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A Look at Engineering Based Approaches to
    Developing Harvest, Processing and
 Controlled Environments for Essential Oil
                Production




                      Murray Hunter
      Centre for Communication & Entrepreneurship
                 University Malaysia Perlis

     Paper presented to the National Conference on Agricultural and Food Mechanization 2012,
                            10-12 January at Pullman, Kuching, Sarawak
The ideal engineer is a composite…He is not a scientist, he is
not a mathematician, he is not a sociologist or a writer; but he
   may use the knowledge and techniques of any of these
         disciplines in solving engineering problems.
                    (N.W. Dougherty, 1955
Over the time that humankind has existed
 upon the earth and society progressed from
   hunter-gatherers to cultivators, we have
encroached upon the Earth’s natural terrestrial
  ecosystems with our agricultural systems.
In fact we do not really understand the
   true interrelationships between the
 variables influencing the results of our
agricultural activities, as most often they
      are not direct cause and effect
      relationships (Lovelock 2005).
Infrastructure      Government
                                                                                                Regulation
                                                                        Positive Inputs          Taxes &
                                             Conducive weather                Water             subsidies
                                                                                                                            Negative Outputs
                    Climate                          Or                     Sunshine              Trade
                                            Floods, droughts, etc            Nitrogen                                             Runoffs, wastes,
                                                                                               environment
                                                                        Agricultural inputs                                          carbon
                                                                                                Research
                Weather                                                   Fertilizers etc
                Rainfall                                                   Knowledge
                 Wind                                                        Labour
               Sunshine
              UV radiation
              Temperature                                                                              Some
                Humidity      Resource inputs,                       Production Processes
                              fertilizers, herbicides,
                                                                                                     recycling
                              insecticides, machinery,                                                back to
   Human                      research capabilities                   Farm size & layout              system
 Habitisation
                                                                    Organisation & methods
       Knowledge               Suitability of conditions
Suppliers & contractors      Pollution (air, land & water)               Propagation
        Pollution                  Labour sources
Attitudes and concerns            Water resources                         Cultivation                          Positive Outputs
                              (create hinterland where                                                            Products
                                     farm part of)
                                                                         Processing
        Physical
      Environment                  Customers
                                   Financing &                            Marketing
                                                                                                                  Revenue flow
                                 various kinds of                                                                   back to
             Soil                     capital
         Topography                                                                                                 system
         Atmosphere
        Natural flora &                                                Negative Inputs
        fauna habitat          Business
         Urbanisation                                                    Adverse physical
                              Environment             Competition           conditions
                                                       Low prices        Pests & diseases
                                    Markets         Changing demand          Pollution
                                    Finance             patterns          Heavy metals
                               Trade environment
                                                                                                     An Agricultural Enterprise as a
                                                                                                                System
Complex algorithms are not linear – too complex to calculate – so we need to be
   guided by heuristical thinking which is in turn guided by “trial & error”
We think only in the short term
We do not truly understand the
interrelationships between the variables
           influencing an action
We discover through trial and error but can
               hypothesize
Location                     Climate                           Genetic Material

                                                      Humidity
                                                                                            Collection

                                                           Temperature                        Purchase
                      Sunshine hours
Topography                                                         UV radiation                 Plant physiology
                               Seasons

  Slope & drainage                                                Propagation                        Yield and
                                      Rainfall                   characteristics                     Chemical
                                                                                                    Constituents
                                                                                                       of the
              Humus                       Nutrients                  Method of extraction           Essential Oil
                                                                     Extraction time
    Compactness                   Drainage & water
                                  holding qualities
                                                                     Pest & weed
                             pH                                        control                    Pre-harvest handling
Mineral residuals                     Irrigation                                                     & preparation
                                                                 Plant
                                                                 densities
                          Soil type                                                          Time & method of
                                                                                                 harvest
                                              Agronomic                       Harvest &
             Soil                             Practices                       Extraction
                                                                              Practices
1.What are the specific technical goals and
objectives?
2.What are the major technology,
infrastructure and climatic constraints
(boundaries)?
3.What are the areas where innovations will
develop quick improvements?
4.What is the probability of successful
outcomes?, and
5.How do we choose between successful
outcomes?
Effectuation is like going to the kitchen cabinet and seeing what ingredients you
 have and then deciding what you can make up for a meal. This is very different
from causation where you have a specific menu in mind and then search out the
                         ingredients to make up the meal.
that there “is also the tendency for Asian countries, including
 Malaysia, to deal with the issue of values in development by
  Importing many technologies and systems wholesale from
     abroad without going through the process of mental
   transformation necessary to master them fully. Although
 Malaysia is going through rapid transformation, our growth
   is one without development in the context of knowledge
      contribution to science, engineering and technology.
         As long as we are consumers and operators of
       sophisticated techniques, plants and technologies
     imported wholesale from abroad, we are to a certain
extent undergoing a technology-less form of industrialization.
   This transformation of values and attitudes is a key issue
             in the nation’s development agenda”[i] .
[i]
 Asma, A., Going Glocal: Cultural Dimensions in Malaysian Management, Kuala Lumpur,
Malaysian Institute of Management, 1995, P. 179.
Essential Oil Crop Harvesting
Selected method often restricted by type of crop



