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© 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1805
CHEMICALLY TREATED COIR FIBER REINFORCED CONCRETE
Pooja B J1, Sanjay B M2, Varshini S R3, Yashwantha L4, Megha S Mahaladkar5
1,2,3,4BE Student, Dept. of Civil Engineering, Vidya Vikas Institute of Engineering and Technology, Karnataka, India
5 Assistant Professor, Dept. Of Civil Engineering, Vidya Vikas Institute of Engineering and Technology, Karnataka,
India
---------------------------------------------------------------------***---------------------------------------------------------------------
Abstract - The study of adding coir fiber (coconut fiber)
into the concrete structure differs in many engineering
properties. Concrete is having a low tensile and also a
flexural property. However, conventional steel reinforced
concrete structures are the most popular method developed
to reduce such problem and it is rather to becoming
expensive for construction in terms of its costs and
sustainability issues also, because of these problems in many
constructions industry they reduce the strength of steel
there by decreasing the strength to overcome these
problem, by adding of coir fiber to the concrete structure
increases the tensile and also the flexural properties and
coir fiber are normally available in nature and it is also eco-
friendly. This experiment was conducted on high strength
concrete with addition of coir fiber with a 4 mix proportions
(0, 0.1%,0.2% and 0.3%) and the compressive strength and
tensile strength of cured concrete is evaluated for 28days.
Stem of dissemination of information about the flood will
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prone zones, hence can save their lives and avoid huge
damages which is occurring from the natural disasters.
Key Words: Fiber-reinforced concrete, coir fibers, chemical
treatment, interfacial bond, mechanical properties,
sustainable construction.
1.INTRODUCTION
Natural fibers are organic fibers are plant sources and
animal products. They are used by humans for thousands
of years for wide range of applications to their abundance,
versatility, and desirable properties. Fibers are extracted
from the plants like sisal, coir, jute, and from animal
sources like wool and silk. Natural fibers possess several
advantageous properties are suitable for various
applications. They are renewable and biodegradable,
making them environmentally friendly alternatives to
synthetic fibers. They also have excellent breathability,
moisture absorption, and thermal insulation properties,
making them comfortable to wear in clothing and textiles.
In addition to their textile applications, plant fibers are
largely used as reinforcement materials in composites,
including in construction materials like concrete and
plastics. Which increase the engineering properties of
composites by providing strength, stiffness, and impact
resistance.
1.1 Coconut Fiber (Coir Fiber)
Coconut fiber (coir fibers) are natural fibers derived from
the husk of coconuts, which are the fruits of the coconut
palm tree (Cocos nucifera). Fibers are extensively used in
other properties due to their unique properties and
versatility. Coconut fibers are obtained from the
innermost layer of coconut husk, known as the mesocarp.
The process typically involves soaking the husks in water
to soften them, followed by mechanical processes such as
beating or retting to separate the fibers from the rest of
the husk. The fibers are then cleaned, dried, and further
processed for different applications.
1.2 Types of Coir Fiber
Coconut fibers are obtained from the outer husk of
coconut shells and are largely used in various industries.
There are classified into two types of coir fibers based on
their extraction process and physical characteristics:
1. Brown coir fiber
2. White coir fiber
Brown Coir Fibers: Brown coconut fibers are obtained
from mature coconut husks. These fibers are thick, strong,
and have a brownish color. They are naturally used in
applications that require durability and strength, such as
mattresses, ropes, carpets, and geotextiles. Brown coir
fibers are also used for erosion control and landscaping
purposes.
White Coir Fibers: White coir fibers are derived from
immature or green coconut husks. They are softer, finer,
and have a lighter color compared to brown coir fibers.
White coir is primarily used in the production of products
that require a finer texture, such as upholstery padding,
cushioning materials, and decorative items. It is also used
for making brushes, doormats, and filling material.
1.3 Test conducted
Several tests are conducted on concrete to assess its
quality, strength, durability, and other properties. Here are
some commonly performed tests on concrete:
1. Compressive Strength Test: This is the most common
and important test for concrete. It determines the
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 10 Issue: 05 | May 2023 www.irjet.net p-ISSN: 2395-0072
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 10 Issue: 05 | May 2023 www.irjet.net p-ISSN: 2395-0072
© 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1806
maximum compressive load a concrete sample can bear
before failure. The test involves applying a gradually
increasing load to a cylindrical or cubical concrete
specimen until it fails.
2. Flexural Strength Test: Also known as the modulus of
rupture test, it measures the tensile strength of concrete. A
beam specimen is subjected to a bending force until it
fractures. This test helps assess the concrete's ability to
resist bending or cracking under load.
3. Splitting Tensile Strength Test: This test measures
the tensile strength of concrete perpendicular to the
applied compressive force. A cylindrical or cubical
concrete specimen is subjected to a diametrical
compressive force until it cracks. The splitting tensile
strength is then calculated based on the applied load.
1.4 Chemical treatment
The recent trends in the development of the newer
materials have led in replacing materials like glass and
carbon reinforced composites with the natural fibers
reinforced composites. However, the main drawback of
natural fibers as reinforcement is that they are
incompatible with thermoplastics due to their hydrophilic
nature which results in the poor interfacial interaction
between the fibers and matrix. This result in poor
mechanical properties of the composites. Therefore, the
modification of natural fibers is required to make them
less hydrophilic. Here an attempt is made to brief about
various chemical treatment on natural fibers.
