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Central Institute of Plastics
Engineering and Technology, INDIA
1
PIPE EXTRUSION
Central Institute of Plastics
Engineering and Technology, INDIA
2
Pipe plant elements
• Extruder
• Die
• Sizing device
• Cooling bath
• Puller
• Cutter or Winder
Central Institute of Plastics
Engineering and Technology, INDIA
3
Pipe Extrusion Plant
Central Institute of Plastics
Engineering and Technology, INDIA
4
MATERIALS
• PVC
• HDPE
• PS
• ABS
Central Institute of Plastics
Engineering and Technology, INDIA
5
PVC Pipes are available in
two forms:
• Rigid PVC or Unplasticised PVC
• Soft PVC or Plasticised PVC
Central Institute of Plastics
Engineering and Technology, INDIA
6
PVC can’t be processed
alone. It needs to be
compounded by adding
different ingredients.
Central Institute of Plastics
Engineering and Technology, INDIA
7
Ingredients added in PVC
compounding
• Plasticizers
• Fillers
• Heat stabilizers
• Lubricants
• Processing aids
• Flame retardants
• Colorants
• Impact modifiers
Central Institute of Plastics
Engineering and Technology, INDIA
8
Plasticisers are used to make
the resin softer, reduce the
viscosity and thus make
processing of PVC easier. Di-
allyl phthalate (DAP) and
di-2-ethyl hexyl phthalate
(DOP) are examples of
common PVC plasticisers.
Central Institute of Plastics
Engineering and Technology, INDIA
9
Heat stabilizers are required to
prevent the thermal degradation of
PVC at the processing temperatures.
The degradation involves resin
discoloration and evolution of HCl. In
the past lead stabilisers have been
used (viz. lead stearates). Owing to
toxicity of Pb, today the most
common stabilisers are based on tin,
viz. di-butyl tin maleate.
Central Institute of Plastics
Engineering and Technology, INDIA
10
RPVC-pipe formulation
PVC Resin (K = 67.68) 100 parts
Tin stabiliser 0.4
Calcium stearate 0.8
Wax 1.2
TiO2 (colorant) 1.0
CaCO3 20 to 40
Central Institute of Plastics
Engineering and Technology, INDIA
11
Lubricants are used to reduce
friction during processing that may
lead to degradation. Two types of
lubricants are used: external and
internal. The former (viz. calcium
stearate and wax) is used to reduce
friction between metal surfaces and
the polymer, the latter (viz. stearic
acid) the friction arising out of
polymer chain slippage.
Central Institute of Plastics
Engineering and Technology, INDIA
12
Fillers and reinforcements are added
for cost reduction (fillers) and
improvement of the mechanical
properties (reinforcements). Both
increase rigidity, hardness, density and
fire retardancy. A typical filler is
calcium carbonate; typical
reinforcements are chopped glass fibre
and mica flakes, while such additives as
clay, talc, and silica are in-between.
Central Institute of Plastics
Engineering and Technology, INDIA
13
Flame retarding agents are
needed for plasticised PVC.
Chlorinated paraffin oil or
wax, oxides of Sb, Mo, P,
or B, as well as aluminium
hydroxide have been used.
Central Institute of Plastics
Engineering and Technology, INDIA
14
Processing aids are added
to rigid PVC to improve
flow through the barrel
and die. To this group of
additives belong polymers
and copolymers miscible
with PVC, e.g., PMMA,
ABS, SAN.
Central Institute of Plastics
Engineering and Technology, INDIA
15
Impact modifiers are added to
improve the impact strength.
Impact modifiers are composed
of at least two parts: one that
ascertains miscibility with PVC,
the other elastomeric in nature
that provides the toughening
effect. Examples of these
include MBS, EVAc, CSR, and
NBR.
Central Institute of Plastics
Engineering and Technology, INDIA
16
PVC compounding is usually
carried out in two stages:
• Dry-blending PVC resin with additives in
an intensive dry mixer, equipped with a
high speed impeller.
• Melt blending in a suitable compounder,
e.g., single-, twin-, or multi-screw
extruders, single or twin shaft
compounders, Kinetic energy mixer, etc.
Central Institute of Plastics
Engineering and Technology, INDIA
17
Sizing equipments
The extrudate emerging from the
pipe die usually shows variation of
diameter, caused by variability of
the rheological melt properties.
Thus, the pipe has to be
calibrated or “sized” while hot.
Central Institute of Plastics
Engineering and Technology, INDIA
18
Four methods are in use for
pipe sizing
• Vacuum trough
• Sizing sleeve
• Extended mandrel
• Sizing plates
Central Institute of Plastics
Engineering and Technology, INDIA
19
Vacuum trough
The pipe, coming out of the die passes
through a long closed trough filled with
cooling water. Inside the trough, the
pipe passes through fixed metal rings
of predetermined size. Since, vacuum
is drawn over the water, the internal
pressure in the soft pipe causes it to
expand against the rings. Thus the
pipe gets the outside diameter.
