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International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 10 Issue: 03 | Mar 2023 www.irjet.net p-ISSN: 2395-0072
BOILER TUBE FAILURE ANALYSIS IN 210MW POWER PLANT
STEAM BOILER
Dr. A PSivasubramaniam1, Sabarinathan G2, Saran M3, Sridharprasad R K4, Subash U5
1professor, Dept. of Mechanical Engineering, Paavai Engineering College , Namakkal, Tamilnadu, India 637018
2,3,4,5 Student, Dept. of Mechanical Engineering, Paavai Engineering College, Namakkal, Tamilnadu, India 637018
---------------------------------------------------------------------***--------------------------------------------------------------------
Abstract- This study is aimed at analyzing the
reasons associated with boiler tube failure. Inspection
and data collected from MTPS - I serve as the basis for
this analysis. Three samples (damaged LTSH tube,
failed Economizer tube and failed RH tube) were
collected from MTPS. Metallographic investigations
were carried out in the samples collected to
understand, interpret and substantiate the probable
reasons that led to tube failure which occur when the
effective strength falls below a critical level. Apart
from visual inspection, optical microscopy, micro-
hardness tests, SEM investigations, chemical analysis
and EDS tests were carried out on various regions of
the failed tubes and the results have been elaborately
discussed. Upon visual inspection, formation of oxide
layers on the inner side of the tube has been noticed
which indicated that the inner side of the tube is
subjected to corrosion. Formation ofoxide layers has
led to inhomogeneous overheating which has thereby
affected the homogeneity of the tube. The main
reason for rupture (hole formation) in the failed
region can be attributed to steam erosion either from
an adjacent failed tube or from soot blower. Besides
steam erosion, flue gas erosion has also occurred due
to unevenvelocity of flue gas which could be catalyzed
by the presence of unburnt coal particles.
Graphitization leading to formation of elongated as
well as spherical graphite nodules and
spheroidization over a period of time were identified
as the major failure mechanisms involved from a
microscopic perspective which could be related with
overheating accompanied by creep leading to
softening of the tube at the failed region thereby
causing ductile fracture from a mechanical
perspective. SEM micrographs showed the formation
of graphite nodules, micro-cracks and void
coalescence. Though occurrences of tube failures in
boiler couldn’t be completely eradicated, they can be
considerably reduced by adopting certain remedial
measuressuggested at the end.
Keywords: Tube failure, metallographic
examination, graphitization, spheroidization,
overheating, creep, erosion, corrosion, ferrite –
pearlite micro structure.
1. INTRODUCTION
As could be observed from the report of Central
Electricity Authority, leakage in water wall tubes, super
heater tubes, re-heater tubes and economizer tubes
accounts for 2.2 % of loss of maximum power
generation. While investigating the root cause of these
leakages, it transpires that the boiler tubes are subjected
to a variety of failures involving one or more of several
mechanisms like erosion, corrosion, stress rupture etc. A
detailed study is warranted for understanding the
various mechanisms leading to failure of boiler tubes.
2. BOILER TUBE FAILURE
The accurate prediction of life of boiler tubes is difficult
because of uncertainties associated with operating
conditions, material properties, erosion/corrosion rate,
geometry of eroded/corroded areas etc. It is very
difficult to identify and locate gradual degradation of
tubes like thinning, crack formation, deformation till it
leads to puncture causing leakages. The only time
interval when the tube can be accessed is during the
planned maintenance as per the schedule besides forced
outages. The symptoms ofleakage in tube are feed water
consumption higher than normal leading to more make
up water, low water level in the boiler drum, pressure
drop in steam, hissing sound emitted by leaking steam,
white smoke from chimney, fluctuations in furnace
pressure.
2.1 VARIOUS NOMENCLATURES INVOLVED IN
TUBE FAILURES
1. Weld failure
2. Secondary tube failure
3. Erosion
4. Corrosion
5. High temperature oxidation
6. Hydrogen attack
7. Caustic corrosion
8. Stress rupture
© 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 440
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 10 Issue: 03 | Mar 2023 www.irjet.net p-ISSN: 2395-0072
2. 2 INVESTIGATION WORK
The investigation was carried out on the following
scrapped tubes reportedly discardedand disposed as
scrap from MTPS.
