The document discusses the joint development of new anhydride-free epoxy-based vacuum pressure impregnation (VPI) systems and mica tapes for large generators and motors. After over two years of cooperation between Huntsman and Isovolta, three potential candidate systems have been identified that are free of anhydrides and other substances of concern. The candidates show promising material properties without tapes and good performance when combined with new tapes developed specifically for them. Further testing of the system candidates is ongoing.
POTENTIAL SERVICES, EXPECTED SERVICES
BASIC SERVICES, CORE BENEFIT, Line of visibility,
Service Design- 8 steps , Gaps Model of Service Quality,Provider Gap 1,Provider Gap 2,Key Factors Leading to Provider Gap 2,Provider Gap 3,Key Factors Leading to Provider Gap 4, Zone of Tolerance
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First of it's kind Project attempted it India , working closely with VP, Innovation ,conceptualizing and devising a framework to gauge Customer Sentiment Index for the Indian Broadband Industry .The deliverable included :-
• Consider customer life-cycle touch-points for a Broadband customer
• Identify & define the relationships between Key determinants of the Broadband services
• Use ACEI Model as the baseline towards the Indian broadband Industry and help understand customer behaviour, their intention to spend, intent to recommend, usage of interactive service, intent to change operator etc
• Help understand key business drivers & their impact on service delivery
• Identify target customer segments for future strategic decisions
Highly appreciated for project completion within 9 months of inception, for first of its kind project attempted in India
Won best Research Project for the Amdocs Innovation Team 2013
Successful Pilot run completion in 2014 displaying huge impact to Amdocs Customer Experience Solutions (CES) Portfolio.
This is complete report you will require to make Export Import Report for India's Global Trade.. Pls give your likes and comments.. and pass on this to others..
POTENTIAL SERVICES, EXPECTED SERVICES
BASIC SERVICES, CORE BENEFIT, Line of visibility,
Service Design- 8 steps , Gaps Model of Service Quality,Provider Gap 1,Provider Gap 2,Key Factors Leading to Provider Gap 2,Provider Gap 3,Key Factors Leading to Provider Gap 4, Zone of Tolerance
Research project on customer sentiment indexAditya Basu
First of it's kind Project attempted it India , working closely with VP, Innovation ,conceptualizing and devising a framework to gauge Customer Sentiment Index for the Indian Broadband Industry .The deliverable included :-
• Consider customer life-cycle touch-points for a Broadband customer
• Identify & define the relationships between Key determinants of the Broadband services
• Use ACEI Model as the baseline towards the Indian broadband Industry and help understand customer behaviour, their intention to spend, intent to recommend, usage of interactive service, intent to change operator etc
• Help understand key business drivers & their impact on service delivery
• Identify target customer segments for future strategic decisions
Highly appreciated for project completion within 9 months of inception, for first of its kind project attempted in India
Won best Research Project for the Amdocs Innovation Team 2013
Successful Pilot run completion in 2014 displaying huge impact to Amdocs Customer Experience Solutions (CES) Portfolio.
This is complete report you will require to make Export Import Report for India's Global Trade.. Pls give your likes and comments.. and pass on this to others..
Offering a unique service which was not not earlier offered into the market is called new service and the process of designing such new service is called New Service Development.
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Summary of changes in vat deduction at source sandra & associatesKhalid Iftekhar
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This snapshot reflects the differences between the two laws in respect to withholding VAT regime. I hope the users will find this helpful
LOCTITE 420 INSTANT ADHESIVE is a general purpose cyanoacrylate wicking type plastic bonder. Mil Spec: Mil-A-46050C Type II Class I. Commercial Item Description A-A-3097: Type II Class 1.
GC-7800 is a classical gas chromatograph instrument which integrates the most advanced chromatography technique and national or international standards with the most extensive applications by the experienced experts of Labthink.
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Watch the presentation of this webinar here: https://bit.ly/3kk0Qs1
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Detailed description:
In this webinar we will discuss the implications of the EU GMP Annex 1 draft on the filtration of medicinal products and how this impacts the validation studies.
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Watch the presentation of this webinar here: https://bit.ly/3kk0Qs1
In this webinar, you will learn:
- About the GMP Annex 1 draft regulatory overview
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Detailed description:
In this webinar we will discuss the implications of the EU GMP Annex 1 draft on the filtration of medicinal products and how this impacts the validation studies.
