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Quantifing separation performance in
gas/liquid separator
- Nikunj Dodiya (15BPE028)
Introduction
• There is a wide range of sizing methods for two-phase
separators, varying from the simple “back-of-the-
envelope” to the far more complicated
• several weaknesses associated with most of these
methods
1. Quantification of feed flow steadiness
2. Entrainment/droplet size distribution quantification
3. Velocity profile/distribution quantification
4. Separator component performance quantification
Separator parts
Separator
• The main objective is to remove droplets of a dispersed
phase from a second continuous phase.
• A secondary requirement is often for the separator to
have some capability to deal with intermittent
flow (slugging)
• Questions important in the sizing and performance
prediction
1. What is the flow pattern at the separator’s inlet?
2. How much of the dispersed phase (liquid droplets) is
present in entrained form?
3. What are the sizes of the droplets?
Flow pattern and entrainment
Flowpipe geometry
• What if the flow has changed direction, for example, at
elbows and fittings, or experienced other flow pattern
disruptions immediately upstream of the separator.
• Typical guidelines are:
1. Provide 10 diameters of straight pipe upstream of the
inlet nozzle without valves, expansions/contractions,
or elbows.
2. If a valve in the feed line near the separator is
required, it should only be a full port gate or ball
valve.
Entrainment
Fig. 5 effect of feedpipe velocity on liquid
entrainment
Entrainment cont-
• The degree of liquid entrainment is a function of the
following variables (among others)
1. Entrainment increases with increasing velocity
2. Entrainment increases with decreasing liquid
surface tension.
Pan and Hanratty (2002)
Entrainment cont-
Droplet Sizes and Distribution
Kataoka et al. (1983)
Kataoka (1983) and
Simmons and Hanratty
(2001)
Droplet Sizes and Distribution
Inlet Device
• Main function of an inlet device
1. Maximization of gas/liquid separation efficiency based on
inlet feed conditions
2. Minimization of droplet shearing
3. Provision of good downstream velocity distributions in the
separated phases
Inlet momentum
Inlet Device Separation Efficiency
Effect of the selected inlet device on downstream
velocity profiles without flow straightening devices
Gas Gravity Separation Section
• Primary function is to reduce the entrained liquid load
not removed by the inlet device.
• A secondary function is the improvement/straightening
of the gas velocity profile.
• Two approaches to sizing this part of the separator to
remove liquid droplets from the gas are the K method
(Souders-Brown equation ) and the droplet settling
theory.
• the droplet settling calculations aim at removing a
target liquid-droplet size (e.g., 150 μm) and all
droplets larger than the target size
Droplet Settling Calculations
Droplet setting calculation
Droplet setting calculation
Separator
Verticle separator :Using the droplet size
distribution and effective actual velocity
correlations,the terminal velocity equation can be
used to calculate the droplet removal efficiency of
the gas gravity separation section
Horizontal separator :
separation efficiency of droplets smaller than dp,100
Mist Extractor
Mist extractor
performance depend
1. Droplet removal
efficiency
2. Gas capacity
3. Liquid handling
Mesh Pads
• A methodology that can be used to quantify droplet
capture efficiency of a mesh-type mist extractor is as
follows:
1. Calculate the Stokes’ number (sometimes called the
inertial impaction parameter) from the following
equation
2. Calculate the single-wire removal efficiency
3. mesh-pad removal efficiency
• Vane-Type Mist Extractors
Droplet Removal Efficiency
• Demisting Cyclones
Droplet Removal Efficiency
Use of Different Mist Extractor
Types in Series
1. A mesh pad followed by a vane pack
2. A mesh pad followed by a demisting cyclone
bundle
• At high gas-flow rates, the mesh pad will be operating
above its capacity limit.
• The mesh pad provides good low-flow droplet
removal performance, while the secondary vane-pack
or demisting cyclone bundle provides high-flow
capacity with improved droplet removal performance
as a result of the larger droplets exiting the mesh pad
Liquid Gravity Separation Section
• The functions of the liquid gravity separation
section depend on the type of separator and its
application, including the following:
1. Degassing of the liquid.
2. Smoothing out of intermittent inlet flow surges
to provide steadier liquid flow to downstream
equipment/processing.
3. To maintain a liquid seal at the bottom of the
separator, a minimum requirement for
instrumentation layout and process control
Quantification of gas entrainment into
liquid by a plunging jet
1. Estimate the effective liquid-jet nozzle diameter.
2. Establish the length of the jet, which is typically the distance from the
inlet device outlet to the separator liquid level.
3. Calculate the effective jet velocity at the point where the jet enters the
liquid pool.
4. Calculate the jet Froude number.
5. Calculate the amount of gas entrained into the liquid pool by the jet.
6. Calculate the depth of penetration of bubbles by the plunging jet (the
release point of the bubbles).