1. Damaged LTSH tube
2. Failed economizer tube
3. Failed RH tube
Material specifications, design and operating
parameters of the LTSH tube as obtained from the
thermal power plant are as follows:
Table 1 - Tube Specifications
To analyze the failure of these tubes, visual
examination was performed by naked eye and images
have been taken by digital camera. The failed
economizer tube and failed RH tube suffered
significant damage while LTSH tube has not suffered
any kind of significant damage.
In order to investigate the potential causes for failure
due to microstructural anomalies or degradations,
specimens of economizer and RH tube were cut
transversely along the cross section of the tube in the
failed region, and randomly chosen region in case of
LTSH tube. The small ring is cut longitudinally to make
small specimens and marked as detailed below.
The method of optical microscopy has been used for
microstructural examinations. Metallographic sample
preparation has been carried out using standard
Micro indentation hardness measurement on the
mounted sample was conducted using Vickers digital
micro hardness tester (model: MMT – X7 No:MM5250X,
Manufacturer MATSUZAWA CO.LTD., Japan).
3.BOILER TUBE FAILURE ANALYSIS
Failure analysis mainly consist of:
 Visual inspection
 Metallographic examination
 Micro hardness test
 Sem investigation
3.1VISUAL INSPECTION
The failed section of the economizer and RH tube was
visually inspected. Figure 3.1 (a) presents an image of as-
received sample of the failed economizer tube and Figure
(b) presents an image of as-received sample of the failed
RH tube. The circularity of the tube cross section is
varying.
By observing cross section of the economizer and RH
tube, it could be noted thathalf of the cross section of the
tube segment was thinner than the other. Figure 3.1 (a)
& (b) presents image after making a single cut along
transverse plane of failed economizer and RH tube
respectively
Figure 3.1 (a): Cross section of LTSHtube
LTSH Economizer RH
Material SA-106 Gr.B SA-106 Gr.B SA-106 Gr.B
Outside diameter
(mm)
44.5 56.0 56.0
Thickness (mm) 4.5 6.0 6.0
Steam / water
inlet temperature
(℃)
340 247 332
Steam / water
outlet temperature
(℃)
420 284 540
Flue gas inlet
temperature (℃)
671 476 1020
Flue gas outlet
temperature (℃)
476 370 828
Service Exposure
(years)
10 15 15
procedures. The sectioned samples are mounted using
hot mounting process which uses thermosetting plastic
compound bakelite to encapsulate the specimen. The
mounting undergoes grinding, polishing using series of
emery paper containing successively finer abrasive
followed by etching. 2% Nital is used as etchant. The
mounted samples are investigated using a Leica DMi8
metallurgical microscope.
© 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 441
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 10 Issue: 03 | Mar 2023 www.irjet.net p-ISSN: 2395-0072
Figure 3.1 (b): Cross section at the failed
region of Economizer tube.
Figure 3.1 (c): Cross section at the failed
region of RH tube.
The measured thicknesses of tube walls at different
segments are as follows:
Table 2 - Thickness of the Economizer tube
in mm
Table 3 - Thickness of the RH tube in mm
Upon thinning, the tube could have failed due to following
two reasons:
1. The reduced thickness could not withstand the
circumferential hoop stressand caused stress rupture.
2. Thinning might have caused over heating which has
led the metal temperatures to exceed their creep
temperature limit.
3.2 METALLOGRAPHIC EXAMINATION
Long term overheating brings about microstructural
changes like grain growth, disintegration of pearlite,
spheroidization of carbides, graphitization and
decarburization leading to loss of strength of the tube
material, eventually resulting in stress rupture or creep
rupture through grain boundary void formation. The first
stage in the transformation is in situ break down of the
pearlite colonies remaining intact but the platelets of iron
carbide become spheroids. The next stage is the
disappearance of pearlite colonies and dispersion of
spherical carbide particles throughout the matrix and
then finally the formation of graphite particles and their
growth.
Figure 3.2 (a)
Affected region of LTSH tube
Figure 3.2 (b) More affected region of Economizer tube
A1 B1 C1 D1 E1 F1
1.34 6.48 6.40 5.58 6.10 4.19
A2 B2 C2 D2 E2 F2
2.09 6.44 6.53 6.50 5.73 3.07
© 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 442
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 10 Issue: 03 | Mar 2023 www.irjet.net p-ISSN: 2395-0072
Figure 3.2 (c) More affected region of RH tube with
significant graphitization
3.3 MICRO HARDNESS TEST
By referring the above table, it could be noted that the
hardness in the thinned portion is lesser than that of the
thick portion. Softening has occurred in the thinned
portion due to overheating. Since yielding / plastic
deformation has occurred in the failed region, the
inference that could be drawn is that the fracture
mechanism involved here is ductile fracture.