ALKALINE TREATMENT
The alkaline treatment is a chemical treatment in which
the natural fibers are immersed in a known concentration
of aqueous sodium hydroxide (NaOH) 1N for a given
temperature and a period of time.
2. MATERIALS AND METHODOLOGY
2.1 Materials
The materials used in this study are:
1. Cement (PPC): UltraTech Cements - 43 Grade
2. Fine Aggregate: M-Sand
3. Coarse Aggregate: Aggregates passing through
20mm IS sieve
4. Coir fibre: Fibre of length 1.5cm, 2.5cm and 3cm
5. Water: Collected from local fresh water
sources
Tests conducted on cement: Various tests are conducted
to evaluate the quality and performance of cement. These
tests help assess properties such as fineness, setting time,
compressive strength, soundness, and chemical
composition.
Here are some common tests conducted on cement:
1. Fineness test
2. Setting time test
3. Soundness test
4. Specific gravity test
Table -1: Test results on cement
SL
NO.
PROPERTY VALUE STANDARD VALUES
( IS8112-1989)
1 Specific gravity of
cement
2.9 Not specified
2 Normal consistency
(%)
33 Not specified
3 Initial setting time of
cement (minutes)
130 30 (minimum)
4 Final setting time of
cement (minutes)
360 600 (maximum)
Test conducted on fine aggregate: Several tests are
conducted on fine aggregates to assess their quality,
suitability, and conformity to specifications. These tests
help determine important characteristics such as particle
size distribution, shape, cleanliness, strength, and
durability. Here are some common tests conducted on fine
aggregates:
1. Sieve analysis
2. Specific gravity
3. Water absorption
Table -2: Test results on fine aggregate
SL NO. PROPERTY RESULTS
1 Specific Gravity 2.5
2 Water absorption 1%
3 Sieve analysis
IS Sieve %
passing
Conforming
to grading
zone II of IS
383:1970
4.75 mm 94
2.36 mm 86
1.18 mm 68
600 µ 48
300 µ 14
150 µ 2
Pan 0.4
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 10 Issue: 05 | May 2023 www.irjet.net p-ISSN: 2395-0072
© 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1807
Test conducted on coarse aggregate: Coarse aggregate
undergoes testing to ensure its compliance with relevant
standards and specifications. Tests such as sieve analysis,
specific gravity, water absorption, and abrasion resistance
help assess the quality and suitability of the aggregate for
concrete production. It's important to note that local
standards, construction practices, and regional availability
of materials may influence the specific use and
characteristics of coarse aggregate in different areas.
Several tests are conducted on coarse aggregate to assess
its quality and suitability for use in concrete.
Here are some common tests conducted on fine
aggregates:
1. Sieve analysis
2. Specific gravity
3. Water absorption
Table -3: Test results on coarse aggregate
Sl. No. PROPERTY RESULTS
1 Specific
Gravity
2.8
2 Water
absorption
0.25%
3
Sieve analysis (passing through IS 20mm Sieve)
IS Sieve Weight
retained
Cumulative %
Weight retained
%
passing
40mm 0 0 100
20mm 362.5 14.5 85.5
10mm 2060.82 96.53 3.07
4.75mm 31.40 98.18 1.82
Pan 0 100 0
2.2 Methodology
MIX DESIGN
Most of the researches have studied the influence of
coconut waste on M20 grade concrete. M20 concrete is a
1:1.5:3 mixture of cement, sand, and aggregate, where
cement makes up one part, sand makes up 1.5 parts, and
aggregate or stone makes up the remaining three parts.
Table -4: M20 Mix design
CEMENT 383.0Kg/m3
WATER 191.6kg/m3
FINE AGGREGATES 727kg/m3
COARSE AGGREGATES 1103kg/m3
WATER CEMENT RATIO (W/C) 0.50
RATIO 1:1.5:3
Calculation Of Quantity of Coir Fiber
Volume of mould (V) = 0.15 x 0.15 x 0.15 = 0.003375 m3
Fiber volume = 0.003375 m3
Fraction (VF) = 0
Fiber (D) = 1140 kg/ m3
No. of specimens (N) = 3
1) Wt. of 0.1 % coir fiber = VF x V x D x N
= (0.1 / 100) x 0.003375 x 1140 x
3
= 0.011 kg
2) Wt. of 0.2 % coir fiber = VF x V x D x N
= (0.2 / 100) x 0.003375 x 1140 x
3
= 0.023 kg
3) Wt. of 0.3 % coir fiber = VF x V x D x N
= (0.3 / 100) x 0.003375 x 1140 x
3
= 0.034 kg
2.3 Chemical Treatment of Fiber
Prepare the NaOH Solution:
Measure the appropriate amount of solid sodium
hydroxide (NaOH) pellets. Add the NaOH pellets to
distilled water in a container, while stirring continuously
to dissolve the pellets.
Continue stirring until all the NaOH is dissolved and a
homogeneous 1N NaOH solution is obtained. Ensure
proper safety precautions while handling NaOH, such as
wearing protective gloves and eyewear, as it is a caustic
substance.
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 10 Issue: 05 | May 2023 www.irjet.net p-ISSN: 2395-0072
© 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1808
Fig 1: Weighing of NaOH Pellets
Fig 2: 1N NaOH Solution
Fiber Preparation:
Obtain natural coir fibers extracted from mature coconut
husks. Cut the coir fibers into suitable lengths of 1.5cm,
2.5cm and 3cm, depending on the desired reinforcement
length in the concrete.
