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MM SCIENCE JOURNAL I 2018 I MARCH
2128
THE POSITION OF THE
JOINTS WITH ANGLE OF
900
AT FRICTION STIR
WELDING (FSW)
WIDIA SETIAWAN1,2, DJAROT B. DARMADI2,
WAHYONO SUPRAPTO2, RUDY SOENOKO2
1 Sekolah Vokasi of Gadjah Mada University,
Yogyakarta, Indonesia
2 University Brawijaya
Malang, Indonesia
DOI : 10.17973/MMSJ.2018_03_201717
e-mail: widia_s@.ugm.ac.id
widia_setiawan64@yahoo.co.id
This research was use aluminum 6061 with 150 mm
length, 50 mm wide, and 10 mm thick. The probe was
made from EMS 45 simple design. Three variations used
of feedrate speed is 10 mm/min, 15 mm/min, and 30
mm/min. Spindle rotation constantly set 2000 rpm, the
heat generated was recorded. Corner-Butt (C-B)joint
determined, the lowest heat generated from 2200C-
3200C and the tensile test was60 MPa. The highest
tensile testwas 163 MPa, achieved by Corner-butt 45 (C-
B 45) joint on 10 mm/min feedrate speed. It was verified
by the heat temperature from 3000C-4200C and clarified
by its micro and macrostructure.
KEYWORDS
Friction Stir Welding, Corner-Butt Joint 450, Corner –
Butt, Feedrate, Aluminum 6061
1. INTRODUCTION
Discovered and patented a solid state welding technique
called friction stir welding (FSW). Solid welding is an easy
welding method to combine metals without requiring
any particular skill [Thomas 1991].This kindof welding
does not require high heat nor feeder electrode.
Thistechnique would eliminate the porosity andpresent
homogenous microstructure and phase. Moreover,
residual stresses are also low. Heat is generated from
friction between the cut surface and the probe[Thomas
1991].
[Mortensen 2011] States that in FSW, the heat is
generated from the spindle rotation and the
joiningoccurs because of the radial force toward the
axial direction. The higher the pressure, the more heat is
generated. Such condition will greatly influence the
result of the welding and affect the material’s mechanic
state.[Ozekcin 2004] says that FSW is a welding method
for two Ferro or non-Ferro metals without liquefication
and can be done with or without pressure. FSW does
not alter the basic characteristics of the metals and is
often performed to aluminum that does not endure post
weld heat treatment (PWHT)
In performing FSW, according to [Cao 2005], the
spinning probe is pressed and penetrated onto the work-
piece’s surface. The friction then generates heat,
therefore connecting the welded materials. [Malarvizhi
2013] has proved that the heat in FSW technique is
influenced by the probe’s diameter. Its size will affect
the formation of micro structure, macro structure, and
the tensile strength on the dissimilar metals welding
between Al 6061 dan AZ 31 Magnesium.
The successfulness of the welding is determined by the
heat generated from the friction between the probe and
the work-piece. The shoulder’s and pin’s diameter of the
probe hold a significant role in generating heat. The
amount of heat generated also depends on the spindle
rotation speed of theuniversal milling machine. The
material correspondingly contributes in generating heat.
According to [Xiong 2013], the steady state
heatgeneratin the plastic state is formulated below.
...............................................1
k = material’s thermal conductivity,
d2T/dx2 = temperature gradient,
q = generated heat, Cp = heat coefficient,
and vdt/dx = speed gradient
According to [Manvatkar 2014], the heat in the peak
temperature and average cooling values are formulated
as follow
Q = x
+
3 .................................................2
τ = shear stress (Kg/mm2), µ= friction coefficient,
P = axial force (Kg), ω =
Shoulder radius (mm), = pin radius =
pin length (mm).
During the welding process, the heat is generated from
the friction by the probe that spins on the work-piece
which eventually creates plastic state compound. This
state can be observed in the thermomechanically
affected zone (TMAZ) [Nandan 2008].
FSW is a current technique in joining aluminum without
feeder electrode required. The heat is generated from
the rotation of welding tool which results in deformation
in the welding area. This joining process is called solid
welding. [Padgett 2003]. FSW can be applied in similar or
dissimilar metals with more efficient result, whereas
liquid welding may cause hot cracking, blow holes, and
distortion [ Kazi 2001, McNelley 2008].
[Silva 2014] concludes that key featureson T- Joint FSW
optimization are 1000 rpm rotation speed, 15 mm
shoulder diameter, 3.9 mm aluminum thickness, and 2.5
MM SCIENCE JOURNAL I 2018 I MARCH
2129
as the ratio value between the pin and shoulder
diameter. The welding speed apparently gives no
significant effect to the mechanic state of FSW joint. The
joining of aluminum with combination of T-Lap Joint and
T-Butt Joint models can be performed with the use of
specific clamping design [Zhao 2013].