3.4 SEM INVESTIGATION
In order to investigate the fracture mechanisms
involved, SEM investigations were conducted through
Scanning Electron Microscope Apreo SEM – Thermo
Scientific funded by SRM IST and micro-fractographs
were taken at various magnifications for un- etched
samples.
Figure 3.4 (a) SEM micrographs of Economizer tube
Figure 3.4 (b) SEM micrographs of RH tube
By referring the SEM micrographs, we could observe the
formation of graphite nodules which confirms the
occurrence of elongated as well as spherical
graphitization. We could also observe the formation of
micro-voids and void coalescence along with micro-
cracks and their growth. Since the main purpose of doing
SEM in our project is to ascertain the formation of
graphite nodules, micro-cracks and void coalescence
which occurs due to diffusion of carbon as a result of
overheating accompanied by creep, we have done SEM on
un-etched specimens. There is a huge scope for
researchers to extend our SEM investigation with
specimens after applying various etchants so that the
formation of new grains with different microstructures
can be observed and appreciated.
Specimen Observed values in HV 300 gm
/Dwell time : 15 seconds
B0 – 0.1 mm from OD 145, 140, 141
B0 – 0.1 mm from ID 130, 139, 131
D0 – 0.1 mm from OD 138, 137, 135
D0 – 0.1 mm from ID 156, 151, 155
Economizer tube–
Thin region
173, 168, 177
Economizer tube–
Medium region
179, 169, 175
Economizer tube –
Thick region
183, 190, 195
RH tube – Thin region 190, 184, 188
RH tube – Medium
region
182, 189, 184
RH tube – Thick region 193, 200, 198
© 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 443
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 10 Issue: 03 | Mar 2023 www.irjet.net p-ISSN: 2395-0072
Apart from optical microscopy, micro-hardness test and
SEM investigation, we have also done chemical analysis
and EDS tests on various specimens and the results are
attached as annexures.
4 CONCLUSION AND RECOMMENDATIONS
1. When we refer to the standards being followed in
industrial thermal power plants mostly in India, we can
find that spheroidal graphitization has been taken into
consideration while designing the boiler operation but
elongated graphitization has not been taken into.
2. Regular thickness measurement consideration
since we could rarely find elongated graphitization being
discussed in available literatures.
3. Since, “chromium forms more stable carbides than
that of iron and molybdenum”, usage of boiler tube
materials with high chromium content can withstand
graphitization which is one of the most predominant
failure mechanisms identified via microscopic
examination.
4. Since yielding / plastic deformation has occurred
in the failed region, the inference that could be drawn
from the micro-hardness test is that the fracture
mechanism involved here is ductile fracture.
5. Standard operating procedure in maintenance
should be adhered to reduce maintenance related
failures such as weld failures.
6. The quality of coal should be ensured to reduce
failures due to erosion.
7. The quality of water treatment with robust
technologies in Demineralization watertreatment plant
(DM plant) should be ensured to avoid failures due to
formationof oxide scales and corrosion.
8. Reduction of fly ash generation which increases
erosion related failures in the design phase naturally
increases the generation of wet ash which causes
detrimental environmental impacts during its disposal
in the ash pond via slurry transportation. Hence, a trade
off must be given between these two while designing
new boilers.
9. By usage of tube materials resistant to high
temperature, we can reduce failures due to creep
mechanism.
10. By usage of tube materials resistant to high
internal pressure (Hoop stress), we can reduce
failures due to stress rupture.
high temperatures and pressures.
5ACKNOWLEDGEMENT
We express our sincere gratitude to our
principal Dr. M. Prem Kumar of Paavai Engineering
College, Namakkal. We also express our sincere gratitude
to the head of the Mechanical department Dr. A.P.
Sivasubramaniam for his constructive suggestions and
encouragement during our project for his valuable
Support,help and guidancethroughoutthisproject.
6 REFERENCES
1. Jutaporn Chaichalerm, Chaiyawat Peeratatsuwan, Thee
Chowwanonthapunya, ‘A metallurgical investigation on a
failed superheater tube used in a thermal biomass power
plant’.
2. S.W. Liu, W.Z. Wang, C.J. Liu, ‘Failure analysis of the
boiler water-wall tube’, Case Studies in Engineering
Failure Analysis 9 (2017) 35-39.
