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Copyright 2001 AADE National Drilling Technical Conference
This paper was prepared for presentation at the AADE 2001 National Drilling Conference, “Drilling Technology- The Next 100 years”, held at the Omni Houston Westside in Houston, Texas, March 27 - 29,
2001. This conference was hosted by the Houston Chapter of the American Association of Drilling Engineers. The information presented in this paper does not reflect any position, claim or endorsement
made or implied by the American Association of Drilling Engineers, their officers or members. Questions concerning the content of this paper should be directed to the individuals listed as author/s of this
work.
Abstract
Controlling weight material sag in invert muds is difficult
in deviated wellbores, where the phenomenon of sag is
not completely understood and simultaneous optimiza-
tion of all hydraulics variables is complex. The fluid must
be designed with a specific rheological profile over the
entire temperature range encountered in the drillpipe
and wellbore. This is particularly difficult for deepwater
wells, where temperatures may vary from near freezing
to greater than 250
o
F. Organophilic clays are especially
well suited for this purpose. In this work, a blend of
specific organophilic clays was used to provide the
rheology necessary to minimize dynamic sag in two
deepwater wells in the Mississippi Canyon, Gulf of
Mexico. Reduction of the sag potential was accom-
plished without an increase in the viscosity profile of the
mud.
Introduction
Sag is defined as a “significant” variation in mud density
(>0.5 to 1 lbm/gal) along the mud column, which is the
result of settling of the weight material. Often this occurs
during the first bottoms-up circulation after a trip, and in
inclined wellbores, sag can result in formation of a bed of
the weighting agent on the low side. Barite is the most
common weighting agent, but the same phenomenon
occurs with other materials, e.g. hematite and calcium
carbonate.
Several distinctively different phenomena can
contribute to sag: static settling, dynamic settling and
slumping.
1
Because of the complexity of the mechan-
ism, control of sag requires an integrated approach.
Control methods usually involve improved mud
formulation and preparation, monitoring and
maintenance, and adequate operational practices.
Staging into the wellbore, increasing the flow rate and
rotating the drillpipe are operational techniques to
reduce the sag potential. Controlling the rheology of the
drilling fluid is another key to minimizing sag potential. It
is well established that static settling is related to the
development of gel structure and viscoelastic properties.
Dynamic sag is more complex, but it appears to
correlate primarily with the low-shear rheology. Two
accepted descriptors of low-shear rheology are the yield
stress (extrapolated from the Herschel-Bulkley model)
and the low-shear-rate yield point (LSRYP), given by:
2
LSRYP = (2x θ3) - θ6 .........................................(1)
where θ3 and θ6 are the Fann 35 Viscometer Readings
at 3 and 6 rpm, respectively.
It has been shown that control of the low-shear
rheology -- and therefore of the dynamic sag -- can be
achieved more effectively with organophilic clays than
with fatty acid based low-shear viscosity enhancers.
2
The situation is more difficult when high-angle wells are
drilled in deepwater environment. The increase in
rheology required to minimize the sag is restricted here
by the low temperature of the fluid in the riser, thus
generating high viscosities and consequently high
equivalent circulating densities (ECDs).
A sag-preventing organophilic clay (SPOC) was
recently developed. The product was initially tested in
laboratory fluids and compared with standard organo-
clays, where it showed very good control of low- shear
rheology and barite sag. To minimize the effect on low-
temperature rheology, a combination of conventional
organoclay and the new product was found to be
optimum. Further testing was conducted in the M-I Sag
Flow Loop to study the effects of varying concentrations
of the new additive and shear on barite sag.
The new product was introduced in a field
application, while drilling the last interval of a high-angle
“S” shaped well in the Gulf of Mexico. The main
treatment was made to the premix that is added to the
drilling fluid to increase the synthetic/water ratio (SWR)
and reduce the amount of low-gravity solids (LGS). The
resulting fluid had higher SWR, less LGS concentration,
similar rheology yet lower sag potential.
A second field application was just completed. The
SPOC was used to reduce significantly the barite sag,
but it was necessary to use a higher concentration of
product for the desired effect.
Laboratory Studies
Preliminary Laboratory Evaluation. In an initial
screening test, the new organophilic clay demonstrated
AADE 01-NC-HO-51
Prevention of Dynamic Sag in Deepwater Invert Emulsion Fluids
C. Aldea, F. B. Growcock, L. J. Lee and J. E. Friedheim, M-I L.L.C.; E. van Oort, Shell Offshore, Inc.
2 C. ALDEA, F. B. GROWCOCK, L. J. LEE AND J. E. FRIEDHEIM, E. VAN OORT AADE 2001
the ability to develop superior low-shear-rate viscosity
(LSRV) and reduce the sag tendency. LSRV was
measured with a Brookfield viscometer at 0.0636 sec
-1
.
Sag tendency was evaluated by a laboratory procedure,
3
which is described below. The fluid used for comparison
was a 14-lbm/gal synthetic-based drilling fluid, with a
synthetic/water ratio (SWR) of 80:20. Using 4 lbm/bbl of
the new product, similar LSRV and sag were measured
as with 6 lbm/bbl of conventional organophilic clay
supplemented by 0.5-lbm/bbl of organic gelling agent
(see Figs. 1 and 2). The new organoclay was also
much more effective in improving the LSRV after a 2-
lbm/bbl increase, as shown in Fig. 2.
An undesirable effect of the SPOC, especially for
deepwater environments, was a higher rheology at cold
temperature (40-60
o
F), compared to that provided by a
conventional organophilic clay (Fig. 3). To reduce this
impact, a combination of the two species was recom-
mended for further testing.
Sag Flow Loop Test (SFLT) and Viscometer Sag Test
(VST). Before testing the SPOC additive in the field,
effects of additive concentration and shear on sag
potential were evaluated in the SFLT and VST.
The Sag Flow Loop is a device that can measure
directly the decrease in mud weight (MW) which results
from barite sag.
1
The test mud is circulated through a 6-
ft long tube at various flow rates and rates of pipe
rotation. Density of the mud is measured continuously
during the test and is corrected to a constant
temperature of 120
o
F. In general, sag is most likely at
an angle of 45-60 degrees. At this angle, the maximum
density decrease is often observed to occur at an
annular velocity of 25 ft/min without pipe rotation. No
drop in MW should occur at maximum flow rate and pipe
rotation. The operating conditions used are given in
Table 1.