Similar experiment by joining aluminum with 3 kinds of
joint model, which are T-lap, T-Butt-Lap, and T-Double-
Butt Joint with specific clamping design.FSW with T joint
is basically performed by pressing the probe onto the
work-piece then moving it toward the welding zone with
particular speed. T-joints can be applied in many
structures as in high pressure container support, bridges
sustainer, and many more. If the T-joints are welded
with liquid welding technique, the residual stress will be
massive and the distortion will occur. Although such
distortion can be minimized with particular heat
treatments, the time and cost required will increase. The
micro structure formed in the nugget zone is soft. That
soft tone area can be expanded if the probe rotation
speed is increased and the travelling speed is decreased
[Cui 2012]. T-joints aluminum welding is essential for
means of transportation such as planes, ships, and car
seats and body structure as well as bridges structure and
high pressure container. T-joint possesses well physical
formwith firm and strong structureas its advantage [Hou
2013].
This research observed Friction Stir welding (FSW) on
aluminum 6061 with the dimension of 150 mm length,
50 mm wide, and 10 mm thick with 450 cut on the edge.
The joints variation applied areCorner-Butt 450 Joint,
andCorner-Butt Joint. The traveling speed varied from 10
mm/min, 15 mm/min, and 30 mm/min with 2000 rpm
probe rotation speed. From the result of experiments
with those variations, the correlation between micro
structure, hardness level, and generated heat were then
analyzed to measure the highest tensile stress score.
2. EXPERIMENTAL PROCEDURES
Compositions Mg Si Cu Mn Fe Cr Ti Zn Al
Content 0.9 0.6 0.25 0.086 0.18 0.1 0.192 0.01 Bal
Table 1. Chemical composition of 6061 aluminum alloy (wt.%)
The aluminum 6061 as the object of this research
contain chemical substance as described in Tab. 1. The
aluminum’s edgewas milled to form 450corner. The
probe was made from hardened EMS 45 with simple
design.
In Fig. 1 is explained, Before welded, the aluminum was
perforated. There were 16 holes, each was at the
distance of 20 mm with another. These holes were used
to place the thermocouple to measure the temperature
using acquisition data.
The temperature distribution measuring at some point
will get a picture of aluminum plastics which will affect
the quality of the connection, this is as will be done in
Fig. 1.
10
20 60
20
150 10
Figure 1. Before welded, the aluminum 6061wasPerforated
Corner-Butt Joint 10 mm/min Corner-Butt 45 Joint 10 mm/min
15 mm/min 15 mm/min
30 mm/min 30 mm/min
Table 2. Joint and traveling speed varied
MM SCIENCE JOURNAL I 2018 I MARCH
2130
Parameter 10 mm/min 15 mm/min 30 mm/min Material study
C-B 45
C-B
Table 3. Welding macrostruckture result
3. RESULT AND DISCUSSION
3.1. Micro structure
Corner-Butt 45 Joint (C-B 45), the micro structure
displays ideal, homogenous blend because the pin probe
could generate sufficient heat in all feedrate speeds to
form plastic state compound around the welding area.
Therefore, the joint could be welded with satisfying
result with 4000 C temperature around the welding
zone(Fig.6). Black spots contained in Fig. 6, is a mix of
ferro the pin probe and material aluminum 6061. This
can be evidenced by increased wear of the probe pin,
pin length and diameter of the pin, and will cause the
connection to be strong.
The feedrate 10 mm/min slurry more perfect, visible
from the slurry flow is shown on the microstructure, and
the black spots more. While at feedrate 15 mm/min
spots that occur more and more visible in the image of
the microstructure occurring point 3.Corner-Butt Joint
(C-B) provides homogenous micro structure and
ubiquitous compound around the welding zone. The pin
probe could properly merge the materials in this type of
joint. The shoulder could generate enough heat to form
plastic state on the welding zone and heat loss could be
reduced. Fig. 2. describes such condition visually. Feed
rate of 15 mm/min mixing that occurs is clearly visible
(Fig. 2). plastically perfect condition it will cause the
connection will be better.
To be concluded, the micro structure on C-B 45and C-B
joints are more satisfactory compared to the other
joints. In these joints, the heat generated could create
wider plastic state compound. The pin probe could also
worked at its finestin those joints and the pressure from
the shoulder could provide constructive support in
stirring the materials. Those factors backed up the
satisfying results of the FSW in these joints.
Corner-Butt 45 Joint (C-B 45)
123 The point of photograph
Figure 2. Micro structure on Corner-Butt 45 Joint (C-B 45) with 10 mm/min feedrate speed (A),15 mm/min feedrate speed
(B), and 30 mm/min feedrate speed (C) shows well-mixed joints.
