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Determination of the Corrosion Rate of a MIC Influenced Pipeline Using Four
Consecutive Pig Runs
Conference Paper · January 2006
DOI: 10.1115/IPC2006-10142
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Lech Grzelak
Delft University of Technology
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May 2007 PGT/Achterbosch, Grzelak/Determining corrosion rates/Page-1
(Page caption)
Pipeline integrity
(Head)
Determining corrosion rates
(Deck)
Gasunie uses data from pig runs and excavations to
examine corrosion defects, determine corrosion rates.
Giorgio G.J. Achterbosch, N.V. Nederlandse Gasunie, Groningen, The Netherlands; and Lech A. Grzelak,
Delft University of Technology, Delft, The Netherlands
In-line inspections have been part of Gasunie’s pipeline integrity verification efforts since the late 1970s. A few
years ago, the discovery of external microbial corrosion (MIC) in one of the high-pressure pipelines changed
the inspection policy from inspection of a randomly selected pipeline once every five years to an inspection
program for the whole high-pressure grid (approximately 5,600 km, or 3,500 mi) to be completed in 10-12
years.
One of the MIC-influenced lines is used to qualify MFL pigs from different suppliers. In the time period
1999-2004, four different MFL qualification runs were performed, resulting in 18 excavations. Corrosion rates
that had been determined by rather simple calculations after every pig run indicated values of 0.2 to 0.3 mm/yr
as an average value for the MIC corrosion.
After the fourth pig run (five years after the first), Gasunie decided to determine the corrosion rate in a
more sophisticated manner. Statistical analyses were performed in cooperation with the mathematical
department of the Technical University of Delft. The goal was to use the data from pig runs and excavations to
extract a suitable subset of corrosion defects, from which the corrosion rate could be determined.
It was decided to use only those defects that were indicated by all suppliers as external corrosion,
thereby leaving out defects that were indicated as “mill defect but possibly corrosion.” A second criterion was
that a defect had to be reported by at least three of the four suppliers. These criteria resulted in a subset of 52
defects to be analyzed.
All of the reported defect depths were corrected for the bias that was determined from the excavation
results. The corrected values were then used to calculate the corrosion rate using three approaches. Two of these
involved calculation of the corrosion rate for every defect; the third determined the corrosion rate for the pool of
defects assuming a corrosion growth that is linear in time. The analysis was performed starting from the
simplest to more sophisticated models. The first and the second approach were simply based on the
unconstrained regression analysis. The third and last model was based on the unbiased measurements and pigs
accuracy. The average corrosion rate for the defects was in the range of 0.12 to 0.24 mm/yr. Dividing the data
set into deep and shallow defects showed that the average corrosion rates for both subsets, 0.23 mm/yr and 0.25
mm/yr, are not significantly different. This underpins one of the assumptions that the corrosion rate is constant.
Inspections and excavations
The N.V. Nederlandse Gasunie gas transportation network consists of approximately 11,600 km (roughly 7,200
mi) of steel pipelines (4 to 48-in. diameters) that was largely built in the mid-1960s and early 1970s. The
network is split into a high-pressure part (5,600 km, 66-80 bar) and a medium-pressure part (600 km, 40 bar).
While the high pressure network is piggable, the medium pressure part does not possess facilities to launch and
receive intelligent pigs.
Until 1999, Gasunie had no indications whatsoever that there was a corrosion problem on one of its
pipelines. Both regular CP measurements as well as observations during excavations or reroutings indicated that
no significant corrosion problem existed. Nevertheless, since 1979, company policy has been to verify pipeline
May 2007 PGT/Achterbosch, Grzelak/Determining corrosion rates/Page-2
integrity periodically by running an intelligent pig through one of its high-pressure lines on average once every
five years. The results of these pig runs confirmed the existing opinion that no corrosion problem existed.
In 1999, a 70-km, 36-in. line in the north of the Netherlands was inspected by an MFL pig as part of the
verification program. The results of the pig run indicated 65 external corrosion features but no internal
corrosion. After a thorough defect assessment by the safety department, it was decided that six indications had
to be excavated and repaired. The first excavation by the end of 1999 led to an unpleasant surprise. At the
excavation, the appearance of the corrosion defect turned out to be totally different from the few corrosion
defects that Gasunie had experienced in the past. Analysis of the corrosion products and the appearance of the
defect led to the conclusion that the corrosion was influenced by sulphate reducing bacteria (SRBs). Similar
experience was obtained at three other excavations. The conclusion was that at four out of the six excavations,
there was evidence of microbially influenced corrosion (MIC). An additional excavation in 2000 showed also
MIC.