Bacterial Retention Testing is a critical part of the manufacturing validation process and is required by all regulatory bodies worldwide. Using case studies, our experts will explain how the Annex 1 draft is incorporated into the filtration systems validation exercise, specifically for integrity testing & PUPSIT (Pre-Use Post Sterilization Integrity Testing), the selection and justification of the appropriate test organism, and validation implications of single versus multiple use.
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In this insightful webinar, Inflectra explores how artificial intelligence (AI) is transforming software development and testing. Discover how AI-powered tools are revolutionizing every stage of the software development lifecycle (SDLC), from design and prototyping to testing, deployment, and monitoring.
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The IoT and OT threat landscape report has been prepared by the Threat Research Team at Sectrio using data from Sectrio, cyber threat intelligence farming facilities spread across over 85 cities around the world. In addition, Sectrio also runs AI-based advanced threat and payload engagement facilities that serve as sinks to attract and engage sophisticated threat actors, and newer malware including new variants and latent threats that are at an earlier stage of development.
The latest edition of the OT/ICS and IoT security Threat Landscape Report 2024 also covers:
State of global ICS asset and network exposure
Sectoral targets and attacks as well as the cost of ransom
Global APT activity, AI usage, actor and tactic profiles, and implications
Rise in volumes of AI-powered cyberattacks
Major cyber events in 2024
Malware and malicious payload trends
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Attacks on counties – USA
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In-depth analysis of the cyber threat landscape across North America, South America, Europe, APAC, and the Middle East
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1. Insights into SAP testing best practices
2. Heatmap utilization for testing
3. Optimization of testing processes
4. Demo
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Execution from the test manager
Orchestrator execution result
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The software team must secure its software delivery process to avoid vulnerability and security breaches. This needs to be achieved with existing tool chains and without extensive rework of the delivery processes. This talk will present strategies and techniques for providing visibility into the true risk of the existing vulnerabilities, preventing the introduction of security issues in the software, resolving vulnerabilities in production environments quickly, and capturing the deployment bill of materials (DBOM).
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Paper presented at SYNERGY workshop at AVI 2024, Genoa, Italy. 3rd June 2024
https://alandix.com/academic/papers/synergy2024-epistemic/
As machine learning integrates deeper into human-computer interactions, the concept of epistemic interaction emerges, aiming to refine these interactions to enhance system adaptability. This approach encourages minor, intentional adjustments in user behaviour to enrich the data available for system learning. This paper introduces epistemic interaction within the context of human-system communication, illustrating how deliberate interaction design can improve system understanding and adaptation. Through concrete examples, we demonstrate the potential of epistemic interaction to significantly advance human-computer interaction by leveraging intuitive human communication strategies to inform system design and functionality, offering a novel pathway for enriching user-system engagements.
Let's dive deeper into the world of ODC! Ricardo Alves (OutSystems) will join us to tell all about the new Data Fabric. After that, Sezen de Bruijn (OutSystems) will get into the details on how to best design a sturdy architecture within ODC.
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JMeter webinar - integration with InfluxDB and GrafanaRTTS
Watch this recorded webinar about real-time monitoring of application performance. See how to integrate Apache JMeter, the open-source leader in performance testing, with InfluxDB, the open-source time-series database, and Grafana, the open-source analytics and visualization application.
In this webinar, we will review the benefits of leveraging InfluxDB and Grafana when executing load tests and demonstrate how these tools are used to visualize performance metrics.
Length: 30 minutes
Session Overview
-------------------------------------------
During this webinar, we will cover the following topics while demonstrating the integrations of JMeter, InfluxDB and Grafana:
- What out-of-the-box solutions are available for real-time monitoring JMeter tests?
- What are the benefits of integrating InfluxDB and Grafana into the load testing stack?
- Which features are provided by Grafana?