A1
B1
C3
A3A2
B2 B3
C2C1
MM SCIENCE JOURNAL I 2018 I MARCH
2131
Corner-Butt Joint (C-B)
123 The point of photograph
Figure 3. Micro structure on Corner-Butt 45 Joint (C-B 45) with 10 mm/min feedrate speed (A), 15 mm/min
feedrate speed (B), and 30 mm/min feedrate speed (C) shows well-mixed joints.
3.2 Temperature distribution
In measuring the temperature, acquisition data, data logger, and thermocouple in the fig. 4 were utilized.
Figure 4. (A) Thermocouple (B) data logger (C) acquisition data
In Corner-Butt 45 (C-B 45) joint with 10 mm/min
feedrate speed, the highest temperature distribution
was 4200 C, nearly 0.8 Melting Point [Tang 1998]. Such
number of temperature was possible to reach because
the pin probe could perfectly fit in between the edges on
the welding track and the shoulder probe was such a
suitable heat generator. The slow process that required
longer time could eventually aid to accomplish the
welding with enough temperature.
A1
B1
C3
A3A2
B2 B3
C2C1
A B C
MM SCIENCE JOURNAL I 2018 I MARCH
2132
Figure 5. Temperature distribution on C-B 45 with 10mm/min,15mm/min, and 30 mm/min feedrate speed
An ample plastic state area was then formed, leading to
a well-mixed joint with a convincing micro structure (fig.
3). With 30 mm/min feedrate speed, the highest
temperature distribution was only 3000 C. The plastic
state then was not formed to the ful lest. Even so, the
pin probe could still penetrate in between the welding
track’s edges so that it could still stir properly and create
decent compound without any porosity (fig. 5).
Figure 6. Temperature distribution on C-B with 10mm/min,15mm/min, and 30 mm/min feedrate speed
MM SCIENCE JOURNAL I 2018 I MARCH
2133
Corner-Butt Joint (C-B) Fig.6 , the highest temperature
distribution was 400 0C, achieved on 10 mm/min
feedrate speed. This could happen because the slow
welding process took longer time to complete. Spending
15 minutes in the practice, the heat generated could
form wider plastic state area on the work-piece. The
sides of the joints that were in direct contact with the
entire surface of the pin probe could absorb heat
straightly, giving a well-merged joint as displayed in its
micro structure. (fig. 3 on A1,A2, and A3). On 15
mm/minfeedrate speed, the highest temperature
distribution was lower in 364 0C (fig. 6), 15 mm/min
feedrate. However, the micro structure (fig. 3 on B1, B2,
and B3) shows a well-merged compound. Direct contact
between the work-piece and the rotating pin probe
could form expected plastic state of the material. On 30
mm/min feedratespeed, the highest temperature
distribution was 309,70C. Similarly, the joint was still
well-connected since there wasn’t much heat loss and
the plastic state was met.
From the narrative Fig.6, it is figured out that the joint
quality is not determined by the generated heat but by
the ability of the pin probe to stir between the edges on
the welding track. Aside of that, the diameter and length
of the pin probe provide significant impact on the joint
quality.
Figure 7. Temperature distribution that occurs from the
thermocouple
Fig. 7 shows the distribution of heat occurs in the solid
welding process, the round start the first 5 minutes of
high heat that occurs above 300 0C, but the heat was still
centered on the probe pin, pin probe further and further
away from the lower heat distribution. Also on arms
probe pin is still below 300 0C. The longer the heat will
flow in all directions.
3.3. Micro hardness
Fig. 8, is showing a micro hardness testing, tested
perpendicular to the FSW connection. There are 12 test
points on the left side and right side of the 6 point
connection. Each point is 500 µm.The micro hardness
Vicker tests show that at low feedrate 10 mm / min
hardness is lower than the feedrate 15 mm / min or
feedrate 30 mm / min. This is because magnesium
aluminum alloys to form magnesium oxide (MgO)
compounds. Then it will result in reduced magnesium
alloy, and the mechanical properties of aluminum is also
reduced.This is consistent with the statement
[Dawood2015; Muhammad 2012].
Corner-Butt 45 Joint (C-B 45)
Thepoint of Microhardness tests
Figure 8. The micro hardness on C-B 45with 10mm/min,15 mm/min, and 30mm/min federate speed
Fig.9 is showing, the connection Corner-Butt also show
the same thing with the connection Corner-Butt 45. the
micro-hardness vickers test shows that, feedrate 10
mm/min will be generated hardness values lower than a
feedrate 15 mm/min or 30 mm/min.
