SlideShare a Scribd company logo
Graphene Growth
JESSICA PATALANO
Goals - Uniformity
 Fluid experiment (monolayer Cu balls and tubes)
 Smoother surface
 Faster flow rate
 Less drag
 Lithium ion battery (multilayer Ni foils)
 Sandwiched between SEI and current collector
 Hold energy better
 10x faster charge time
Goals - Uniformity
 Monolayer Graphene
 Much easier because of the nature of the material
 Bilayer Graphene (thickness < 1 nm)
 Gas-sensing properties
 Could be better at managing heat of high-power electrical devices
 Appropriate number of layers balances electrical conductivity with transparency
Process
 Initial cleaning – copper items
 DI water, acetone, repeat
 Ammonium persulfate bath
 Tubes – sonicate, then electropolish
 Initial cleaning – nickel items
 DI water, acetone, isopropanol
Process
 Pressure must be at 50 torr to open vacuum tube and mount sample
 Flushing the system
 100 sccm of methane for 10 minutes
 100 sccm of hydrogen for 10 minutes
 100 sccm of argon for 10 minutes
Process
 Oxide removal in furnace
 35 sccm of hydrogen
 Temperatures
 Nickel – 1000°C
 Copper - 1035°C
 Cooking times
 Foils and nickel foam: 70 minutes
 Copper tubes and ball: 50 minutes
Process – Methane Exposure
 Ni foil (few layer)
 CH4/H2 – 35/2 sccm
 30 minutes
 Ni foam
 CH4/H2 – 35/2 sccm
 5 minutes
Nickel foil and foam – 20x
Process – Methane Exposure
 Copper balls and tubes
 CH4/H2 – 40/15 sccm
 30 minutes
Copper ball and tube control – 20x
Before cleaning
Copper ball and tube with graphene?
Tube, 100x
Ball, 20x
Tube, 20x
Process – Methane Exposure
 Monolayer Graphene on Cu foil
 CH4/H2 – 35/2 sccm
 30 minutes
 Bilayer Graphene on Cu foil
 CH4/H2 – 16/70 sccm
 120 minutes
Copper foil
Monolayer, 20x Bilayer, 100x
Future Goals
 Confirm graphene growth on Cu tubes and balls
 Uniform samples on Ni foil and foam
Sources
 http://physicsworld.com/cws/article/news/2010/may/12/few-layer-graphene-
keeps-its-cool
 http://www.crcnetbase.com/doi/abs/10.1201/b19461-35
 “Thermal properties of graphene and few-layer graphene: applications in
electronics” http://ndl.ee.ucr.edu/IET-Review-2015.pdf

More Related Content

Similar to Graphene growth

Santosh_Kr_Yadav_RAIM08
Santosh_Kr_Yadav_RAIM08Santosh_Kr_Yadav_RAIM08
Santosh_Kr_Yadav_RAIM08
Santosh Kumar Yadav
 
Synthesis of radiometals from solid targets used for radiolabeling
Synthesis of radiometals from solid targets used for radiolabelingSynthesis of radiometals from solid targets used for radiolabeling
Synthesis of radiometals from solid targets used for radiolabeling
Comecer
 
Hot wire Anemometer: microfabrication
Hot wire Anemometer: microfabricationHot wire Anemometer: microfabrication
Hot wire Anemometer: microfabrication
davidecamm
 
application of carbon nano tube in chromatography
application of carbon nano tube in chromatographyapplication of carbon nano tube in chromatography
application of carbon nano tube in chromatography
Abdolah Karimgolan
 
Heat loss in bare and lagged pipes
Heat loss in bare and lagged pipesHeat loss in bare and lagged pipes
Heat loss in bare and lagged pipes
Nicely Jane Eleccion
 
Mattson-RTP-3000.pdf
Mattson-RTP-3000.pdfMattson-RTP-3000.pdf
Mattson-RTP-3000.pdf
ACAllen2
 
Reformer Tube Metallurgy: Design Considerations; Failure Mechanisms; Inspecti...
Reformer Tube Metallurgy: Design Considerations; Failure Mechanisms; Inspecti...Reformer Tube Metallurgy: Design Considerations; Failure Mechanisms; Inspecti...
Reformer Tube Metallurgy: Design Considerations; Failure Mechanisms; Inspecti...
Gerard B. Hawkins
 