7. Estimate the bubble size distribution.
8. Perform the bubble size separation calculations based on the separator
geometry, including whether vertical or horizontal, the flow rates,and fluid
properties. The calculations are analogous to those used for liquid droplet
settling in the gas gravity separation section
Handling Intermittent Flow
• If the slug/surge volumes cannot be quantified in advance with a
multiphase flow simulator, for example, the following approaches
provide allowance for intermittent feed flow behavior:
1. Inflate the steady-state flow rates, and size the vessel using
standard procedures. Table 6 provides typical flow-rate multipliers
based on the upstream feed supply configuration
2. Estimate the slug/surge volumes. This requires an understanding
of the various mechanisms that cause slugging and quantification of
the slug/surge volumes involved. In the absence of better
information, the slug size can be assumed to be from 3 to 5 seconds
of liquid-full flow at feedpipe velocity. In-plant separators
downstream of the inlet separation equipment would not be
expected to see large slugs. A slug size based on 1 sec of liquid-full
pipe at feed-flow velocity seems reasonable for these separators.
Handling intermittent flow
Conclusion
• The equations and methods that can be used to improve the
quantification of gas/liquid separation performance
compared with traditional techniques.
• The key aspects of the recommended methodology include
quantification of the following:
1. The amount of gas (liquid) entrained in the form of
droplets (bubbles)
2. The size distribution of the entrained droplets (bubbles)
3. The continuous phase (gas or liquid) velocities
4. Droplet (bubble) separation performance based on 1–3
above and the geometry of the separator
• Presented approach to gas/liquid separator design and
rating that more accurately reflects the physics involved.
Thank you
Reference
• Gas/Liquid Separators: Quantifying Separation Performance—Part 1, 2
& 3 -Mark Bothamley • JM Campbell/PetroSkills | 22 July 2013
• Simmons, M.J.H. and Hanratty, T.J. 2001. Droplet Size Measurements in
Horizontal Annular Gas-Liquid Flow. Int. J. Multiphase Flow 27 (5)
• Kataoka, I., Ishii, M., and Mishima, K. 1983. Generation and Size
Distribution of Droplets in Gas-Liquid Annular Two-Phase Flow. ASME
Journal
• Ishii, M. and Grolmes, M.A. 1975. Inception Criteria for Droplet
Entrainment in Two-Phase Concurrent Film Flow. AIChE J. 21 (2)
• Viles, J.C. 1993. Predicting Liquid Re-Entrainmen in Horizontal
Separators. J Pet Tech 45 (5)

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Qualification of separation performance in gas\liquid separation

  • 1. Quantifing separation performance in gas/liquid separator - Nikunj Dodiya (15BPE028)
  • 2. Introduction • There is a wide range of sizing methods for two-phase separators, varying from the simple “back-of-the- envelope” to the far more complicated • several weaknesses associated with most of these methods 1. Quantification of feed flow steadiness 2. Entrainment/droplet size distribution quantification 3. Velocity profile/distribution quantification 4. Separator component performance quantification
  • 4. Separator • The main objective is to remove droplets of a dispersed phase from a second continuous phase. • A secondary requirement is often for the separator to have some capability to deal with intermittent flow (slugging) • Questions important in the sizing and performance prediction 1. What is the flow pattern at the separator’s inlet? 2. How much of the dispersed phase (liquid droplets) is present in entrained form? 3. What are the sizes of the droplets?
  • 5. Flow pattern and entrainment
  • 6. Flowpipe geometry • What if the flow has changed direction, for example, at elbows and fittings, or experienced other flow pattern disruptions immediately upstream of the separator. • Typical guidelines are: 1. Provide 10 diameters of straight pipe upstream of the inlet nozzle without valves, expansions/contractions, or elbows. 2. If a valve in the feed line near the separator is required, it should only be a full port gate or ball valve.