Fig 4: Extraction of Coir Fiber From Matured Coconut
Husks
Fig 5: Coir Fibers in Different Length
Immerse the coir fibers in the prepared 1N NaOH solution
for 2hours. Ensure that the fibers are completely
submerged in the solution and provide sufficient space for
them to expand.
Fig 6: Coir Fiber During Treatment
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 10 Issue: 05 | May 2023 www.irjet.net p-ISSN: 2395-0072
© 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1809
Fiber Treatment:
During the immersion period, gently agitate or stir the
fibers at regular intervals to ensure proper penetration
and contact with the NaOH solution. The NaOH solution
reacts with the lignin present in the coir fibers, removing
impurities and enhancing fiber-matrix bonding properties.
After the required immersion time, remove the fibers from
the NaOH solution.
Fig 7: Treated Coir Fiber
Drying:
Allow the fibers to air-dry in room temperature or a well-
ventilated area for 24 hours, such as natural sun-drying or
mechanical drying, to remove excess moisture. Ensure that
the fibers are completely dry before incorporating them
into the concrete mix to prevent excess water absorption
during mixing.
Fig 8: Treated Coir Fiber in Dry Condition After 24 Hours
Incorporation into Concrete Mix:
Mix the chemically treated and dried coir fibers with the
other concrete ingredients according to the desired mix
proportions of 0.1%, 0.2% and 0.3% and mixing
methodology.
Fig 9: Weight of Treated Coir Fiber For 3 Different Mix
Proportion
Gradually add the fibers into the concrete mixer during the
mixing process to ensure even distribution and proper
bonding between the fibers and the concrete matrix.
Continue mixing until the fibers are uniformly dispersed
throughout the concrete mixture.
Fig 10: Treated Coir Fiber Mixed with Concrete
It is important to note that the specific treatment duration,
concentration of NaOH solution, and other parameters
may vary based on research findings, project
requirements, and available resources. It is advisable to
refer to relevant literature, expert guidance, and conduct
preliminary trials to optimize the chemical treatment
process for 1N NaOH chemically treated coir fiber
reinforced concrete.
2.4 Casting of chemically treated coir fibre reinforced
concrete
The calculated amount of cement and fine aggregate are
mixed together until a uniform mix is obtained. Fibres at
varying amounts of 0.1%, 0.2% and 0.3% to that of weight
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 10 Issue: 05 | May 2023 www.irjet.net p-ISSN: 2395-0072
© 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1810
of cement are taken. Coir fibre strands are cut into a length
of 1.5,2.5 and 3cm. Then the fibers are immersed in 1N
NaOH solution for 2 hours and dried for 24hours in room
temperature. It is then added to the mix. Coarse aggregates
are then added to the same and mixed, followed by
addition of water. Care should be taken to add water
slowly in stages so as to prevent bleeding which may affect
the strength formation of concrete. It is placed in the
moulds of standard dimensions, compacted and finished.
Casting of mould size 150 x 150 x 150 mm is also same for
different percentages (i.e., 0.1%, 0.2% and 0.3%). Three
cubes are casted for each percentage for compressive test.
Estimation of split tensile strength for cylinder is 150 x
300 mm long using CTM machine of the capacity 300T.
Flexural strength test for beam is 150 x 150 x 170 mm
length using CTM machine of its capacity 300T.
Fig 11: Chemically Treated Coir Fiber Reinforced Concrete
are Moulded
Fig 12: Chemically Treated Coir Fiber Reinforced Concrete are
Unmoulded
3. RESULTS AND DISCUSSION
COMPRESSIVE STRENGTH TEST:
The compressive strength test is a fundamental test
conducted on hardened concrete to determine its ability to
withstand axial compressive loads. It is one of the most
important tests for assessing the quality and performance
of concrete. when conducting compressive strength tests to
ensure accuracy, consistency, and comparability of the
results. The compressive strength test helps assess the
concrete's ability to resist compression and is critical for
evaluating the structural performance of concrete elements
in various applications.
Table -5: 28 Days Compressive Strength Test Result
(N/Mm 2 )
% OF FIBER
ADDED
28 DAYS COMPRESSIVE STRENGTH TEST
RESULT (N/mm 2 )
15mm 25mm 30mm
0 22 22.03 23.04
0.1 25.03 26.7 29.01
0.2 25.13 26.9 29.89
0.3 25.7 27.03 30.02
Chart -1: Compressive Strength Test 28days Result
Split Tensile Strength Test:
Determination of split tensile strength for cylinder
150X300mm long using CTM machine of capacity 300T,
this is for each cube as per IS516-1959. Tensile strength is
the capacity of a material or structure to withstand
tension. It is measured on concrete cylinders of standard
dimensions using a Universal Testing machine. Both
conventional and fibre reinforced specimens were tested at
varying percentages of fibre and the average value was
obtained.
0
10
20
30
40
50
1 2 3 4 5 6 7 8
COMPRESSIVE
STRENGTH
% OF COIR FIBER ADDED
% OF FIBER
% OF FIBER
% OF FIBER
% OF FIBER
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 10 Issue: 05 | May 2023 www.irjet.net p-ISSN: 2395-0072
© 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1811
Table -6: 28 Days Split Tensile Strength Test Result
(N/Mm2 )
% OF
FIBER
ADDED
28 DAYS SPLIT TENSILE STRENGTH TEST
RESULT (N/mm2 )
15mm 25mm 30mm
0 3.41 3.58 3.64
0.1 3.52 3.77 3.91
0.2 3.64 3.85 4.01
0.3 3.52 3.7 3.68
Chart -2: Split Tensile Strength Test 28days Result
Flexural Strength Test:
Flexure strength test for beam 150X150X170mm length
using CTM machine of capacity 300T, this is for each cube
as per IS516-1959. Flexural strength of concrete is
considered as an index of tensile strength of concrete.