- Demonstration of InfluxDB and Grafana using a practice web application
To view the webinar recording, go to:
https://www.rttsweb.com/jmeter-integration-webinar
Leading Change strategies and insights for effective change management pdf 1.pdf
Egmont Kattnig Isovolta
1. Advanced Materials
New Anhydride-free Epoxy-based
Vacuum Pressure Impregnation Systems and
New Mica-tapes for Large Generators and Motors
C. Beisele Dr. E. Kattnig
Huntsman Advanced Materials Isovolta AG
Switzerland Austria
3. Advanced Materials
Outline
1. Introduction
- REACH
- Replacement issue
2. Joint development of new MHHPA-free Electrical Insulation Systems
3. Target profile
4. New candidates
- Bath material properties without tape
- System properties with new tapes
5. Next steps in the project
6. Summary & Conclusions
3
4. Advanced Materials
4
The REACH Process: Latest view: Sunset date for
(M)HHPA June 2023 if no authorisation
The REACH process and current Anhydride status
SVHC list
Proposal
list Annex
XIV
Annex
XIV
MHHPA and
HHPA were
added to the
SVHC candidate
list on Dec, 19th
2012
ECHA added
(M)HHPA to
priority list on
Sept 2018
Public
Consultation Sunset date
Until Dec 4th 2018,
affected parties
can submit info on
economic, social,
health & environ-
mental impact of
(M)HHPA inclusion
to Annex XIV
Decision process
of MSC
EC
Decision
making
Application
for
Authori-
sation of
(M)HHPA:
18 months
June
2018
* Dec 2019
Decision
making by EC
on (M)HHPA:
Expected to
take 18
months
LAD
Author
isation
* June 2020
Sunset
period for
(M)HHPA:
18 months
*June 2023
(M)HHPA use
restricted in
EU if no
authorisation
*Earliest estimated timeline, based on todays available information
5. Advanced Materials5
1. Why MHHPA is used today for VPI
• Excellent stability of the VPI-bath (distilled BLR + MHHPA)
• Low tan delta at high temperature
• High thermal aging stability
• Long term experience
2. Issues in replacement
• Alternative anhydrides tend to increase bath viscosity
• Alternative anhydrides show higher tan delta at high temperature
• Available pre-catalyzed anhydride-free VPI system:
- higher viscous
- high hot tan delta
- less thermal aging stable
O
O
O
VPI of Large Generators and Motors
8. Advanced Materials8
Current state of the art:
Electrical Insulation System, consisting of
1.) Impregnation system, consisting of epoxy resin and MHHPA
2.) Mica tape, containing a catalyst (Zn-naphthenate) promoting the polyaddition of
epoxy and anhydrides
New Concept:
1.) New Impregnation system, epoxy-based and free of anhydride
2.) New Mica tape, containing a catalyst promoting the homopolymerisation of
epoxy
Joint development of new EIS by specialists for each part
(Huntsman for resin / Isovolta for tape)
2. Joint Development of New MHHPA-free
Electrical Insulation Systems
9. Advanced Materials
After >2 years of cooperation and intensive lab work,
3 potential candidates have been identified
9
Joint development of new ANH-free VPI system combining leading knowledge
in Mica tape (incl. catalyst) and impregnation resin
2014: 10 potential candidates have been identified
Screening of catalysts and selection of 5 promising candidates:
Pre trials on reactivity, Tg, etc
Development of bath formulations & pre-trials with catalyst in Mica tapes
Development of bath systems / determination of recommended catalyst contents
Measurement of bath data & Storage stability test
Pre-tests of combinations: new bath systems with new tapes pre-selection of 3 candidates
Next steps:
Pilot productions of tapes and bath
Application tests of system
Customer sampling of new tape and new bath
Optimisation of bath and tapes
3 potential
candidates
identified
> 2 years
cooperation and lab
work
10 candiates
2012 2013-2015 2016 2017 2017-2020
Technology approach and complexity
10. Advanced Materials10
• Material properties
- EHS + REACH: SVHC-free Anhydride-free, no critical volatiles
- Viscosity: No must criteria (Ref.: 30 mPas @ 60 °C), important: good impregnation
- Bath stability: ∆η (10 d @ 60 °C) < 2.2 mPas