                                       Most herbaceous crops can be mowed




 Many flowers must be hand picked




                                    Innovative systems can be designed and
                                    developed
A Basic Harvest to Distillation Flowchart for
                   Peppermint Oil



    Determination of Harvest time
            (Sampling)




                                             10 tonne fresh herb per Ha.
    Mowing and leaving to wilt on
               field                         Fresh herb contains 80%
                                             moisture




                Wilting                      Must wilt to 50% moisture
                                             level where ‘crisp and
                                             brittle’



    Pick up with forage harvester
                                             Collect 6 tonne of dry herb



                                             Must insure that herb is not
     Deliver to Distillation system          bruised.
                                             Use cartridge or box to
                                             avoid too much handling

                                             Volume of 4 m2 per tonne
                                             of herb.
              Distillation
                                             If single charge, yield 15kg
                                             oil
Assume 35 minutes distillation time, 10
minutes change over, 6.90 litres/minute      If distillate ratio is 0.062/1
steam rate per minute. 9 hours will handle   (oil/water), then 241.8 litres
12 tonnes of dried herb in a vat of 4m 3.    water required for
                                             distillation.
Effectuation in Tea Tree (Melaleuca
      alterniafolia) Harvester
           Development




                           Harvester must make a
                               clean cut here
Harvester must damage the stumps
                                   To promote coppice
                                         growth
RM 4,200,000
RM 200,000
How we really develop new pieces of
equipment utilized for complex tasks
Effectuation in Distillation
      Development
Distillation Principals: Latent Heat
• Molecule speed and energy             Amount of heat required to vapourise a unit
dependent upon temperature              mass of liquid, without raising the
•Change from liquid to gas state        temperature of the vapour above that of the
requires energy                         liquid is called LATENT HEAT of vapourisation
•Due to motion of molecules, all
compounds with determinable
boiling points will emit vapours
from their surafaces, if area closed
this will insert pressure upon the
molecule, termed vapour pressure
•These vapours will saturate the
molecule and take up additional
molecules
•This saturated vapour will carry
other molecules




                Heat and relative pressures are important in distillation
Distillation Principlas Mixed Vapours


   Molecules of                                            Molecules of
   water vapour
                              Molecules of
                                                           water vapour
   a                          water and gas                b
                              vapour



                         Liquid water   Liquid oil
   Liquid                                                  Liquid oil b
   water a               a              b




Eg. Water 99.6c              Together at 99.6c        Eg linalyl acetate
                                                      226c
       The composition of mixed vapours from immiscible liquids
Releasing Oil from Plant Materials

 In steam distillation water condenses of plant surfaces and
 latent heat surrounds the material and raises volatile materials
 to boiling point
Releasing Oil from Plant Materials
    Method of Oil Release through Putative Impression from
    Leaves



                        General vapour space 99c

         98c saturated mixed        Region of oil vapour
                                                                                Vapour phase
         vapour                     elution



Herb surface

       Water liquid            mixed liquids      oil liquids   water liquids
Wild Collection & Distillation




                            Tea Tree
                            Australia
Small Holder (Patchouli Indonesia)
Cambodia (Lemongrass, Cajuput)
Influencing Factors                                                       Historical
       Compound
    characteristics
(volatility/mol. Weight)
 Surrounding Material                                    Compounds          Highly volatile
                                                         mixed with           terpenes
                                                         waxes, also
                                                         lactones,
 Low/medium volatility/stable
                                                         esters etc.