3. P. Sakthivel, S. Kalaimani, Dr. R. Sasikumar, ‘Analysis of
Tube Failure in Water Tube boiler’.
4. Rajat Gupta, S.N. Singh, V. Sehadri, ‘Prediction of
uneven wear in a slurry pipeline on the basis of
measurements in a pot tester’.
5. Xue, S., Guo, R., Hu, F., Ding, K., Liu, L., Zheng, L., Yang, T.,
‘Analysis of the causes of leakages and preventive
strategies of boiler water- wall tubes in a thermal power
plant’, Engineering Failure Analysis (2020), doi:
http://dx.doi.org/10.1016/j.engfailanal.2020.104381.
6. Vahid Javaheri, David Porter, Veli- Tapani Kuokkala,
‘Slurry erosion of steel- Review of tests, mechanisms and
materials’, Wear 408-409 (2018) 248-273.
7. AHMED ELKHOLY, ‘PREDICTION OF ABRASION WEAR
FOR SLURRY PUMP MATERIALS’, Wear, 84 (1983) 39 –
49.
8. F. Dehnavi, A. Eslami, F. Ashrafizadeh, ‘A case study on
failure of superheater tubes in an industrial power plant’,
Engineering Failure Analysis (2017), doi:
10.1016/j.engfailanal.2017.07.007.
11. Usage of supercritical boilers in an emerging
technology where we could eliminate the latent heat
required for converting water to steam which there by
reduces coal consumption. However, this
technology is profitable as far as boiler tube failures
are concerned only upon usage of tube materials that
could withstand
© 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 444
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056
Volume: 10 Issue: 03 | Mar 2023 www.irjet.net p-ISSN: 2395-0072
9. Babak Hagahighat-Shishavan, Hossein Firouzi-Nerbin,
Massoud Nazarian-Samani, Pooria Ashtari, Farzad
Nasirpouri, ‘Failure analysis of a superheater tube
ruptured in a power plant boiler: Main causes and
preventive strategies’, Engineering Failure Analysis 98
(2019) 131-140.
10. Rajat K. Roy, Swapan K. Das, Ashis K. Panda and
Amitava Mitra, ‘Analysis of Superheater Boiler Tubes
Failed through Non-linear Heating’, Procedia Engineering
86 (2014) 926-932.
© 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 445

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BOILER TUBE FAILURE ANALYSIS IN 210MW POWER PLANT STEAM BOILER

  • 1. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 10 Issue: 03 | Mar 2023 www.irjet.net p-ISSN: 2395-0072 BOILER TUBE FAILURE ANALYSIS IN 210MW POWER PLANT STEAM BOILER Dr. A PSivasubramaniam1, Sabarinathan G2, Saran M3, Sridharprasad R K4, Subash U5 1professor, Dept. of Mechanical Engineering, Paavai Engineering College , Namakkal, Tamilnadu, India 637018 2,3,4,5 Student, Dept. of Mechanical Engineering, Paavai Engineering College, Namakkal, Tamilnadu, India 637018 ---------------------------------------------------------------------***-------------------------------------------------------------------- Abstract- This study is aimed at analyzing the reasons associated with boiler tube failure. Inspection and data collected from MTPS - I serve as the basis for this analysis. Three samples (damaged LTSH tube, failed Economizer tube and failed RH tube) were collected from MTPS. Metallographic investigations were carried out in the samples collected to understand, interpret and substantiate the probable reasons that led to tube failure which occur when the effective strength falls below a critical level. Apart from visual inspection, optical microscopy, micro- hardness tests, SEM investigations, chemical analysis and EDS tests were carried out on various regions of the failed tubes and the results have been elaborately discussed. Upon visual inspection, formation of oxide layers on the inner side of the tube has been noticed which indicated that the inner side of the tube is subjected to corrosion. Formation ofoxide layers has led to inhomogeneous overheating which has thereby affected the homogeneity of the tube. The main reason for rupture (hole formation) in the failed region can be attributed to steam erosion either from an adjacent failed tube or from soot blower. Besides steam erosion, flue gas erosion has also occurred due to unevenvelocity of flue gas which could be catalyzed by the presence of unburnt coal particles. Graphitization leading to formation of elongated as well as spherical graphite nodules and spheroidization over a period of time were identified as the major failure mechanisms involved from a microscopic perspective which could be related with overheating accompanied by creep leading to softening of the tube at the failed region thereby causing ductile fracture from a mechanical perspective. SEM micrographs showed the formation of graphite nodules, micro-cracks and void coalescence. Though occurrences of tube failures in boiler couldn’t be completely eradicated, they can be considerably reduced by adopting certain remedial measuressuggested at the end. Keywords: Tube failure, metallographic examination, graphitization, spheroidization, overheating, creep, erosion, corrosion, ferrite – pearlite micro structure. 