White Paper Selection Parameters for Vacuum Oil Purifiers

1. Selection Parameters for Vacuum Oil
Purifiers
WHITE PAPER
© 2017 AGC Refining & Filtration LLC

2. AGC REFINING & FILTRATION
SELECTION PARAMETERS FOR VACUUM OIL PURIFIERS 2
Contents
Introduction 3
Types of Contaminants 3
Design Flow Rate of the Purifier 4
Rate of Removal of Contaminants 5
Contaminant Removal Efficiency (Efficiency of Purification) 5
Cost of a Purifier 9
Trade-offs 10
Drying out of Transformer Insulation 12
References 13
Appendix 1: Sample Systems 14

3. AGC REFINING & FILTRATION
SELECTION PARAMETERS FOR VACUUM OIL PURIFIERS 3
Introduction
The proper selection of a vacuum purifier for oil—whether it is for transformer oil, lubrication oil, hydraulic
fluid, or thermal oil—involves the consideration of many factors. Yet strangely enough, most buyers of oil
purifiers spend relatively little time on the selection process. Since these systems usually involve high
capital cost, it is important to understand the different types and what capabilities and limitations they
possess. The only objective of purification is re-use; and with proper procedures, oil can last indefinitely.
What then are the parameters to consider when purchasing a vacuum oil purifier?
 Type of contaminants to be removed by the purifier
 Flow rate of the purifier
 The efficiency or rate of removal of contaminants by the purifier
 The cost of the purifier
 Trade-offs
Types of Contaminants
The most common contaminants that must be removed from transformer oil include:
 moisture (from condensation or cooling water leakage, etc.),
 gases (from leaking compressor gas seals, etc.),
 solids (from dust, corrosion, bacterial growth, etc.), and
 acidity (from hydrolysis, etc.).
Oil purification and re-use has proven to make good economic sense. Cost of new oil is rising as is the
expense of disposing of contaminated oil. Before considering the economics of oil purification, you must
know what the contaminants are that must be removed before the oil can be re-used. To find out what the
predominant contaminants are, take several samples over a period of time and have them analyzed.
Typical analyses performed on the samples are:
 particle size distribution,
 moisture,
 dissolved gases,
 acidity,
 viscosity, and
 flash point.
Since the rates of contamination and the individual quantities often vary widely, this data is necessary for
the manufacturer to design of an effective purifier. Standard “off-the-shelf” systems often cannot provide
satisfactory results.

4. AGC REFINING & FILTRATION
SELECTION PARAMETERS FOR VACUUM OIL PURIFIERS 4
Design Flow Rate of the Purifier
Determining the capacity or flow rate of an oil purifier depends on:
 the rate at which the contaminants enter into the main oil reservoir and
 the required efficiency (i.e. how fast does the purifier need to purify the oil to stay ahead of the
incoming contamination).
Figure 1: General Schematic of the Oil Purification Process
Contamination of a volume of oil, whether inside a transformer or in a compressor lube oil reservoir,
occurs at varying rates. Whether qualitatively (moisture, solids, or gases) or quantitatively (in ppm or
percent), it is important to get some idea of what the rate of contamination is, before determining the
capacity of the purifier. In other words, a 1000-gallon reservoir of dirty oil does not necessarily need a
purifier with a 1,000 gallon per hour flow capacity if the rate of contamination entry is small and relatively
constant.
The reason for this is that a purifier with a capacity of 1,000 gallons per hour does not necessarily mean
that this 1,000 gallon volume of oil is clean after going through the purifier for an hour. This is because a
purifier has a certain fixed efficiency of purification. This means that during each pass of 1,000 gallons per
hour through the purifier, only a certain amount of contaminants is removed. This is the so-called
“multiple-pass” purification process.
In the case of a vacuum purifier, the amount of contaminants removed depends on the depth of vacuum
and the amount of heat applied to the oil during its passage through the purifier, as well as the initial
concentrations, types and partial pressures of those contaminants (more on removal efficiency later).
However, while most vacuum purifiers are designed for partial but progressive removal of contaminants