Tensile stresses are likely to develop in concrete due to
drying shrinkage, rusting of steel reinforcement,
temperature gradients and many other reasons. Beam tests
are conducted to determine flexural strength of concrete.
In flexural tests on beam theoretical maximum tensile
strength is obtained at bottom of beam and is called
modulus of rupture, which depends on dimension of beam
and position of loading.
Table -7: 28 Days Flexural Strength Test Result (N/Mm 2 )
% OF
FIBER
ADDED
28 DAYS FLEXURAL STRENGTH TEST
RESULT (N/mm2 )
15mm 25mm 30mm
0 3.82 4.16 5.03
0.1 3.96 4.29 5.67
0.2 4.32 4.53 4.79
0.3 4.35 4.42 4.57
Chart -3: Flexural Strength Test 28days Result
RESULT:
The addition of 0.3% of treated coir fiber at length of
15mm, 25mm and 30mm improve in the result of
compression strength test, split tensile strength test and
flexural strength test, with best outcome observed for
30mm length chemically treated coir fiber reinforced
concrete.
4. CONCLUSIONS
1. The concrete can be reinforced as coir fiber, which has
been proven to be a successful material.
2. Test were carried out in labs all around the world to
see the performance of concrete would be impacted by
coconut fibers.
3. Coconut fiber is the perfect material for creating a
lightweight version of concrete. Coir fibers are less
dense than concrete and so the total weight of
construction.
4. The coir fibers increase concrete specifications and aid
in lowering environmental pollution. The study
findings support the idea that no more than 1% of the
fiber fraction should be used. Coir fibers has low heat
conductivity hence it promotes natural cooling.
5. Improved Fiber-Matrix Bond: Chemical treatment of
coir fiber with 1N NaOH can enhance the adhesion
between the fiber and the concrete matrix. This
treatment helps remove impurities and surface
contaminants from the fibers, allowing for better
bonding and improved mechanical properties of the
reinforced concrete.
6. Enhanced Mechanical Properties: The addition of
chemically treated coir fibers to concrete can lead to
improvements in mechanical properties such as tensile
strength, flexural strength, and impact resistance. The
0
1
2
3
4
5
1 2 3 4 5 6 7 8
SPLIT
TENSILE
STRENGTH
% OF COIR FIBER ADDED
% OF FIBER
% OF FIBER
% OF FIBER
% OF FIBER
0
1
2
3
4
5
6
1 2 3 4 5 6 7 8
FLEXURAL
STRENGTH
% OF COIR FIBER ADDED
% OF FIBER
% OF FIBER
% OF FIBER
% OF FIBER
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 10 Issue: 05 | May 2023 www.irjet.net p-ISSN: 2395-0072
© 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1812
treated fibers act as reinforcement, effectively
distributing stresses within the concrete and enhancing
its overall performance.
7. Reduction in Cracking and Shrinkage: The presence of
coir fibers, especially when chemically treated, can help
mitigate cracking and shrinkage in concrete. The fibers
act as internal reinforcement, providing additional
tensile strength and controlling the development of
cracks, thereby improving the durability and longevity
of the concrete structures.
8. It is important to note that these conclusions are
generalized and based on the potential benefits
associated with chemically treated coir fiber reinforced
concrete.
REFERENCES
1. Durability Study on Coir Fibre Reinforced Concrete
Nithin Sam1 1P.G Student, Department of Civil
Engineering, Albertian Institute of Science and
Technology, Kerala, India Sheeja M K2 2Assistant
Professor, Department of Civil Engineering, Albertian
Institute of Science and Technology, Kerala, India.
2. Concrete Reinforced with Coconut Fibres V. Sai Uday1 ,
B.Ajitha2 M.Tech Student1 , Assistant Professor2
Department of Civil Engineering JNTUA College of
Engineering, Ananthapuram, AP, India.
3. EXPERIMENTAL STUDY ON COIR FIBRE MIXED
CONCRETE 1Achudhan 2M.J. Ienamul Hasan Ali, 3S.
Senthamizh Sankar, 4K. Saikumar 1Assistant Professor,
Faculty, Department of Civil Engineering, Sri Sai Ram
Institute of Technology, India 2,3,4 Under Graduate
Students, Department of Civil Engineering, Sri Sai Ram
Institute of Technology, India.
4. A Review on Coir Fiber Reinforced Polymer Composite
U.S. Bongarde1, B.K. Khot2 1,2Assistant Professor,
Department of Mechanical Engineering, Textile and
Engineering Institute, Ichalkaranji, 416115, India.
5. Role of coconut coir fiber in concrete Article in
Materials Today: Proceedings · February 2020
Habibunnisa Syed Vignan's Foundation For Science,
Technology and Research (Deemed to be Unive.. 5
PUBLICATIONS 35 CITATIONS Nerella Ruben Vignan
University 54 PUBLICATIONS 2,114 CITATIONS.