                    Distillation                Solvent                      Cold
                                               Extraction                  Pressing


                                                                            Automated
                                                                            harvest and
  Influencing Factors                           Harvest and
                                                                             distillation
    Price vis. Market                        later load system                system
          Volume
  Plant cell structures
         Field size
        Topography
Soil/field characteristics
    Part of plant (i.e.,                                                      Extensive
       rhizome/leaf)                    Manual                               large scale
         Coppice                                         High --- Low
                                      harvesting                               farming
                                                            Value
                                         due to
                                         scale,
                                        material,                      Specialties
     Distillation                     investment




       Hydro                 Material
                           Characteristics                                   „Finer‟
                                                       CO2                 composition
                                                                            spectrum
      Steam                  Solubility in
                               water
                                                                             Individual
                                                    Fractional
                                                                               aroma
                                                    Distillation
                                                                            compounds
   Destructive               Material
                           Characteristics
Phase One Experimentation
Phase two Scale up
Lid with Clamps
                                                                                     Corrugated Iron Condenser Tank
                                                          Vapour Outlet Running
                                                           into Corrugated Tank




                    Distillation Vat
                                           Vapour Outlet Running Pipe for
                                                                “T”
Counterweight                               into Corrugated Tank Pressure
                                                                Equalisation




                                                                               Oil
                Welded Steel Mesh Bottom
                                                                          Water



   Brick
Compartment      “Firebox” for wood fire



                                                       Constant Level Separator
                                                           Tank
Mixed Vapour Out
                              Critical to understand
Re-vapourisation
                             this behaviour to scale
                                         up
Re-condensation

Re-vapourisation


Re-condensation


Re-vapourisation


Re-condensation

Re-vapourisation


Re-condensation

Re-vapourisation

Re-condensation


        Steam in
Each box can be distilled on rotation
                                      or both together, governed by boiler
                                                    capacity.



                             Boiler




        Box No. 1.                           Box No. 2.


                                           Condensers


Boxes driven in by tractor
and coupled up to steam
  inlet and condenser.

                                           Separators
Conclusion
Technical and social disciplines are
  undergoing convergence which can be
   seen in the way many industries are
 merging together into one. Convergence
     is creeping into the research and
    development process where trans-
 disciplinary approaches are required to
solve problems. Being an engineer is not
   good enough in isolation. In order to
create, an engineer must have knowledge
  across a number of disciplines so that
 knowledge can be synergized into some
  meaningful expressions in the form of
     new applications and inventions.
“Issues facing society to be solved”                      New Forms of
                                                                    Expression
       Other disciplines of                                       Insight Expressed
          knowledge

                                                  Application &
Microbiology
                    Our current Knowledge          Invention

          Biology                Trans-disciplinary synergy of                  Deep Insight
                                          knowledge
                                                                          Engineering


               Agriculture                                            Physics



                                      Chemistry
                                                           Biochemistry
Australia                 2139

         Brunei        3

          China                         3910

      Indonesia        6

           India           627

          Japan                                                                                            26906

Dem. Rep. Korea        4

 Republic Korea                                5935

       Malaysia        54

   New Zealand         316
                       15                             This phenomenon can be seen at a national
     Philippines
                                                      level if one looks at the number of resident
      Singapore            402
                                                      patents filed per million population in each
       Thailand        12                             country.

       Vietnam         9

                   0                5000              10000         15000         20000         25000         30000
Source: WIPO Statistics                               Number of International Patents Filed by Residents
Knowledge without application is useless in
       creating tangible benefits to society,
      but hopefully this paper has shed light
      that it is not knowledge in itself that is
     important rather the ability to apply it.
      And the ability to apply it doesn’t rely
       upon formulae, theory or algorithm,
      but rather emergent thinking and the
 heuristics have developed. This is a neglected
part of engineering education and this is also the
 quality that makes a good engineer stand out
              from the rest of the pack.
Thank
 You

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A look at engineering based approaches to developing harvestProcessing and Controlled Environments for Essential Oil Production

