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Keiretsu Forum Mark Mitchell, Ceramic Filter Program Manager 
LLNL-PRES-561172 
This work was performed under the auspices of the 
U.S. Department of Energy by Lawrence Livermore 
National Laboratory under contract DE-AC52-07NA27344. 
Lawrence Livermore National Security, LLC 
Conceptual Cut Away View
 Novel inorganic ceramic materials 
in a metal housing 
 Scalable 
• Full Scale Nuclear Application (1000 
cfm): 
— 2’ X 2’ x 11.5”, 50 kg 
• Mini (70 cfm): 
— 8.5” x 8.5” x 11.5”, 4.5 kg 
• Commercial units can be engineered 
to weigh less 
Mini-Assembly 
Lawrence Livermore National Laboratory LLNL-PRES-561172 
2 
Full-Scale Assembly
 Survive elevated temperature, moisture, corrosion 
and fires better than existing technology. 
 Increase safety of operations – by performing the 
safety function within a wider operational range. 
 Provide for in-situ cleaning and reuse, thereby 
reducing secondary waste. 
 Minimize costs and risks of contamination posed by 
“hot breaks”. 
Lawrence Livermore National Laboratory LLNL-PRES-561172 
3
Filtration efficiency 
tunable to market 
specifications 
Substitution of 
ceramic HEPA filters 
into existing filtration 
systems enables a 
regulatory ecosystem 
that engenders 
greater safety, cost 
effectiveness, and 
efficiency. 
Lawrence Livermore National Laboratory LLNL-PRES-561172 4
 Semiconductor Fabrication 
 Clean rooms 
 Aerospace Manufacturing 
 Petroleum Processing 
 Biotech/Biopharmaceutical 
 Pharmaceutical Manufacturing 
 Clean Coal Power Generation 
 Hazardous Chemicals Processing 
Lawrence Livermore National Laboratory LLNL-PRES-561172 
5 
 Mining 
 Metals Processing 
 Wastewater Treatment 
 Agriculture 
 Dyes 
 Defense Industries 
 Nuclear Power Generation 
 Non-reactor Nuclear Facilities
 Selected optimal ceramic substrates, coatings, 
and application technologies 
 Tested proof-of-concept filter 
 Developed manufacturing tooling 
 Innovations that facilitate continuous system 
operation, e.g., 
• Process operations in a chemical plant 
• Ventilation during a fire in a nuclear facility 
 IP based on 30 years of HEPA filter research 
Lawrence Livermore National Laboratory LLNL-PRES-561172 
6 
3 tube types 
Ceramic 
Substrate 
Coating
 Complete: ASME 510 leak test at 
LLNL industrial hygiene laboratory 
• Individual components and 
assembled HEPA filter 
 Complete: Independent Certification 
Testing 
• Verification of HEPA filtration (> 99.97% 
filtration efficiency) at 
— 30 cfm (dP 2.8”) 
— 71 cfm (dP 6.1”) 
Lawrence Livermore National Laboratory LLNL-PRES-561172 
7
 Independent Qualification 
Testing 
 Utilize HTTU to study HEPA 
filter behavior as effected by 
fire conditions 
Lawrence Livermore National Laboratory LLNL-PRES-561172 
8
Traditional HEPA 
Filter 
Ceramic HEPA filter 
Purchase price for 1” x 1” x 1” size $200 to $300 $2,000 (Cost of components purchased as 
single items; can be reduced with bulk 
purchasing) 
Current assembly and testing time (can be 
reduced significantly with automation): 8 hrs 
Cost of install & replacement (including 
package, waste shipment, & waste disposal) 
for process equipment, fume hood, etc. 
(depends on class of waste) 
$16,000 per filter Same: $16,000 per filter 
Cost of install & replacement (including 
package, waste shipment, & waste disposal) 
in ventilation system (depends on class of 
waste) 
$2,700 per filter (LLW) Same: $2700 per filter (LLW) 
Light Use (light dust/moisture/corrosive 
environment) 
3 to 5 years 
operational life 
Infinite 
Challenging Use (heavy dust/moisture/ 
corrosive environment) 
Short operational life Infinite (with cleaning) 
Savings Up to $14,000 every replacement interval 
Lawrence Livermore National Laboratory LLNL-PRES-561172 9
 Ceramic HEPA filters offer unique capabilities and 
benefits 
• Safer with large life-cycle cost savings potential 
• Make possible additional process innovations 
 Completed successful proof-of-concept, verified by 
independent testing 
 Portfolio of inventions 
 Applicable to a wide range of industries 
Lawrence Livermore National Laboratory LLNL-PRES-561172 
10
Annemarie Meike 
meike1@llnl.gov 
Lawrence Livermore National Laboratory LLNL-PRES-561172 11