1. INTRODUCTION As could be observed from the report of Central Electricity Authority, leakage in water wall tubes, super heater tubes, re-heater tubes and economizer tubes accounts for 2.2 % of loss of maximum power generation. While investigating the root cause of these leakages, it transpires that the boiler tubes are subjected to a variety of failures involving one or more of several mechanisms like erosion, corrosion, stress rupture etc. A detailed study is warranted for understanding the various mechanisms leading to failure of boiler tubes. 2. BOILER TUBE FAILURE The accurate prediction of life of boiler tubes is difficult because of uncertainties associated with operating conditions, material properties, erosion/corrosion rate, geometry of eroded/corroded areas etc. It is very difficult to identify and locate gradual degradation of tubes like thinning, crack formation, deformation till it leads to puncture causing leakages. The only time interval when the tube can be accessed is during the planned maintenance as per the schedule besides forced outages. The symptoms ofleakage in tube are feed water consumption higher than normal leading to more make up water, low water level in the boiler drum, pressure drop in steam, hissing sound emitted by leaking steam, white smoke from chimney, fluctuations in furnace pressure. 2.1 VARIOUS NOMENCLATURES INVOLVED IN TUBE FAILURES 1. Weld failure 2. Secondary tube failure 3. Erosion 4. Corrosion 5. High temperature oxidation 6. Hydrogen attack 7. Caustic corrosion 8. Stress rupture © 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 440
  • 2. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 10 Issue: 03 | Mar 2023 www.irjet.net p-ISSN: 2395-0072 2. 2 INVESTIGATION WORK The investigation was carried out on the following scrapped tubes reportedly discardedand disposed as scrap from MTPS. 1. Damaged LTSH tube 2. Failed economizer tube 3. Failed RH tube Material specifications, design and operating parameters of the LTSH tube as obtained from the thermal power plant are as follows: Table 1 - Tube Specifications To analyze the failure of these tubes, visual examination was performed by naked eye and images have been taken by digital camera. The failed economizer tube and failed RH tube suffered significant damage while LTSH tube has not suffered any kind of significant damage. In order to investigate the potential causes for failure due to microstructural anomalies or degradations, specimens of economizer and RH tube were cut transversely along the cross section of the tube in the failed region, and randomly chosen region in case of LTSH tube. The small ring is cut longitudinally to make small specimens and marked as detailed below. The method of optical microscopy has been used for microstructural examinations. Metallographic sample preparation has been carried out using standard Micro indentation hardness measurement on the mounted sample was conducted using Vickers digital micro hardness tester (model: MMT – X7 No:MM5250X, Manufacturer MATSUZAWA CO.LTD., Japan). 3.BOILER TUBE FAILURE ANALYSIS Failure analysis mainly consist of:  Visual inspection  Metallographic examination  Micro hardness test  Sem investigation 3.1VISUAL INSPECTION The failed section of the economizer and RH tube was visually inspected. Figure 3.1 (a) presents an image of as- received sample of the failed economizer tube and Figure (b) presents an image of as-received sample of the failed RH tube. The circularity of the tube cross section is varying. By observing cross section of the economizer and RH tube, it could be noted thathalf of the cross section of the tube segment was thinner than the other. Figure 3.1 (a) & (b) presents image after making a single cut along transverse plane of failed economizer and RH tube respectively Figure 3.1 (a): Cross section of LTSHtube LTSH Economizer RH Material SA-106 Gr.B SA-106 Gr.B SA-106 Gr.B Outside diameter (mm) 44.5 56.0 56.0 Thickness (mm) 4.5 6.0 6.0 Steam / water inlet temperature (℃) 340 247 332 Steam / water outlet temperature (℃) 420 284 540 Flue gas inlet temperature (℃) 671 476 1020 Flue gas outlet temperature (℃) 476 370 828 Service Exposure (years) 10 15 15 procedures. The sectioned samples are mounted using hot mounting process which uses thermosetting plastic compound bakelite to encapsulate the specimen. The mounting undergoes grinding, polishing using series of emery paper containing successively finer abrasive followed by etching. 2% Nital is used as etchant. The mounted samples are investigated using a Leica DMi8 metallurgical microscope. © 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 441