  • 1. A Look at Engineering Based Approaches to Developing Harvest, Processing and Controlled Environments for Essential Oil Production Murray Hunter Centre for Communication & Entrepreneurship University Malaysia Perlis Paper presented to the National Conference on Agricultural and Food Mechanization 2012, 10-12 January at Pullman, Kuching, Sarawak
  • 2. The ideal engineer is a composite…He is not a scientist, he is not a mathematician, he is not a sociologist or a writer; but he may use the knowledge and techniques of any of these disciplines in solving engineering problems. (N.W. Dougherty, 1955
  • 3. Over the time that humankind has existed upon the earth and society progressed from hunter-gatherers to cultivators, we have encroached upon the Earth’s natural terrestrial ecosystems with our agricultural systems.
  • 4. In fact we do not really understand the true interrelationships between the variables influencing the results of our agricultural activities, as most often they are not direct cause and effect relationships (Lovelock 2005).
  • 5. Infrastructure Government Regulation Positive Inputs Taxes & Conducive weather Water subsidies Negative Outputs Climate Or Sunshine Trade Floods, droughts, etc Nitrogen Runoffs, wastes, environment Agricultural inputs carbon Research Weather Fertilizers etc Rainfall Knowledge Wind Labour Sunshine UV radiation Temperature Some Humidity Resource inputs, Production Processes fertilizers, herbicides, recycling insecticides, machinery, back to Human research capabilities Farm size & layout system Habitisation Organisation & methods Knowledge Suitability of conditions Suppliers & contractors Pollution (air, land & water) Propagation Pollution Labour sources Attitudes and concerns Water resources Cultivation Positive Outputs (create hinterland where Products farm part of) Processing Physical Environment Customers Financing & Marketing Revenue flow various kinds of back to Soil capital Topography system Atmosphere Natural flora & Negative Inputs fauna habitat Business Urbanisation Adverse physical Environment Competition conditions Low prices Pests & diseases Markets Changing demand Pollution Finance patterns Heavy metals Trade environment An Agricultural Enterprise as a System
  • 6. Complex algorithms are not linear – too complex to calculate – so we need to be guided by heuristical thinking which is in turn guided by “trial & error”
  • 7. We think only in the short term
  • 8. We do not truly understand the interrelationships between the variables influencing an action
  • 9. We discover through trial and error but can hypothesize
  • 10. Location Climate Genetic Material Humidity Collection Temperature Purchase Sunshine hours Topography UV radiation Plant physiology Seasons Slope & drainage Propagation Yield and Rainfall characteristics Chemical Constituents of the Humus Nutrients Method of extraction Essential Oil Extraction time Compactness Drainage & water holding qualities Pest & weed pH control Pre-harvest handling Mineral residuals Irrigation & preparation Plant densities Soil type Time & method of harvest Agronomic Harvest & Soil Practices Extraction Practices
  • 11. 1.What are the specific technical goals and objectives? 2.What are the major technology, infrastructure and climatic constraints (boundaries)? 3.What are the areas where innovations will develop quick improvements? 4.What is the probability of successful outcomes?, and 5.How do we choose between successful outcomes?
  • 12. Effectuation is like going to the kitchen cabinet and seeing what ingredients you have and then deciding what you can make up for a meal. This is very different from causation where you have a specific menu in mind and then search out the ingredients to make up the meal.
  • 13.
  • 14. that there “is also the tendency for Asian countries, including Malaysia, to deal with the issue of values in development by Importing many technologies and systems wholesale from abroad without going through the process of mental transformation necessary to master them fully. Although Malaysia is going through rapid transformation, our growth is one without development in the context of knowledge contribution to science, engineering and technology. As long as we are consumers and operators of sophisticated techniques, plants and technologies imported wholesale from abroad, we are to a certain extent undergoing a technology-less form of industrialization. This transformation of values and attitudes is a key issue in the nation’s development agenda”[i] . [i] Asma, A., Going Glocal: Cultural Dimensions in Malaysian Management, Kuala Lumpur, Malaysian Institute of Management, 1995, P. 179.
  • 15. Essential Oil Crop Harvesting
  • 16. Selected method often restricted by type of crop Most herbaceous crops can be mowed Many flowers must be hand picked Innovative systems can be designed and developed
  • 17. A Basic Harvest to Distillation Flowchart for Peppermint Oil Determination of Harvest time (Sampling) 10 tonne fresh herb per Ha. Mowing and leaving to wilt on field Fresh herb contains 80% moisture Wilting Must wilt to 50% moisture level where ‘crisp and brittle’ Pick up with forage harvester Collect 6 tonne of dry herb Must insure that herb is not Deliver to Distillation system bruised. Use cartridge or box to avoid too much handling Volume of 4 m2 per tonne of herb. Distillation If single charge, yield 15kg oil Assume 35 minutes distillation time, 10 minutes change over, 6.90 litres/minute If distillate ratio is 0.062/1 steam rate per minute. 9 hours will handle (oil/water), then 241.8 litres 12 tonnes of dried herb in a vat of 4m 3. water required for distillation.