From the results, Gasunie concluded that it was no longer safe to assume that other lines were free of
this corrosion problem. Therefore, the inspection policy was revised. It was decided to start an in-line inspection
program for all high-pressure lines to be completed in a timeframe of approximately ten years. When starting
the inspection program, the company realized that a reliable corrosion rate is paramount to determine a re-
inspection time interval for its pipelines. As a consequence, a corrosion rate was calculated every time a new pig
run was performed through the pipe. This was done by comparing the reported defect dimensions of supplier A
to the reported dimensions of supplier B; and then A to C, and so one. But because of the relatively short time
interval between the pig runs, the uncertainty of the reported defect dimensions is dominant and prevents the
calculation of a reliable corrosion rate. Corrosion rates that were calculated using simple comparison of defects
indicated average values of 0.2 to 0.3 mm/yr. But the standard deviation of these values was of the same order
of magnitude or even larger.
However, after the fourth pig run, which took place almost five years after the first run, Gasunie was of
the opinion that it would be possible to determine the corrosion rate using more sophisticated statistical
techniques. Because of long-standing relationship with the mathematical department of Delft Technical
University, this department was asked to help analyze the available data using statistically sound techniques.
First approach
In the first approach, all the defects are pooled in one dataset, and no corrosion rate is calculated for individual
defects but only for the dataset as a whole. The first step was to see if there was a basis to accept the hypothesis
that the measurement errors for all MFL pigs are from the same population, and are normally distributed. This
was the case. According to the maximum likelihood estimation for the measurement error, the parameters are 0
(mean) and 0.91 (for a standard deviation). If it is assumed that for all the errors, there is no correlation between
them, then the task of finding a corrosion rate associated with all the measurements is equivalent to a Gauss
Markov regression analysis.
If it is also assumed that the corrosion rate is uniform over time (i.e., corrosion growth is linear), then an
application of the Least Squares Error (LSE) method gives a linear description of the corrosion growth in the
following form: t
y 1
0 ˆ
ˆ 
 
 . Standard calculations give that the estimators for unknown parameters are: 42
.
2
0
ˆ 


and 12
.
0
1
ˆ 
 . Coefficient 1
̂ is equivalent to the measurement of the corrosion rate (mm/yr), so the LSE model
estimated a corrosion rate for the calibrated measurements of 0.12 mm/yr with 95% confidence interval (0.05,
0.20) (Figure 1).
A determination coefficient was then calculated to see how well the model fit the data. A goodness of fit
measure resulted in 04
.
0
2

R . This was not satisfactory, because it indicated that there was hardly a correlation
between the two parameters. According to the model, the initiation time for corrosion is 20 years (years since
pipeline installation).
Even though the estimated parameters are in an acceptable range, this approach has significant
drawbacks. Most notably, the model:
May 2007 PGT/Achterbosch, Grzelak/Determining corrosion rates/Page-3
 Does not distinguish defects
 Does not take into account that some of the defects are improving in time (decreasing defect’s depth
which is physically impossible), or for some the defects initiation time is before pipeline installation
 the model assumes that all the defects have one corrosion rate
Second approach
As noted above, the first approach had significant drawbacks. The second approach proposes a way of dealing
with some of the enumerated disadvantages. As before, it is assumed that corrosion growth is linear in time. The
second model checks what the corrosion rate is, and analyzes the defects individually. That is, the model no
longer assumes that there is only one corrosion rate for all the defects, but instead calculates a corrosion rate per
defect. A simple regression analysis applied to each unbiased defect is depicted in Figure 2.
From the histogram presented in Figure 2, it is clear that in many cases, simple regression analysis
applied to each defect resulted in negative corrosion rates. The mean corrosion rate according to this model is
0.16 mm/yr, which is close to the result obtained before. However, the 95% confidence interval for the
corrosion rate is quite different: -0.31, 0.54. The 95% confidence interval comprises negative values.
The number of the defects indicating either negative corrosion rate or corrosion initiation time before the
pipeline installation is 16. One way of dealing with a negative corrosion rate is to remove all the outliers from
the dataset. However, such treatment is undesirable, since the dataset consists of 30% bad defects. Further
investigation confirmed that the corrosion rate follows a normal distribution. The initiation time of the corrosion
is presented in Figure 3, also in the form of a histogram. The red bars indicate an initiation time outside the
interval determined by the time of pipeline installation (t=0 [yr]) and the time of the last inspection (t=44.25
[yr]). However, the Least Squares Errors approach produces negative corrosion rates or initiation times before
pipeline installation. Therefore, an alternative model for the presented models was developed. This was the third
approach.
Third approach
TUDelft constructed a model in such a way that the following constraints had to be met:
 Corrosion rates had to be positive
 Initiation time had to fall in the lifetime of the pipeline.
The model was based on a maximum likelihood estimation, which was in turn based on measurement
distributions for the function describing the corrosion growth in time. The model takes into account information
about the measurement error distribution for each specific pig, and, according to these distributions, assigns
weights to the measurements. Moreover, this model also takes into account the distributions obtained from the
calibration procedure. These distributions are used in order to assign weights to the pigs in such a way that the
pig with the smallest level of uncertainty (smallest standard deviation for the error distribution) will get the
highest weight. So it is natural that a pig which is accurate will influence the final results much more than a pig
with a lower level of accuracy.