M.S.ThesisDefense
M.S.ThesisDefenseM.S.ThesisDefense
M.S.ThesisDefense
Nicole Pacheco
 
Softening point of bitumious
Softening point of bitumiousSoftening point of bitumious
Softening point of bitumious
Taha Samir
 
Vapor growth of binary and ternary phosphorus-based semiconductors into TiO2 ...
Vapor growth of binary and ternary phosphorus-based semiconductors into TiO2 ...Vapor growth of binary and ternary phosphorus-based semiconductors into TiO2 ...
Vapor growth of binary and ternary phosphorus-based semiconductors into TiO2 ...
Pawan Kumar
 
Ihcp analysis of qc10 vs nak80 (9 nov 2010)linkedin
Ihcp analysis of qc10 vs nak80 (9 nov 2010)linkedinIhcp analysis of qc10 vs nak80 (9 nov 2010)linkedin
Ihcp analysis of qc10 vs nak80 (9 nov 2010)linkedin
mikekraemer
 
Ihcp Analysis Of Qc10 Vs Nak80 (9 Nov 2010)Linkedin
Ihcp Analysis Of Qc10 Vs Nak80 (9 Nov 2010)LinkedinIhcp Analysis Of Qc10 Vs Nak80 (9 Nov 2010)Linkedin
Ihcp Analysis Of Qc10 Vs Nak80 (9 Nov 2010)Linkedin
mikekraemer
 
Maliha ela
Maliha elaMaliha ela
Maliha ela
Maliha Ela
 
Studyoftheeffectofagingconditiononstrengthhardnessof6063t5alloy 130117231644-...
Studyoftheeffectofagingconditiononstrengthhardnessof6063t5alloy 130117231644-...Studyoftheeffectofagingconditiononstrengthhardnessof6063t5alloy 130117231644-...
Studyoftheeffectofagingconditiononstrengthhardnessof6063t5alloy 130117231644-...
Ramesh Mishra
 
CNT
CNTCNT
F10 lec01 overview
F10 lec01 overviewF10 lec01 overview
F10 lec01 overview
fredhvcc
 
Thapar_Paarth_2015GOMD-hj
Thapar_Paarth_2015GOMD-hjThapar_Paarth_2015GOMD-hj
Thapar_Paarth_2015GOMD-hj
Paarth Thapar
 
carbon nanotube antenna
carbon nanotube antenna carbon nanotube antenna
carbon nanotube antenna
sree3724
 
Fabrication of through silicon-via (tsv) by copper
Fabrication of through silicon-via (tsv) by copperFabrication of through silicon-via (tsv) by copper
Fabrication of through silicon-via (tsv) by copper
Mirza Baig
 
SLIDE VIVA APRIL 2016
SLIDE VIVA APRIL 2016SLIDE VIVA APRIL 2016
SLIDE VIVA APRIL 2016
myrahalimi
 

Similar to Graphene growth (20)

Santosh_Kr_Yadav_RAIM08
Santosh_Kr_Yadav_RAIM08Santosh_Kr_Yadav_RAIM08
Santosh_Kr_Yadav_RAIM08
 
Synthesis of radiometals from solid targets used for radiolabeling
Synthesis of radiometals from solid targets used for radiolabelingSynthesis of radiometals from solid targets used for radiolabeling
Synthesis of radiometals from solid targets used for radiolabeling
 
Hot wire Anemometer: microfabrication
Hot wire Anemometer: microfabricationHot wire Anemometer: microfabrication
Hot wire Anemometer: microfabrication
 
application of carbon nano tube in chromatography
application of carbon nano tube in chromatographyapplication of carbon nano tube in chromatography
application of carbon nano tube in chromatography
 
Heat loss in bare and lagged pipes
Heat loss in bare and lagged pipesHeat loss in bare and lagged pipes
Heat loss in bare and lagged pipes
 
Mattson-RTP-3000.pdf
Mattson-RTP-3000.pdfMattson-RTP-3000.pdf
Mattson-RTP-3000.pdf
 
Reformer Tube Metallurgy: Design Considerations; Failure Mechanisms; Inspecti...
Reformer Tube Metallurgy: Design Considerations; Failure Mechanisms; Inspecti...Reformer Tube Metallurgy: Design Considerations; Failure Mechanisms; Inspecti...
Reformer Tube Metallurgy: Design Considerations; Failure Mechanisms; Inspecti...
 