MM SCIENCE JOURNAL I 2018 I MARCH
2134
Corner-Butt Joint (C-B)
The point of microhardness tests
Figure 9. The micro hardness on C-Bwith 10mm/min,15 mm/min, and 30mm/min federate speed
3.4. Tensile tests
Fig 10. In connection C-B 45 feedrate10 mm/min showed
the greatest tensile strength. This is caused by oxides
which occur many binds with Magnesium, which will
improve the mechanical properties. Also are plastic
materials that are formed more and more, and will be
perfectly stirred by the pin probe.In connection strength
of its C-B is lower than 45. This is due to the probe pin is
not capable of stirring the plastic material is perfect,
because the plastic material that goes directly into the
cold. Oxides which occur also unable to bind
Magnesium, thereby decreasing the mechanical
properties.
Temperature distribution in Figure 6, supporting a
decrease in mechanical properties. Because MgSi will be
stable at 2000C, at temperatures above 2000C MgSi will
settle and dissolve spread by mixing the probe pin. It
also will reduce the mechanical properties [Dawood
2015].
Figure 10. Tensile test result on all joints with 10mm/min,15 mm/min, and 30mm/min feedrate speed.
4. CONCLUSIONS
The finest mixture was achieved by C-B 45and C-Bjoints
on all feedratespeeds because the pin probe could
penetrate between the edges of the joint and stir them
well.High temperature distribution above 4000C could be
achieved by all joint variations on 10 mm/minfeedrate
speed because the duration taken to complete the
welding was longer up to 15 minutes.The micro hardness
value above 52 HVN was formed by all joint variations on
30 mm/minfeedrate speed because the temperature
distribution with such speed was low,therefore the
Magnesium loss was just minimum. The highest tensile
test score was 163.7 MPaby C-B 45jointon 10 mm/min
feedrate speed. The temperature distribution reached
4200C, consequently forming plastic state on the work-
piece.For this joint, the temperature distribution
reached 4200C.
MPa
MM SCIENCE JOURNAL I 2018 I MARCH
2135
ACKNOWLEDGEMENT
Authors thank to Head of LPPM Gadjah Mada University
and the Dean of Sekolah Vokasi for providing and
entrusting the researcher to conduct this research and
seminar.
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CONTACT:
Widia Setiawan, ST., MT
Gadjah Mada University
Sekolah Vokasi of Gadjah Mada University
Yogyakarta, Indonesia
Jl. Yacaranda Sekip Unit IV Bulaksumur
Yogyakarta 55281, Indonesia
Tel.+622746491301
Email:widia_setiawan64@yahoo.co.id
widia_s@.ugm.ac.id

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The position of the joints with angle of 90° at friction stir welding (FSW)

  • 1. MM SCIENCE JOURNAL I 2018 I MARCH 2128 THE POSITION OF THE JOINTS WITH ANGLE OF 900 AT FRICTION STIR WELDING (FSW) WIDIA SETIAWAN1,2, DJAROT B. DARMADI2, WAHYONO SUPRAPTO2, RUDY SOENOKO2 1 Sekolah Vokasi of Gadjah Mada University, Yogyakarta, Indonesia 2 University Brawijaya Malang, Indonesia DOI : 10.17973/MMSJ.2018_03_201717 e-mail: widia_s@.ugm.ac.id widia_setiawan64@yahoo.co.id This research was use aluminum 6061 with 150 mm length, 50 mm wide, and 10 mm thick. The probe was made from EMS 45 simple design. Three variations used of feedrate speed is 10 mm/min, 15 mm/min, and 30 mm/min. Spindle rotation constantly set 2000 rpm, the heat generated was recorded. Corner-Butt (C-B)joint determined, the lowest heat generated from 2200C- 3200C and the tensile test was60 MPa. The highest tensile testwas 163 MPa, achieved by Corner-butt 45 (C- B 45) joint on 10 mm/min feedrate speed. It was verified by the heat temperature from 3000C-4200C and clarified by its micro and macrostructure. KEYWORDS Friction Stir Welding, Corner-Butt Joint 450, Corner – Butt, Feedrate, Aluminum 6061 1. INTRODUCTION Discovered and patented a solid state welding technique called friction stir welding (FSW). Solid welding is an easy welding method to combine metals without requiring any particular skill [Thomas 1991].This kindof welding does not require high heat nor feeder electrode. Thistechnique would eliminate the porosity andpresent homogenous microstructure and phase. Moreover, residual stresses are also low. Heat is generated from friction between the cut surface and the probe[Thomas 1991]. [Mortensen 2011] States that in FSW, the heat is generated from the spindle rotation and the joiningoccurs because of the radial force toward the axial direction. The higher the pressure, the more heat is generated. Such condition will greatly influence the result of the welding and affect the material’s mechanic state.