SlideShare a Scribd company logo
1 of 34
Download to read offline
i | P a g e
SCHOOL OF MECHANICAL ENGINEERING
REPORT ON CAPSTON PROJECT
TITLE: DESIGN & FABRICATION OF A LOW COST SPIN COATER
Submitted to Lovely Professional University
In partial fulfillment of the requirement for the award of
“DEGREE OF BACHELOR OF TECHNOLOGY [MECHANICAL
ENGINEERING]”
Submitted By
Name Registration No.
 SAURABH PANDEY 11102793
 KAPIL RAGHUWANSHI 11105326
 SUDHIR YADAV 11108007
 PUNEET KUMAR 11111389
Research Supervisor
Mr. Sumit shoor
UID. 14602
Assistant Professor
School Of Mechanical Engineering
ii | P a g e
CERTIFICATE
This is certified that Saurabh Pandey, Kapil Raghuwanshi, Sudhir Yadav, Puneet Kumar have
complete this capstone project of – Design & Fabrication of Low Cost Spin Coater under my
guidance. During this project they have done most efforts to study and understand the subject in
detail. In addition to the books mentioned in the bibliography they have referred various study
material, magazine, websites, research papers and notes to complete this project. During this
project they have been very much curious and enthusiast to understand the spirit of the expert
documentation and procedures.
We wish them best of luck.
Research Supervisor
Mr. Sumit Shoor
14602
Asst. Professor
School Of Mechanical Engg. Signature of Supervisor
iii | P a g e
DECLARATION
This is to certify that we are the student of School Of Mechanical Engineering, pursuing
Bachelor of Technology(Mechanical Engineering) have completed capstone project on topic
“Design & Fabrication of Low Cost Spin Coater” for partial fulfillment of degree of Bachelor
of Technology to Lovely professional University, Phagwara (PUNJAB).We solemnly declare
that the work done by us is original and no copy of it has been submitted to Lovely Professional
University or any other university for award of any other degree/fellowship.
Name Registration Number Signature
 Saurabh Pandey 11102793
 Kapil Raghuwanshi 11105326
 Sudhir Yadav 11108007
 Puneet Kumar 11111389
iv | P a g e
Acknowledgement
Itakethis opportunitytopresent myvotes ofthanks toallthoseguidepost whoreallyactedas lightening pillars
to enlighten our way throughout this project that has led to successful and satisfactorycompletion of
this study. We are really grateful to our teacher for providing us with an opportunity to undertake
this project in this university and providing us with all the facilities. We are highly thankful to
Mr. Sumit Shoor(Asst. Professor) for his active support, valuable time and advice, whole-
hearted guidance, sincere cooperation and pains-taking involvement during the study
and in completing the assignment of preparing the said project within the time
stipulated.
Lastly, we are thankful to all those particularly the various friends who have been
instrumental in creating proper, healthy and conductive environment and including
new and fresh innovative ideas for us during the project, their help, it would have
been extremely difficult for us to prepare the project in a time bound framework.
v | P a g e
ABSTRACT
The goal of this capstone project was designing a low cost spin coater which works
economically.
With the help of this spin coater we can create a thin film on the flat surface of any work piece.
This process is basically follows the principle of Centrifugal Force which draws a rotating body
away from the centre of rotation.
The thickness of film depends on different factors which are as follows:
 Concentration of the Solution
 Rotational Speed
 Rotation Time
So these above are some factors which can affect the thickness of the film. By taking care of
these above said factors we can get the desired thickness of film of any substrate.
Spin Coating is a fast and easy method to generate thin and homogeneous films out of solutions.
vi | P a g e
TABLE OF CONTENTS
Title Page
Cover Page i
Certificate ii
Declaration iii
Acknowledgement iv
Abstract v
Table of Contents vi – vii
List of figures viii
List of Graph ix
List of Tables x
CHAPTER 1 Introduction 1 - 4
1.1 Definition and brief history of Spin Coating 1
1.2 Physics of Spin Coating 2
1.3 Industrial uses of spin Coating technology 2
1.4 Common spin coating defects 2 -3
1.5 The Spinning Coating Process 4
1.6 Objective of Project 4
CHAPTER 2 Literature Review 5 - 8
2.1 Introduction 5
2.1.1 Spin Coater with a touch screen interface 5
2.1.2 Cost effective home-made Spin Coater 6 - 7
for depositing thin films
2.1.3 Design & Fabrication of a Low cost effective 7
Spin Coater for deposition of thin films
2.1.4 A comprehensive study of spin coating as a 8
thin film deposition technique and coating Equipment