5. AGC REFINING & FILTRATION
SELECTION PARAMETERS FOR VACUUM OIL PURIFIERS 5
during several passes through the equipment, a purifier can be designed to remove almost all known
contaminants in a single pass through the purification system. This is the so-called “single-pass”
purification system.
Rate of Removal of Contaminants
The removal efficiency of a purifier is defined as the amount of contaminants removed during each pass
through the system.
The length of time it takes to purify the entire volume of oil in a reservoir is therefore a function of the
removal efficiency of the purifier. The higher the efficiency, the faster the contaminants are removed.
If the oil reservoir holds 1,000 gallons and the purifier capacity is 200 gallons per hour, the reservoir will
be turned over in 1,000 ÷ 200 = 5 hours.
This does not mean that all contaminants have been removed.
It just means that after 5 hours, 1,000 gallons has been pumped through the purifier and contaminants
have been partially removed.
Most purifiers are designed for partial removal of contaminants during each pass through the purifier. In
the case of moisture, if the initial total water (free, emulsified & dissolved) concentration is 200 wppm and
each pass through the purifier removes 50 wppm, if should take four passes through the purifier to
remove all the moisture. But, what comes out of the purifier (50 ppm moisture) is returned to the reservoir
where the oil still contains 200 wppm of moisture.
Thus, during each pass that removes 50 ppm of moisture, the oil is returned to a reservoir of oil that has
an ever decreasing moisture concentration. The purification system will eventually purify the entire
volume of the reservoir, if it operates continuously and contaminant removal stays ahead of the incoming
contamination rate. Most purifiers are designed for continuous “kidney-loop” operation. (See Figure 1
above)
This brings us to the parameter of purifier efficiency.
Contaminant Removal Efficiency (Efficiency of
Purification)
As stated earlier the efficiency of purification or the degree to which contaminants are removed during
each pass through the purifier depends on:
 the temperature to which the oil is raised during the each pass through the purifier and

6. AGC REFINING & FILTRATION
SELECTION PARAMETERS FOR VACUUM OIL PURIFIERS 6
 the depth of the vacuum in the purifier’s vacuum vessel.
Temperature
At the design flow rate, the purification efficiency depends on the amount of heat transferred to the
contaminated oil during each pass through the purifier. The heat must be supplied by special low watt-
density in-line heaters that prevent localized hot spots that could carbonize the oil, foul the elements with
deposits and reduce the heating capacity.
For instance, if the temperature of the contaminated oil in the tank is 70° F and assuming that at the
design flow the heat supplied by the heaters during each pass is 70° F, then during each pass through
the purifier, the oil passing through the heaters increases in temperature from 70° F to 140° F. This is the
normally close to the temperature for the removal of contaminants. The oil is then returned to the tank,
which is still at 70° F. This continues during several passes, until the temperature in the entire tank is at
140° F.
Vacuum
The vacuum system is the heart of the vacuum purification process.
In addition to applied heat, it is the second most critical parameter in the purification of oil and the one
most often neglected by buyers.
The reason for the importance of vacuum is: the degree to which contaminants are removed during each
pass through the purifier is directly related to the vacuum applied to the oil during the purification process.
(See Figure 2)
Furthermore, the depth and reliability of the vacuum system is directly related to the capacity and quality
of the vacuum pump. Of course the quality and type of the vacuum pump is directly related to its cost,
which is the reason many manufacturers substitute less expensive, lower quality and less reliable vacuum
pumps. (See the section on trade-offs)
Since most purchases are price-driven, buyers seldom bother to find out the difference in quality of the
vacuum pumps presented in competitor’s equipment.
Mass Transfer
Another reason why vacuum and temperature are the most important parameters for a purification system
is that both work together to create the mass transfer conditions necessary to vaporize and remove the
contaminants such as moisture and dissolved gases.

7. AGC REFINING & FILTRATION
SELECTION PARAMETERS FOR VACUUM OIL PURIFIERS 7
Figure 2: Effect of Vacuum on Purifier Performance
The process of vacuum purification is based on the principle of vacuum distillation, a common chemical
engineering process used to split crude oil into fractions.
In a vessel that is placed under vacuum, the oil is dispersed in a thin film, over a large surface area (such
as distillation trays or Rashig Rings™). By applying both heat and vacuum, the contaminants are
vaporized from this thin film of oil and removed by vacuum, at a rate based on their lowered boiling
points.
Like any physical process, this removal is dependent on vacuum, temperature and residence time (the
time the oil spends flowing over the trays or rings in a thin film while exposed to a high vacuum).
Some manufacturers use coalescer elements in their vacuum vessels, the assumption being that these
will separate moisture from the oil under a vacuum. This concept has several drawbacks, not in the least
are the removal of additives and the creation of a difficult to control foam in the vacuum vessel. This often