- Gel time: 10 min. @140 °C (wish)
• Processing requirements
- Curing temp.: <200 °C (must) <150 °C (wish)
- Curing time < 24 h
- Nr. of components: 1
- Bath temperature: <70 °C
- Stability of catalyst in tape: Comparable to reference
• Cured properties
- Tg: 120 – 160 °C (must) 140 – 150 °C (wish)
- Strength: comparable to AH-reference (~40 MPa)
- Thermal aging stability: TI >180 °C (must) TI > 200 °C (wish)
- Hot tan delta: <10 % @ 155 °C
3. Target Profile
11. Advanced Materials11
New Epoxy systems based on 3 different homo-polymerization catalysts
+ Anhydride-free
+ No REACH issue
+ Good working hygiene
+ Single-component Constance of composition
+ Superior bath stability
+ No tank cooling need
+ (Partly) lower hot tan delta
~ Various reactivity levels
- Higher viscosity
- Higher curing temperatures
4. New Bath Materials
12. Advanced Materials12
Reference New 1 New 2 New 3
Catalyst-type Zn-Napht. Catalyst "DY" Catalyst "EP" Catalyst "MA"
Bath systems
MY 790-1 /
HY 1102
LME 11173
(11243)
LME 11173
(11242)
LME 11096-1
Initial viscosity bath (Rheomat)
25°C mPa s 250 2309 2309 388
60°C mPa s 31 94 94 46
80°C mPa s 15 37 37 21
Viscosity at 60°C (VST 1000) mPa s 31,0 100,3 100,3 46,4
Viscosity at 60°C, after 10 d at 60 °C mPa s 33,0 100,3 100,3 46,0
gel time 80°C 33h 42 min > 5 days 8h 50 min
gel time 120°C 28 min 30s 2h 12 min 5 min 40s
gel time 140°C 21 min * 6 min 20s 17 min 30s 2 min
Cure condition
(for test specimen preparation)
16h 90°C +
10h 140°C
4h 100°C +
10h 170°C
4h 125°C +
12h 170°C
2h 90°C +
2h 130°C +
10h 180°C
Tg (DSC) °C 144 * 153 / 154 140 / 142 173 / 194 (TMA)
Tensile strength MPa 45* 43 49 36
Elongation at break % 1.75* 1,8 2,5 1,2
T (5% ∆m) in TGA (20K/min) °C 390* 420 420 380
Loss factor tan δ (50 Hz, 155 °C) % 8.0* 4,7 2,7 5,8
* Catalyst for testing without tape was 0.16 pbw DY 9577 / 0.04 pbw DY 073-1
New AH-free VPI Systems vs. Reference
(data without tape)
13. Advanced Materials
LME 11096-1 – Impact of lower curing T
LME 11096-1 99.84 99.84
XB 6079 A (Mayer catal.) 0.16 0.16
Initial viscosity at (without accelerator*)
25°C mPa s 388 388
30°C 291 291
40°C mPa s 142 142
60°C mPa s 46.4 46.4
80°C mPa s 21.1 21.1
DSC Reaction (10°/min / 30 - 350°C)
max. Peak / Enthalpie 153 / 477 153 / 477
GZ 70°C (Gelnorm) 18h 15 min 18h 15 min
GZ 80°C (Gelnorm) 8h 50 min 8h 50 min
GZ 90°C (Gelnorm) 3h 42 min 3h 42 min
GZ 100°C (Gelnorm) 56 min 30s 56 min 30s
GZ 120°C (Gelnorm) 5 min 40s 5 min 40s
GZ 140°C (Gelnorm) 2 min 2 min
cure cycle 2h 90°C+2h 130°C+10h 180°C 2h 90°C+2h 130°C+20h 160°C
TGA 35 - 800°C (20°/min)
5% loss °C 385 385
Tg / TMA (DSC) °C 173 / 194 140/145
E-Modulus from flexural strength MPa 3335 3295
Flexural strength MPa 77 74
Surface strain % 2.2 2.2
E-Modulus from tensile strength MPa 3215 3205
Tensile strength MPa 36 29
Elongation at break % 1.2 0.9
Shrinkage Length % 1.31 1.30
Loss factor tan δ (50 Hz)
at 155°C % 5.8 7.4
14. Advanced Materials
Tape Materials and Composition
14
Uncalcinated mica paper: 160 g/m2
Glass carrier: 24 g/m2
Resin content: 10-15 g/m2
• Different resin components and application technics tested (design A-F) to
fine-tune:
− Mechanic properties and mica consolidation
− Mica-glass adhesion
− Catalyst immobilization
− Compatibility with VPI resin
Accelerator: MA, DY, and EP
• Accelerator amount in tapes can be adjusted to further optimize curing
behavior and dielectric properties
Mica
Resin
Glass
15. Advanced Materials
Hot Dissipation Factor of Lab Samples
15
54
69
78
46
0
20
40
60
80
100
120
EP-LME11173 DY-LME11173 MA-LME11096-1 Zn-EpoxyAnhydride
DF at 155 °C [‰]
16. Advanced Materials
Test Productions and Mechanical
Properties of Tapes
16
Sample
Number
Catalyst Design
Resin
(g/m2)
tan δδδδ
(‰)
Tensile
strength
(N/cm)
Bending
stiffness
(N/m)
Edge tear
resistance
(N)
16E114 MA A 17 78 134 67 94
16E115 DY A 20 69 131 30 -
Design A: material is too tacky
16E145 DY B 15 60 117 34 198
16E146 DY C 16 87 131 38 210
Design B and C: improved mechanical properties; Design C still tacky at 50 °°°°C
