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Water repellency & Waterproof
Breathable Fabrics and repellency test
method
Water repellency
Water repellent is a state characterized by the non-
spreading of water globules on a textile material.This
term is not normally applied to a water-repellent finish
impervious to air.This is generally referred to as water
proof. It is generally done by treated fabric with fat,
wax, rubber etc.
14/3/2014 Vignesh Dhanabalan (M.Tech) - vigneshdhanabalan@hotmail.com
Requirements of Water Repellency
Textiles
Purpose and Scope
• This method of test is especially suitable for screening if
any textile has been given a water-repellency finishes. It
is not intended for use in measuring the penetration of
water through the fabric.
Terminology
• Water Repellency: in textiles, the characteristic of a fiber,
yarn or fabric to resist wetting
14/3/2014 Vignesh Dhanabalan (M.Tech) - vigneshdhanabalan@hotmail.com
Water Repellency Classification
Grade Classification
100 (ISO5 ) Excellent
90 (ISO 4) Very Good
80 (ISO 3) Good
70 (ISO 2) - ---
50 (ISO 1) - ---
0 ----
14/3/2014 Vignesh Dhanabalan (M.Tech) - vigneshdhanabalan@hotmail.com
Principles of moisture vapor transfer:
Absorption, transmition and desorption of
the water vapor by the fibers.
Diffusion of the water vapor through the air
spaces between the fibers.
Transmition of water vapor by forced
convection
Capillary pressure and capillary raise are determined using
P = 2γLV cos  / Rc , L = ((Rcγ cos /2)* t1/2
P = capillary pressure L = liquid pressure
Rc – capillary radius t and  - time and viscosity
Transport Mechanism:
Capillary’s diameter and surface energy
Properties required for breathable fabrics:
Soft feel, light weight and Durable
Easy care/launderability
Rapid drying to prevent
catching cold.
Good air and water vapor permeability.
Rapid moisture absorption and conveyance capacity
Optimum heat and
moisture regulation
(thermo-regularity
effect)
Absorption of
surplus heat.
Dimensionally stable even when
comes in contact to water
No/Minimum water
absorption of the layer of
clothing just positioned to
the skin.
Producing breathable fabrics:
Smart Breathable fabrics (PCP)
SMP – PU material Micro porous Membrane
Densely Woven Fabric
(Micro denier<10 micron)
Closely woven fabrics
(oxford weave) up to 20 min
Various methods for
generating microspores
membrane and coating:
•Mechanical fibrillation (Film) - PTFE films – biaxial stretched- negative poissons
ratio - 50– 400 µm – crystallinity of polymer >98% - 9 billion pores /inch2 -
•Wet coagulation - ultrafine pores < 1µm – salt leaching - Requires Precise
control below 3 µm.
•Thermo coagulation - volatile solvent - PU dissolved in methyl ethyl ketone,
toluene, and water, having 15–20% solid
•Foam coating - fluorocarbon (FC) polymer, PU coating – soft n flexible - abrasion
•Radio frequency (RF)/ion/UV or E beaming - Sputtering ofTeflon by Ar gas
Application of Polyurethane coating:
• Pore dia of 0.0004 µm possible
•PU-based film designed (Permatex) by J.B. Broadley coated on fabrics offers a
vapor permeability of at least 70%.
•Grabotter membrane (Grabo Ltd.) used in waterproof shoes is a PU-based film.
•Micro porous PU film is being produced by Acordis (Tarka) is applied by a
transfer process from the release paper and it can be applied to almost any type
of substrate.
Knife coating
Floating knife
Extrusion
Calendaring
Curtain coating
Gurave coating
Reverse roll
Testing of Breathability of Fabrics using different techniques:
S.no Methodology Standard Purpose
1 Sweating Guarded Hot Plate
Tests
(ISO 11092, ISO
1999, and ASTM F
1868)
Measurement of thermal and water-vapor resistance under
steady-state conditions
2 Upright Cup Method ASTM E96 Water Vapor Transmission of Materials , permeability,
plastics (general), plastic sheet and film, sheet material3 Inverted Cup Method ASTM E96
4 Desiccant Inverted Cup Test
Method
E96 M-05
5 Dynamic Moisture
Permeation Cell Test
ASTM F 2298
Standard Test Methods for Water Vapor Diffusion
Resistance and Air Flow Resistance of Clothing Materials
Using the Dynamic Moisture Permeation
6 Moisture vapor transmition
cell
ASTM D1653 - 13 Moisture vapor transmition behavior of fabric
7 Dynamic moisture
permeable cell
ASTM F2298-
03(2009) e1
Moisture transmition capability of cell
Relative water vapor permeability (%):
Heat loss when the fabric is placed on the measuring head X 100
Heat loss from bare measuring head
The main requirements for WVPI are based on
•Water vapor permeability index percentage.