8. AGC REFINING & FILTRATION
SELECTION PARAMETERS FOR VACUUM OIL PURIFIERS 8
requires the purifier to be shut down for element change-out and cleaning.
In a properly designed purifier the contaminants that have been separated from the oil are sent through
the vacuum pump exhaust and to the atmosphere.
In this part of the process it is essential that before reaching the vacuum pump the vapor that consists of
moisture and other (corrosive) gases is passed through an evaporator and collected in a condensate
collection tank before it reaches the vacuum pump. The vapor mixture would otherwise corrode the pump
internals, reduce the pump oil viscosity, and ultimately cause failure of the pump. Many manufacturers of
vacuum purifiers neglect this.
In a high-quality vacuum purifier, the vacuum system is the most important and consequently, the most
expensive part.
Figure 3: A Typical Two-stage Vacuum System
In lubrication oil applications, a single-stage vacuum system that produces a vacuum of 1 torr is often
sufficient to remove minor amounts of moisture and gas. These are so-called low-vacuum Systems.
However, to achieve moisture levels below 5 wppm and to remove almost all entrained and dissolved
gases such as for transformer oil, a two-stage vacuum system (see photo) producing a minimum of 10-3
to 10-4 torr is required.

9. AGC REFINING & FILTRATION
SELECTION PARAMETERS FOR VACUUM OIL PURIFIERS 9
It is possible to design a purification system that will remove all contaminants in a single pass. Power
companies that must purify large oil-filled transformers in a timely manner often need this.
This requires a large system with a high flow rate, a deep vacuum and single-pass purification capacity.
The deep vacuum capacity is also used to dry out the transformer’s cellulose insulation under high
vacuum and to return the dehydrated, purified oil to the transformer, while still under vacuum.
Figure 4: A Large High-Vacuum Transformer Oil Purifier
Cost of a Purifier
The preceding discussion makes it obvious that the cost of a purifier depends on the following:
 the design flow rate and
 the level of oil cleanliness (removal of contaminants) required.
Thus, the prospective buyer must begin by asking:
 “What is my budget,” and
 “What can I get for it?”
Then the options available are, (from low cost to high cost, respectively):
1. a low vacuum, low flow rate system (low cost, low removal efficiency requiring many passes),
2. a low vacuum, high flow rate system (moderate cost, low removal efficiency requiring several
passes),
3. a high vacuum, low volume system (moderate cost, high removal efficiency requiring one to three
passes), and
4. a high vacuum, high volume system. (high cost, high removal efficiency requiring one pass).

10. AGC REFINING & FILTRATION
SELECTION PARAMETERS FOR VACUUM OIL PURIFIERS 10
Figure 5: Vacuum Levels for Various Types of Vacuum Pumps
Trade-offs
There are many purifiers on the market that claim high contaminant removal rates at relatively high flow
rates.
However, to achieve high contaminant removal rates a system with deep vacuum and high pumping
speed is required. This is only accomplished at a minimum vacuum of 10-3 torr. This level can only be
achieved at high flow rates by a two-stage vacuum system consisting of a blower and a main vacuum
pump.
A low-vacuum pump (1 torr) cannot remove moisture below 10 wppm as is often claimed. (See Figures 2
and 6)
Here a trade-off used by many manufacturers is to use a low-vacuum, rotary-vane-type pump. Besides
the low vacuum, rotary-vane pumps have a relatively low reliability and decreasing efficiency with age
due to the ever-increasing wear of the vanes.
The amount of heat required for purification at high flow rates exceeds the heater capacity on most low-
vacuum purifiers. Thus, it takes much longer to purify the reservoir volume of contaminated oil.
Thus, the claims of removal rates are often exaggerated and can only be verified by careful sampling and
analyses for which most customers do not have the facility or the patience. Allen purifiers provide as an
option an on-stream water-in-oil analyzer to indicate removal capacity in real time.
Low-vacuum and low-efficiency systems will leave most of the contaminants in the oil.

11. AGC REFINING & FILTRATION
SELECTION PARAMETERS FOR VACUUM OIL PURIFIERS 11
Low-vacuum and high flow rate systems will also leave most contaminants in the oil while taking an
excessive amount of time to reach what little they remove.
High-vacuum and moderate- to high-volume systems will remove almost all contaminants and will often
leave the oil in better condition than when it was new.
Figure 6: Summary of Parameters Influencing the Selection of a Vacuum Oil Purifier
Purifier design flow rate depends on:
 the rate at which the contaminant enters the lube oil tank (for instance water or gas leaking from
the seals into the oil or moisture entering a transformer through a breather) and
 the budgeted cost of the purifier.
Contaminant removal efficiency depends on:
 the design flow rate,
 the amount of heat supplied to the oil during each pass through the purifier,
 the depth of the vacuum applied to the oil, and
 the budgeted cost of the purifier.
The number of passes required to achieve purification depends on:
 the initial level of contamination,
 the amount of heat supplied,