In contrast, the VST is used to make a quick
evaluation of the sag potential by measuring the
increase in MW at the bottom of a rotational viscometer
thermocup.
3
In order to promote sag, the viscometer is
rotated at 100 rpm for 30 minutes. The difference
between the final and the initial density is used as an
indication of the dynamic sag potential.
The experimental conditions for the two sag tests are
not the same; hence the specific values obtained from
the VST usually do not agree with the SFLT results.
However, the trends observed with the two devices
usually agree very well. A fluid is considered to have
moderate-to-low sag tendency when the density change
is less than 0.15 - 0.2 lbm/gal measured by the SFLT
and less than 1 lbm/gal on the VST.
The SPOC was tested as a treatment of a 14.3-
lbm/gal synthetic-based mud at concentrations of 2 and
4 lbm/bbl (see Table 2 for the composition of the base
mud). The base mud and the treated mud were each
sheared at 6000 rpm for 30 min with a Silverson
shearing device (Model # L4RT) and hot-rolled at 150
o
F
for 16 hr prior to the SFLT. After the first round of
SFLT’s, each test fluid was sheared again for a total time
of 1 hr and 2 hr (including the initial 30 min) and re-
tested.
Effect of Shear. The effect of shear on barite sag
tendency is illustrated in Fig. 4. An initial shear of 30
min resulted in a maximum MW drop of 0.27 lbm/gal.
After a total shear of 1 hr, the MW drop was reduced to
0.22 lbm/gal, and it was further reduced to 0.19 lbm/gal
after a total shear of 2 hr. The shear helped to tighten
the emulsion and improve particle size distribution, thus
enhancing suspension quality and reducing sag
tendency of the mud. The reduction in sag tendency
was also indicated by the VST results. SFLT, VST and
Electrical Stability (ES) Test results as a function of
shear are compared in Fig. 5. The rheology of each
tested fluid was measured with Fann 35A and Chandler
3500 viscometers at 75, 120, and 150
o
F. The latter
instrument is equipped with an F-0.2 spring for
measuring viscosity at shear rates as low as 0.1 rpm.
Fig. 6 shows the rheology measured at 120
o
F for
different periods of shear. The changes in rheology due
to shear appear to be insignificant; however, a general
trend of increasing viscosity with increasing period of
shear is discernible. The changes at low shear rates
also correlate well with SFLT and VST results. One of
the authors does not agree on what is more effective in
sag reduction: increasing the duration of shear or finding
the optimal way of transferring energy to the fluid (i.e.
cavitation, extension or shear).
Effect of Sag-Preventing Organophilic Clay. The
impact of organophilic clay on sag prevention was found
to be more significant and effective than that of shear.
This is clearly illustrated in Fig. 7. The fluids in Fig. 7 all
had been sheared for a total of 2 hr. After each
treatment of 2-lbm/bbl organophilic clay, the maximum
MW drop measured with the SFLT was reduced 50%,
e.g., from 0.38 lbm/gal for the base mud to 0.18 lbm/gal
with 2 lbm/bbl, and to 0.07 lbm/gal with 4 lbm/bbl of
organophilic clay. This rapid decrease in sag tendency
can be directly associated with addition of the
organophilic clay.
Rheological measurements using Fann 35 and
Chandler 3500 viscometers showed a rapid increase in
viscosity after treatment with organophilic clay,
particularly at the lower end of the shear rate. Such an
effect was also observed with shear, but this one was
apparently much more significant in magnitude. The
rheograms from the base mud before and after
organophilic clay treatment are shown in Fig. 8. A good
correlation between the treatment level of organophilic
clay and the results from VST and ES measurements
was also obvious (see Fig. 9).
AADE 2001 PREVENTION OF DYNAMIC SAG IN DEEPWATER INVERT EMULSION FLUIDS 3
Field Applications
Case History #1. A complex geometry well was being
drilled from a deepwater platform in the Mississippi
Canyon - Gulf of Mexico. The operator was concerned
that while drilling the 10
5
/8-in. final section, a barite bed
might form on the extended high-angle portion preceding
this interval (see Fig. 11). The use of a blend of
conventional organoclay and SPOC was recommended
to minimize sag and maintain optimal rheology while
drilling the last part of this well.
The initial properties of the drilling fluid after it was
weighted up to 13 lbm/gal are presented in Table 2. The
plastic viscosity (PV) was considered high for the given
MW and SWR. This was related to the increased LGS
concentration observed at the beginning of the drilling
interval. The VST density difference was 0.75 lbm/gal,
indicating a moderate-to-low sag tendency.
One of the main goals after the drilling began was to
increase the SWR and to reduce the LGS concentration.
Adding a premixed fluid with synthetic oil, emulsifier,
surfactant and lime is typically an easy way to do this.
Barite is added to maintain the MW. To counter the
increase in sag tendency that the dilution treatment was
expected to bring about, 1.5-lbm/bbl conventional
organoclay and 0.5-lbm/bbl SPOC were added to the
premix. These concentrations were thought to be low
enough to produce minimal impact on rheology and still
minimize the sag potential.
The treatment was applied during a conditioning trip.
The properties of the treated fluid are presented in Table
2. LGS concentration was reduced by 3%, from 12.3%
to 9.3%, and as a consequence PV was reduced from
35 to 27 cP. SWR was increased from 70:30 to 73:27.
The sag potential determined with the VST was not just
maintained, but it was actually reduced after this
treatment, from 0.74 to 0.37 lbm/gal. After conditioning
the mud, a trip was made to pick up a PDC bit and
drilling assembly. When circulation resumed – after
approximately 24 hours – no significant MW variation
that could be related to sag was observed.
The premix was added almost continuously to the
system, and the well was drilled to TD without any
problems. Not only was there no evidence of barite sag,
but the large amount and high integrity of the cuttings
indicated excellent hole cleaning; for such a difficult well
geometry, these results were considered very
successful. The treatment with premix using the blend
of two organophilic clays proved to be efficient in
controlling rheology while minimizing the sag potential.