6. Mechanical and Durability Performance of Coconut
Fiber Reinforced Concrete: A State-of-the-Art Review
Article in Materials · May 2022. 7 authors, including:
Jawad Ahmad Master of Science in Structural
Engineering 60 PUBLICATIONS 513 CITATIONS, Ali
Majdi Al-Mustaqbal University College 93
PUBLICATIONS 195 CITATIONS, Amin Al-Fakih King
Fahd University of Petroleum and Minerals 51
PUBLICATIONS 739 CITATIONS and Ahmed Farouk
Deifalla Future University in Egypt 130 PUBLICATIONS
1,117 CITATIONS.

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CHEMICALLY TREATED COIR FIBER REINFORCED CONCRETE

  • 1. © 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1805 CHEMICALLY TREATED COIR FIBER REINFORCED CONCRETE Pooja B J1, Sanjay B M2, Varshini S R3, Yashwantha L4, Megha S Mahaladkar5 1,2,3,4BE Student, Dept. of Civil Engineering, Vidya Vikas Institute of Engineering and Technology, Karnataka, India 5 Assistant Professor, Dept. Of Civil Engineering, Vidya Vikas Institute of Engineering and Technology, Karnataka, India ---------------------------------------------------------------------***--------------------------------------------------------------------- Abstract - The study of adding coir fiber (coconut fiber) into the concrete structure differs in many engineering properties. Concrete is having a low tensile and also a flexural property. However, conventional steel reinforced concrete structures are the most popular method developed to reduce such problem and it is rather to becoming expensive for construction in terms of its costs and sustainability issues also, because of these problems in many constructions industry they reduce the strength of steel there by decreasing the strength to overcome these problem, by adding of coir fiber to the concrete structure increases the tensile and also the flexural properties and coir fiber are normally available in nature and it is also eco- friendly. This experiment was conducted on high strength concrete with addition of coir fiber with a 4 mix proportions (0, 0.1%,0.2% and 0.3%) and the compressive strength and tensile strength of cured concrete is evaluated for 28days. Stem of dissemination of information about the flood will bring a peaceful mind to the households leaving in the flood prone zones, hence can save their lives and avoid huge damages which is occurring from the natural disasters. Key Words: Fiber-reinforced concrete, coir fibers, chemical treatment, interfacial bond, mechanical properties, sustainable construction. 1.INTRODUCTION Natural fibers are organic fibers are plant sources and animal products. They are used by humans for thousands of years for wide range of applications to their abundance, versatility, and desirable properties. Fibers are extracted from the plants like sisal, coir, jute, and from animal sources like wool and silk. Natural fibers possess several advantageous properties are suitable for various applications. They are renewable and biodegradable, making them environmentally friendly alternatives to synthetic fibers. They also have excellent breathability, moisture absorption, and thermal insulation properties, making them comfortable to wear in clothing and textiles. In addition to their textile applications, plant fibers are largely used as reinforcement materials in composites, including in construction materials like concrete and plastics. Which increase the engineering properties of composites by providing strength, stiffness, and impact resistance. 1.1 Coconut Fiber (Coir Fiber) Coconut fiber (coir fibers) are natural fibers derived from the husk of coconuts, which are the fruits of the coconut palm tree (Cocos nucifera). Fibers are extensively used in other properties due to their unique properties and versatility. Coconut fibers are obtained from the innermost layer of coconut husk, known as the mesocarp. The process typically involves soaking the husks in water to soften them, followed by mechanical processes such as beating or retting to separate the fibers from the rest of the husk. The fibers are then cleaned, dried, and further processed for different applications. 1.2 Types of Coir Fiber Coconut fibers are obtained from the outer husk of coconut shells and are largely used in various industries. There are classified into two types of coir fibers based on their extraction process and physical characteristics: 1. Brown coir fiber 2. White coir fiber Brown Coir Fibers: Brown coconut fibers are obtained from mature coconut husks. These fibers are thick, strong, and have a brownish color. They are naturally used in applications that require durability and strength, such as mattresses, ropes, carpets, and geotextiles. Brown coir fibers are also used for erosion control and landscaping purposes. White Coir Fibers: White coir fibers are derived from immature or green coconut husks. They are softer, finer, and have a lighter color compared to brown coir fibers. White coir is primarily used in the production of products that require a finer texture, such as upholstery padding, cushioning materials, and decorative items. It is also used for making brushes, doormats, and filling material. 1.3 Test conducted Several tests are conducted on concrete to assess its quality, strength, durability, and other properties. Here are some commonly performed tests on concrete: 1. Compressive Strength Test: This is the most common and important test for concrete. It determines the International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 10 Issue: 05 | May 2023 www.irjet.net p-ISSN: 2395-0072