M.S.ThesisDefense
M.S.ThesisDefenseM.S.ThesisDefense
M.S.ThesisDefense
 
Softening point of bitumious
Softening point of bitumiousSoftening point of bitumious
Softening point of bitumious
 
Vapor growth of binary and ternary phosphorus-based semiconductors into TiO2 ...
Vapor growth of binary and ternary phosphorus-based semiconductors into TiO2 ...Vapor growth of binary and ternary phosphorus-based semiconductors into TiO2 ...
Vapor growth of binary and ternary phosphorus-based semiconductors into TiO2 ...
 
Ihcp analysis of qc10 vs nak80 (9 nov 2010)linkedin
Ihcp analysis of qc10 vs nak80 (9 nov 2010)linkedinIhcp analysis of qc10 vs nak80 (9 nov 2010)linkedin
Ihcp analysis of qc10 vs nak80 (9 nov 2010)linkedin
 
Ihcp Analysis Of Qc10 Vs Nak80 (9 Nov 2010)Linkedin
Ihcp Analysis Of Qc10 Vs Nak80 (9 Nov 2010)LinkedinIhcp Analysis Of Qc10 Vs Nak80 (9 Nov 2010)Linkedin
Ihcp Analysis Of Qc10 Vs Nak80 (9 Nov 2010)Linkedin
 
Maliha ela
Maliha elaMaliha ela
Maliha ela
 
Studyoftheeffectofagingconditiononstrengthhardnessof6063t5alloy 130117231644-...
Studyoftheeffectofagingconditiononstrengthhardnessof6063t5alloy 130117231644-...Studyoftheeffectofagingconditiononstrengthhardnessof6063t5alloy 130117231644-...
Studyoftheeffectofagingconditiononstrengthhardnessof6063t5alloy 130117231644-...
 
CNT
CNTCNT
CNT
 
F10 lec01 overview
F10 lec01 overviewF10 lec01 overview
F10 lec01 overview
 
Thapar_Paarth_2015GOMD-hj
Thapar_Paarth_2015GOMD-hjThapar_Paarth_2015GOMD-hj
Thapar_Paarth_2015GOMD-hj
 
carbon nanotube antenna
carbon nanotube antenna carbon nanotube antenna
carbon nanotube antenna
 
Fabrication of through silicon-via (tsv) by copper
Fabrication of through silicon-via (tsv) by copperFabrication of through silicon-via (tsv) by copper
Fabrication of through silicon-via (tsv) by copper
 
SLIDE VIVA APRIL 2016
SLIDE VIVA APRIL 2016SLIDE VIVA APRIL 2016
SLIDE VIVA APRIL 2016
 

Recently uploaded

Medical Orthopedic PowerPoint Templates.pptx
Medical Orthopedic PowerPoint Templates.pptxMedical Orthopedic PowerPoint Templates.pptx
Medical Orthopedic PowerPoint Templates.pptx
terusbelajar5
 
Shallowest Oil Discovery of Turkiye.pptx
Shallowest Oil Discovery of Turkiye.pptxShallowest Oil Discovery of Turkiye.pptx
Shallowest Oil Discovery of Turkiye.pptx
Gokturk Mehmet Dilci
 
Compexometric titration/Chelatorphy titration/chelating titration
Compexometric titration/Chelatorphy titration/chelating titrationCompexometric titration/Chelatorphy titration/chelating titration
Compexometric titration/Chelatorphy titration/chelating titration
Vandana Devesh Sharma
 
Sharlene Leurig - Enabling Onsite Water Use with Net Zero Water
Sharlene Leurig - Enabling Onsite Water Use with Net Zero WaterSharlene Leurig - Enabling Onsite Water Use with Net Zero Water
Sharlene Leurig - Enabling Onsite Water Use with Net Zero Water
Texas Alliance of Groundwater Districts
 
molar-distalization in orthodontics-seminar.pptx
molar-distalization in orthodontics-seminar.pptxmolar-distalization in orthodontics-seminar.pptx
molar-distalization in orthodontics-seminar.pptx
Anagha Prasad
 
EWOCS-I: The catalog of X-ray sources in Westerlund 1 from the Extended Weste...
EWOCS-I: The catalog of X-ray sources in Westerlund 1 from the Extended Weste...EWOCS-I: The catalog of X-ray sources in Westerlund 1 from the Extended Weste...
EWOCS-I: The catalog of X-ray sources in Westerlund 1 from the Extended Weste...
Sérgio Sacani
 