  • 3. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 10 Issue: 03 | Mar 2023 www.irjet.net p-ISSN: 2395-0072 Figure 3.1 (b): Cross section at the failed region of Economizer tube. Figure 3.1 (c): Cross section at the failed region of RH tube. The measured thicknesses of tube walls at different segments are as follows: Table 2 - Thickness of the Economizer tube in mm Table 3 - Thickness of the RH tube in mm Upon thinning, the tube could have failed due to following two reasons: 1. The reduced thickness could not withstand the circumferential hoop stressand caused stress rupture. 2. Thinning might have caused over heating which has led the metal temperatures to exceed their creep temperature limit. 3.2 METALLOGRAPHIC EXAMINATION Long term overheating brings about microstructural changes like grain growth, disintegration of pearlite, spheroidization of carbides, graphitization and decarburization leading to loss of strength of the tube material, eventually resulting in stress rupture or creep rupture through grain boundary void formation. The first stage in the transformation is in situ break down of the pearlite colonies remaining intact but the platelets of iron carbide become spheroids. The next stage is the disappearance of pearlite colonies and dispersion of spherical carbide particles throughout the matrix and then finally the formation of graphite particles and their growth. Figure 3.2 (a) Affected region of LTSH tube Figure 3.2 (b) More affected region of Economizer tube A1 B1 C1 D1 E1 F1 1.34 6.48 6.40 5.58 6.10 4.19 A2 B2 C2 D2 E2 F2 2.09 6.44 6.53 6.50 5.73 3.07 © 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 442
  • 4. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 10 Issue: 03 | Mar 2023 www.irjet.net p-ISSN: 2395-0072 Figure 3.2 (c) More affected region of RH tube with significant graphitization 3.3 MICRO HARDNESS TEST By referring the above table, it could be noted that the hardness in the thinned portion is lesser than that of the thick portion. Softening has occurred in the thinned portion due to overheating. Since yielding / plastic deformation has occurred in the failed region, the inference that could be drawn is that the fracture mechanism involved here is ductile fracture. 3.4 SEM INVESTIGATION In order to investigate the fracture mechanisms involved, SEM investigations were conducted through Scanning Electron Microscope Apreo SEM – Thermo Scientific funded by SRM IST and micro-fractographs were taken at various magnifications for un- etched samples. Figure 3.4 (a) SEM micrographs of Economizer tube Figure 3.4 (b) SEM micrographs of RH tube By referring the SEM micrographs, we could observe the formation of graphite nodules which confirms the occurrence of elongated as well as spherical graphitization. We could also observe the formation of micro-voids and void coalescence along with micro- cracks and their growth. Since the main purpose of doing SEM in our project is to ascertain the formation of graphite nodules, micro-cracks and void coalescence which occurs due to diffusion of carbon as a result of overheating accompanied by creep, we have done SEM on un-etched specimens. There is a huge scope for researchers to extend our SEM investigation with specimens after applying various etchants so that the formation of new grains with different microstructures can be observed and appreciated. Specimen Observed values in HV 300 gm /Dwell time : 15 seconds B0 – 0.1 mm from OD 145, 140, 141 B0 – 0.1 mm from ID 130, 139, 131 D0 – 0.1 mm from OD 138, 137, 135 D0 – 0.1 mm from ID 156, 151, 155 Economizer tube– Thin region 173, 168, 177 Economizer tube– Medium region 179, 169, 175 Economizer tube – Thick region 183, 190, 195 RH tube – Thin region 190, 184, 188 RH tube – Medium region 182, 189, 184 RH tube – Thick region 193, 200, 198 © 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 443