vii | P a g e
CHAPTER 3 Material and Modeling 9-16
3.1 Introduction 9
3.2 Materials/Parts used in the making of the project 9
3.3 Specification of Materials/Equipments 10-12
3.4 Modeling of spin coater 12-15
3.4.1 Key stages of spin coating 13-15
3.6 Cost Analysis 16
CHAPTER 4 Results & Discussion 17 - 20
4.1 Introduction 17
4.2 Result 17 - 19
4.2.1 Graph between film thickness Vs spin time 18
4.2.2 Graph between film thickness Vs spin speed 18- 19
4.3 Spin coating troubleshooting process 19- 20
CHAPTER 5 Conclusion & Future scope 20 - 21
5.1 Conclusion 21 - 22
5.1.1 Advantage 21
5.1.2 Disadvantage 21 - 22
5.2 Future scope 22
References 23- 24
viii | P a g e
LIST OF FIGUERS
FIGURE 1.1 Spin Coating using Centrifugal force Page No. 1
FIGURE 1.2 Defects occurs from spin coating Page No. 3
FIGURE 1.3 Defects occurs from spin coating Page No. 3
FIGURE 1.4 Dispense of coating fluid at the centre Page No. 4
FIGURE 2.1 Touch screen interface
Page No. 5
FIGURE 2.2 Chuck with adjustable Clamps Page No. 6
FIGURE 3.1 Front View of outer cabinet Page No. 10
FIGURE 3.2 High speed sewing machine motor Page No. 11
FIGURE 3.3
Front & Rear view of the Disk with
Clamping arrangement Page No. 12
FIGURE 3.4 Final design of spin coater Page No. 13
FIGURE 3.5 Key stages of spin coating process Page No. 14
FIGURE 4.1 First experiment Page No. 17
ix | P a g e
LIST OF GRAPHS
GRAPH 4.1 Relationship between film
thickness and spinning time
Page No. 18
GRAPH 4.2 Relationship between film
thickness and spinning time
Page No. 19
x | P a g e
LIST OF TABLE
TABLE 3.1 Cost analysis Page No. 16
TABLE 4.1 Troubleshooting Page No. 20
TABLE 4.2 Troubleshooting Page No. 20
1 | P a g e
CHAPTER 01
INTRODUCTION
Spin Coating is basically a procedure which is used to deposit uniform thin films to any flat
surface of work piece. Usually a small amount of coating material is applied on the centre of the
work piece’s surface when the disk is spinning at very low speed. Here in this process we are
using the basic principle of centrifugal force. This is applied due to the spinning of Disk.
FIG. 1.1 Spin Coating using Centrifugal force [1]
1.1 Definition and brief history of Spin Coating
 A process in which solution is spread evenly over a surface using centripetal force when
the disk is rotating.
 Spin Coating will result in a relatively uniform thin film of a specific thickness.
 Spin Coating is an important way of creating thin films in the microelectronics industry
where we need thin films coating.
 Spin Coating was first used to apply coatings of paints and pitch around seventy years
ago.
 In 1958 Emsile et. Al. developed the first spin coating model.
 This model has been used as a basis for future more specific or complicated models.
2 | P a g e
1.2 Physics of Spin Coating
Spin Coating process basically uses the principle of Centrifugal force. When the disk is rotating
in any direction, a centrifugal force generates which draws rotating body away from the centre of
rotation. We will further discuss about the centrifugal force here:
Centrifugal Force
Centrifugal force is the apparent force that draws a rotating body away from the centre of
rotation. It is caused by the inertia of the body.[2]
1.3 Industrial uses of Spin Coating technology
 Photo resists for patterning wafers in micro circuit production.
 Insulating layers for micro circuit fabrication such as polymers.
 Flat screen display coatings.
 Antireflection coatings and conductive oxides.
 DVD & CD ROM.
 Television tube antireflection coatings.
1.4 Common Spin Coating Defects
There occur lots of defects after completing the coating processes. Some of them are as follows:
 Bubbles on the surface of the Coated substrate.
 These bubbles occurs when fluid is deposited as the wafer is spinning, and may be
caused by a faulty dispense tip.
 A swirling pattern may be observed.
3 | P a g e
FIG. 1.2 Defects occurs from spin coating[3]
 Causes :-
 Fluid deposited off centre.
 Acceleration too high.
 Spin time too short.
 Exhaust rate too high.
 A mark or circle in the centre of the wafer could indicate a chuck mark.
FIG. 1.3 Defects occurs from spin coating[3]
 If a Chuck mark occurs the type of chuck should be changed.
 Uncoated areas on substrate occur when to little fluid is deposited on the substrate.
 Pinhole defects can be caused by 1) Air Bubbles 2) particles in fluid/ Substrate
.
4 | P a g e
1.5 Spin Coating process
A typical Spin Coating Process basically consist of four steps which consist of a Dispense step in
which the coating fluid material is deposited onto the surface of work piece, a high speed spin