12. AGC REFINING & FILTRATION
SELECTION PARAMETERS FOR VACUUM OIL PURIFIERS 12
 the depth of vacuum supplied, and
 the design flow rate of the purifier.
The cost of the purifier depends on:
 the design flow rate,
 the number of heaters required to achieve the proper purification temperature,
 the type of vacuum pump supplied (rotary vane or single- or two-stage lobe-type pump),
 the level of purification required,
 the amount and sophistication of the instrumentation, control, alarm and safety features (PLC
control, state-of-the-art electronics, etc.), and
 additional pre- and post-filtration for solids, acid removal, color restoration, etc.
Drying out of Transformer Insulation
An added benefit of a high-vacuum (two-stage vacuum) system is that it is strong enough to pull a
vacuum on the entire transformer and leave it under vacuum for a number of hours—even days—to dry
out the cellulose insulation inside the transformer. (See also The Aging of Cellulose in Transformers)
A dry ice moisture trap allows the operator to determine when enough moisture has been removed from
the transformer insulation by weighing the amount of ice accumulated in the trap. However, other
methods exist that can gauge the degree of dryness of the cellulose insulation.
After the dehydrated oil is returned to the transformer under vacuum, the remaining moisture in the
cellulose will migrate to the dry oil until a new equilibrium is established between the moisture in the
cellulose and the oil.
Note: The vacuum dehydrator required for purification of lubrication oil such as lube and seal oil for a gas
compressor differs from the one for purification of transformer oil. Hydrocarbon process gas is often
entrained and dissolved in the oil. However, the vacuum required for removal is lower. In addition, the
process gases must be condensed in a refrigerated condensing system before they can reach the single-
stage vacuum pump and cause damage.

13. AGC REFINING & FILTRATION
SELECTION PARAMETERS FOR VACUUM OIL PURIFIERS 13
References
1. Adams, M.A. & H.P. Bloch. “Vacuum Distillation Methods for Lube Oils Increase Turbomachinery
Reliability” (proceedings of the Seventeenth Turbomachinery Symposium, 1988).
2. “AFI-101, Water Activity in Oil” (internal publication, 2007).
3. “AFI-102, Vacuum Distillation for Industrial Oil” (internal publication, 2006).
4. “AFI-105, The Aging of Cellulose Insulation in Transformers” (internal publication, 2005).
5. “AFI-106, Maintenance of Mineral Transformer Oil, Part 1” (internal publication, 2007).
6. “AFI-107, Deterioration of Transformer Oil, Part 2” (internal publication, 2007).
7. “Aramco ATPR-321-677 Lubrication Oil Sampling Program Results 1980-1985 FCC, CHD units
and Wet Gas Compressor Rotating Equipment” (internal report, Saudi Aramco Shedgum NGL
Plant, January 1985).
8. “Evaluation of Vacuum Dehydrator Test Units” (internal report, Saudi Aramco Mobil Refinery,
Yanbu, Saudi Arabia, December 1993).
9. “Lubrication Oil Recovery using an Allen Oil Conditioner” (internal report, Refineria Isla, Aruba,
1990).

14. AGC REFINING & FILTRATION
SELECTION PARAMETERS FOR VACUUM OIL PURIFIERS 14
Appendix 1: Sample Systems
Figure 7: An Allen High Capacity Transformer Oil Purifier
1. Air cooler
2. Accumulator tank
3. High-vacuum booster pump
4. Electric hose reel
5. Main vacuum pump
Showing the main vacuum pump and high-vacuum booster pump as well as the air-cooled condensing system

15. AGC REFINING & FILTRATION
SELECTION PARAMETERS FOR VACUUM OIL PURIFIERS 15
Figure 8: An Allen Transformer Oil Purifier
1. Control panel
2. Automatic vent valve
3. Filter vessel
4. Relief valve
5. Low-watt density in-line heaters
Showing the heaters and a two-element filter vessel

16. AGC REFINING & FILTRATION
SELECTION PARAMETERS FOR VACUUM OIL PURIFIERS 16
Figure 9: A Transformer Oil Purifier
1. Filter vessel
2. Water-in-oil analyzer read out (optional)
3. Flow meter/totalizer
4. Basket strainer
Showing the flow meter/totalizer and in-line basket strainer
Figure 10: A High-Vacuum Transformer Oil Purifier
For oil volumes of 20,000 gallons and over

17. www.AGCInternational.com
3045 East Elm Street
Springfield, Missouri 65802, USA
Toll Free: +1 800 865 3208
Phone: +1 417 865 2844