•Resistance to water penetration.
•Cold cracking temperature.
•Surface wetting (spray rating) after cleaning.
For a typical breathable fabric the acceptable parameters should have
•Water-vapor permeability (min 5000gm-2 for 24 hrs)
•Water proofness min 130 cm (hydrostatic pressure)
•Wind proofness less than 1.5 ml/cm2/second @ 1M bar
Water Proof rating:
Waterproof Rating
(mm)
Resistance provided Withstand capabilities
0-5,000 mm
No resistance to some resistance
to moisture
Light rain, dry snow, no pressure
6,000-10,000 mm
Rainproof and waterproof under
light pressure
Light rain, average snow, light pressure
11,000-15,000 mm
Rainproof and waterproof except
under high pressure
Moderate rain, average snow, light pressure
16,000-20,000 mm
Rainproof and waterproof under
high pressure
Heavy rain, wet snow, some pressure
20,000 mm+
Rainproof and waterproof under
very high pressure
Heavy rain, wet snow, high pressure
For example : 10000/10000 – First number represents water proofness of fabric and
second number represents breathability of the fabric. Higher the value better is the result
Application
3M incise tape 9948Neo-G knee support
Breathable snow protect
mountain wear
Fire man
Protective
Apparel
Racer Suite
Ventile Roofing Membrane
Somatex Casing layer
14/3/2014
Conclusion:
• Comfort property has become the most prime objective of the
buyer/consumer where breathability of the fabric with water
proofness has been the primary importance in areas that do not
enjoy the evergreen nature.
• Extensive research is required to understand the relationship
between segmental ventilation and local comfort of the fabric
subjected to active usage of the person.
Thanks to all.

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Water Repellency & Breathable Fabrics Test Methods

  • 1. Water repellency & Waterproof Breathable Fabrics and repellency test method
  • 2. Water repellency Water repellent is a state characterized by the non- spreading of water globules on a textile material.This term is not normally applied to a water-repellent finish impervious to air.This is generally referred to as water proof. It is generally done by treated fabric with fat, wax, rubber etc. 14/3/2014 Vignesh Dhanabalan (M.Tech) - vigneshdhanabalan@hotmail.com
  • 3. Requirements of Water Repellency Textiles Purpose and Scope • This method of test is especially suitable for screening if any textile has been given a water-repellency finishes. It is not intended for use in measuring the penetration of water through the fabric. Terminology • Water Repellency: in textiles, the characteristic of a fiber, yarn or fabric to resist wetting 14/3/2014 Vignesh Dhanabalan (M.Tech) - vigneshdhanabalan@hotmail.com
  • 4. Water Repellency Classification Grade Classification 100 (ISO5 ) Excellent 90 (ISO 4) Very Good 80 (ISO 3) Good 70 (ISO 2) - --- 50 (ISO 1) - --- 0 ---- 14/3/2014 Vignesh Dhanabalan (M.Tech) - vigneshdhanabalan@hotmail.com
  • 5. Principles of moisture vapor transfer: Absorption, transmition and desorption of the water vapor by the fibers. Diffusion of the water vapor through the air spaces between the fibers. Transmition of water vapor by forced convection
  • 6. Capillary pressure and capillary raise are determined using P = 2γLV cos  / Rc , L = ((Rcγ cos /2)* t1/2 P = capillary pressure L = liquid pressure Rc – capillary radius t and  - time and viscosity Transport Mechanism: Capillary’s diameter and surface energy
  • 7. Properties required for breathable fabrics: Soft feel, light weight and Durable Easy care/launderability Rapid drying to prevent catching cold. Good air and water vapor permeability. Rapid moisture absorption and conveyance capacity Optimum heat and moisture regulation (thermo-regularity effect) Absorption of surplus heat. Dimensionally stable even when comes in contact to water No/Minimum water absorption of the layer of clothing just positioned to the skin.