step to thin the fluid, and a drying step eliminate excess coating fluid from the resulting film.
 Loading Of Substrate
FIG. 1.4 Dispense of coating fluid at the centre
 Dispense of Coating fluid on Substrate
 Film Casting And Drying
 Process Complete
This method was first described by Emslie et al. (1958) and Meyerhofer Et al. (1978) using
several simplifications.[4]
1.6 Objective of Project
The basic object of this project is to Design a low cost spin Coater which will effective as well as
economical. We tried here to Design a Spin Coater which is of low cost but fully functional.
5 | P a g e
CHAPTER 2
LITRATURE REVIEW
2.1 Introduction
In very simple words spin coating is a method used to apply a layer of uniform thickness of thin
films to any work piece of flat surface. And the mechanism used for spin coating is known as
spin coater. So for getting some knowledge about above said project we need some basic
knowledge about the project which we got from some research papers, magazines, books etc. &
some of here as follows :
2.1.1 Spin Coater with a touch screen interface
Here according to Mr. Gurucharan V. Karnad(Dept. of Physics, Indian institute of science,
Bangalore), et. Al. Spin Coating is one of the coating technique used to apply thin uniform films
to flat surface of work piece. A spin coater is a machine used for spin coating , and is one of the
most ubiquitous instrument in any laboratory dealing with micro fluidic devices.
Run Time Setting Menu Display Screen RPM Setting
FIG. 2.1 [5]
They made a spin coater with a touch screen panel interface which cost about 350USD. The user
input is through the touch screen panel interface, where parameters like duration of spin and spin
speed can be entered. Real time speed is also displayed alongside.
6 | P a g e
In these spin coater the substrate is mounted either using a double- side tape or a set of clamps.
Improvements with the help of vacuums chuck, computer interfacing etc. can be done as per
necessity.
FIG. 2.2 Chuck with adjustable Clamps
So here talking about our project we are using manual holding device over chuck for the
mounting of substrate. We studied in an article that there is a problem of entering fuid into the
vacuum pipe occurs when we are using vacuum chuck so we decide here not to use vacuum
chuck.[6]
2.1.2 Cost effective home-made Spin Coater for depositing thin
films
Writer : Mohua Fardousi et. Al.
A simple low cost spin coater design has been described in this paper. This low cost coating
system is used to deposit thin films. The system can be easily built with the basic knowledge of
machine and electronics.
According to them this project can be done using a DC motor and electronic circuit , Designed to
control the spinning speed. The spinning speed varies from 350- 3800 rpm.
7 | P a g e
Talking about our project we used 230 volts regulator for controlling the speed of Motor. We
want to make a low cost project which are having very less complications so we did not used any
electronic circuit to avoid complications.[7]
2.1.3 Design & Fabrication of a Low cost effective Spin Coater for
deposition of thin films
Writer : Mohammad Meftahul Ferdaus et. Al.
According to authors this paper tells us about the design and fabrication of a low cost spin coater for
depositing thin films on any flat substrate. In simple words spin coater is a machine that can dispense a
liquid fluid onto a substrate equally.
Some unique desirable properties of Spin coating machine such as ability to make defect free and uniform
thickness of thin film, accuracy when talking about rotation control together with a closed optimized
process chamber etc. are maintained in this prototype spin coater.
The materials used for making thin film liquefied in a volatile solvent. Here the system is fabricated by
using a dc motor and simple electronics circuit, in which the spinning speed can be controlled very easily.
In this design the spinning speed is up to 3,000 rpm that can be controlled step by step manually.
Thin film deposition by this cost effective spin coater is a very simple technique and can be used widely
for preparing films of uniform thickness.[8]
So as we said above we were trying to reduce complication from the project so we used regulator
for controlling the speed of motor. We can regulate motor from 300 rpm to 9000 rpm.
8 | P a g e
2.1.4 A comprehensive study of spin coating as a thin film
deposition technique and coating Equipment
Writer : M. D. Tyona, Advances in Material Research, Vol. 2, No. 4(2013) 181 – 193 et. Al.
According to the author spin coating machine designed and fabricated using affordable
components. The system was easily built with the knowledge of mechanics, fluid mechanics and