Assuming that the function associated with i’th defect is linear in time ( t
i
i
i
i
t
i
f 1
0
)
1
,
0
,
( 


 
 ), then TUDelft’s
model is defined in the following way:
 
R
i
i
j
T
i
f )
1
,
0
,
(
: 
 – theoretical function with two parameters, associated with i’th defect (number of
defects is 52)
 j
T – time since pipeline installation at j’th inspection
 j
i
d – unbiased depth of defect i, measured at j’th inspection
 i
w – nominal wall thickness where i’th defect was observed (two cases: 11.2 for 10 defects and 12.86
for 42 defects).
 4

m – total number of inspections
May 2007 PGT/Achterbosch, Grzelak/Determining corrosion rates/Page-4
 j
i
P, – measurement error density function of defect i1
observed at j’th inspection.
The likelihood estimation is optimal when the following function is maximized:
0
1
i
0
1
/
0
0
0
1
:
subject to
1
)
,
0
1
(
,
i
L
:
maximize


















i
i
i
w
i
m
T
i
m
j
j
i
d
i
j
T
i
j
i
P
Another advantage of the model is that the model also allows analysis of under/over estimation for a
certain groups of defects (clusters). The results of the corrosion rate obtained by the model are presented in
Figure 4. Because of the constraints, the model’s output is in harmony with the physical corrosion properties.
None of the corrosion rates are negative.
In the other two approaches, the corrosion rate distribution was normally distributed. But using the third
approach, it is quite different. There is no basis to reject the hypothesis that the corrosion rate is Beta distributed
(with parameters 1.25 and 3.92) (Figure 5). The model says that all the initiation times are in acceptable time
intervals. However, 16 of the defects initiate at the time of pipeline installation- this is indicated with a lighter
blue color in the picture above. The outcome of this is that the initiation time distribution is a composition of
two distributions, discrete in 0 and continuous elsewhere. The continuous part is also Beta distributed (with
parameters 1.60 and 0.50). A small summary of the results of the corrosion rate and the corrosion initiation time
are presented in Table 1.
As seen in Table 1, all the results obtained from the model are acceptable because they are physically
possible. The model derived at TUDelft, even for a bad dataset, gives reasonable and acceptable results. The
results show that the model gives a corrosion rate that is approximately 0.05 higher than the previous ones. The
reason for this is the following: in the previous cases, the result of corrosion rate was an outcome of all
corrosion rates (including negative values), which resulted in a lower average value.
Depth influence on the corrosion rate
In order to investigate whether the defects’ depths have a significant influence on the corrosion rate, the dataset
of 52 unbiased measurements is divided into two subsets. First, the average for each defect was calculated. The
weights were associated with the measurement errors’ standard deviations; i.e., an accurate pig has the highest
weight. Then, the dataset was divided into two subsets, namely “shallow” and “deep” defects, in such a way that
the MFL pig with the lowest number of observations had an equal number of measurements in both sets. The
TUDelft model was applied for both subsets.
The mean corrosion rate for deep defects turned out to be 0.25 mm/yr, and for shallower ones the rate is
0.23 mm/yr. However, statistically, there is no basis to reject the null hypothesis that these mean values are the
same. Hence, it follows that statistically the corrosion rates for deep and shallow defects are not significantly
different. The histograms of the rates for shallow and deep defects are presented in Figures 6 and 7. In both
cases (shallow and deep defects), there is no basis to reject the hypothesis that the corrosion rates are from a
beta distribution.
Although the number of measurements is equal in both subsets, the number of defects is not the same in
these two sets. The number of shallow defects, according to the presented criterion, is 34. The rest (18) are deep
defects. Analysis showed that if the set of unbiased measurements is divided in such a way that the number of
shallow and deep defects is equal in both subsets, it leads to the same conclusion that there is no significant
difference in corrosion rates.
1
A measurement error density function for each defect can depend on the cluster, from which the defect comes. I.e. one defect can have a few distributions- one per
individual cluster
May 2007 PGT/Achterbosch, Grzelak/Determining corrosion rates/Page-5
Conclusions
In order to determine reliably the bias for an MFL pigging device, it is crucial to have multiple reference defects
in the pipeline for which the dimensions are well known. These can then be used to calibrate the MFL reported
values. For the described pipeline, the number of available reference points was limited but still made it
possible to estimate the bias for every pig. It became clear that there are large differences between different
suppliers: the interpretation, clustering and sizing of defects give rise to numerous situations in which it is not
clear which supplier is right.