  • 2. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 10 Issue: 05 | May 2023 www.irjet.net p-ISSN: 2395-0072 © 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1806 maximum compressive load a concrete sample can bear before failure. The test involves applying a gradually increasing load to a cylindrical or cubical concrete specimen until it fails. 2. Flexural Strength Test: Also known as the modulus of rupture test, it measures the tensile strength of concrete. A beam specimen is subjected to a bending force until it fractures. This test helps assess the concrete's ability to resist bending or cracking under load. 3. Splitting Tensile Strength Test: This test measures the tensile strength of concrete perpendicular to the applied compressive force. A cylindrical or cubical concrete specimen is subjected to a diametrical compressive force until it cracks. The splitting tensile strength is then calculated based on the applied load. 1.4 Chemical treatment The recent trends in the development of the newer materials have led in replacing materials like glass and carbon reinforced composites with the natural fibers reinforced composites. However, the main drawback of natural fibers as reinforcement is that they are incompatible with thermoplastics due to their hydrophilic nature which results in the poor interfacial interaction between the fibers and matrix. This result in poor mechanical properties of the composites. Therefore, the modification of natural fibers is required to make them less hydrophilic. Here an attempt is made to brief about various chemical treatment on natural fibers. ALKALINE TREATMENT The alkaline treatment is a chemical treatment in which the natural fibers are immersed in a known concentration of aqueous sodium hydroxide (NaOH) 1N for a given temperature and a period of time. 2. MATERIALS AND METHODOLOGY 2.1 Materials The materials used in this study are: 1. Cement (PPC): UltraTech Cements - 43 Grade 2. Fine Aggregate: M-Sand 3. Coarse Aggregate: Aggregates passing through 20mm IS sieve 4. Coir fibre: Fibre of length 1.5cm, 2.5cm and 3cm 5. Water: Collected from local fresh water sources Tests conducted on cement: Various tests are conducted to evaluate the quality and performance of cement. These tests help assess properties such as fineness, setting time, compressive strength, soundness, and chemical composition. Here are some common tests conducted on cement: 1. Fineness test 2. Setting time test 3. Soundness test 4. Specific gravity test Table -1: Test results on cement SL NO. PROPERTY VALUE STANDARD VALUES ( IS8112-1989) 1 Specific gravity of cement 2.9 Not specified 2 Normal consistency (%) 33 Not specified 3 Initial setting time of cement (minutes) 130 30 (minimum) 4 Final setting time of cement (minutes) 360 600 (maximum) Test conducted on fine aggregate: Several tests are conducted on fine aggregates to assess their quality, suitability, and conformity to specifications. These tests help determine important characteristics such as particle size distribution, shape, cleanliness, strength, and durability. Here are some common tests conducted on fine aggregates: 1. Sieve analysis 2. Specific gravity 3. Water absorption Table -2: Test results on fine aggregate SL NO. PROPERTY RESULTS 1 Specific Gravity 2.5 2 Water absorption 1% 3 Sieve analysis IS Sieve % passing Conforming to grading zone II of IS 383:1970 4.75 mm 94 2.36 mm 86 1.18 mm 68 600 µ 48 300 µ 14 150 µ 2 Pan 0.4
  • 3. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 10 Issue: 05 | May 2023 www.irjet.net p-ISSN: 2395-0072 © 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1807 Test conducted on coarse aggregate: Coarse aggregate undergoes testing to ensure its compliance with relevant standards and specifications. Tests such as sieve analysis, specific gravity, water absorption, and abrasion resistance help assess the quality and suitability of the aggregate for concrete production. It's important to note that local standards, construction practices, and regional availability of materials may influence the specific use and characteristics of coarse aggregate in different areas. Several tests are conducted on coarse aggregate to assess its quality and suitability for use in concrete. Here are some common tests conducted on fine aggregates: 1. Sieve analysis 2. Specific gravity 3. Water absorption Table -3: Test results on coarse aggregate Sl. No. PROPERTY RESULTS 1 Specific Gravity 2.8 2 Water absorption 0.25% 3 Sieve analysis (passing through IS 20mm Sieve) IS Sieve Weight retained Cumulative % Weight retained % passing 40mm 0 0 100 20mm 362.5 14.5 85.5 10mm 2060.82 96.53 3.07 4.75mm 31.40 98.18 1.82 Pan 0 100 0 2.2 Methodology MIX DESIGN Most of the researches have studied the influence of coconut waste on M20 grade concrete. M20 concrete is a 1:1.5:3 mixture of cement, sand, and aggregate, where cement makes up one part, sand makes up 1.5 parts, and aggregate or stone makes up the remaining three parts. Table -4: M20 Mix design CEMENT 383.0Kg/m3 WATER 191.6kg/m3 FINE AGGREGATES 727kg/m3 COARSE AGGREGATES 1103kg/m3 WATER CEMENT RATIO (W/C) 0.50 RATIO 1:1.5:3 Calculation Of Quantity of Coir Fiber Volume of mould (V) = 0.15 x 0.15 x 0.15 = 0.003375 m3 Fiber volume = 0.003375 m3 Fraction (VF) = 0 Fiber (D) = 1140 kg/ m3 No. of specimens (N) = 3 1) Wt. of 0.1 % coir fiber = VF x V x D x N = (0.1 / 100) x 0.003375 x 1140 x 3 = 0.011 kg 2) Wt. of 0.2 % coir fiber = VF x V x D x N = (0.2 / 100) x 0.003375 x 1140 x 3 = 0.023 kg 3) Wt. of 0.3 % coir fiber = VF x V x D x N = (0.3 / 100) x 0.003375 x 1140 x 3 = 0.034 kg 2.3 Chemical Treatment of Fiber Prepare the NaOH Solution: Measure the appropriate amount of solid sodium hydroxide (NaOH) pellets. Add the NaOH pellets to distilled water in a container, while stirring continuously to dissolve the pellets. Continue stirring until all the NaOH is dissolved and a homogeneous 1N NaOH solution is obtained. Ensure proper safety precautions while handling NaOH, such as wearing protective gloves and eyewear, as it is a caustic substance.