basics of electronics. This equipment employs majorly three basic components and two circuit
units in its operation.
These includes a high speed Dc motor, a proximity sensor mounted at a distance of about 15mm
from a reflective metal attached to the spindle of the motor to detect every passage of reflective
metal at its front and generate pulses.
Talking about our project we are neither using any kind of sensor here nor any electronic circuit
for reducing or controlling the speed of motor. In the process of making our project we are
focusing on making a low cost Spin Coater. That’s why here we used a 230 volt Regulator for
controlling the speed of motor.[9]
9 | P a g e
CHAPTER 03
MATERIAL AND MODELING
3.1 Introduction
Material and Modeling is an important part of the project report. In which we will discuss here
about the materials, equipments etc. what we used during making of our project as well as the
modeling of spin coater and spin coating process. Here also we will discuss about the design of
the project as well as we will do cost analysis of the project.
3.2 Materials/Equipments used in the making of the project
Materials and equipments are the base for making of any project. Here in the making of our
project we used Tin for the outer covering inside which we will assemble all the other
equipments like motor, shafts, pulley, belt, other electronic parts etc.
We used here Pewter for making clamps because of its several properties like it is very less in
their weight comparing to other metals or any things.
We used here a plastic pot for the upper covering of Disk as it is very less in weight. As we were
trying to reduce the weight of our project. We also used a syringe for deposition of fluid exactly
at the centre in exact measurement.[10]
We used here hard board for making the disk because of its light weight. Another reason for
using of hard board’s disk is its ease of cleaning as after every deposition of fluid some fluid may
be shown there on the disk.
10 | P a g e
3.3 Specification of Materials/Equipment
As we said that we used here Tin for making the outer covering of body. So the
specification/Size of the Tin part was as given below:
We used 2 Parts of Tin here both are of same size 23” * 9” & after that we gave them a design as
shown below here:
Below shown is the front view of the outer cabinet:
FIG 3.1 Front View of outer cabinet
Another important equipment used here is motor. Which plays a very important role is working
of project. Specification of motor is as given below:
Basically we need here a motor which is having very high speed as well as that speed can
controlled by any external means. So we used here High speed sewing machine motor here as it
has speed about 9000 revolution per minute. Which is comparatively very high than other spin
motors etc.[11]
Talking about our requirement we need a motor here which can work in between 300 to 6500
Rpm and that can be controlled by any external means like regulator etc.
11 | P a g e
Specification of Motor:
AMPS 0.5
HORSE POWER 1/12
CYCLE 50. Hz
VOLTS 220/230 V
R.P.M. 9000
FIG. 3.2 High speed sewing machine motor
We also used here a syringe of 10ml for the depositing of coating fluid in exact volume at the
centre. We fitted the syringe at the centre of the top cover.
Talking about the disk we used hard board for making the disk because of its different properties
as we explained before in the report.
We also used here pewter for making of the holding arrangement and then we assemble those
pewter with the disk which is as shown below in the figure:
12 | P a g e
FIG. 3.3 Front & Rear view of the Disk with Clamping arrangement
Then there are some other things which we use here in the making of our projects are as follows:
A shaft of Dia. 6 mm
2 nos. pulley of Internal Dia. 6mm
1 plastic pot with cover for top cover
Some screw bolts etc.
3.4 Modeling of spin coater
As already spin coating has been continuously used in the different industry long before, hardly
even a single theoretical study has been initiated. An exact theory of spin coating would allow
better understanding of design and control of the process in its various applications. Several
years of industrial production operations have shown that the depositions of thin films, which
constitute the main utilization of the spin coating process, are quasi perfectly controlled.
However, any progress in developing mathematical models should be probably more helpful in
the case of heat resistant dielectric insulating films (polyamides or other materials).[12]
13 | P a g e
FIG. 3.4 Final design of spin coater
3.4.1 Key stages of spin coating