  • 7. Entrainment Fig. 5 effect of feedpipe velocity on liquid entrainment
  • 8. Entrainment cont- • The degree of liquid entrainment is a function of the following variables (among others) 1. Entrainment increases with increasing velocity 2. Entrainment increases with decreasing liquid surface tension. Pan and Hanratty (2002)
  • 10. Droplet Sizes and Distribution Kataoka et al. (1983) Kataoka (1983) and Simmons and Hanratty (2001)
  • 11. Droplet Sizes and Distribution
  • 12. Inlet Device • Main function of an inlet device 1. Maximization of gas/liquid separation efficiency based on inlet feed conditions 2. Minimization of droplet shearing 3. Provision of good downstream velocity distributions in the separated phases Inlet momentum
  • 14. Effect of the selected inlet device on downstream velocity profiles without flow straightening devices
  • 15. Gas Gravity Separation Section • Primary function is to reduce the entrained liquid load not removed by the inlet device. • A secondary function is the improvement/straightening of the gas velocity profile. • Two approaches to sizing this part of the separator to remove liquid droplets from the gas are the K method (Souders-Brown equation ) and the droplet settling theory. • the droplet settling calculations aim at removing a target liquid-droplet size (e.g., 150 μm) and all droplets larger than the target size
  • 19. Separator Verticle separator :Using the droplet size distribution and effective actual velocity correlations,the terminal velocity equation can be used to calculate the droplet removal efficiency of the gas gravity separation section Horizontal separator : separation efficiency of droplets smaller than dp,100
  • 20. Mist Extractor Mist extractor performance depend 1. Droplet removal efficiency 2. Gas capacity 3. Liquid handling
  • 21. Mesh Pads • A methodology that can be used to quantify droplet capture efficiency of a mesh-type mist extractor is as follows: 1. Calculate the Stokes’ number (sometimes called the inertial impaction parameter) from the following equation 2. Calculate the single-wire removal efficiency 3. mesh-pad removal efficiency
  • 22. • Vane-Type Mist Extractors Droplet Removal Efficiency • Demisting Cyclones Droplet Removal Efficiency
  • 23. Use of Different Mist Extractor Types in Series 1. A mesh pad followed by a vane pack 2. A mesh pad followed by a demisting cyclone bundle • At high gas-flow rates, the mesh pad will be operating above its capacity limit. • The mesh pad provides good low-flow droplet removal performance, while the secondary vane-pack or demisting cyclone bundle provides high-flow capacity with improved droplet removal performance as a result of the larger droplets exiting the mesh pad
  • 24. Liquid Gravity Separation Section • The functions of the liquid gravity separation section depend on the type of separator and its application, including the following: 1. Degassing of the liquid. 2. Smoothing out of intermittent inlet flow surges to provide steadier liquid flow to downstream equipment/processing. 3. To maintain a liquid seal at the bottom of the separator, a minimum requirement for instrumentation layout and process control
  • 25. Quantification of gas entrainment into liquid by a plunging jet 1. Estimate the effective liquid-jet nozzle diameter. 2. Establish the length of the jet, which is typically the distance from the inlet device outlet to the separator liquid level. 3. Calculate the effective jet velocity at the point where the jet enters the liquid pool. 4. Calculate the jet Froude number. 5. Calculate the amount of gas entrained into the liquid pool by the jet. 6. Calculate the depth of penetration of bubbles by the plunging jet (the release point of the bubbles). 7. Estimate the bubble size distribution. 8. Perform the bubble size separation calculations based on the separator geometry, including whether vertical or horizontal, the flow rates,and fluid properties. The calculations are analogous to those used for liquid droplet settling in the gas gravity separation section
  • 26. Handling Intermittent Flow • If the slug/surge volumes cannot be quantified in advance with a multiphase flow simulator, for example, the following approaches provide allowance for intermittent feed flow behavior: 1. Inflate the steady-state flow rates, and size the vessel using standard procedures. Table 6 provides typical flow-rate multipliers based on the upstream feed supply configuration 2. Estimate the slug/surge volumes. This requires an understanding of the various mechanisms that cause slugging and quantification of the slug/surge volumes involved. In the absence of better information, the slug size can be assumed to be from 3 to 5 seconds of liquid-full flow at feedpipe velocity. In-plant separators downstream of the inlet separation equipment would not be expected to see large slugs. A slug size based on 1 sec of liquid-full pipe at feed-flow velocity seems reasonable for these separators.
  • 28. Conclusion • The equations and methods that can be used to improve the quantification of gas/liquid separation performance compared with traditional techniques. • The key aspects of the recommended methodology include quantification of the following: 1. The amount of gas (liquid) entrained in the form of droplets (bubbles) 2. The size distribution of the entrained droplets (bubbles) 3. The continuous phase (gas or liquid) velocities 4. Droplet (bubble) separation performance based on 1–3 above and the geometry of the separator • Presented approach to gas/liquid separator design and rating that more accurately reflects the physics involved.
  • 30. Reference • Gas/Liquid Separators: Quantifying Separation Performance—Part 1, 2 & 3 -Mark Bothamley • JM Campbell/PetroSkills | 22 July 2013 • Simmons, M.J.H. and Hanratty, T.J. 2001. Droplet Size Measurements in Horizontal Annular Gas-Liquid Flow. Int. J. Multiphase Flow 27 (5) • Kataoka, I., Ishii, M., and Mishima, K. 1983. Generation and Size Distribution of Droplets in Gas-Liquid Annular Two-Phase Flow. ASME Journal • Ishii, M. and Grolmes, M.A. 1975. Inception Criteria for Droplet Entrainment in Two-Phase Concurrent Film Flow. AIChE J. 21 (2) • Viles, J.C. 1993. Predicting Liquid Re-Entrainmen in Horizontal Separators. J Pet Tech 45 (5)