Because the measurement uncertainty of the MFL tool is dominant compared to the corrosion growth in
the time period between the pig runs, it is very difficult to determine a reliable corrosion rate per defect. But by
assuming a similar corrosion process (MIC) for each defect, based on evaluation of the MFL signals, historical
CP measurements and results of excavations, in combination with the assumption of a linear corrosion growth,
it was possible to calculate a realistic corrosion rate for this pipeline. Depending on the approach that was used,
a value for the average corrosion rate of 0.12 mm/yr (approach 1), 0.16 mm/yr (approach 2), or 0.24 mm/yr
(approach 3) was obtained. The numbers for the 95% upper bound values were respectively 0.20 mm/yr, 0.54
and 0.62 mm/yr.
For each of the reported defects of supplier A, it was estimated whether it was likely to be an MIC defect
or not. The experience of excavations, the specific pattern of MFL signals for MIC defects, and the clock
position of defects was used to make this decision on MIC likelihood. From the defects reported by supplier A,
it was estimated that 15% was probably not MIC. If we assume that this percentage also holds for the 52 defects
that resulted from the matching process, the conclusion is that the vast majority of defects in this line are
microbially influenced. Hence the corrosion rate is largely determined by this corrosion process. If we compare
this value to values that are often quoted for MIC, being 0.4 mm/yr or higher, this obtained value is in the lower
range. Informal contacts with other transmission companies that also have experience with external MIC
confirm the validity of this value.
The assumption that the corrosion process is linear was underpinned by the analyses of two subsets:
deep and shallow defects. For both subsets, a similar average corrosion rate was calculated: 0.23 mm/yr and
0.25 mm/yr. The difference is not significant.
Now that corrosion rates have been determined, Gasunie will have to decide how to use these values for
the calculation of a re-inspection interval for this line. The calculation will probably be done in a deterministic
way for every defect, taking into account measurement uncertainties and the uncertainty of the corrosion rate.
Another point to be addressed is the question of whether these values can be used for other lines as well.
Currently, an analysis on the results of 40 pig runs is performed to find out if other pipelines show similar
corrosion characteristics. For those lines that have a similar corrosion distribution, it seems realistic to use
similar corrosion rates for the calculation of re-inspection intervals.
Another interesting use for these corrosion rates is within Gasunie’s Direct Assessment (DA) program.
In this program, failure frequencies are calculated based on assumptions of corrosion distribution and corrosion
rates. Hence, reliable values for corrosion rates are paramount for the quality of this program.
Future work
Since the discovery of MIC, Gasunie has been searching for possibilities to establish a corrosion model for MIC
based on soil parameters. So far it has not been possible to identify the relevant parameters and correlate them
to the defect sizes. But it is striking that MIC often concentrates in certain parts of the pipeline (Figure 8) or in
certain parts of the Netherlands.
In the network, there is a certain area where two lines that are approximately 50 meters apart have
concentrations of MIC, within one kilometer. And on similar lines running at 300 meters parallel of those lines,
no MIC has been discovered. Recent efforts have been focused on this area to find out why these differences
exist. Indications suggest that very local soil differences may cause the difference in corrosion types. Last
summer, another eight excavations were performed on the pipeline in question. The information obtained on
corrosion types and defect sizes will be used to check the assumptions made so far, and to further calibrate the
May 2007 PGT/Achterbosch, Grzelak/Determining corrosion rates/Page-6
pig results.
Acknowledgments
The authors wish to acknowledge the efforts of their Gasunie colleagues, including Robbert van
der Scheer, Asim Saglam, Karine Kutrowski, Robert Kuik, Piet van Mastrigt, Wytze Sloterdijk, Paul Wesselius
and Eric Jager; and professors Roger M. Cooke, Professor Thomas A. Mazzuchi and Daniel Lewandowski of
TUDelft. Based on a paper presented at the ASME IPC 2006 International Pipeline Conference, September 25-
29, 2006, Calgary, Alberta, Canada.
(Figures)
Figure 1. Defect depth in time.
(was Figure 5)
Figure 2. Corrosion rate distribution.
(was Figure 6)
May 2007 PGT/Achterbosch, Grzelak/Determining corrosion rates/Page-7
Figure 3. Distribution of initiation time.
(was Figure 7)
Figure 4. Corrosion rate distribution for the third approach.
(was Figure 8)
May 2007 PGT/Achterbosch, Grzelak/Determining corrosion rates/Page-8
Figure 5. Distribution of initiation time for the third approach.
(was Figure 9)
Figure 6. Distribution of corrosion rates for shallow defects.
(was Figure 10)
May 2007 PGT/Achterbosch, Grzelak/Determining corrosion rates/Page-9
Figure 7. Distribution of corrosion rates for deep defects.
(was Figure 11)
Figure 8. Corrosion rates along the pipeline.
(was Figure 12)
(Tables)
Table 1. Corrosion rate and initiation time for the third approach.