[Ozekcin 2004] says that FSW is a welding method for two Ferro or non-Ferro metals without liquefication and can be done with or without pressure. FSW does not alter the basic characteristics of the metals and is often performed to aluminum that does not endure post weld heat treatment (PWHT) In performing FSW, according to [Cao 2005], the spinning probe is pressed and penetrated onto the work- piece’s surface. The friction then generates heat, therefore connecting the welded materials. [Malarvizhi 2013] has proved that the heat in FSW technique is influenced by the probe’s diameter. Its size will affect the formation of micro structure, macro structure, and the tensile strength on the dissimilar metals welding between Al 6061 dan AZ 31 Magnesium. The successfulness of the welding is determined by the heat generated from the friction between the probe and the work-piece. The shoulder’s and pin’s diameter of the probe hold a significant role in generating heat. The amount of heat generated also depends on the spindle rotation speed of theuniversal milling machine. The material correspondingly contributes in generating heat. According to [Xiong 2013], the steady state heatgeneratin the plastic state is formulated below. ...............................................1 k = material’s thermal conductivity, d2T/dx2 = temperature gradient, q = generated heat, Cp = heat coefficient, and vdt/dx = speed gradient According to [Manvatkar 2014], the heat in the peak temperature and average cooling values are formulated as follow Q = x + 3 .................................................2 τ = shear stress (Kg/mm2), µ= friction coefficient, P = axial force (Kg), ω = Shoulder radius (mm), = pin radius = pin length (mm). During the welding process, the heat is generated from the friction by the probe that spins on the work-piece which eventually creates plastic state compound. This state can be observed in the thermomechanically affected zone (TMAZ) [Nandan 2008]. FSW is a current technique in joining aluminum without feeder electrode required. The heat is generated from the rotation of welding tool which results in deformation in the welding area. This joining process is called solid welding. [Padgett 2003]. FSW can be applied in similar or dissimilar metals with more efficient result, whereas liquid welding may cause hot cracking, blow holes, and distortion [ Kazi 2001, McNelley 2008]. [Silva 2014] concludes that key featureson T- Joint FSW optimization are 1000 rpm rotation speed, 15 mm shoulder diameter, 3.9 mm aluminum thickness, and 2.5
  • 2. MM SCIENCE JOURNAL I 2018 I MARCH 2129 as the ratio value between the pin and shoulder diameter. The welding speed apparently gives no significant effect to the mechanic state of FSW joint. The joining of aluminum with combination of T-Lap Joint and T-Butt Joint models can be performed with the use of specific clamping design [Zhao 2013]. Similar experiment by joining aluminum with 3 kinds of joint model, which are T-lap, T-Butt-Lap, and T-Double- Butt Joint with specific clamping design.FSW with T joint is basically performed by pressing the probe onto the work-piece then moving it toward the welding zone with particular speed. T-joints can be applied in many structures as in high pressure container support, bridges sustainer, and many more. If the T-joints are welded with liquid welding technique, the residual stress will be massive and the distortion will occur. Although such distortion can be minimized with particular heat treatments, the time and cost required will increase. The micro structure formed in the nugget zone is soft. That soft tone area can be expanded if the probe rotation speed is increased and the travelling speed is decreased [Cui 2012]. T-joints aluminum welding is essential for means of transportation such as planes, ships, and car seats and body structure as well as bridges structure and high pressure container. T-joint possesses well physical formwith firm and strong structureas its advantage [Hou 2013]. This research observed Friction Stir welding (FSW) on aluminum 6061 with the dimension of 150 mm length, 50 mm wide, and 10 mm thick with 450 cut on the edge. The joints variation applied areCorner-Butt 450 Joint, andCorner-Butt Joint. The traveling speed varied from 10 mm/min, 15 mm/min, and 30 mm/min with 2000 rpm probe rotation speed. From the result of experiments with those variations, the correlation between micro structure, hardness level, and generated heat were then analyzed to measure the highest tensile stress score. 2. EXPERIMENTAL PROCEDURES Compositions Mg Si Cu Mn Fe Cr Ti Zn Al Content 0.9 0.6 0.25 0.086 0.18 0.1 0.192 0.01 Bal Table 1. Chemical composition of 6061 aluminum alloy (wt.%) The aluminum 6061 as the object of this research contain chemical substance as described in Tab. 1. The aluminum’s edgewas milled to form 450corner. The probe was made from hardened EMS 45 with simple design. In Fig. 1 is explained, Before welded, the aluminum was perforated. There were 16 holes, each was at the distance of 20 mm with another. These holes were used to place the thermocouple to measure the temperature using acquisition data. The temperature distribution measuring at some point will get a picture of aluminum plastics which will affect the quality of the connection, this is as will be done in Fig. 1. 10 20 60 20 150 10 Figure 1. Before welded, the aluminum 6061wasPerforated Corner-Butt Joint 10 mm/min Corner-Butt 45 Joint 10 mm/min 15 mm/min 15 mm/min 30 mm/min 30 mm/min Table 2. Joint and traveling speed varied