Case History #2. The SPOC was considered a viable
alternative in a highly deviated deepwater production
well drilled in the Mississippi Canyon area of the Gulf of
Mexico, relatively close to the previous well but from a
different platform. The operator was concerned that sag
might occur after an extensive logging period. An initial
concentration of 0.5-lbm/bbl SPOC was maintained in
the system prior to logging. The drilling fluid properties
after this treatment are presented in Table 3. The
wellbore was logged via toolpush, and it took two
attempts and over 76 hours to finalize the operation.
After circulation resumed, some barite sag was
observed, with 0.4 to 0.6-lbm/gal reduction in mud
density at the flowline for the initial flow during the first
bottoms-up trip and 1.0-lbm/bbl increase in mud density
for the tail-end flow.
The drilling fluid was circulated and conditioned at
this point. An addition of SPOC was made to increase
the total concentration to 1 lbm/bbl. The fluid was also
treated with organic gelling agents to reduce the static
settling. As presented in Table 3, the treated fluid had
higher YP, higher gels and low-shear rheology. YP was
increased from 20 to 23 lbf/100 ft
2
, 10-sec/10-min/30-
min gel strengths were increased from 16/21/21 to
21/25/26 lbf/100 ft
2
and the 3-rpm reading was increased
from 9 to 12. The sag potential measured by VST was
0.5-lbm/gal MW differential, which indicated that no
major sag should occur. After logging again for over 45
hours, when circulation was resumed before drilling
ahead, the MW variation during the first bottoms-up trip
was only +0.3 lbm/gal.
The system was weighted up to 14.0 lbm/gal and the
well drilled to its final planned depth. After logging for 52
hours, the well was circulated, and it showed a MW
variation again of only +0.3 lbm/gal. The SPOC
concentration was increased from 1.0 to 1.2 lbm/gal.
VST density difference was 0.1 lbm/gal. While
circulating prior to running liner, sag was within the same
limits, 0.3 lbm/gal on the light side, and 0.3 on the heavy
side. This density variation was considered manageable
for the given conditions, and sag was considered
minimal. The use of SPOC at 1 lbm/bbl was considered
successful, while a concentration of 1.2 lbm/bbl was
considered too high, inasmuch as it generated high
viscosity at the flow-line temperature. At a temperature
of around 75
o
F, the Marsh funnel viscosity was
increased from 90 to 108 sec (see Table 4). This re-
enforces the idea that excessive SPOC treatment may
affect the rheology at cold temperature.
An optimal treatment to minimize sag should consider
the rheology throughout the whole temperature range,
from seafloor to bottomhole. It is also necessary to treat
both dynamic and static settling, which requires
optimizing the relative amounts of organophilic clays and
organic gelling agents.
Conclusions
Sag is a complex process, involving static settling,
dynamic settling and slumping. An integrated approach
involving improved mud formulation and preparation,
monitoring and maintenance, and adequate operational
practices should always be used to minimize sag.
This paper describes a method of controlling the fluid
4 C. ALDEA, F. B. GROWCOCK, L. J. LEE AND J. E. FRIEDHEIM, E. VAN OORT AADE 2001
rheology by use of a special organophilic clay in
conjunction with other rheology modifiers. The following
are the main conclusions derived from this work:
1. Initial laboratory work showed that 4 lbm/bbl of SPOC
generated similar LSRV and sag -- with lower PV and
gels – to those provided by 6 lbm/bbl of conventional
organophilic clay supplemented by 0.5-lbm/bbl of
organic gelling agent.
2. SPOC has tendency to increase cold temperature
rheology more than conventional clays. A blend of
conventional and sag-preventing clays is therefore
recommended for deepwater applications.
3. As demonstrated by a flow-loop test, exposing the
fluid to additional shear enhanced suspension quality
and reduced sag tendency.
4. The use of SPOC in a field treatment caused a
notable improvement in the attempt to minimize sag
while decreasing LGS and increasing SWR. The
treatment consisted of 1.5-lbm/bbl conventional clay
and 0.5-lbm/bbl SPOC added to the dilution fluid.
5. A more aggressive field treatment was used to
minimize a sag problem that occurred after extensive
logging. The treatment consisted of 1-lbm/bbl SPOC
supplemented by organic gelling agents.
Nomenclature
ECD = Equivalent Circulating Density (lbm/gal)
ES = Electrical Stability (V)
LGS = Low-Gravity Solids (%v/v)
LSRV = Low-Shear Rate Viscosity (lbf/100 ft
2
)
LSRYP = Low-Shear Rate Yield Point (lbf/100 ft
2
)
MW = Mud Weight or Density (lbm/gal)
PDC = Polycrystalline Diamond Compact
PV = Plastic Viscosity (cP)
rpm = revolutions per minute
SFLT = Sag Flow Loop Test
SPOC = Sag-Preventing Organophilic Clay
SWR = Synthetic/Water Ratio
VST = Viscometer Sag Test
YP = Yield Point (lbf/100 ft
2
)
θ3, θ6 = Fann 35 Viscometer Readings at 3 and 6 rpm
Acknowledgments
The authors thank the managements of M-I L.L.C., Shell
Offshore, Inc. and Shell Deepwater Production, Inc. for
permission to publish this paper. We also give special
thanks to M-I project engineer Tim Browning for
preparing the information package for the second field
application, and to mud engineers Dale Shank, Jerry
Ard, Mike Willford, Mark Wells, Robert Doyle, David
Humbles and Joseph Gant for their full support during
the two field trials.
References
1. Hanson, P. M., et al.: “Investigation of Barite ‘Sag’ in
Weighted Drilling Fluids in Highly Deviated Wells,” SPE
20423, SPE Annual Technical Conf., New Orleans, Sept
23-26, 1990.
2. Bern, P. A., et al.: “The Influence of Drilling Variables on
Barite Sag,” SPE 36670, SPE Annual Technical Conf,
Denver, Oct 6-9, 1996.
3. Jefferson, D. T.: “New Procedure Helps Monitor Sag in the
Field,” ASME 91-PET-3, American Society of Mechanical
Engineers Energy Sources Technical Conf., Houston, Jan
20-24, 1991.