Thornton ESPP slides UK WW Network 4_6_24.pdf
Thornton ESPP slides UK WW Network 4_6_24.pdfThornton ESPP slides UK WW Network 4_6_24.pdf
Thornton ESPP slides UK WW Network 4_6_24.pdf
European Sustainable Phosphorus Platform
 
Oedema_types_causes_pathophysiology.pptx
Oedema_types_causes_pathophysiology.pptxOedema_types_causes_pathophysiology.pptx
Oedema_types_causes_pathophysiology.pptx
muralinath2
 
NuGOweek 2024 Ghent programme overview flyer
NuGOweek 2024 Ghent programme overview flyerNuGOweek 2024 Ghent programme overview flyer
NuGOweek 2024 Ghent programme overview flyer
pablovgd
 
The debris of the ‘last major merger’ is dynamically young
The debris of the ‘last major merger’ is dynamically youngThe debris of the ‘last major merger’ is dynamically young
The debris of the ‘last major merger’ is dynamically young
Sérgio Sacani
 
ESR spectroscopy in liquid food and beverages.pptx
ESR spectroscopy in liquid food and beverages.pptxESR spectroscopy in liquid food and beverages.pptx
ESR spectroscopy in liquid food and beverages.pptx
PRIYANKA PATEL
 
Equivariant neural networks and representation theory
Equivariant neural networks and representation theoryEquivariant neural networks and representation theory
Equivariant neural networks and representation theory
Daniel Tubbenhauer
 
Topic: SICKLE CELL DISEASE IN CHILDREN-3.pdf
Topic: SICKLE CELL DISEASE IN CHILDREN-3.pdfTopic: SICKLE CELL DISEASE IN CHILDREN-3.pdf
Topic: SICKLE CELL DISEASE IN CHILDREN-3.pdf
TinyAnderson
 
Applied Science: Thermodynamics, Laws & Methodology.pdf
Applied Science: Thermodynamics, Laws & Methodology.pdfApplied Science: Thermodynamics, Laws & Methodology.pdf
Applied Science: Thermodynamics, Laws & Methodology.pdf
University of Hertfordshire
 
Eukaryotic Transcription Presentation.pptx
Eukaryotic Transcription Presentation.pptxEukaryotic Transcription Presentation.pptx
Eukaryotic Transcription Presentation.pptx
RitabrataSarkar3
 
bordetella pertussis.................................ppt
bordetella pertussis.................................pptbordetella pertussis.................................ppt
bordetella pertussis.................................ppt
kejapriya1
 
SAR of Medicinal Chemistry 1st by dk.pdf
SAR of Medicinal Chemistry 1st by dk.pdfSAR of Medicinal Chemistry 1st by dk.pdf
SAR of Medicinal Chemistry 1st by dk.pdf
KrushnaDarade1
 
Unlocking the mysteries of reproduction: Exploring fecundity and gonadosomati...
Unlocking the mysteries of reproduction: Exploring fecundity and gonadosomati...Unlocking the mysteries of reproduction: Exploring fecundity and gonadosomati...
Unlocking the mysteries of reproduction: Exploring fecundity and gonadosomati...
AbdullaAlAsif1
 
Authoring a personal GPT for your research and practice: How we created the Q...
Authoring a personal GPT for your research and practice: How we created the Q...Authoring a personal GPT for your research and practice: How we created the Q...
Authoring a personal GPT for your research and practice: How we created the Q...
Leonel Morgado
 
8.Isolation of pure cultures and preservation of cultures.pdf
8.Isolation of pure cultures and preservation of cultures.pdf8.Isolation of pure cultures and preservation of cultures.pdf
8.Isolation of pure cultures and preservation of cultures.pdf
by6843629
 

Recently uploaded (20)

Medical Orthopedic PowerPoint Templates.pptx
Medical Orthopedic PowerPoint Templates.pptxMedical Orthopedic PowerPoint Templates.pptx
Medical Orthopedic PowerPoint Templates.pptx
 
Shallowest Oil Discovery of Turkiye.pptx
Shallowest Oil Discovery of Turkiye.pptxShallowest Oil Discovery of Turkiye.pptx
Shallowest Oil Discovery of Turkiye.pptx
 
Compexometric titration/Chelatorphy titration/chelating titration
Compexometric titration/Chelatorphy titration/chelating titrationCompexometric titration/Chelatorphy titration/chelating titration
Compexometric titration/Chelatorphy titration/chelating titration
 