Results
Corrosion
rate
Initiation
time
Mean
0.24
[mm/yr]
22.16
[yr]
95%conf.
intervals
Lower
bound
0.038 0 [yr]
Upper
bound
0.62 38.36 [yr]
(was Table 8)
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Determination of the corrosion rate of a mic influenced pipeline using four consecutive pig runs 2006

  • 1. See discussions, stats, and author profiles for this publication at: https://www.researchgate.net/publication/267598524 Determination of the Corrosion Rate of a MIC Influenced Pipeline Using Four Consecutive Pig Runs Conference Paper · January 2006 DOI: 10.1115/IPC2006-10142 CITATIONS 10 READS 466 2 authors, including: Some of the authors of this publication are also working on these related projects: Novel Methods in Computational Finance View project Computational Finance Course View project Lech Grzelak Delft University of Technology 64 PUBLICATIONS   565 CITATIONS    SEE PROFILE All content following this page was uploaded by Lech Grzelak on 15 November 2017. The user has requested enhancement of the downloaded file.
  • 2. May 2007 PGT/Achterbosch, Grzelak/Determining corrosion rates/Page-1 (Page caption) Pipeline integrity (Head) Determining corrosion rates (Deck) Gasunie uses data from pig runs and excavations to examine corrosion defects, determine corrosion rates. Giorgio G.J. Achterbosch, N.V. Nederlandse Gasunie, Groningen, The Netherlands; and Lech A. Grzelak, Delft University of Technology, Delft, The Netherlands In-line inspections have been part of Gasunie’s pipeline integrity verification efforts since the late 1970s. A few years ago, the discovery of external microbial corrosion (MIC) in one of the high-pressure pipelines changed the inspection policy from inspection of a randomly selected pipeline once every five years to an inspection program for the whole high-pressure grid (approximately 5,600 km, or 3,500 mi) to be completed in 10-12 years. One of the MIC-influenced lines is used to qualify MFL pigs from different suppliers. In the time period 1999-2004, four different MFL qualification runs were performed, resulting in 18 excavations. Corrosion rates that had been determined by rather simple calculations after every pig run indicated values of 0.2 to 0.3 mm/yr as an average value for the MIC corrosion. After the fourth pig run (five years after the first), Gasunie decided to determine the corrosion rate in a more sophisticated manner. Statistical analyses were performed in cooperation with the mathematical department of the Technical University of Delft. The goal was to use the data from pig runs and excavations to extract a suitable subset of corrosion defects, from which the corrosion rate could be determined. It was decided to use only those defects that were indicated by all suppliers as external corrosion, thereby leaving out defects that were indicated as “mill defect but possibly corrosion.” A second criterion was that a defect had to be reported by at least three of the four suppliers. These criteria resulted in a subset of 52 defects to be analyzed. All of the reported defect depths were corrected for the bias that was determined from the excavation results. The corrected values were then used to calculate the corrosion rate using three approaches. Two of these involved calculation of the corrosion rate for every defect; the third determined the corrosion rate for the pool of defects assuming a corrosion growth that is linear in time. The analysis was performed starting from the simplest to more sophisticated models. The first and the second approach were simply based on the unconstrained regression analysis. The third and last model was based on the unbiased measurements and pigs accuracy. The average corrosion rate for the defects was in the range of 0.12 to 0.24 mm/yr. Dividing the data set into deep and shallow defects showed that the average corrosion rates for both subsets, 0.23 mm/yr and 0.25 mm/yr, are not significantly different. This underpins one of the assumptions that the corrosion rate is constant. Inspections and excavations The N.V. Nederlandse Gasunie gas transportation network consists of approximately 11,600 km (roughly 7,200 mi) of steel pipelines (4 to 48-in. diameters) that was largely built in the mid-1960s and early 1970s. The network is split into a high-pressure part (5,600 km, 66-80 bar) and a medium-pressure part (600 km, 40 bar). While the high pressure network is piggable, the medium pressure part does not possess facilities to launch and receive intelligent pigs. Until 1999, Gasunie had no indications whatsoever that there was a corrosion problem on one of its pipelines. Both regular CP measurements as well as observations during excavations or reroutings indicated that no significant corrosion problem existed. Nevertheless, since 1979, company policy has been to verify pipeline
  • 3. May 2007 PGT/Achterbosch, Grzelak/Determining corrosion rates/Page-2 integrity periodically by running an intelligent pig through one of its high-pressure lines on average once every five years. The results of these pig runs confirmed the existing opinion that no corrosion problem existed. In 1999, a 70-km, 36-in. line in the north of the Netherlands was inspected by an MFL pig as part of the verification program. The results of the pig run indicated 65 external corrosion features but no internal corrosion. After a thorough defect assessment by the safety department, it was decided that six indications had to be excavated and repaired. The first excavation by the end of 1999 led to an unpleasant surprise. At the excavation, the appearance of the corrosion defect turned out to be totally different from the few corrosion defects that Gasunie had experienced in the past. Analysis of the corrosion products and the appearance of the defect led to the conclusion that the corrosion was influenced by sulphate reducing bacteria (SRBs). Similar