Table 1
Operating conditions of Sag Flow Loop Test
Operating Conditions Comments
Wellbore ID (in.) 2.0
Clear acrylic tube allows visual
examination of barite sag
Pipe OD (in.) ¾
Well Angle (degrees) 60
Maximum sag develops between 45 and
60 degrees
Pipe Eccentricity 0.80
Flow Rate (gal/min) 2.8 - 28
Annular Velocity (ft/min) 25 – 250
Max. sag develops at 25 ft/min annular
velocity with no pipe rotation
Pipe Rotation (rpm) 0 - 250 Pipe rotation can reduce sag
AADE 2001 PREVENTION OF DYNAMIC SAG IN DEEPWATER INVERT EMULSION FLUIDS 5
Table 2
Composition of SBM Used in Sag Tests
Base Fluid (bbl) 0.563
Viscosifier (lbm/bbl) 2
Emulsifier (lbm/bbl) 8
Lime (lbm/bbl) 6
CaCl2 Brine (bbl) 0.154
Barite (lbm/bbl) 363
SWR 80:20
Mud Weight (lbm/gal) 14.3
Table 3
Comparison of Fluid Properties Before and After Treatment
Case History #1
Initial Treated
MW (lbm/gal) 13 13
SWR 70:30 72:28
PV (cP) 35 27
YP (lbf/100 ft
2
) 19 13
10-sec/10-min Gels (lbf/100 ft
2
) 21/23 17/20
LGS (%) 12.3 9.3
VST ∆MW (lbm/gal) 0.75 0.37
Table 4
Comparison of Fluid Properties Before and After Treatment
Case History #2
Initial
0.5-lbm/bbl
SPOC
Treatment #1
1-lbm/bbl
SPOC
Treatment #2
1.2-lbm/bbl
SPOC
MW (lbm/gal) 13 13.1 14
SWR 75:25 75:25 76:24
PV (cP) 21 23 29
YP (lbf/100 ft
2
) 20 23 22
10-sec/10-min/ 30-min Gels (lbf/100 ft
2
) 16/21/21 21/25/26 19/21/18
Marsh Funnel Viscosity (sec) 85 @ 71
o
F 90 @ 71
o
F 108 @ 71
o
F
LGS (%) 5.4 5.7 5.1
VST ∆MW (lbm/gal) 0.75 0.5 0.1
Max. MW @ bottoms up (lbm/gal) 14 13.3 14.3
Min. MW @ bottoms up (lbm/gal) 12.4 12.7 13.7
6 C. ALDEA, F. B. GROWCOCK, L. J. LEE AND J. E. FRIEDHEIM, E. VAN OORT AADE 2001
0
0.5
1
1.5
2
2.5
3
MWDifference(ppg) VST MW Delta (ppg)
BASE + 2 ppb
S
a
g
T
e
n
d
e
n
c
y
Conventional organophilic clay +
LSRV modifier
SPOC
+ 2 ppb BASE
Fig. 1 – Effect of organophilic clays on sag tendency measured by VST in laboratory
fluids.
5000
15000
25000
35000
45000
55000
65000
75000
LSRV,cP
LSRV 1min (cP)
LSRV 2min (cP)
LSRV 3min (cP)
BASE
BASE+ 2 ppb
+ 2 ppb
Conventional organophilic clay +
LSRV modifier
SPOC
Fig. 2 – Effect of organophilic clays on Brookfield LSRV in laboratory fluids.
AADE 2001 PREVENTION OF DYNAMIC SAG IN DEEPWATER INVERT EMULSION FLUIDS 7
10
100
1000
10000
1 10 100 1000
Shear Rate (sec
-1
)
Viscosity(cP)
Conv. Clay @ 40F
SPOC @ 40F
Conv. Clay @ 150F
SPOC @ 150F
Fig. 3 – Effect of 4-lb/bbl organophilic clays on rheology of SBM at different
temperatures.
-0.40
-0.35
-0.30
-0.25
-0.20
-0.15
-0.10
-0.05
0.00
0.05
0.10
0 10 20 30 40 50 60 70 80 90 100 110 120
T i m e ( m i n )
DensityVariation@120°F(ppg)
T o t a l S h e a r = 3 0 m i n .
T o t a l S h e a r = 1 h o u r
T o t a l S h e a r = 2 h o u r s
S h e a r w a s p e r f o r m e d o n a S i l v e r s o n m i x e r a t 6 0 0 0 r p m
Fig. 4 – Density variation curves with 2-lbm/bbl treatment of organophilic clay and three
stages of shearing with a 14.3-lb/gal SBM.
8 C. ALDEA, F. B. GROWCOCK, L. J. LEE AND J. E. FRIEDHEIM, E. VAN OORT AADE 2001
0
0.2
0.4
0.6
0.8
1
1.2
1.4
30' Shear 1hr Shear 2hr Shear
MudWt(lbm/gal)
0
200
400
600
800
1000
1200
1400
ES(V)
SFLT VST ES
Fig. 5 – Effect of shear on SFLT, VST and ES results.
1
10
100
0.1 1 10 100 1000
Shear Rate, rpm
FannDialReading,degree
30' Shear 1hr Shear 2hr Shear
Fig. 6 – Effect of shear on rheology of 14.3-lb/gal SBM treated with 2-lbm/bbl
organoclay.
AADE 2001 PREVENTION OF DYNAMIC SAG IN DEEPWATER INVERT EMULSION FLUIDS 9
-0.40
-0.35
-0.30
-0.25
-0.20
-0.15
-0.10
-0.05
0.00
0.05
0.10
0 10 20 30 40 50 60 70 80 90 100 110 120
Time (min)
DensityVariation@120°F(ppg)
2ppb Conv. Clay
2ppb Conv. Clay + 2ppb SPOC
2 ppb Conv. Clay + 4ppb SPOC
Shear was performed on a Silverson mixer at 6000 rpm
Fig. 7 – Effect of SPOC addition to 14.3-lb/gal SBM illustrated by SFLT density variation
curves.
1
10
100
0.1 1 10 100 1000
Shear Rate, rpm
FannDialReading,degree
Base 2 ppb 4 ppb
Fig. 8 – Effect of organophilic clay content on rheology of 14.3-lb/gal SBM sheared for 2
hours.
10 C. ALDEA, F. B. GROWCOCK, L. J. LEE AND J. E. FRIEDHEIM, E. VAN OORT AADE 2001
0
0.2
0.4
0.6
0.8
1
1.2
1.4
1.6
1.8
2
Base 2 ppb 4 ppb
MudWt.(lbm/gal)
0
200
400
600
800
1000
1200
1400
1600
1800
2000
ES(V)
SFLT VST ES
Fig. 9 – Effect of SPOC Addition on SFLT, VST, and ES results.