  • 8. Producing breathable fabrics: Smart Breathable fabrics (PCP) SMP – PU material Micro porous Membrane Densely Woven Fabric (Micro denier<10 micron) Closely woven fabrics (oxford weave) up to 20 min
  • 9. Various methods for generating microspores membrane and coating: •Mechanical fibrillation (Film) - PTFE films – biaxial stretched- negative poissons ratio - 50– 400 µm – crystallinity of polymer >98% - 9 billion pores /inch2 - •Wet coagulation - ultrafine pores < 1µm – salt leaching - Requires Precise control below 3 µm. •Thermo coagulation - volatile solvent - PU dissolved in methyl ethyl ketone, toluene, and water, having 15–20% solid •Foam coating - fluorocarbon (FC) polymer, PU coating – soft n flexible - abrasion •Radio frequency (RF)/ion/UV or E beaming - Sputtering ofTeflon by Ar gas
  • 10. Application of Polyurethane coating: • Pore dia of 0.0004 µm possible •PU-based film designed (Permatex) by J.B. Broadley coated on fabrics offers a vapor permeability of at least 70%. •Grabotter membrane (Grabo Ltd.) used in waterproof shoes is a PU-based film. •Micro porous PU film is being produced by Acordis (Tarka) is applied by a transfer process from the release paper and it can be applied to almost any type of substrate. Knife coating Floating knife Extrusion Calendaring Curtain coating Gurave coating Reverse roll
  • 11. Testing of Breathability of Fabrics using different techniques: S.no Methodology Standard Purpose 1 Sweating Guarded Hot Plate Tests (ISO 11092, ISO 1999, and ASTM F 1868) Measurement of thermal and water-vapor resistance under steady-state conditions 2 Upright Cup Method ASTM E96 Water Vapor Transmission of Materials , permeability, plastics (general), plastic sheet and film, sheet material3 Inverted Cup Method ASTM E96 4 Desiccant Inverted Cup Test Method E96 M-05 5 Dynamic Moisture Permeation Cell Test ASTM F 2298 Standard Test Methods for Water Vapor Diffusion Resistance and Air Flow Resistance of Clothing Materials Using the Dynamic Moisture Permeation 6 Moisture vapor transmition cell ASTM D1653 - 13 Moisture vapor transmition behavior of fabric 7 Dynamic moisture permeable cell ASTM F2298- 03(2009) e1 Moisture transmition capability of cell
  • 12. Relative water vapor permeability (%): Heat loss when the fabric is placed on the measuring head X 100 Heat loss from bare measuring head The main requirements for WVPI are based on •Water vapor permeability index percentage. •Resistance to water penetration. •Cold cracking temperature. •Surface wetting (spray rating) after cleaning. For a typical breathable fabric the acceptable parameters should have •Water-vapor permeability (min 5000gm-2 for 24 hrs) •Water proofness min 130 cm (hydrostatic pressure) •Wind proofness less than 1.5 ml/cm2/second @ 1M bar
  • 13. Water Proof rating: Waterproof Rating (mm) Resistance provided Withstand capabilities 0-5,000 mm No resistance to some resistance to moisture Light rain, dry snow, no pressure 6,000-10,000 mm Rainproof and waterproof under light pressure Light rain, average snow, light pressure 11,000-15,000 mm Rainproof and waterproof except under high pressure Moderate rain, average snow, light pressure 16,000-20,000 mm Rainproof and waterproof under high pressure Heavy rain, wet snow, some pressure 20,000 mm+ Rainproof and waterproof under very high pressure Heavy rain, wet snow, high pressure For example : 10000/10000 – First number represents water proofness of fabric and second number represents breathability of the fabric. Higher the value better is the result
  • 14. Application 3M incise tape 9948Neo-G knee support Breathable snow protect mountain wear Fire man Protective Apparel Racer Suite Ventile Roofing Membrane Somatex Casing layer 14/3/2014
  • 15. Conclusion: • Comfort property has become the most prime objective of the buyer/consumer where breathability of the fabric with water proofness has been the primary importance in areas that do not enjoy the evergreen nature. • Extensive research is required to understand the relationship between segmental ventilation and local comfort of the fabric subjected to active usage of the person.