experience was obtained at three other excavations. The conclusion was that at four out of the six excavations, there was evidence of microbially influenced corrosion (MIC). An additional excavation in 2000 showed also MIC. From the results, Gasunie concluded that it was no longer safe to assume that other lines were free of this corrosion problem. Therefore, the inspection policy was revised. It was decided to start an in-line inspection program for all high-pressure lines to be completed in a timeframe of approximately ten years. When starting the inspection program, the company realized that a reliable corrosion rate is paramount to determine a re- inspection time interval for its pipelines. As a consequence, a corrosion rate was calculated every time a new pig run was performed through the pipe. This was done by comparing the reported defect dimensions of supplier A to the reported dimensions of supplier B; and then A to C, and so one. But because of the relatively short time interval between the pig runs, the uncertainty of the reported defect dimensions is dominant and prevents the calculation of a reliable corrosion rate. Corrosion rates that were calculated using simple comparison of defects indicated average values of 0.2 to 0.3 mm/yr. But the standard deviation of these values was of the same order of magnitude or even larger. However, after the fourth pig run, which took place almost five years after the first run, Gasunie was of the opinion that it would be possible to determine the corrosion rate using more sophisticated statistical techniques. Because of long-standing relationship with the mathematical department of Delft Technical University, this department was asked to help analyze the available data using statistically sound techniques. First approach In the first approach, all the defects are pooled in one dataset, and no corrosion rate is calculated for individual defects but only for the dataset as a whole. The first step was to see if there was a basis to accept the hypothesis that the measurement errors for all MFL pigs are from the same population, and are normally distributed. This was the case. According to the maximum likelihood estimation for the measurement error, the parameters are 0 (mean) and 0.91 (for a standard deviation). If it is assumed that for all the errors, there is no correlation between them, then the task of finding a corrosion rate associated with all the measurements is equivalent to a Gauss Markov regression analysis. If it is also assumed that the corrosion rate is uniform over time (i.e., corrosion growth is linear), then an application of the Least Squares Error (LSE) method gives a linear description of the corrosion growth in the following form: t y 1 0 ˆ ˆ     . Standard calculations give that the estimators for unknown parameters are: 42 . 2 0 ˆ    and 12 . 0 1 ˆ   . Coefficient 1 ̂ is equivalent to the measurement of the corrosion rate (mm/yr), so the LSE model estimated a corrosion rate for the calibrated measurements of 0.12 mm/yr with 95% confidence interval (0.05, 0.20) (Figure 1). A determination coefficient was then calculated to see how well the model fit the data. A goodness of fit measure resulted in 04 . 0 2  R . This was not satisfactory, because it indicated that there was hardly a correlation between the two parameters. According to the model, the initiation time for corrosion is 20 years (years since pipeline installation). Even though the estimated parameters are in an acceptable range, this approach has significant drawbacks. Most notably, the model:
  • 4. May 2007 PGT/Achterbosch, Grzelak/Determining corrosion rates/Page-3  Does not distinguish defects  Does not take into account that some of the defects are improving in time (decreasing defect’s depth which is physically impossible), or for some the defects initiation time is before pipeline installation  the model assumes that all the defects have one corrosion rate Second approach As noted above, the first approach had significant drawbacks. The second approach proposes a way of dealing with some of the enumerated disadvantages. As before, it is assumed that corrosion growth is linear in time. The second model checks what the corrosion rate is, and analyzes the defects individually. That is, the model no longer assumes that there is only one corrosion rate for all the defects, but instead calculates a corrosion rate per defect. A simple regression analysis applied to each unbiased defect is depicted in Figure 2. From the histogram presented in Figure 2, it is clear that in many cases, simple regression analysis applied to each defect resulted in negative corrosion rates. The mean corrosion rate according to this model is 0.16 mm/yr, which is close to the result obtained before. However, the 95% confidence interval for the corrosion rate is quite different: -0.31, 0.54. The 95% confidence interval comprises negative values. The number of the defects indicating either negative corrosion rate or corrosion initiation time before the pipeline installation is 16. One way of dealing with a negative corrosion rate is to remove all the outliers from the dataset. However, such treatment is undesirable, since the dataset consists of 30% bad defects. Further investigation confirmed that the corrosion rate follows a normal distribution. The initiation time of the corrosion is presented in Figure 3, also in the form of a histogram. The red bars indicate an initiation time outside the interval determined by the time of pipeline installation (t=0 [yr]) and the time of the last inspection (t=44.25 [yr]). However, the Least Squares Errors approach produces negative corrosion rates or initiation times before pipeline installation. Therefore, an alternative model for the presented models was developed. This was the third approach. Third approach TUDelft constructed a model