Technology (IJRET), Volume: 02 Issue:08. [3] Ke-cheng He, Rong-xin Guo, Qian-minMa,FengYan,Zhi- wei Lin, and Yan-Lin Sun (2016), ‘Experimental Research on High Temperature Resistance of Modified Lightweight Concrete after Exposure to Elevated Temperatures,’ Advances in Materials Science and Engineering, Volume 2016. [4] Franz-Josef Ulm Oliver Coussy and Zdenek P.BaxankEvaluated (1996), ‘The effect of thermal damage and thermal de cohesion up on the stress state and cracking at structural level’. [5] Gyu-Yong Kim, Young-Sun Kim, Tae-Gyu Lee (2009), ‘Mechanical properties of high strength concrete subjected to high temperature by stressed test’ Transaction of Nonferrous Metal Society of China,Volume 19, Supplement 1. [6] H. G. Mundle (2014), ‘Variation in strength of concrete subjected to high temperature’, International Journal of Research in Engineering & Technology’, Vol. 2, Issue 2. [7] R. Sri Ravindrarajah, R. Lopez and H. Reslan (2015), ‘Effect of Variation of Elevated Temperature on Compressive Strength of Metakaolin Concrete’, Literature Study International Journal of Current Engineering and Technology,Vol.5, No.8. [8] R V Balendran, T Maqsood, A Nadeem[2013], ‘The fire resistance properties of concrete’.