  • 3. MM SCIENCE JOURNAL I 2018 I MARCH 2130 Parameter 10 mm/min 15 mm/min 30 mm/min Material study C-B 45 C-B Table 3. Welding macrostruckture result 3. RESULT AND DISCUSSION 3.1. Micro structure Corner-Butt 45 Joint (C-B 45), the micro structure displays ideal, homogenous blend because the pin probe could generate sufficient heat in all feedrate speeds to form plastic state compound around the welding area. Therefore, the joint could be welded with satisfying result with 4000 C temperature around the welding zone(Fig.6). Black spots contained in Fig. 6, is a mix of ferro the pin probe and material aluminum 6061. This can be evidenced by increased wear of the probe pin, pin length and diameter of the pin, and will cause the connection to be strong. The feedrate 10 mm/min slurry more perfect, visible from the slurry flow is shown on the microstructure, and the black spots more. While at feedrate 15 mm/min spots that occur more and more visible in the image of the microstructure occurring point 3.Corner-Butt Joint (C-B) provides homogenous micro structure and ubiquitous compound around the welding zone. The pin probe could properly merge the materials in this type of joint. The shoulder could generate enough heat to form plastic state on the welding zone and heat loss could be reduced. Fig. 2. describes such condition visually. Feed rate of 15 mm/min mixing that occurs is clearly visible (Fig. 2). plastically perfect condition it will cause the connection will be better. To be concluded, the micro structure on C-B 45and C-B joints are more satisfactory compared to the other joints. In these joints, the heat generated could create wider plastic state compound. The pin probe could also worked at its finestin those joints and the pressure from the shoulder could provide constructive support in stirring the materials. Those factors backed up the satisfying results of the FSW in these joints. Corner-Butt 45 Joint (C-B 45) 123 The point of photograph Figure 2. Micro structure on Corner-Butt 45 Joint (C-B 45) with 10 mm/min feedrate speed (A),15 mm/min feedrate speed (B), and 30 mm/min feedrate speed (C) shows well-mixed joints. A1 B1 C3 A3A2 B2 B3 C2C1
  • 4. MM SCIENCE JOURNAL I 2018 I MARCH 2131 Corner-Butt Joint (C-B) 123 The point of photograph Figure 3. Micro structure on Corner-Butt 45 Joint (C-B 45) with 10 mm/min feedrate speed (A), 15 mm/min feedrate speed (B), and 30 mm/min feedrate speed (C) shows well-mixed joints. 3.2 Temperature distribution In measuring the temperature, acquisition data, data logger, and thermocouple in the fig. 4 were utilized. Figure 4. (A) Thermocouple (B) data logger (C) acquisition data In Corner-Butt 45 (C-B 45) joint with 10 mm/min feedrate speed, the highest temperature distribution was 4200 C, nearly 0.8 Melting Point [Tang 1998]. Such number of temperature was possible to reach because the pin probe could perfectly fit in between the edges on the welding track and the shoulder probe was such a suitable heat generator. The slow process that required longer time could eventually aid to accomplish the welding with enough temperature. A1 B1 C3 A3A2 B2 B3 C2C1 A B C
  • 5. MM SCIENCE JOURNAL I 2018 I MARCH 2132 Figure 5. Temperature distribution on C-B 45 with 10mm/min,15mm/min, and 30 mm/min feedrate speed An ample plastic state area was then formed, leading to a well-mixed joint with a convincing micro structure (fig. 3). With 30 mm/min feedrate speed, the highest temperature distribution was only 3000 C. The plastic state then was not formed to the ful lest. Even so, the pin probe could still penetrate in between the welding track’s edges so that it could still stir properly and create decent compound without any porosity (fig. 5). Figure 6. Temperature distribution on C-B with 10mm/min,15mm/min, and 30 mm/min feedrate speed