in such a way that the following constraints had to be met:  Corrosion rates had to be positive  Initiation time had to fall in the lifetime of the pipeline. The model was based on a maximum likelihood estimation, which was in turn based on measurement distributions for the function describing the corrosion growth in time. The model takes into account information about the measurement error distribution for each specific pig, and, according to these distributions, assigns weights to the measurements. Moreover, this model also takes into account the distributions obtained from the calibration procedure. These distributions are used in order to assign weights to the pigs in such a way that the pig with the smallest level of uncertainty (smallest standard deviation for the error distribution) will get the highest weight. So it is natural that a pig which is accurate will influence the final results much more than a pig with a lower level of accuracy. Assuming that the function associated with i’th defect is linear in time ( t i i i i t i f 1 0 ) 1 , 0 , (       ), then TUDelft’s model is defined in the following way:   R i i j T i f ) 1 , 0 , ( :   – theoretical function with two parameters, associated with i’th defect (number of defects is 52)  j T – time since pipeline installation at j’th inspection  j i d – unbiased depth of defect i, measured at j’th inspection  i w – nominal wall thickness where i’th defect was observed (two cases: 11.2 for 10 defects and 12.86 for 42 defects).  4  m – total number of inspections
  • 5. May 2007 PGT/Achterbosch, Grzelak/Determining corrosion rates/Page-4  j i P, – measurement error density function of defect i1 observed at j’th inspection. The likelihood estimation is optimal when the following function is maximized: 0 1 i 0 1 / 0 0 0 1 : subject to 1 ) , 0 1 ( , i L : maximize                   i i i w i m T i m j j i d i j T i j i P Another advantage of the model is that the model also allows analysis of under/over estimation for a certain groups of defects (clusters). The results of the corrosion rate obtained by the model are presented in Figure 4. Because of the constraints, the model’s output is in harmony with the physical corrosion properties. None of the corrosion rates are negative. In the other two approaches, the corrosion rate distribution was normally distributed. But using the third approach, it is quite different. There is no basis to reject the hypothesis that the corrosion rate is Beta distributed (with parameters 1.25 and 3.92) (Figure 5). The model says that all the initiation times are in acceptable time intervals. However, 16 of the defects initiate at the time of pipeline installation- this is indicated with a lighter blue color in the picture above. The outcome of this is that the initiation time distribution is a composition of two distributions, discrete in 0 and continuous elsewhere. The continuous part is also Beta distributed (with parameters 1.60 and 0.50). A small summary of the results of the corrosion rate and the corrosion initiation time are presented in Table 1. As seen in Table 1, all the results obtained from the model are acceptable because they are physically possible. The model derived at TUDelft, even for a bad dataset, gives reasonable and acceptable results. The results show that the model gives a corrosion rate that is approximately 0.05 higher than the previous ones. The reason for this is the following: in the previous cases, the result of corrosion rate was an outcome of all corrosion rates (including negative values), which resulted in a lower average value. Depth influence on the corrosion rate In order to investigate whether the defects’ depths have a significant influence on the corrosion rate, the dataset of 52 unbiased measurements is divided into two subsets. First, the average for each defect was calculated. The weights were associated with the measurement errors’ standard deviations; i.e., an accurate pig has the highest weight. Then, the dataset was divided into two subsets, namely “shallow” and “deep” defects, in such a way that the MFL pig with the lowest number of observations had an equal number of measurements in both sets. The TUDelft model was applied for both subsets. The mean corrosion rate for deep defects turned out to be 0.25 mm/yr, and for shallower ones the rate is 0.23 mm/yr. However, statistically, there is no basis to reject the null hypothesis that these mean values are the same. Hence, it follows that statistically the corrosion rates for deep and shallow defects are not significantly different. The histograms of the rates for shallow and deep defects are presented in Figures 6 and 7. In both cases (shallow and deep defects), there is no basis to reject the hypothesis that the corrosion rates are from a beta distribution. Although the number of measurements is equal in both subsets, the number of defects is not the same in these two sets. The number of shallow defects, according to the presented criterion, is 34. The rest (18) are deep defects. Analysis showed that if the set of unbiased measurements is divided in such a way that the number of shallow and deep defects is equal in both subsets, it leads to the same conclusion that there is no significant difference in corrosion rates. 1 A measurement error density function for each defect can depend on the cluster, from which the defect comes. I.e. one defect can have a few distributions- one per individual cluster