16E166 EP B 13 47 104 76 87
16E167 EP D 12 64 130 78 189
16E168 MA B 12 89 100 68 130
16E169 MA D 11 78 121 68 153
Design D: no blocking; tapes are a little stiff but otherwise good mechanics
17E167 MA E 14 57 115 44 141
17E168 MA F 15 55 116 49 142
Design E and F: more flexible tapes with good mechanics
17. Advanced Materials
Mechanical Properties and Dissipation
Factor of MA-tapes Design B, D, and F
17
68
100
130
89
68
121
153
78
49
116
142
55
0
40
80
120
160
200
bending stiffness
[N/m]
tensile strength
[N/cm]
edge tear resistance
[N]
dissipation factor at
155 °C [‰]
16E168 (MA - Design B)
16E169 (MA - Design C)
17E168 (MA - Design F)
18. Advanced Materials18
No mica detachment on roll (16 h at 40 °C)
and during processing
Good processability but small wrinkles
around corners
Flexibility should be further improved
Test Productions and Mechanical
Properties MA-tape, Design F
21. Advanced Materials21
Application Tests
MA-tapes and LME 11096-1
Six bars with MA-tape Design E (16E167) and Design F (16E168) were
prepared and tested
− Impregnation behavior (capacity trend during impregnation)
− Dissipation factor after curing of test bars
− Thermal cycling of test bars
− Voltage endurance test at 3xUn
− Compatibility with system tapes
27. Advanced Materials27
Voltage Endurance at 3x Un
MA-tapes 17E167 and 17E168
Bar ID
Insulation
Material
Time in h kV/mm
average
value
standard
deviation
Test
Voltage in
kV
Insulation
thickness
Organic
Content
[%]
Un in kV
17-201
Poroband
17E167
29,2 16,6
25,2 6,0 33,0
1,99 28,2
1117-202 29,8 17,0 1,94 29,2
17-203 16,7 16,9 1,95 28,6
17-207
Poroband
17E168
22,6 17,1
23,3 4,6 33,0
1,93 28,7
1117-208 29,2 17,2 1,92 27,9
17-209 18,1 17,3 1,91 27,7
28. Advanced Materials28
No wash-out during impregnation
with LME 11096-1
Insufficient bonding after curingafter impregnation
Cover Tape and OCP: MA-System
Impregnation and Curing
no adhesion after curing
Standard tape
Isosseal 4307
No wash-out during impregnation
with LME 11096-1
Insufficient bonding after curing
Conductive tape containing MA-
accelerator in development
29. Advanced Materials29
Stress Grading and MA-System
Impregnation and Curing
EGSB 4308
after impregnation
after curing
after impregnation
after curing
Standard Tape
Disintegration during impregnation
Rough and brittle surface
Stable during impregnation and cure
30. Advanced Materials30
• REACH issue with (M)HHPA due to respiratory sensitization
• MHHPA is difficult to replace for VPI - combines excellent electrical,
mechanical, aging, application technical and economic characteristics
• Isovolta and Huntsman are jointly developing new AH-free electrical
insulation systems for VPI (bath and tapes) to overcome REACH issue
• 3 new epoxy systems presented
• Single component, very good bath stability, no tank cooling
• New tapes produced on production scale
• Target of hot tan delta <10 %@155 °C could be met for all 3 systems
• Tapes show good processability and wettability
• Next steps: Further dielectric testing, tape optimization and customer
trials
• Development and optimization of system tapes (OCP, EGSB, etc.) and
auxiliary materials
Summary & Conclusion
31. Advanced Materials31
References
Beisele, C., Brasch, M., Kattnig, E.: New MHHPA-free Epoxy-based Vacuum Pressure Impregnation Systems and New Mica-tapes for
Large Generators and Motors; Insucon 2017 Conference, Birmingham, UK, May 16-18, 2017
Beisele, C.; Bär, D.; Colliard, S.: TRADITIONAL AND NEW EPOXY SYSTEMS FOR VACUUM PRESSURE IMPREGNATION OF
ELECTRICAL MACHINE, Insucon 2013 Conference, Birmingham, UK, May 29 – 31, 2013
Beisele, C. and Bär, D., “Epoxy Systems for Vacuum Pressure Impregnation of Electrical Machines”, ELROMA 2012 International
Conference on Rotating Machines, Mumbai, India, April 19-20 (2012)
AGREEMENT OF THE MEMBER STATE COMMITTEE ON THE IDENTIFICATION OF HEXAHYDROMETHYLPHTHALIC
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Datasheet Poroband ME 2072 Isovolta AG