Central Institute of Plastics
Engineering and Technology, INDIA
20
Sizing sleeve
This method fixes the outside pipe
diameter as it hardens by contact with
a water-cooled metal sleeve. The
contact is achieved by air pressure
inside the pipe or by drawing vacuum
through the perforated inside surface
of the sleeve. The method produces
glossy, smooth, closely controlled outer
surface.
Central Institute of Plastics
Engineering and Technology, INDIA
21
Extended mandrel
This method uses a water-cooled
metal mandrel that extends
beyond the die. Shrinkage of pipe
as it cools helps to keep a light
contact with the mandrel. Thus
this method provides additional
internal cooling and internal
support.
Central Institute of Plastics
Engineering and Technology, INDIA
22
Sizing plates
This method involves pulling the
pipe through a series of brass or
stainless steel plates. Air pressure
in the pipe forces it against the
plates, thus controlling the outside
pipe diameter. This method is
mainly used for smaller diameter
pipes.
Central Institute of Plastics
Engineering and Technology, INDIA
23
Cooling water troughs
• During the sizing also the pipe gets
cooled.
• Cooling is done by spraying water over
the surface of the pipe.
• The length of the cooling troughs for PE
is longer than for PVC.
Central Institute of Plastics
Engineering and Technology, INDIA
24
Pulling Machines
• Pulling machines maintain uniform pipe
size.
• Pullers are either the caterpillar type or
the gripping wheel type.
• The puller speed is controlled by
electrical, electronic or magnetic speed
variators.
Central Institute of Plastics
Engineering and Technology, INDIA
25
Controls
• They provide automatic measurements and
control of pipe size.
• In one system the capacitance of the pipe is
measured and is related to the thickness.
• The sensing head moves around the pipe,
showing when the pipe is out of round and
when it is generally too heavy or too light.
• All these systems can be made to feed back
to control the puller or the extruder drive.
Central Institute of Plastics
Engineering and Technology, INDIA
26
Cutting devices
• Circular saw cutters, with blades specially
designed for cutting plastics, are used to cut
the pipe into specified lengths.
• Automatic cutting devices are also used.
They travel with the pipe to cut, then after
cutting go back to pick up the next pipe
length.
• Larger sizes are sawed to length.
Central Institute of Plastics
Engineering and Technology, INDIA
27
Coiling devices
• Smaller diameter Soft PVC and HDPE
pipes are coiled on a large centre-wood
reel.
• In simple methods pipe is coiled by a
band rank.

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e._pipe_extrusion..ppt and pipe production

  • 1. Central Institute of Plastics Engineering and Technology, INDIA 1 PIPE EXTRUSION
  • 2. Central Institute of Plastics Engineering and Technology, INDIA 2 Pipe plant elements • Extruder • Die • Sizing device • Cooling bath • Puller • Cutter or Winder
  • 3. Central Institute of Plastics Engineering and Technology, INDIA 3 Pipe Extrusion Plant
  • 4. Central Institute of Plastics Engineering and Technology, INDIA 4 MATERIALS • PVC • HDPE • PS • ABS
  • 5. Central Institute of Plastics Engineering and Technology, INDIA 5 PVC Pipes are available in two forms: • Rigid PVC or Unplasticised PVC • Soft PVC or Plasticised PVC
  • 6. Central Institute of Plastics Engineering and Technology, INDIA 6 PVC can’t be processed alone. It needs to be compounded by adding different ingredients.
  • 7. Central Institute of Plastics Engineering and Technology, INDIA 7 Ingredients added in PVC compounding • Plasticizers • Fillers • Heat stabilizers • Lubricants • Processing aids • Flame retardants • Colorants • Impact modifiers
  • 8. Central Institute of Plastics Engineering and Technology, INDIA 8 Plasticisers are used to make the resin softer, reduce the viscosity and thus make processing of PVC easier. Di- allyl phthalate (DAP) and di-2-ethyl hexyl phthalate (DOP) are examples of common PVC plasticisers.
  • 9. Central Institute of Plastics Engineering and Technology, INDIA 9 Heat stabilizers are required to prevent the thermal degradation of PVC at the processing temperatures. The degradation involves resin discoloration and evolution of HCl. In the past lead stabilisers have been used (viz. lead stearates). Owing to toxicity of Pb, today the most common stabilisers are based on tin, viz. di-butyl tin maleate.
  • 10. Central Institute of Plastics Engineering and Technology, INDIA 10 RPVC-pipe formulation PVC Resin (K = 67.68) 100 parts Tin stabiliser 0.4 Calcium stearate 0.8 Wax 1.2 TiO2 (colorant) 1.0 CaCO3 20 to 40
  • 11. Central Institute of Plastics Engineering and Technology, INDIA 11 Lubricants are used to reduce friction during processing that may lead to degradation. Two types of lubricants are used: external and internal. The former (viz. calcium stearate and wax) is used to reduce friction between metal surfaces and the polymer, the latter (viz. stearic acid) the friction arising out of polymer chain slippage.