VirtualVirtual
HydraulicsHydraulics
®
Directional Profile
0 2 4 6 8 10 12
0
2
4
6
8
10
12
14
Horizontal Displacement (1000 ft)
TrueVerticalDepth(1000ft)
Fig. 10 – Directional profile of the well described in Case History #1.

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Prevention of dynamic sag in deepwater invert emulsion fluid

  • 1. Copyright 2001 AADE National Drilling Technical Conference This paper was prepared for presentation at the AADE 2001 National Drilling Conference, “Drilling Technology- The Next 100 years”, held at the Omni Houston Westside in Houston, Texas, March 27 - 29, 2001. This conference was hosted by the Houston Chapter of the American Association of Drilling Engineers. The information presented in this paper does not reflect any position, claim or endorsement made or implied by the American Association of Drilling Engineers, their officers or members. Questions concerning the content of this paper should be directed to the individuals listed as author/s of this work. Abstract Controlling weight material sag in invert muds is difficult in deviated wellbores, where the phenomenon of sag is not completely understood and simultaneous optimiza- tion of all hydraulics variables is complex. The fluid must be designed with a specific rheological profile over the entire temperature range encountered in the drillpipe and wellbore. This is particularly difficult for deepwater wells, where temperatures may vary from near freezing to greater than 250 o F. Organophilic clays are especially well suited for this purpose. In this work, a blend of specific organophilic clays was used to provide the rheology necessary to minimize dynamic sag in two deepwater wells in the Mississippi Canyon, Gulf of Mexico. Reduction of the sag potential was accom- plished without an increase in the viscosity profile of the mud. Introduction Sag is defined as a “significant” variation in mud density (>0.5 to 1 lbm/gal) along the mud column, which is the result of settling of the weight material. Often this occurs during the first bottoms-up circulation after a trip, and in inclined wellbores, sag can result in formation of a bed of the weighting agent on the low side. Barite is the most common weighting agent, but the same phenomenon occurs with other materials, e.g. hematite and calcium carbonate. Several distinctively different phenomena can contribute to sag: static settling, dynamic settling and slumping. 1 Because of the complexity of the mechan- ism, control of sag requires an integrated approach. Control methods usually involve improved mud formulation and preparation, monitoring and maintenance, and adequate operational practices. Staging into the wellbore, increasing the flow rate and rotating the drillpipe are operational techniques to reduce the sag potential. Controlling the rheology of the drilling fluid is another key to minimizing sag potential. It is well established that static settling is related to the development of gel structure and viscoelastic properties. Dynamic sag is more complex, but it appears to correlate primarily with the low-shear rheology. Two accepted descriptors of low-shear rheology are the yield stress (extrapolated from the Herschel-Bulkley model) and the low-shear-rate yield point (LSRYP), given by: 2 LSRYP = (2x θ3) - θ6 .........................................(1) where θ3 and θ6 are the Fann 35 Viscometer Readings at 3 and 6 rpm, respectively. It has been shown that control of the low-shear rheology -- and therefore of the dynamic sag -- can be achieved more effectively with organophilic clays than with fatty acid based low-shear viscosity enhancers. 2 The situation is more difficult when high-angle wells are drilled in deepwater environment. The increase in rheology required to minimize the sag is restricted here by the low temperature of the fluid in the riser, thus generating high viscosities and consequently high equivalent circulating densities (ECDs). A sag-preventing organophilic clay (SPOC) was recently developed. The product was initially tested in laboratory fluids and compared with standard organo- clays, where it showed very good control of low- shear rheology and barite sag. To minimize the effect on low- temperature rheology, a combination of conventional organoclay and the new product was found to be optimum. Further testing was conducted in the M-I Sag Flow Loop to study the effects of varying concentrations of the new additive and shear on barite sag. The new product was introduced in a field application, while drilling the last interval of a high-angle “S” shaped well in the Gulf of Mexico. The main treatment was made to the premix that is added to the drilling fluid to increase the synthetic/water ratio (SWR) and reduce the amount of low-gravity solids (LGS). The resulting fluid had higher SWR, less LGS concentration, similar rheology yet lower sag potential. A second field application was just completed. The SPOC was used to reduce significantly the barite sag, but it was necessary to use a higher concentration of product for the desired effect. Laboratory Studies Preliminary Laboratory Evaluation. In an initial screening test, the new organophilic clay demonstrated AADE 01-NC-HO-51 Prevention of Dynamic Sag in Deepwater Invert Emulsion Fluids C. Aldea, F. B. Growcock, L. J. Lee and J. E. Friedheim, M-I L.L.C.; E. van Oort, Shell Offshore, Inc.