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Indestructible Ultra-filtration: Ceramic HEPA Filters by Mark Mitchell

  • 1. Keiretsu Forum Mark Mitchell, Ceramic Filter Program Manager LLNL-PRES-561172 This work was performed under the auspices of the U.S. Department of Energy by Lawrence Livermore National Laboratory under contract DE-AC52-07NA27344. Lawrence Livermore National Security, LLC Conceptual Cut Away View
  • 2.  Novel inorganic ceramic materials in a metal housing  Scalable • Full Scale Nuclear Application (1000 cfm): — 2’ X 2’ x 11.5”, 50 kg • Mini (70 cfm): — 8.5” x 8.5” x 11.5”, 4.5 kg • Commercial units can be engineered to weigh less Mini-Assembly Lawrence Livermore National Laboratory LLNL-PRES-561172 2 Full-Scale Assembly
  • 3.  Survive elevated temperature, moisture, corrosion and fires better than existing technology.  Increase safety of operations – by performing the safety function within a wider operational range.  Provide for in-situ cleaning and reuse, thereby reducing secondary waste.  Minimize costs and risks of contamination posed by “hot breaks”. Lawrence Livermore National Laboratory LLNL-PRES-561172 3
  • 4. Filtration efficiency tunable to market specifications Substitution of ceramic HEPA filters into existing filtration systems enables a regulatory ecosystem that engenders greater safety, cost effectiveness, and efficiency. Lawrence Livermore National Laboratory LLNL-PRES-561172 4
  • 5.  Semiconductor Fabrication  Clean rooms  Aerospace Manufacturing  Petroleum Processing  Biotech/Biopharmaceutical  Pharmaceutical Manufacturing  Clean Coal Power Generation  Hazardous Chemicals Processing Lawrence Livermore National Laboratory LLNL-PRES-561172 5  Mining  Metals Processing  Wastewater Treatment  Agriculture  Dyes  Defense Industries  Nuclear Power Generation  Non-reactor Nuclear Facilities
  • 6.  Selected optimal ceramic substrates, coatings, and application technologies  Tested proof-of-concept filter  Developed manufacturing tooling  Innovations that facilitate continuous system operation, e.g., • Process operations in a chemical plant • Ventilation during a fire in a nuclear facility  IP based on 30 years of HEPA filter research Lawrence Livermore National Laboratory LLNL-PRES-561172 6 3 tube types Ceramic Substrate Coating
  • 7.  Complete: ASME 510 leak test at LLNL industrial hygiene laboratory • Individual components and assembled HEPA filter  Complete: Independent Certification Testing • Verification of HEPA filtration (> 99.97% filtration efficiency) at — 30 cfm (dP 2.8”) — 71 cfm (dP 6.1”) Lawrence Livermore National Laboratory LLNL-PRES-561172 7
  • 8.  Independent Qualification Testing  Utilize HTTU to study HEPA filter behavior as effected by fire conditions Lawrence Livermore National Laboratory LLNL-PRES-561172 8
  • 9. Traditional HEPA Filter Ceramic HEPA filter Purchase price for 1” x 1” x 1” size $200 to $300 $2,000 (Cost of components purchased as single items; can be reduced with bulk purchasing) Current assembly and testing time (can be reduced significantly with automation): 8 hrs Cost of install & replacement (including package, waste shipment, & waste disposal) for process equipment, fume hood, etc. (depends on class of waste) $16,000 per filter Same: $16,000 per filter Cost of install & replacement (including package, waste shipment, & waste disposal) in ventilation system (depends on class of waste) $2,700 per filter (LLW) Same: $2700 per filter (LLW) Light Use (light dust/moisture/corrosive environment) 3 to 5 years operational life Infinite Challenging Use (heavy dust/moisture/ corrosive environment) Short operational life Infinite (with cleaning) Savings Up to $14,000 every replacement interval Lawrence Livermore National Laboratory LLNL-PRES-561172 9
  • 10.  Ceramic HEPA filters offer unique capabilities and benefits • Safer with large life-cycle cost savings potential • Make possible additional process innovations  Completed successful proof-of-concept, verified by independent testing  Portfolio of inventions  Applicable to a wide range of industries Lawrence Livermore National Laboratory LLNL-PRES-561172 10
  • 11. Annemarie Meike meike1@llnl.gov Lawrence Livermore National Laboratory LLNL-PRES-561172 11

Editor's Notes

  1. Funded to use the currently developed, independent test stand used to qualify other HEPA filters for nuclear applications