  • 6. May 2007 PGT/Achterbosch, Grzelak/Determining corrosion rates/Page-5 Conclusions In order to determine reliably the bias for an MFL pigging device, it is crucial to have multiple reference defects in the pipeline for which the dimensions are well known. These can then be used to calibrate the MFL reported values. For the described pipeline, the number of available reference points was limited but still made it possible to estimate the bias for every pig. It became clear that there are large differences between different suppliers: the interpretation, clustering and sizing of defects give rise to numerous situations in which it is not clear which supplier is right. Because the measurement uncertainty of the MFL tool is dominant compared to the corrosion growth in the time period between the pig runs, it is very difficult to determine a reliable corrosion rate per defect. But by assuming a similar corrosion process (MIC) for each defect, based on evaluation of the MFL signals, historical CP measurements and results of excavations, in combination with the assumption of a linear corrosion growth, it was possible to calculate a realistic corrosion rate for this pipeline. Depending on the approach that was used, a value for the average corrosion rate of 0.12 mm/yr (approach 1), 0.16 mm/yr (approach 2), or 0.24 mm/yr (approach 3) was obtained. The numbers for the 95% upper bound values were respectively 0.20 mm/yr, 0.54 and 0.62 mm/yr. For each of the reported defects of supplier A, it was estimated whether it was likely to be an MIC defect or not. The experience of excavations, the specific pattern of MFL signals for MIC defects, and the clock position of defects was used to make this decision on MIC likelihood. From the defects reported by supplier A, it was estimated that 15% was probably not MIC. If we assume that this percentage also holds for the 52 defects that resulted from the matching process, the conclusion is that the vast majority of defects in this line are microbially influenced. Hence the corrosion rate is largely determined by this corrosion process. If we compare this value to values that are often quoted for MIC, being 0.4 mm/yr or higher, this obtained value is in the lower range. Informal contacts with other transmission companies that also have experience with external MIC confirm the validity of this value. The assumption that the corrosion process is linear was underpinned by the analyses of two subsets: deep and shallow defects. For both subsets, a similar average corrosion rate was calculated: 0.23 mm/yr and 0.25 mm/yr. The difference is not significant. Now that corrosion rates have been determined, Gasunie will have to decide how to use these values for the calculation of a re-inspection interval for this line. The calculation will probably be done in a deterministic way for every defect, taking into account measurement uncertainties and the uncertainty of the corrosion rate. Another point to be addressed is the question of whether these values can be used for other lines as well. Currently, an analysis on the results of 40 pig runs is performed to find out if other pipelines show similar corrosion characteristics. For those lines that have a similar corrosion distribution, it seems realistic to use similar corrosion rates for the calculation of re-inspection intervals. Another interesting use for these corrosion rates is within Gasunie’s Direct Assessment (DA) program. In this program, failure frequencies are calculated based on assumptions of corrosion distribution and corrosion rates. Hence, reliable values for corrosion rates are paramount for the quality of this program. Future work Since the discovery of MIC, Gasunie has been searching for possibilities to establish a corrosion model for MIC based on soil parameters. So far it has not been possible to identify the relevant parameters and correlate them to the defect sizes. But it is striking that MIC often concentrates in certain parts of the pipeline (Figure 8) or in certain parts of the Netherlands. In the network, there is a certain area where two lines that are approximately 50 meters apart have concentrations of MIC, within one kilometer. And on similar lines running at 300 meters parallel of those lines, no MIC has been discovered. Recent efforts have been focused on this area to find out why these differences exist. Indications suggest that very local soil differences may cause the difference in corrosion types. Last summer, another eight excavations were performed on the pipeline in question. The information obtained on corrosion types and defect sizes will be used to check the assumptions made so far, and to further calibrate the
  • 7. May 2007 PGT/Achterbosch, Grzelak/Determining corrosion rates/Page-6 pig results. Acknowledgments The authors wish to acknowledge the efforts of their Gasunie colleagues, including Robbert van der Scheer, Asim Saglam, Karine Kutrowski, Robert Kuik, Piet van Mastrigt, Wytze Sloterdijk, Paul Wesselius and Eric Jager; and professors Roger M. Cooke, Professor Thomas A. Mazzuchi and Daniel Lewandowski of TUDelft. Based on a paper presented at the ASME IPC 2006 International Pipeline Conference, September 25- 29, 2006, Calgary, Alberta, Canada. (Figures) Figure 1. Defect depth in time. (was Figure 5) Figure 2. Corrosion rate distribution. (was Figure 6)
  • 8. May 2007 PGT/Achterbosch, Grzelak/Determining corrosion rates/Page-7 Figure 3. Distribution of initiation time. (was Figure 7) Figure 4. Corrosion rate distribution for the third approach. (was Figure 8)
  • 9. May 2007 PGT/Achterbosch, Grzelak/Determining corrosion rates/Page-8 Figure 5. Distribution of initiation time for the third approach. (was Figure 9) Figure 6. Distribution of corrosion rates for shallow defects. (was Figure 10)
  • 10. May 2007 PGT/Achterbosch, Grzelak/Determining corrosion rates/Page-9 Figure 7. Distribution of corrosion rates for deep defects. (was Figure 11) Figure 8. Corrosion rates along the pipeline. (was Figure 12) (Tables) Table 1. Corrosion rate and initiation time for the third approach. Results Corrosion rate Initiation time Mean 0.24 [mm/yr] 22.16 [yr] 95%conf. intervals Lower bound 0.038 0 [yr] Upper bound 0.62 38.36 [yr] (was Table 8) View publication stats View publication stats