  • 2. 2 C. ALDEA, F. B. GROWCOCK, L. J. LEE AND J. E. FRIEDHEIM, E. VAN OORT AADE 2001 the ability to develop superior low-shear-rate viscosity (LSRV) and reduce the sag tendency. LSRV was measured with a Brookfield viscometer at 0.0636 sec -1 . Sag tendency was evaluated by a laboratory procedure, 3 which is described below. The fluid used for comparison was a 14-lbm/gal synthetic-based drilling fluid, with a synthetic/water ratio (SWR) of 80:20. Using 4 lbm/bbl of the new product, similar LSRV and sag were measured as with 6 lbm/bbl of conventional organophilic clay supplemented by 0.5-lbm/bbl of organic gelling agent (see Figs. 1 and 2). The new organoclay was also much more effective in improving the LSRV after a 2- lbm/bbl increase, as shown in Fig. 2. An undesirable effect of the SPOC, especially for deepwater environments, was a higher rheology at cold temperature (40-60 o F), compared to that provided by a conventional organophilic clay (Fig. 3). To reduce this impact, a combination of the two species was recom- mended for further testing. Sag Flow Loop Test (SFLT) and Viscometer Sag Test (VST). Before testing the SPOC additive in the field, effects of additive concentration and shear on sag potential were evaluated in the SFLT and VST. The Sag Flow Loop is a device that can measure directly the decrease in mud weight (MW) which results from barite sag. 1 The test mud is circulated through a 6- ft long tube at various flow rates and rates of pipe rotation. Density of the mud is measured continuously during the test and is corrected to a constant temperature of 120 o F. In general, sag is most likely at an angle of 45-60 degrees. At this angle, the maximum density decrease is often observed to occur at an annular velocity of 25 ft/min without pipe rotation. No drop in MW should occur at maximum flow rate and pipe rotation. The operating conditions used are given in Table 1. In contrast, the VST is used to make a quick evaluation of the sag potential by measuring the increase in MW at the bottom of a rotational viscometer thermocup. 3 In order to promote sag, the viscometer is rotated at 100 rpm for 30 minutes. The difference between the final and the initial density is used as an indication of the dynamic sag potential. The experimental conditions for the two sag tests are not the same; hence the specific values obtained from the VST usually do not agree with the SFLT results. However, the trends observed with the two devices usually agree very well. A fluid is considered to have moderate-to-low sag tendency when the density change is less than 0.15 - 0.2 lbm/gal measured by the SFLT and less than 1 lbm/gal on the VST. The SPOC was tested as a treatment of a 14.3- lbm/gal synthetic-based mud at concentrations of 2 and 4 lbm/bbl (see Table 2 for the composition of the base mud). The base mud and the treated mud were each sheared at 6000 rpm for 30 min with a Silverson shearing device (Model # L4RT) and hot-rolled at 150 o F for 16 hr prior to the SFLT. After the first round of SFLT’s, each test fluid was sheared again for a total time of 1 hr and 2 hr (including the initial 30 min) and re- tested. Effect of Shear. The effect of shear on barite sag tendency is illustrated in Fig. 4. An initial shear of 30 min resulted in a maximum MW drop of 0.27 lbm/gal. After a total shear of 1 hr, the MW drop was reduced to 0.22 lbm/gal, and it was further reduced to 0.19 lbm/gal after a total shear of 2 hr. The shear helped to tighten the emulsion and improve particle size distribution, thus enhancing suspension quality and reducing sag tendency of the mud. The reduction in sag tendency was also indicated by the VST results. SFLT, VST and Electrical Stability (ES) Test results as a function of shear are compared in Fig. 5. The rheology of each tested fluid was measured with Fann 35A and Chandler 3500 viscometers at 75, 120, and 150 o F. The latter instrument is equipped with an F-0.2 spring for measuring viscosity at shear rates as low as 0.1 rpm. Fig. 6 shows the rheology measured at 120 o F for different periods of shear. The changes in rheology due to shear appear to be insignificant; however, a general trend of increasing viscosity with increasing period of shear is discernible. The changes at low shear rates also correlate well with SFLT and VST results. One of the authors does not agree on what is more effective in sag reduction: increasing the duration of shear or finding the optimal way of transferring energy to the fluid (i.e. cavitation, extension or shear). Effect of Sag-Preventing Organophilic Clay. The impact of organophilic clay on sag prevention was found to be more significant and effective than that of shear. This is clearly illustrated in Fig. 7. The fluids in Fig. 7 all had been sheared for a total of 2 hr. After each treatment of 2-lbm/bbl organophilic clay, the maximum MW drop measured with the SFLT was reduced 50%, e.g., from 0.38 lbm/gal for the base mud to 0.18 lbm/gal with 2 lbm/bbl, and to 0.07 lbm/gal with 4 lbm/bbl of organophilic clay. This rapid decrease in sag tendency can be directly associated with addition of the organophilic clay. Rheological measurements using Fann 35 and Chandler 3500 viscometers showed a rapid increase in viscosity after treatment with organophilic clay, particularly at the lower end of the shear rate. Such an effect was also observed with shear, but this one was apparently much more significant in magnitude. The rheograms from the base mud before and after organophilic clay treatment are shown in Fig. 8. A good correlation between the treatment level of organophilic clay and the results from VST and ES measurements was also obvious (see Fig. 9).