  • 4. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 10 Issue: 05 | May 2023 www.irjet.net p-ISSN: 2395-0072 © 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1808 Fig 1: Weighing of NaOH Pellets Fig 2: 1N NaOH Solution Fiber Preparation: Obtain natural coir fibers extracted from mature coconut husks. Cut the coir fibers into suitable lengths of 1.5cm, 2.5cm and 3cm, depending on the desired reinforcement length in the concrete. Fig 4: Extraction of Coir Fiber From Matured Coconut Husks Fig 5: Coir Fibers in Different Length Immerse the coir fibers in the prepared 1N NaOH solution for 2hours. Ensure that the fibers are completely submerged in the solution and provide sufficient space for them to expand. Fig 6: Coir Fiber During Treatment
  • 5. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 10 Issue: 05 | May 2023 www.irjet.net p-ISSN: 2395-0072 © 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1809 Fiber Treatment: During the immersion period, gently agitate or stir the fibers at regular intervals to ensure proper penetration and contact with the NaOH solution. The NaOH solution reacts with the lignin present in the coir fibers, removing impurities and enhancing fiber-matrix bonding properties. After the required immersion time, remove the fibers from the NaOH solution. Fig 7: Treated Coir Fiber Drying: Allow the fibers to air-dry in room temperature or a well- ventilated area for 24 hours, such as natural sun-drying or mechanical drying, to remove excess moisture. Ensure that the fibers are completely dry before incorporating them into the concrete mix to prevent excess water absorption during mixing. Fig 8: Treated Coir Fiber in Dry Condition After 24 Hours Incorporation into Concrete Mix: Mix the chemically treated and dried coir fibers with the other concrete ingredients according to the desired mix proportions of 0.1%, 0.2% and 0.3% and mixing methodology. Fig 9: Weight of Treated Coir Fiber For 3 Different Mix Proportion Gradually add the fibers into the concrete mixer during the mixing process to ensure even distribution and proper bonding between the fibers and the concrete matrix. Continue mixing until the fibers are uniformly dispersed throughout the concrete mixture. Fig 10: Treated Coir Fiber Mixed with Concrete It is important to note that the specific treatment duration, concentration of NaOH solution, and other parameters may vary based on research findings, project requirements, and available resources. It is advisable to refer to relevant literature, expert guidance, and conduct preliminary trials to optimize the chemical treatment process for 1N NaOH chemically treated coir fiber reinforced concrete. 2.4 Casting of chemically treated coir fibre reinforced concrete The calculated amount of cement and fine aggregate are mixed together until a uniform mix is obtained. Fibres at varying amounts of 0.1%, 0.2% and 0.3% to that of weight
  • 6. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 10 Issue: 05 | May 2023 www.irjet.net p-ISSN: 2395-0072 © 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1810 of cement are taken. Coir fibre strands are cut into a length of 1.5,2.5 and 3cm. Then the fibers are immersed in 1N NaOH solution for 2 hours and dried for 24hours in room temperature. It is then added to the mix. Coarse aggregates are then added to the same and mixed, followed by addition of water. Care should be taken to add water slowly in stages so as to prevent bleeding which may affect the strength formation of concrete. It is placed in the moulds of standard dimensions, compacted and finished. Casting of mould size 150 x 150 x 150 mm is also same for different percentages (i.e., 0.1%, 0.2% and 0.3%). Three cubes are casted for each percentage for compressive test. Estimation of split tensile strength for cylinder is 150 x 300 mm long using CTM machine of the capacity 300T. Flexural strength test for beam is 150 x 150 x 170 mm length using CTM machine of its capacity 300T. Fig 11: Chemically Treated Coir Fiber Reinforced Concrete are Moulded Fig 12: Chemically Treated Coir Fiber Reinforced Concrete are Unmoulded 3. RESULTS AND DISCUSSION COMPRESSIVE STRENGTH TEST: The compressive strength test is a fundamental test conducted on hardened concrete to determine its ability to withstand axial compressive loads. It is one of the most important tests for assessing the quality and performance of concrete. when conducting compressive strength tests to ensure accuracy, consistency, and comparability of the results. The compressive strength test helps assess the concrete's ability to resist compression and is critical for evaluating the structural performance of concrete elements in various applications. Table -5: 28 Days Compressive Strength Test Result (N/Mm 2 ) % OF FIBER ADDED 28 DAYS COMPRESSIVE STRENGTH TEST RESULT (N/mm 2 ) 15mm 25mm 30mm 0 22 22.03 23.04 0.1 25.03 26.7 29.01 0.2 25.13 26.9 29.89 0.3 25.7 27.03 30.02 Chart -1: Compressive Strength Test 28days Result Split Tensile Strength Test: Determination of split tensile strength for cylinder 150X300mm long using CTM machine of capacity 300T, this is for each cube as per IS516-1959. Tensile strength is the capacity of a material or structure to withstand tension. It is measured on concrete cylinders of standard dimensions using a Universal Testing machine. Both conventional and fibre reinforced specimens were tested at varying percentages of fibre and the average value was obtained. 0 10 20 30 40 50 1 2 3 4 5 6 7 8 COMPRESSIVE STRENGTH % OF COIR FIBER ADDED % OF FIBER % OF FIBER % OF FIBER % OF FIBER