  • 6. MM SCIENCE JOURNAL I 2018 I MARCH 2133 Corner-Butt Joint (C-B) Fig.6 , the highest temperature distribution was 400 0C, achieved on 10 mm/min feedrate speed. This could happen because the slow welding process took longer time to complete. Spending 15 minutes in the practice, the heat generated could form wider plastic state area on the work-piece. The sides of the joints that were in direct contact with the entire surface of the pin probe could absorb heat straightly, giving a well-merged joint as displayed in its micro structure. (fig. 3 on A1,A2, and A3). On 15 mm/minfeedrate speed, the highest temperature distribution was lower in 364 0C (fig. 6), 15 mm/min feedrate. However, the micro structure (fig. 3 on B1, B2, and B3) shows a well-merged compound. Direct contact between the work-piece and the rotating pin probe could form expected plastic state of the material. On 30 mm/min feedratespeed, the highest temperature distribution was 309,70C. Similarly, the joint was still well-connected since there wasn’t much heat loss and the plastic state was met. From the narrative Fig.6, it is figured out that the joint quality is not determined by the generated heat but by the ability of the pin probe to stir between the edges on the welding track. Aside of that, the diameter and length of the pin probe provide significant impact on the joint quality. Figure 7. Temperature distribution that occurs from the thermocouple Fig. 7 shows the distribution of heat occurs in the solid welding process, the round start the first 5 minutes of high heat that occurs above 300 0C, but the heat was still centered on the probe pin, pin probe further and further away from the lower heat distribution. Also on arms probe pin is still below 300 0C. The longer the heat will flow in all directions. 3.3. Micro hardness Fig. 8, is showing a micro hardness testing, tested perpendicular to the FSW connection. There are 12 test points on the left side and right side of the 6 point connection. Each point is 500 µm.The micro hardness Vicker tests show that at low feedrate 10 mm / min hardness is lower than the feedrate 15 mm / min or feedrate 30 mm / min. This is because magnesium aluminum alloys to form magnesium oxide (MgO) compounds. Then it will result in reduced magnesium alloy, and the mechanical properties of aluminum is also reduced.This is consistent with the statement [Dawood2015; Muhammad 2012]. Corner-Butt 45 Joint (C-B 45) Thepoint of Microhardness tests Figure 8. The micro hardness on C-B 45with 10mm/min,15 mm/min, and 30mm/min federate speed Fig.9 is showing, the connection Corner-Butt also show the same thing with the connection Corner-Butt 45. the micro-hardness vickers test shows that, feedrate 10 mm/min will be generated hardness values lower than a feedrate 15 mm/min or 30 mm/min.
  • 7. MM SCIENCE JOURNAL I 2018 I MARCH 2134 Corner-Butt Joint (C-B) The point of microhardness tests Figure 9. The micro hardness on C-Bwith 10mm/min,15 mm/min, and 30mm/min federate speed 3.4. Tensile tests Fig 10. In connection C-B 45 feedrate10 mm/min showed the greatest tensile strength. This is caused by oxides which occur many binds with Magnesium, which will improve the mechanical properties. Also are plastic materials that are formed more and more, and will be perfectly stirred by the pin probe.In connection strength of its C-B is lower than 45. This is due to the probe pin is not capable of stirring the plastic material is perfect, because the plastic material that goes directly into the cold. Oxides which occur also unable to bind Magnesium, thereby decreasing the mechanical properties. Temperature distribution in Figure 6, supporting a decrease in mechanical properties. Because MgSi will be stable at 2000C, at temperatures above 2000C MgSi will settle and dissolve spread by mixing the probe pin. It also will reduce the mechanical properties [Dawood 2015]. Figure 10. Tensile test result on all joints with 10mm/min,15 mm/min, and 30mm/min feedrate speed. 4. CONCLUSIONS The finest mixture was achieved by C-B 45and C-Bjoints on all feedratespeeds because the pin probe could penetrate between the edges of the joint and stir them well.High temperature distribution above 4000C could be achieved by all joint variations on 10 mm/minfeedrate speed because the duration taken to complete the welding was longer up to 15 minutes.The micro hardness value above 52 HVN was formed by all joint variations on 30 mm/minfeedrate speed because the temperature distribution with such speed was low,therefore the Magnesium loss was just minimum. The highest tensile test score was 163.7 MPaby C-B 45jointon 10 mm/min feedrate speed. The temperature distribution reached 4200C, consequently forming plastic state on the work- piece.For this joint, the temperature distribution reached 4200C. MPa