  • 3. AADE 2001 PREVENTION OF DYNAMIC SAG IN DEEPWATER INVERT EMULSION FLUIDS 3 Field Applications Case History #1. A complex geometry well was being drilled from a deepwater platform in the Mississippi Canyon - Gulf of Mexico. The operator was concerned that while drilling the 10 5 /8-in. final section, a barite bed might form on the extended high-angle portion preceding this interval (see Fig. 11). The use of a blend of conventional organoclay and SPOC was recommended to minimize sag and maintain optimal rheology while drilling the last part of this well. The initial properties of the drilling fluid after it was weighted up to 13 lbm/gal are presented in Table 2. The plastic viscosity (PV) was considered high for the given MW and SWR. This was related to the increased LGS concentration observed at the beginning of the drilling interval. The VST density difference was 0.75 lbm/gal, indicating a moderate-to-low sag tendency. One of the main goals after the drilling began was to increase the SWR and to reduce the LGS concentration. Adding a premixed fluid with synthetic oil, emulsifier, surfactant and lime is typically an easy way to do this. Barite is added to maintain the MW. To counter the increase in sag tendency that the dilution treatment was expected to bring about, 1.5-lbm/bbl conventional organoclay and 0.5-lbm/bbl SPOC were added to the premix. These concentrations were thought to be low enough to produce minimal impact on rheology and still minimize the sag potential. The treatment was applied during a conditioning trip. The properties of the treated fluid are presented in Table 2. LGS concentration was reduced by 3%, from 12.3% to 9.3%, and as a consequence PV was reduced from 35 to 27 cP. SWR was increased from 70:30 to 73:27. The sag potential determined with the VST was not just maintained, but it was actually reduced after this treatment, from 0.74 to 0.37 lbm/gal. After conditioning the mud, a trip was made to pick up a PDC bit and drilling assembly. When circulation resumed – after approximately 24 hours – no significant MW variation that could be related to sag was observed. The premix was added almost continuously to the system, and the well was drilled to TD without any problems. Not only was there no evidence of barite sag, but the large amount and high integrity of the cuttings indicated excellent hole cleaning; for such a difficult well geometry, these results were considered very successful. The treatment with premix using the blend of two organophilic clays proved to be efficient in controlling rheology while minimizing the sag potential. Case History #2. The SPOC was considered a viable alternative in a highly deviated deepwater production well drilled in the Mississippi Canyon area of the Gulf of Mexico, relatively close to the previous well but from a different platform. The operator was concerned that sag might occur after an extensive logging period. An initial concentration of 0.5-lbm/bbl SPOC was maintained in the system prior to logging. The drilling fluid properties after this treatment are presented in Table 3. The wellbore was logged via toolpush, and it took two attempts and over 76 hours to finalize the operation. After circulation resumed, some barite sag was observed, with 0.4 to 0.6-lbm/gal reduction in mud density at the flowline for the initial flow during the first bottoms-up trip and 1.0-lbm/bbl increase in mud density for the tail-end flow. The drilling fluid was circulated and conditioned at this point. An addition of SPOC was made to increase the total concentration to 1 lbm/bbl. The fluid was also treated with organic gelling agents to reduce the static settling. As presented in Table 3, the treated fluid had higher YP, higher gels and low-shear rheology. YP was increased from 20 to 23 lbf/100 ft 2 , 10-sec/10-min/30- min gel strengths were increased from 16/21/21 to 21/25/26 lbf/100 ft 2 and the 3-rpm reading was increased from 9 to 12. The sag potential measured by VST was 0.5-lbm/gal MW differential, which indicated that no major sag should occur. After logging again for over 45 hours, when circulation was resumed before drilling ahead, the MW variation during the first bottoms-up trip was only +0.3 lbm/gal. The system was weighted up to 14.0 lbm/gal and the well drilled to its final planned depth. After logging for 52 hours, the well was circulated, and it showed a MW variation again of only +0.3 lbm/gal. The SPOC concentration was increased from 1.0 to 1.2 lbm/gal. VST density difference was 0.1 lbm/gal. While circulating prior to running liner, sag was within the same limits, 0.3 lbm/gal on the light side, and 0.3 on the heavy side. This density variation was considered manageable for the given conditions, and sag was considered minimal. The use of SPOC at 1 lbm/bbl was considered successful, while a concentration of 1.2 lbm/bbl was considered too high, inasmuch as it generated high viscosity at the flow-line temperature. At a temperature of around 75 o F, the Marsh funnel viscosity was increased from 90 to 108 sec (see Table 4). This re- enforces the idea that excessive SPOC treatment may affect the rheology at cold temperature. An optimal treatment to minimize sag should consider the rheology throughout the whole temperature range, from seafloor to bottomhole. It is also necessary to treat both dynamic and static settling, which requires optimizing the relative amounts of organophilic clays and organic gelling agents. Conclusions Sag is a complex process, involving static settling, dynamic settling and slumping. An integrated approach involving improved mud formulation and preparation, monitoring and maintenance, and adequate operational practices should always be used to minimize sag. This paper describes a method of controlling the fluid
  • 4. 4 C. ALDEA, F. B. GROWCOCK, L. J. LEE AND J. E. FRIEDHEIM, E. VAN OORT AADE 2001 rheology by use of a special organophilic clay in conjunction with other rheology modifiers. The following are the main conclusions derived from this work: 1. Initial laboratory work showed that 4 lbm/bbl of SPOC generated similar LSRV and sag -- with lower PV and gels – to those provided by 6 lbm/bbl of conventional organophilic clay supplemented by 0.5-lbm/bbl of organic gelling agent. 2. SPOC has tendency to increase cold temperature rheology more than conventional clays. A blend of conventional and sag-preventing clays is therefore recommended for deepwater applications. 3. As demonstrated by a flow-loop test, exposing the fluid to additional shear enhanced suspension quality and reduced sag tendency. 4. The use of SPOC in a field treatment caused a notable improvement in the attempt to minimize sag while decreasing LGS and increasing SWR. The treatment consisted of 1.5-lbm/bbl conventional clay and 0.5-lbm/bbl SPOC added to the dilution fluid. 