  • 12. Central Institute of Plastics Engineering and Technology, INDIA 12 Fillers and reinforcements are added for cost reduction (fillers) and improvement of the mechanical properties (reinforcements). Both increase rigidity, hardness, density and fire retardancy. A typical filler is calcium carbonate; typical reinforcements are chopped glass fibre and mica flakes, while such additives as clay, talc, and silica are in-between.
  • 13. Central Institute of Plastics Engineering and Technology, INDIA 13 Flame retarding agents are needed for plasticised PVC. Chlorinated paraffin oil or wax, oxides of Sb, Mo, P, or B, as well as aluminium hydroxide have been used.
  • 14. Central Institute of Plastics Engineering and Technology, INDIA 14 Processing aids are added to rigid PVC to improve flow through the barrel and die. To this group of additives belong polymers and copolymers miscible with PVC, e.g., PMMA, ABS, SAN.
  • 15. Central Institute of Plastics Engineering and Technology, INDIA 15 Impact modifiers are added to improve the impact strength. Impact modifiers are composed of at least two parts: one that ascertains miscibility with PVC, the other elastomeric in nature that provides the toughening effect. Examples of these include MBS, EVAc, CSR, and NBR.
  • 16. Central Institute of Plastics Engineering and Technology, INDIA 16 PVC compounding is usually carried out in two stages: • Dry-blending PVC resin with additives in an intensive dry mixer, equipped with a high speed impeller. • Melt blending in a suitable compounder, e.g., single-, twin-, or multi-screw extruders, single or twin shaft compounders, Kinetic energy mixer, etc.
  • 17. Central Institute of Plastics Engineering and Technology, INDIA 17 Sizing equipments The extrudate emerging from the pipe die usually shows variation of diameter, caused by variability of the rheological melt properties. Thus, the pipe has to be calibrated or “sized” while hot.
  • 18. Central Institute of Plastics Engineering and Technology, INDIA 18 Four methods are in use for pipe sizing • Vacuum trough • Sizing sleeve • Extended mandrel • Sizing plates
  • 19. Central Institute of Plastics Engineering and Technology, INDIA 19 Vacuum trough The pipe, coming out of the die passes through a long closed trough filled with cooling water. Inside the trough, the pipe passes through fixed metal rings of predetermined size. Since, vacuum is drawn over the water, the internal pressure in the soft pipe causes it to expand against the rings. Thus the pipe gets the outside diameter.
  • 20. Central Institute of Plastics Engineering and Technology, INDIA 20 Sizing sleeve This method fixes the outside pipe diameter as it hardens by contact with a water-cooled metal sleeve. The contact is achieved by air pressure inside the pipe or by drawing vacuum through the perforated inside surface of the sleeve. The method produces glossy, smooth, closely controlled outer surface.
  • 21. Central Institute of Plastics Engineering and Technology, INDIA 21 Extended mandrel This method uses a water-cooled metal mandrel that extends beyond the die. Shrinkage of pipe as it cools helps to keep a light contact with the mandrel. Thus this method provides additional internal cooling and internal support.
  • 22. Central Institute of Plastics Engineering and Technology, INDIA 22 Sizing plates This method involves pulling the pipe through a series of brass or stainless steel plates. Air pressure in the pipe forces it against the plates, thus controlling the outside pipe diameter. This method is mainly used for smaller diameter pipes.
  • 23. Central Institute of Plastics Engineering and Technology, INDIA 23 Cooling water troughs • During the sizing also the pipe gets cooled. • Cooling is done by spraying water over the surface of the pipe. • The length of the cooling troughs for PE is longer than for PVC.
  • 24. Central Institute of Plastics Engineering and Technology, INDIA 24 Pulling Machines • Pulling machines maintain uniform pipe size. • Pullers are either the caterpillar type or the gripping wheel type. • The puller speed is controlled by electrical, electronic or magnetic speed variators.
  • 25. Central Institute of Plastics Engineering and Technology, INDIA 25 Controls • They provide automatic measurements and control of pipe size. • In one system the capacitance of the pipe is measured and is related to the thickness. • The sensing head moves around the pipe, showing when the pipe is out of round and when it is generally too heavy or too light. • All these systems can be made to feed back to control the puller or the extruder drive.
  • 26. Central Institute of Plastics Engineering and Technology, INDIA 26 Cutting devices • Circular saw cutters, with blades specially designed for cutting plastics, are used to cut the pipe into specified lengths. • Automatic cutting devices are also used. They travel with the pipe to cut, then after cutting go back to pick up the next pipe length. • Larger sizes are sawed to length.
  • 27. Central Institute of Plastics Engineering and Technology, INDIA 27 Coiling devices • Smaller diameter Soft PVC and HDPE pipes are coiled on a large centre-wood reel. • In simple methods pipe is coiled by a band rank.