Sharlene Leurig - Enabling Onsite Water Use with Net Zero Water
Sharlene Leurig - Enabling Onsite Water Use with Net Zero WaterSharlene Leurig - Enabling Onsite Water Use with Net Zero Water
Sharlene Leurig - Enabling Onsite Water Use with Net Zero Water
 
molar-distalization in orthodontics-seminar.pptx
molar-distalization in orthodontics-seminar.pptxmolar-distalization in orthodontics-seminar.pptx
molar-distalization in orthodontics-seminar.pptx
 
EWOCS-I: The catalog of X-ray sources in Westerlund 1 from the Extended Weste...
EWOCS-I: The catalog of X-ray sources in Westerlund 1 from the Extended Weste...EWOCS-I: The catalog of X-ray sources in Westerlund 1 from the Extended Weste...
EWOCS-I: The catalog of X-ray sources in Westerlund 1 from the Extended Weste...
 
Thornton ESPP slides UK WW Network 4_6_24.pdf
Thornton ESPP slides UK WW Network 4_6_24.pdfThornton ESPP slides UK WW Network 4_6_24.pdf
Thornton ESPP slides UK WW Network 4_6_24.pdf
 
Oedema_types_causes_pathophysiology.pptx
Oedema_types_causes_pathophysiology.pptxOedema_types_causes_pathophysiology.pptx
Oedema_types_causes_pathophysiology.pptx
 
NuGOweek 2024 Ghent programme overview flyer
NuGOweek 2024 Ghent programme overview flyerNuGOweek 2024 Ghent programme overview flyer
NuGOweek 2024 Ghent programme overview flyer
 
The debris of the ‘last major merger’ is dynamically young
The debris of the ‘last major merger’ is dynamically youngThe debris of the ‘last major merger’ is dynamically young
The debris of the ‘last major merger’ is dynamically young
 
ESR spectroscopy in liquid food and beverages.pptx
ESR spectroscopy in liquid food and beverages.pptxESR spectroscopy in liquid food and beverages.pptx
ESR spectroscopy in liquid food and beverages.pptx
 
Equivariant neural networks and representation theory
Equivariant neural networks and representation theoryEquivariant neural networks and representation theory
Equivariant neural networks and representation theory
 
Topic: SICKLE CELL DISEASE IN CHILDREN-3.pdf
Topic: SICKLE CELL DISEASE IN CHILDREN-3.pdfTopic: SICKLE CELL DISEASE IN CHILDREN-3.pdf
Topic: SICKLE CELL DISEASE IN CHILDREN-3.pdf
 
Applied Science: Thermodynamics, Laws & Methodology.pdf
Applied Science: Thermodynamics, Laws & Methodology.pdfApplied Science: Thermodynamics, Laws & Methodology.pdf
Applied Science: Thermodynamics, Laws & Methodology.pdf
 
Eukaryotic Transcription Presentation.pptx
Eukaryotic Transcription Presentation.pptxEukaryotic Transcription Presentation.pptx
Eukaryotic Transcription Presentation.pptx
 
bordetella pertussis.................................ppt
bordetella pertussis.................................pptbordetella pertussis.................................ppt
bordetella pertussis.................................ppt
 
SAR of Medicinal Chemistry 1st by dk.pdf
SAR of Medicinal Chemistry 1st by dk.pdfSAR of Medicinal Chemistry 1st by dk.pdf
SAR of Medicinal Chemistry 1st by dk.pdf
 
Unlocking the mysteries of reproduction: Exploring fecundity and gonadosomati...
Unlocking the mysteries of reproduction: Exploring fecundity and gonadosomati...Unlocking the mysteries of reproduction: Exploring fecundity and gonadosomati...
Unlocking the mysteries of reproduction: Exploring fecundity and gonadosomati...
 
Authoring a personal GPT for your research and practice: How we created the Q...
Authoring a personal GPT for your research and practice: How we created the Q...Authoring a personal GPT for your research and practice: How we created the Q...
Authoring a personal GPT for your research and practice: How we created the Q...
 
8.Isolation of pure cultures and preservation of cultures.pdf
8.Isolation of pure cultures and preservation of cultures.pdf8.Isolation of pure cultures and preservation of cultures.pdf
8.Isolation of pure cultures and preservation of cultures.pdf
 

Graphene growth