5. A more aggressive field treatment was used to minimize a sag problem that occurred after extensive logging. The treatment consisted of 1-lbm/bbl SPOC supplemented by organic gelling agents. Nomenclature ECD = Equivalent Circulating Density (lbm/gal) ES = Electrical Stability (V) LGS = Low-Gravity Solids (%v/v) LSRV = Low-Shear Rate Viscosity (lbf/100 ft 2 ) LSRYP = Low-Shear Rate Yield Point (lbf/100 ft 2 ) MW = Mud Weight or Density (lbm/gal) PDC = Polycrystalline Diamond Compact PV = Plastic Viscosity (cP) rpm = revolutions per minute SFLT = Sag Flow Loop Test SPOC = Sag-Preventing Organophilic Clay SWR = Synthetic/Water Ratio VST = Viscometer Sag Test YP = Yield Point (lbf/100 ft 2 ) θ3, θ6 = Fann 35 Viscometer Readings at 3 and 6 rpm Acknowledgments The authors thank the managements of M-I L.L.C., Shell Offshore, Inc. and Shell Deepwater Production, Inc. for permission to publish this paper. We also give special thanks to M-I project engineer Tim Browning for preparing the information package for the second field application, and to mud engineers Dale Shank, Jerry Ard, Mike Willford, Mark Wells, Robert Doyle, David Humbles and Joseph Gant for their full support during the two field trials. References 1. Hanson, P. M., et al.: “Investigation of Barite ‘Sag’ in Weighted Drilling Fluids in Highly Deviated Wells,” SPE 20423, SPE Annual Technical Conf., New Orleans, Sept 23-26, 1990. 2. Bern, P. A., et al.: “The Influence of Drilling Variables on Barite Sag,” SPE 36670, SPE Annual Technical Conf, Denver, Oct 6-9, 1996. 3. Jefferson, D. T.: “New Procedure Helps Monitor Sag in the Field,” ASME 91-PET-3, American Society of Mechanical Engineers Energy Sources Technical Conf., Houston, Jan 20-24, 1991. Table 1 Operating conditions of Sag Flow Loop Test Operating Conditions Comments Wellbore ID (in.) 2.0 Clear acrylic tube allows visual examination of barite sag Pipe OD (in.) ¾ Well Angle (degrees) 60 Maximum sag develops between 45 and 60 degrees Pipe Eccentricity 0.80 Flow Rate (gal/min) 2.8 - 28 Annular Velocity (ft/min) 25 – 250 Max. sag develops at 25 ft/min annular velocity with no pipe rotation Pipe Rotation (rpm) 0 - 250 Pipe rotation can reduce sag
  • 5. AADE 2001 PREVENTION OF DYNAMIC SAG IN DEEPWATER INVERT EMULSION FLUIDS 5 Table 2 Composition of SBM Used in Sag Tests Base Fluid (bbl) 0.563 Viscosifier (lbm/bbl) 2 Emulsifier (lbm/bbl) 8 Lime (lbm/bbl) 6 CaCl2 Brine (bbl) 0.154 Barite (lbm/bbl) 363 SWR 80:20 Mud Weight (lbm/gal) 14.3 Table 3 Comparison of Fluid Properties Before and After Treatment Case History #1 Initial Treated MW (lbm/gal) 13 13 SWR 70:30 72:28 PV (cP) 35 27 YP (lbf/100 ft 2 ) 19 13 10-sec/10-min Gels (lbf/100 ft 2 ) 21/23 17/20 LGS (%) 12.3 9.3 VST ∆MW (lbm/gal) 0.75 0.37 Table 4 Comparison of Fluid Properties Before and After Treatment Case History #2 Initial 0.5-lbm/bbl SPOC Treatment #1 1-lbm/bbl SPOC Treatment #2 1.2-lbm/bbl SPOC MW (lbm/gal) 13 13.1 14 SWR 75:25 75:25 76:24 PV (cP) 21 23 29 YP (lbf/100 ft 2 ) 20 23 22 10-sec/10-min/ 30-min Gels (lbf/100 ft 2 ) 16/21/21 21/25/26 19/21/18 Marsh Funnel Viscosity (sec) 85 @ 71 o F 90 @ 71 o F 108 @ 71 o F LGS (%) 5.4 5.7 5.1 VST ∆MW (lbm/gal) 0.75 0.5 0.1 Max. MW @ bottoms up (lbm/gal) 14 13.3 14.3 Min. MW @ bottoms up (lbm/gal) 12.4 12.7 13.7
  • 6. 6 C. ALDEA, F. B. GROWCOCK, L. J. LEE AND J. E. FRIEDHEIM, E. VAN OORT AADE 2001 0 0.5 1 1.5 2 2.5 3 MWDifference(ppg) VST MW Delta (ppg) BASE + 2 ppb S a g T e n d e n c y Conventional organophilic clay + LSRV modifier SPOC + 2 ppb BASE Fig. 1 – Effect of organophilic clays on sag tendency measured by VST in laboratory fluids. 5000 15000 25000 35000 45000 55000 65000 75000 LSRV,cP LSRV 1min (cP) LSRV 2min (cP) LSRV 3min (cP) BASE BASE+ 2 ppb + 2 ppb Conventional organophilic clay + LSRV modifier SPOC Fig. 2 – Effect of organophilic clays on Brookfield LSRV in laboratory fluids.
  • 7. AADE 2001 PREVENTION OF DYNAMIC SAG IN DEEPWATER INVERT EMULSION FLUIDS 7 10 100 1000 10000 1 10 100 1000 Shear Rate (sec -1 ) Viscosity(cP) Conv. Clay @ 40F SPOC @ 40F Conv. Clay @ 150F SPOC @ 150F Fig. 3 – Effect of 4-lb/bbl organophilic clays on rheology of SBM at different temperatures. -0.40 -0.35 -0.30 -0.25 -0.20 -0.15 -0.10 -0.05 0.00 0.05 0.10 0 10 20 30 40 50 60 70 80 90 100 110 120 T i m e ( m i n ) DensityVariation@120°F(ppg) T o t a l S h e a r = 3 0 m i n . T o t a l S h e a r = 1 h o u r T o t a l S h e a r = 2 h o u r s S h e a r w a s p e r f o r m e d o n a S i l v e r s o n m i x e r a t 6 0 0 0 r p m Fig. 4 – Density variation curves with 2-lbm/bbl treatment of organophilic clay and three stages of shearing with a 14.3-lb/gal SBM.
  • 8. 8 C. ALDEA, F. B. GROWCOCK, L. J. LEE AND J. E. FRIEDHEIM, E. VAN OORT AADE 2001 0 0.2 0.4 0.6 0.8 1 1.2 1.4 30' Shear 1hr Shear 2hr Shear MudWt(lbm/gal) 0 200 400 600 800 1000 1200 1400 ES(V) SFLT VST ES Fig. 5 – Effect of shear on SFLT, VST and ES results. 1 10 100 0.1 1 10 100 1000 Shear Rate, rpm FannDialReading,degree 30' Shear 1hr Shear 2hr Shear Fig. 6 – Effect of shear on rheology of 14.3-lb/gal SBM treated with 2-lbm/bbl organoclay.
  • 9. AADE 2001 PREVENTION OF DYNAMIC SAG IN DEEPWATER INVERT EMULSION FLUIDS 9 -0.40 -0.35 -0.30 -0.25 -0.20 -0.15 -0.10 -0.05 0.00 0.05 0.10 0 10 20 30 40 50 60 70 80 90 100 110 120 Time (min) DensityVariation@120°F(ppg) 2ppb Conv. Clay 2ppb Conv. Clay + 2ppb SPOC 2 ppb Conv. Clay + 4ppb SPOC Shear was performed on a Silverson mixer at 6000 rpm Fig. 7 – Effect of SPOC addition to 14.3-lb/gal SBM illustrated by SFLT density variation curves. 1 10 100 0.1 1 10 100 1000 Shear Rate, rpm FannDialReading,degree Base 2 ppb 4 ppb Fig. 8 – Effect of organophilic clay content on rheology of 14.3-lb/gal SBM sheared for 2 hours.
  • 10. 10 C. ALDEA, F. B. GROWCOCK, L. J. LEE AND J. E. FRIEDHEIM, E. VAN OORT AADE 2001 0 0.2 0.4 0.6 0.8 1 1.2 1.4 1.6 1.8 2 Base 2 ppb 4 ppb MudWt.(lbm/gal) 0 200 400 600 800 1000 1200 1400 1600 1800 2000 ES(V) SFLT VST ES Fig. 9 – Effect of SPOC Addition on SFLT, VST, and ES results. VirtualVirtual HydraulicsHydraulics ® Directional Profile 0 2 4 6 8 10 12 0 2 4 6 8 10 12 14 Horizontal Displacement (1000 ft) TrueVerticalDepth(1000ft) Fig. 10 – Directional profile of the well described in Case History #1.