  • 7. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 10 Issue: 05 | May 2023 www.irjet.net p-ISSN: 2395-0072 © 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1811 Table -6: 28 Days Split Tensile Strength Test Result (N/Mm2 ) % OF FIBER ADDED 28 DAYS SPLIT TENSILE STRENGTH TEST RESULT (N/mm2 ) 15mm 25mm 30mm 0 3.41 3.58 3.64 0.1 3.52 3.77 3.91 0.2 3.64 3.85 4.01 0.3 3.52 3.7 3.68 Chart -2: Split Tensile Strength Test 28days Result Flexural Strength Test: Flexure strength test for beam 150X150X170mm length using CTM machine of capacity 300T, this is for each cube as per IS516-1959. Flexural strength of concrete is considered as an index of tensile strength of concrete. Tensile stresses are likely to develop in concrete due to drying shrinkage, rusting of steel reinforcement, temperature gradients and many other reasons. Beam tests are conducted to determine flexural strength of concrete. In flexural tests on beam theoretical maximum tensile strength is obtained at bottom of beam and is called modulus of rupture, which depends on dimension of beam and position of loading. Table -7: 28 Days Flexural Strength Test Result (N/Mm 2 ) % OF FIBER ADDED 28 DAYS FLEXURAL STRENGTH TEST RESULT (N/mm2 ) 15mm 25mm 30mm 0 3.82 4.16 5.03 0.1 3.96 4.29 5.67 0.2 4.32 4.53 4.79 0.3 4.35 4.42 4.57 Chart -3: Flexural Strength Test 28days Result RESULT: The addition of 0.3% of treated coir fiber at length of 15mm, 25mm and 30mm improve in the result of compression strength test, split tensile strength test and flexural strength test, with best outcome observed for 30mm length chemically treated coir fiber reinforced concrete. 4. CONCLUSIONS 1. The concrete can be reinforced as coir fiber, which has been proven to be a successful material. 2. Test were carried out in labs all around the world to see the performance of concrete would be impacted by coconut fibers. 3. Coconut fiber is the perfect material for creating a lightweight version of concrete. Coir fibers are less dense than concrete and so the total weight of construction. 4. The coir fibers increase concrete specifications and aid in lowering environmental pollution. The study findings support the idea that no more than 1% of the fiber fraction should be used. Coir fibers has low heat conductivity hence it promotes natural cooling. 5. Improved Fiber-Matrix Bond: Chemical treatment of coir fiber with 1N NaOH can enhance the adhesion between the fiber and the concrete matrix. This treatment helps remove impurities and surface contaminants from the fibers, allowing for better bonding and improved mechanical properties of the reinforced concrete. 6. Enhanced Mechanical Properties: The addition of chemically treated coir fibers to concrete can lead to improvements in mechanical properties such as tensile strength, flexural strength, and impact resistance. The 0 1 2 3 4 5 1 2 3 4 5 6 7 8 SPLIT TENSILE STRENGTH % OF COIR FIBER ADDED % OF FIBER % OF FIBER % OF FIBER % OF FIBER 0 1 2 3 4 5 6 1 2 3 4 5 6 7 8 FLEXURAL STRENGTH % OF COIR FIBER ADDED % OF FIBER % OF FIBER % OF FIBER % OF FIBER
  • 8. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 10 Issue: 05 | May 2023 www.irjet.net p-ISSN: 2395-0072 © 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 1812 treated fibers act as reinforcement, effectively distributing stresses within the concrete and enhancing its overall performance. 7. Reduction in Cracking and Shrinkage: The presence of coir fibers, especially when chemically treated, can help mitigate cracking and shrinkage in concrete. The fibers act as internal reinforcement, providing additional tensile strength and controlling the development of cracks, thereby improving the durability and longevity of the concrete structures. 8. It is important to note that these conclusions are generalized and based on the potential benefits associated with chemically treated coir fiber reinforced concrete. REFERENCES 1. Durability Study on Coir Fibre Reinforced Concrete Nithin Sam1 1P.G Student, Department of Civil Engineering, Albertian Institute of Science and Technology, Kerala, India Sheeja M K2 2Assistant Professor, Department of Civil Engineering, Albertian Institute of Science and Technology, Kerala, India. 2. Concrete Reinforced with Coconut Fibres V. Sai Uday1 , B.Ajitha2 M.Tech Student1 , Assistant Professor2 Department of Civil Engineering JNTUA College of Engineering, Ananthapuram, AP, India. 3. EXPERIMENTAL STUDY ON COIR FIBRE MIXED CONCRETE 1Achudhan 2M.J. Ienamul Hasan Ali, 3S. Senthamizh Sankar, 4K. Saikumar 1Assistant Professor, Faculty, Department of Civil Engineering, Sri Sai Ram Institute of Technology, India 2,3,4 Under Graduate Students, Department of Civil Engineering, Sri Sai Ram Institute of Technology, India. 4. A Review on Coir Fiber Reinforced Polymer Composite U.S. Bongarde1, B.K. Khot2 1,2Assistant Professor, Department of Mechanical Engineering, Textile and Engineering Institute, Ichalkaranji, 416115, India. 5. Role of coconut coir fiber in concrete Article in Materials Today: Proceedings · February 2020 Habibunnisa Syed Vignan's Foundation For Science, Technology and Research (Deemed to be Unive.. 5 PUBLICATIONS 35 CITATIONS Nerella Ruben Vignan University 54 PUBLICATIONS 2,114 CITATIONS. 6. Mechanical and Durability Performance of Coconut Fiber Reinforced Concrete: A State-of-the-Art Review Article in Materials · May 2022. 7 authors, including: Jawad Ahmad Master of Science in Structural Engineering 60 PUBLICATIONS 513 CITATIONS, Ali Majdi Al-Mustaqbal University College 93 PUBLICATIONS 195 CITATIONS, Amin Al-Fakih King Fahd University of Petroleum and Minerals 51 PUBLICATIONS 739 CITATIONS and Ahmed Farouk Deifalla Future University in Egypt 130 PUBLICATIONS 1,117 CITATIONS.