  • 18. Effectuation in Tea Tree (Melaleuca alterniafolia) Harvester Development Harvester must make a clean cut here
  • 19. Harvester must damage the stumps To promote coppice growth
  • 21.
  • 22.
  • 23.
  • 24.
  • 26. How we really develop new pieces of equipment utilized for complex tasks
  • 28. Distillation Principals: Latent Heat • Molecule speed and energy Amount of heat required to vapourise a unit dependent upon temperature mass of liquid, without raising the •Change from liquid to gas state temperature of the vapour above that of the requires energy liquid is called LATENT HEAT of vapourisation •Due to motion of molecules, all compounds with determinable boiling points will emit vapours from their surafaces, if area closed this will insert pressure upon the molecule, termed vapour pressure •These vapours will saturate the molecule and take up additional molecules •This saturated vapour will carry other molecules Heat and relative pressures are important in distillation
  • 29. Distillation Principlas Mixed Vapours Molecules of Molecules of water vapour Molecules of water vapour a water and gas b vapour Liquid water Liquid oil Liquid Liquid oil b water a a b Eg. Water 99.6c Together at 99.6c Eg linalyl acetate 226c The composition of mixed vapours from immiscible liquids
  • 30. Releasing Oil from Plant Materials In steam distillation water condenses of plant surfaces and latent heat surrounds the material and raises volatile materials to boiling point
  • 31. Releasing Oil from Plant Materials Method of Oil Release through Putative Impression from Leaves General vapour space 99c 98c saturated mixed Region of oil vapour Vapour phase vapour elution Herb surface Water liquid mixed liquids oil liquids water liquids
  • 32. Wild Collection & Distillation Tea Tree Australia
  • 35. Influencing Factors Historical Compound characteristics (volatility/mol. Weight) Surrounding Material Compounds Highly volatile mixed with terpenes waxes, also lactones, Low/medium volatility/stable esters etc. Distillation Solvent Cold Extraction Pressing Automated harvest and Influencing Factors Harvest and distillation Price vis. Market later load system system Volume Plant cell structures Field size Topography Soil/field characteristics Part of plant (i.e., Extensive rhizome/leaf) Manual large scale Coppice High --- Low harvesting farming Value due to scale, material, Specialties Distillation investment Hydro Material Characteristics „Finer‟ CO2 composition spectrum Steam Solubility in water Individual Fractional aroma Distillation compounds Destructive Material Characteristics
  • 38. Lid with Clamps Corrugated Iron Condenser Tank Vapour Outlet Running into Corrugated Tank Distillation Vat Vapour Outlet Running Pipe for “T” Counterweight into Corrugated Tank Pressure Equalisation Oil Welded Steel Mesh Bottom Water Brick Compartment “Firebox” for wood fire Constant Level Separator Tank
  • 39. Mixed Vapour Out Critical to understand Re-vapourisation this behaviour to scale up Re-condensation Re-vapourisation Re-condensation Re-vapourisation Re-condensation Re-vapourisation Re-condensation Re-vapourisation Re-condensation Steam in
  • 40. Each box can be distilled on rotation or both together, governed by boiler capacity. Boiler Box No. 1. Box No. 2. Condensers Boxes driven in by tractor and coupled up to steam inlet and condenser. Separators
  • 41.
  • 42.
  • 43.
  • 44.
  • 45.
  • 47. Technical and social disciplines are undergoing convergence which can be seen in the way many industries are merging together into one. Convergence is creeping into the research and development process where trans- disciplinary approaches are required to solve problems. Being an engineer is not good enough in isolation. In order to create, an engineer must have knowledge across a number of disciplines so that knowledge can be synergized into some meaningful expressions in the form of new applications and inventions.
  • 48. “Issues facing society to be solved” New Forms of Expression Other disciplines of Insight Expressed knowledge Application & Microbiology Our current Knowledge Invention Biology Trans-disciplinary synergy of Deep Insight knowledge Engineering Agriculture Physics Chemistry Biochemistry
  • 49. Australia 2139 Brunei 3 China 3910 Indonesia 6 India 627 Japan 26906 Dem. Rep. Korea 4 Republic Korea 5935 Malaysia 54 New Zealand 316 15 This phenomenon can be seen at a national Philippines level if one looks at the number of resident Singapore 402 patents filed per million population in each Thailand 12 country. Vietnam 9 0 5000 10000 15000 20000 25000 30000 Source: WIPO Statistics Number of International Patents Filed by Residents
  • 50. Knowledge without application is useless in creating tangible benefits to society, but hopefully this paper has shed light that it is not knowledge in itself that is important rather the ability to apply it. And the ability to apply it doesn’t rely upon formulae, theory or algorithm, but rather emergent thinking and the heuristics have developed. This is a neglected part of engineering education and this is also the quality that makes a good engineer stand out from the rest of the pack.