The operation of spin coating can be effectively modeled by dividing the whole process into four
stages sketched in Figure 10, which are deposition, spin-up (increase in rpm), spin-off (decrease
in rpm) and evaporation of solvents. The first three are commonly sequential, but spin-off and
evaporation usually overlap. Stage 3 and stage 4 are the two stages that have the most impact on
final coating thickness.
Deposition:
During the first stage, solution is provided to fall on rotating substrates from syringes and the
substrate is accelerated to the desired speed. Spreading of the solution takes place due to
centrifugal force and height is reduced to critical height. This is the stage of delivering an excess
14 | P a g e
of the liquid to be coated to the surface of the substrate a portion of which’s immediately covered
or “wetted”.
FIG. 3.5 Key stages of spin coating process[13]
Spin-up:
The second stage is when the substrate is accelerated up to its final, desired, rotation speed. This
stage is usually characterized by aggressive fluid expulsion from the wafer surface by the
rotational motion. Because of the initial depth of fluid on the wafer surface, spiral vortices may
briefly be present during this stage; these would form as a result of the twisting motion caused by
the inertia that the top of the fluid layer exerts while the wafer below rotates faster and faster.
Eventually, the fluid is thin enough to be completely co-rotating with the wafer and any evidence
of fluid thickness differences is gone. Ultimately, the wafer reaches its desired speed and the
fluid is thin enough that the viscous shear drag exactly balances the rotational accelerations.[14]
15 | P a g e
Stable fluid outflow:
This stage is also known as spin down process in which the speed of rotating of disk will get
decrease slowly. The third stage is when the substrate is spinning at a constant rate and fluid
viscous forces dominate fluid thinning behavior. This stage is characterized by gradual fluid
thinning.
Evaporation:
When spin-off stage ends the film drying stage begins. During this stage centrifugal out flow
stops and further shrinkage is due to solvent loss. This results in the formation of thin film on the
substrate. The fourth stage is when the substrate is spinning at a constant rate and solvent
evaporation dominates the coating thinning behavior. In this, the rate of evaporation depends on
two factors (a) the difference in partial pressure (actually chemical potential) of each solvent
species between the free surface of the liquid layer and the bulk of the gas flowing nearby.
During the evaporation stage the suspended or dissolved solids may grow so concentrated at the
liquid surface as to form a high viscosity, low diffusivity layer or solid skin.[15]
16 | P a g e
3.5 Cost Analysis
Cost analysis is the portion where we will discuss about the cost of different used products,
materials as well as cost of the equipments etc.
The cost of every product/material/equipments is as shown below in the table:
TABLE:
Materials/Equipments
Names
Cost
Motor 1300
Tin for outer covering 700
Plastic pot 130
Syringe 10
Disk 200
Clamp 100
Shaft 50
Belt 10
Screw Bolts 50
Wires 20
Regulator 25
Plugs 25
Pulley 200
Welding Charges 200
TOTAL COST 3000
TABLE 3.1 Cost analysis
17 | P a g e
CHAPTER 04
RESULT & DISCUSSION
4.1 Introduction
Here, we will discuss about different factors which affects coating as well as we will perform our
experiment and will put the result here. We will also discuss here the troubleshooting of spin
coating process.
4.2 Result
We perform on our project by taking a glass lid and the coating solution is the mixture of color
and water. Fill that solution in syringe and place the glass lid on disk and tighten by the clamps.
Place the top cover on its position.
After that start the machine and control the speed of motor with the help of the regulator. The
speed should be about 300 rpm at the time of starting the at the same speed press the syringe so
that deposition of the coating fluid can be occurs at the centre of glass lid.
Then slowly increase the speed of motor up to 6500 rpm. This is the second process of spin
coating leave as it is for 60 seconds and then slowly decreases the speed and bring it to around
1000 rpm so that evaporation can be occurs.
As we said before we perform a demonstration and what we got is as shown below:
FIG. 4.1 First experiment
18 | P a g e
4.2.1 Graph between film thickness Vs spin time
There are several factors which affect the thickness of film. Basic Initial conditions that can be
recommended for a good film deposition are the following:

1) The spinning disk should be perfectly leveled horizontally.
2) The deposited solution should wet the substrate.
3) The substrate must be clean and free from any kind of dust particles.
4) The solution should be homogeneous and uniform.
The relationship of film thickness with spinning time is as shown in graph below:
GRAPH 4.1 Relationship between film thickness and spinning time
So here above is the graph showing the relationship between film thicknesses Vs. spinning time
As its shown here by increasing the spin time we can reduce the thickness of film.
4.2.2 Graph between film thickness Vs spin speed
Another factor which affects the film thickness is spin speed. So the relationship between film
thickness and spin speed is as shown in graph below:
We can get from the below graph that we can reduce the film thickness by increase in spin speed.
19 | P a g e
GRAPH 4.2 Relationship Between film thickness and spin speed
There are several methods for the thin film deposition. Among all the advantages of spin-coating
methods are: available equipments, no time-consuming delays, fast operating and low cost. The
important factors are:
• Fluid viscosity.
• Solution concentration
• Angular speed.
• Spin Time.
• Evaporation rate of solvent.
Applications: In insulating layers for microcircuit fabrication (like: polymers, SOG), microcircuit
production, flat screen display coatings, antireflection coatings, in dielectric application and
microelectronic industries for the fabrication of integrated circuits.
4.3 Spin coating troubleshooting process
As already explained, there are number of major factors which affect the coating process. Some
of them are these as follows spin speed, acceleration, spin time and exhaust. Following is a list of
issues to consider for specific process problems.
20 | P a g e
Film too thin
Reason Solution
Spin speed too high Select lower speed
Spin time too long Decrease time during high speed step
TABLE 4.1 Troubleshooting
Film too thick
Spin speed too low Select higher speed
Spin time too short Increase time during high speed step
TABLE 4.2 Troubleshooting
Air bubbles on wafer surface
1) Air bubbles in dispensed fluid (resin)
2) Dispense tip is cut unevenly or has burrs or defects
Comets, streaks, or flares
1) Fluid velocity (dispense rate) is too high
2) Spin bowl exhaust rate is too high
3) Resist sits on wafer too long prior to spin
4) Spin speed and acceleration setting is too high
5) Particles exist on substrate surface prior to dispense
6) Fluid is not being dispensed at the center of the substrate surface
Swirl pattern
1) Spin bowl exhaust rate is too high
2) Fluid is striking substrate surface off center
3) Spin speed and acceleration setting is too high
4) Spin time too short
21 | P a g e
CHAPTER 05
Conclusion & Future scope
5.1 Conclusion
A cost effective spin-coater was successfully designed and fabricated. The total system is very
simple. Spin coaters are ideal tools for the preparation of thin films. In this work, thin films are
successfully prepared by spin-coating method. This spin coater can also be used for film
deposition of different types of precursor solution.
From this review we conclude that one can understand the basic physics behind the spin coating
process. And establish the relationship between film thickness Vs. time and speed.
.
5.1.1 Advantages
As evidenced by its maturity, spin coating has many advantages in coating operations with its
biggest advantage being the absence of coupled process variables. Film thickness is easily
