In this presentation, you will be familiar with VSM and Magnetic characterization of materials, especially ferromagnetic materials via their magnetic hysteresis loop.
3. VSM & Hysteresis Loop 3
Magnet Poles
Loudspeaker
assembly
Oscillating Sample
Sample coils
Fig. 2- VSM magnetic setup.
4. VSM & Hysteresis Loop 4
𝐵 = 𝜇0(𝐻 + 𝑀)
H
B
Magneticinduction
Field strenght
H
M
Magnetization
Fig.3- B-H and M-H curves.
5. VSM & Hysteresis Loop 5
Fig 4- Net magnetization (M), the averaged sum of many individual quantum spins, can
be treated as a regular vector in classical physics.
𝑀 =
𝑑𝑚
𝑑𝑉
7. VSM & Hysteresis Loop 7
Fig. 6- Microcrystalline grains within a piece of Nd2Fe14B (the alloy used in neodymium
magnets) with magnetic domains made visible with a Kerr microscope.
8. VSM & Hysteresis Loop 8
Fig. 7- Magnetization of domains in an applied magnetic field.
9. VSM & Hysteresis Loop 9
Fig. 8- Domain growth and rotation in a ferromagnetic material and the associated
magnetization curve M versus H.
10. VSM & Hysteresis Loop 10
Fig. 9- Typical magnetization curves of
(a) a diamagnetic;
(b) a paramagnetic or antiferromagnetic; and
(c) a ferromagnetic of ferrimagnetic.
11. VSM & Hysteresis Loop 11
Fig. 10- A typical hysteresis loop of ferromagnetic material.
Hysteresis
loop
Saturation
Magnetization
The
Coercivity
The
Remanence
𝜇′ 𝑚𝑎𝑥
The
Hysteresis
Loss
Initial
permiability
…
12. VSM & Hysteresis Loop 12
Fig. 11- Initial curve and saturation magnetization of a typical hysteresis loop.
Saturation magnetization
Initial state
13. VSM & Hysteresis Loop 13
Fig. 12- Remanent magnetization of a typical hysteresis loop.
The remanent
14. VSM & Hysteresis Loop 14
Fig. 13- The coercivity of a typical hysteresis loop of ferromagnetic material.
The Coercivity
16. VSM & Hysteresis Loop 16
Fig. 15- Work required to saturate a unit volume of ferromagnetic material.
17. VSM & Hysteresis Loop 17
Fig. 16- Demagnetizing curve of a permanent magnet.
18. VSM & Hysteresis Loop 18
Fig. 17- The power, or energy, required to demagnetize the permanent
magnet.
19. VSM & Hysteresis Loop 19
Fig. 18- The fourth quadrant of the B-H
curve for a permanent magnetic material.
20. VSM & Hysteresis Loop 20
Fig. 19- Squareness of a Hysteresis loop.
21. VSM & Hysteresis Loop 21
12.5 Oe
125 Oe Hard Magnetic materials
Soft Magnetic materials
Fig. 20- schematic reprensatation of soft and hard ferromagnetic materials.
22. VSM & Hysteresis Loop 22
Fig. 21- Dependdence of the hysteresis loop of iron or steel on hardness caused by the addition of
carbon.
23. VSM & Hysteresis Loop 23
Fig. 22- Anhystertic magnetization curve
The
magnetization
curve would
therefore be
reversible.
30. VSM & Hysteresis Loop 30
Fig. 28- Schematic reprensatation of the Barkhausen effect.
Microstructure of the material
and
Stress
31. VSM & Hysteresis Loop 31
Fig. 29- The effect of temperature on (a) the hysteresis loop and (b) the
remenance
Remanence is zero.
32. VSM & Hysteresis Loop 32
Fig. 30–Influence of temperature on the hysteresis loops near
the transition point (Tc=300k).
33. VSM & Hysteresis Loop 33
Fig. 31–Hysteresis loops at different temperatures in
a) sample No1-Fe3.9Co64.82B10.2Si12Cr9Mo0.08 (Tc=61.5 ℃) and
b) sample No2- Fe5Co27.4B12.26Si12.26Ni43.08 (Tc= 48 ℃).
34. VSM & Hysteresis Loop 34
Fig. 32–Magnetization of Gd5Si2Ge2 measured from the low temperature
FM phase to the high temperature PM phase.
35. VSM & Hysteresis Loop 35
Table 1- Curie temperature of some materials
36. VSM & Hysteresis Loop 36
Fig. 33-Effect of the tensile stress on the hysteresis loop of the amorphous
Co71Fe5B11Si10Cr3 microwire in a glass shell.