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Synthesis of Shape-Controlled
Metal Nanoparticles
Roxana Y. Treviño
SEM Images of Octahedron Shaped
Nanoparticles:
• SEM Pd Nanoparticle Octahedron Shape- • SEM Au Nanoparticle (hypothesis/results)
Octahedron Shape (72hrs at 35,000
magnification)-
SEM (Repeat) Pd
Nanoparticle
Octahedron Shape (2
weeks and 4 days):
• Size of Pd
nanoparticle
is 10µm at
1,500
magnification
• About 100X’s
too large if
needing
100nm in size
Conclusion:
• Leave in solution for at least a week
before taking SEM images to allow
nanoparticles to grow on their individual
crystallographic planes.
• And look for nanoparticles at a higher
magnification than X35,000.

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Presentation number4

  • 1. Synthesis of Shape-Controlled Metal Nanoparticles Roxana Y. Treviño
  • 2. SEM Images of Octahedron Shaped Nanoparticles: • SEM Pd Nanoparticle Octahedron Shape- • SEM Au Nanoparticle (hypothesis/results) Octahedron Shape (72hrs at 35,000 magnification)-
  • 3. SEM (Repeat) Pd Nanoparticle Octahedron Shape (2 weeks and 4 days): • Size of Pd nanoparticle is 10µm at 1,500 magnification • About 100X’s too large if needing 100nm in size
  • 4. Conclusion: • Leave in solution for at least a week before taking SEM images to allow nanoparticles to grow on their individual crystallographic planes. • And look for nanoparticles at a higher magnification than X35,000.