changed by changing spin speed, or switching to a different viscosity photo resist. But among the
alternative coating techniques, many have multiple coupled parameters, making coating control
more complex. Another advantage of spin coating is the ability of the film to get progressively
more uniform as it thins, and if the film ever becomes completely uniform during the coating
process, it will remain so for the duration of the process. It is low cost and fast operating system.
The maturity of spin coating implies many of the issues involved in spin coating have been
studied and a lot of information exists on the subject.
5.1.2 Disadvantages
The disadvantages of spin coating are few, but they are becoming more important as substrate
size increases and photo resist costs rise. Large substrates cannot be spun at a sufficiently high
rate in order to allow the film to thin. The biggest disadvantage of spin coating is its lack of
material efficiency. Typical spin coating processes utilize only 2–5% of the material dispensed
22 | P a g e
onto the substrate, while the remaining 95–98% is flung off in to the coating bowl and disposed.
Not only are the prices of the photo resist increasing substantially, but disposal costs increasing
as well. If economically feasible manufacturing costs are to be maintained, a method for
improving this material utilization is of primary importance, especially in the flat panel display
area.
5.2 Future scope
By including microprocessor in the main circuit we can include the auto on/off system. We also
can add a digital display to know the speed, time and other necessary readings.
23 | P a g e
REFERENCE
[1] A G Emsile, F T Bonner and L G Peek J. Appl. Phys. 29 858 (1958)
[2] D Meyerhofer J. Appl. Phys. A9 3993 (1978)
[3] D E Bornside, C W Macosko et al, J. Imaging Tech. 13 122 (1987)
[4] R K Yonkoski and D S Soane J. Appl. Phys. 72 725 (1992)
[5] C J Lawrence and W Zhou Journal of Non-Newtonian Fluid Mechanics 39 137 (1991)
[6] S Middleman An Introduction to Fluid Dynamics (New York : John Wiley and Sons) (1998)
[7] O Omar, A K Ray, A K Hassan and F Davis Supramolecular Science 4 417 (1997)
[8] W W Flack, D S Soong, A T Bell and D W Hess J. Appl. Phys. 56 1199 (1983)
[9] http://www.cise.columbia.edu/clean/process/spintheory.pdf
[10] http://www.mse.arizona.edu/faculty/birnie/Coatings
[11] Ohring, M. (1992), ‘The Materials Science of Thin Films’, Academic Press limited, 24-28
Oval Road, London, NW1, 7DX, UK, pp. XIII. Moshfegh, A. Z. Känel, H.V., Kashyap, S.C.,
and Wuttig, M. (2003), ‘Proceedings of the International Workshop on Physics And Technology
Of Thin Films’, World Scientific Publishing Co. Pvt Ltd. 5 Toh Tuck Link, Singapore, 596224
Tehran, Iran, pp. IX.
[12] Seshan, K. (2002), ‘Handbook of thin-film Deposition processes and techniques: Principles,
Methods, Equipment and Applications’, 2nd ed, Norwich, New York, U.S.A.: Noyes
publications, William andrew publishing.
24 | P a g e
[13] Aguilar, R.G., and López, J.O. (2011), ‘Low cost instrumentation for spin-coating
deposition of thin films in an undergraduate laboratory’, Latin American Journal of Physics
Education, 5 (2), 368-373.
[14] Smirnov, M.A., Rambu, P., Baban, C., and Rusu, G.I. (2010), ‘Electronic Transport
Properties in Polycrystalline ZnO Thin Films’, Journal of Advanced Research in Physics, 1 (2),
021011.
[15] Sevvanthi, P. Claude, A., Jayanthi, C., and Poiyamozhi, A. (2012), ‘Instrumentation for
fabricating an indigenous spin coating apparatus and growth of zinc oxide thin films and their
characterizations’, Advances in Applied Science Research, 3 (6), 3573-3580.