  • 8. MM SCIENCE JOURNAL I 2018 I MARCH 2135 ACKNOWLEDGEMENT Authors thank to Head of LPPM Gadjah Mada University and the Dean of Sekolah Vokasi for providing and entrusting the researcher to conduct this research and seminar. REFERENCES [Cao 2005] Cao, G. and Kou, S. Friction stir welding of 2219 aluminum: behavior of 6 (AI2Cu) particles. The Welding Journal, 2005 [Cui 2012] Cui, L., Yang, X., Zhou, G, Xu, X. and Shen. Z. Characteristics of defects and tensile behaviors on friction stir welded AA6061-T4. Material Science and Engineering: A, vol. 543, pp. 58-68.Available from:http://www.sciencedirect.com/science/article/pii/ S0921509312002511 [Dawood 2015] Dawood, H. I., Kahtan, S., Mohammed., Rahmat, A. and Uday, M. B. The influence of the surface roughness on the microstructures and mechanical properties of 6061 aluminiumalloy using friction stir welding. Surface and Coatings Technology, vol. 270, pp. 271-283. Available from: http://www.sciencedirect.com/science/article/pii/S0257 897215001814 [Hou 2013] Hou, X., Yang, X., Cui, L. and Zhou, G. Influences of joint geometry on defects and mechanical properties of friction stir welded AA6061-T4 T-joints. Materials & Design, volume 53, pp. 106-117. Available from: http://www.sciencedirect.com/science/article/pii/S0261 306913005955 [Kazi 2001] Kazi, S. H. and Murr, L. E. Complex flow phenomena associated with friction-stir welding of aluminum alloys. In: Mishra RS, et al., editors. Friction stir welding and processing. USA: Warrendale, 2001. p. 139–151. [Malarvizhi 2013] Malarvizhi, S. and Balasubramanian, V. Influences of tool shoulder diameter to plate thickness ratio (D/T) on stir zone formation and tensile properties of friction stir welded dissimilar joints of AA6061 aluminum–AZ31B magnesium alloys. Materials & Design, vol. 40, pp. 453-460. Available from: http://www.sciencedirect.com/science/article/pii/S0261 306912002427. [Manvatkar 2014] Manvatkar, V., de, A. Svensson, L. E. and DebRoy, T. Cooling rates and peak temperatures during friction stir welding of a high-carbon steel. Scripta Materialia, Vol. 94, pp. 36-39.Available from:http://www.sciencedirect.com/science/article/pii/ S1359646214003637 [McNelley 2008] McNelley, T. R., Swaminathan, S. and Su, J. Q. Recrystallization mechanisms during friction stir welding/processing of aluminum alloys. Scripta Mater,vol.58, pp. 349–54. Available from: http://www.sciencedirect.com/science/article/pii/S1359 646207007464 [Mortensen 2011] Mortensen, K. S.,Jensen, C. G., Conrad, L. C. and Losee, F. Mechanicalproperties and microstructures of inertia-friction-welded 416 stainless steel. Utah: Departement of Mechanical, Brigham Young University, 2011. [Muhammad 2012] Muhammad, S. R. The effect magnesium content on aluminum toward tensile strength, and basicmicrostructure. Indonesia: University of North of Sumatra, 2012. [Nandan 2008] Nandan, R., DebRoy, T. and Bhadeshia, H. K. D. H. Recent advances in friction-stir welding process, weldment structure and properties.Progress in Materials Science, vol. 53, no.6, pp. 980-1023. Available from: http://www.sciencedirect.com/science/article/pii/S0079 64250800039X [Ozekcin 2004] Ozekcin, A., Jin, H. W., Koo, Y. J., Bangaru, N. V., Ayer, R., Vaughn, G. A microstructural study of friction stir welded joints of carbon steels. The International Society of Offshore and Polar Engineers, 2004 [Padgett 2003] Padgett, P. N., Paglia, C. and Buchheit, R. G. Characterization of corrosion behaviour in friction stir weld Al–Li–Cu AF/C458 Alloy.Friction stir welding and processing II. USA: Warrendale, 2003 [Silva 2014] Silva, A. C. F., Braga, D. F. O., de Figueiredo, M. A. V. and Moreira, P. M. G. P. Friction stir welded T- joints optimization. Materials & Design, vol. 55, pp. 120- 127. Available from:http://www.sciencedirect.com/science/article/pii/ S0261306913008686 [Tang 1998] Tang, W., Guo, X., McClure, J. C., Murr, L. E. and Nunes, A. Heat Input and Temperature Distribution in Friction Stir Welding. Journal of Materials Processing & Manufacturing Science, vol. 7, no. 2, pp. 163-172. [Thomas 1991] Thomas, W. M., Nicholas E. D., Needham, J. C., Murch, M. G., Templesmith, P. and Dawes, C. J. G. B Patent Application No. 9125978.8 (December 1991). [Xiong 2013] Xiong, J. T., Li, J. L., Wei, Y. N., Zhang, F. S. and Huang, W. D. An analytical model of steady-state continuous drive friction welding, a state key laboratory of solidification processing. China: Northwestern Polytechnical University,2013. [Zhao 2013] Zhao, Y., Zhou, L., Wang, Q., Yan, K. and Zou, J. Defects and tensile properties of 6013 aluminum alloy T-joints by friction stir welding. Material & Design, vol. 57, pp.146-155. Available from: http://www.sciencedirect.com/science/article/pii/S0261 306913011540 CONTACT: Widia Setiawan, ST., MT Gadjah Mada University Sekolah Vokasi of Gadjah Mada University Yogyakarta, Indonesia Jl. Yacaranda Sekip Unit IV Bulaksumur Yogyakarta 55281, Indonesia Tel.+622746491301 Email:widia_setiawan64@yahoo.co.id widia_s@.ugm.ac.id