  • 5. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 10 Issue: 03 | Mar 2023 www.irjet.net p-ISSN: 2395-0072 Apart from optical microscopy, micro-hardness test and SEM investigation, we have also done chemical analysis and EDS tests on various specimens and the results are attached as annexures. 4 CONCLUSION AND RECOMMENDATIONS 1. When we refer to the standards being followed in industrial thermal power plants mostly in India, we can find that spheroidal graphitization has been taken into consideration while designing the boiler operation but elongated graphitization has not been taken into. 2. Regular thickness measurement consideration since we could rarely find elongated graphitization being discussed in available literatures. 3. Since, “chromium forms more stable carbides than that of iron and molybdenum”, usage of boiler tube materials with high chromium content can withstand graphitization which is one of the most predominant failure mechanisms identified via microscopic examination. 4. Since yielding / plastic deformation has occurred in the failed region, the inference that could be drawn from the micro-hardness test is that the fracture mechanism involved here is ductile fracture. 5. Standard operating procedure in maintenance should be adhered to reduce maintenance related failures such as weld failures. 6. The quality of coal should be ensured to reduce failures due to erosion. 7. The quality of water treatment with robust technologies in Demineralization watertreatment plant (DM plant) should be ensured to avoid failures due to formationof oxide scales and corrosion. 8. Reduction of fly ash generation which increases erosion related failures in the design phase naturally increases the generation of wet ash which causes detrimental environmental impacts during its disposal in the ash pond via slurry transportation. Hence, a trade off must be given between these two while designing new boilers. 9. By usage of tube materials resistant to high temperature, we can reduce failures due to creep mechanism. 10. By usage of tube materials resistant to high internal pressure (Hoop stress), we can reduce failures due to stress rupture. high temperatures and pressures. 5ACKNOWLEDGEMENT We express our sincere gratitude to our principal Dr. M. Prem Kumar of Paavai Engineering College, Namakkal. We also express our sincere gratitude to the head of the Mechanical department Dr. A.P. Sivasubramaniam for his constructive suggestions and encouragement during our project for his valuable Support,help and guidancethroughoutthisproject. 6 REFERENCES 1. Jutaporn Chaichalerm, Chaiyawat Peeratatsuwan, Thee Chowwanonthapunya, ‘A metallurgical investigation on a failed superheater tube used in a thermal biomass power plant’. 2. S.W. Liu, W.Z. Wang, C.J. Liu, ‘Failure analysis of the boiler water-wall tube’, Case Studies in Engineering Failure Analysis 9 (2017) 35-39. 3. P. Sakthivel, S. Kalaimani, Dr. R. Sasikumar, ‘Analysis of Tube Failure in Water Tube boiler’. 4. Rajat Gupta, S.N. Singh, V. Sehadri, ‘Prediction of uneven wear in a slurry pipeline on the basis of measurements in a pot tester’. 5. Xue, S., Guo, R., Hu, F., Ding, K., Liu, L., Zheng, L., Yang, T., ‘Analysis of the causes of leakages and preventive strategies of boiler water- wall tubes in a thermal power plant’, Engineering Failure Analysis (2020), doi: http://dx.doi.org/10.1016/j.engfailanal.2020.104381. 6. Vahid Javaheri, David Porter, Veli- Tapani Kuokkala, ‘Slurry erosion of steel- Review of tests, mechanisms and materials’, Wear 408-409 (2018) 248-273. 7. AHMED ELKHOLY, ‘PREDICTION OF ABRASION WEAR FOR SLURRY PUMP MATERIALS’, Wear, 84 (1983) 39 – 49. 8. F. Dehnavi, A. Eslami, F. Ashrafizadeh, ‘A case study on failure of superheater tubes in an industrial power plant’, Engineering Failure Analysis (2017), doi: 10.1016/j.engfailanal.2017.07.007. 11. Usage of supercritical boilers in an emerging technology where we could eliminate the latent heat required for converting water to steam which there by reduces coal consumption. However, this technology is profitable as far as boiler tube failures are concerned only upon usage of tube materials that could withstand © 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 444
  • 6. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395-0056 Volume: 10 Issue: 03 | Mar 2023 www.irjet.net p-ISSN: 2395-0072 9. Babak Hagahighat-Shishavan, Hossein Firouzi-Nerbin, Massoud Nazarian-Samani, Pooria Ashtari, Farzad Nasirpouri, ‘Failure analysis of a superheater tube ruptured in a power plant boiler: Main causes and preventive strategies’, Engineering Failure Analysis 98 (2019) 131-140. 10. Rajat K. Roy, Swapan K. Das, Ashis K. Panda and Amitava Mitra, ‘Analysis of Superheater Boiler Tubes Failed through Non-linear Heating’, Procedia Engineering 86 (2014) 926-932. © 2023, IRJET | Impact Factor value: 8.226 | ISO 9001:2008 Certified Journal | Page 445