More Related Content

What's hot

Lithography and Nanolithography
Lithography and NanolithographyLithography and Nanolithography
Lithography and NanolithographySaheem Anwar
 
06.presentation on coating methods
06.presentation on coating methods06.presentation on coating methods
06.presentation on coating methodsSHRIKANT ATHAVALE
 
Mechanism of graphene growth by chemical vapour deposition on transition metals
Mechanism of graphene growth by chemical vapour deposition on transition metals Mechanism of graphene growth by chemical vapour deposition on transition metals
Mechanism of graphene growth by chemical vapour deposition on transition metals Ramachandra SN
 
Materials Characterization Technique Lecture Notes
Materials Characterization Technique Lecture NotesMaterials Characterization Technique Lecture Notes
Materials Characterization Technique Lecture NotesFellowBuddy.com
 
Sol gel coating
Sol gel coatingSol gel coating
Sol gel coatingengrktk
 
Surface modification
Surface modificationSurface modification
Surface modificationtranslateds
 
Cvd & pvd by shreya
Cvd & pvd by shreyaCvd & pvd by shreya
Cvd & pvd by shreyaShreya Modi
 
Vapor deposition (CVD & PVD) on tools
Vapor deposition (CVD & PVD) on toolsVapor deposition (CVD & PVD) on tools
Vapor deposition (CVD & PVD) on toolsMuhammad Umair Akram
 
Thin film deposition using spray pyrolysis
Thin film deposition using spray pyrolysisThin film deposition using spray pyrolysis
Thin film deposition using spray pyrolysisMUHAMMAD AADIL
 
Superhydrophobic materials
Superhydrophobic materialsSuperhydrophobic materials
Superhydrophobic materialsAnis Syed
 
Pulse laser depostion of thin film
Pulse laser depostion of thin filmPulse laser depostion of thin film
Pulse laser depostion of thin filmAbdalla Darwish
 
Chemical vapour deposition
Chemical vapour depositionChemical vapour deposition
Chemical vapour depositionSethu Ram
 

What's hot (20)

Photoresist coating
Photoresist coating Photoresist coating
Photoresist coating
 
Lithography and Nanolithography
Lithography and NanolithographyLithography and Nanolithography
Lithography and Nanolithography
 
Rani
RaniRani
Rani
 
06.presentation on coating methods
06.presentation on coating methods06.presentation on coating methods
06.presentation on coating methods
 
Mechanism of graphene growth by chemical vapour deposition on transition metals
Mechanism of graphene growth by chemical vapour deposition on transition metals Mechanism of graphene growth by chemical vapour deposition on transition metals
Mechanism of graphene growth by chemical vapour deposition on transition metals
 
Ch15
Ch15Ch15
Ch15
 
Etching
EtchingEtching
Etching
 
Materials Characterization Technique Lecture Notes
Materials Characterization Technique Lecture NotesMaterials Characterization Technique Lecture Notes
Materials Characterization Technique Lecture Notes
 
Sol gel coating
Sol gel coatingSol gel coating
Sol gel coating
 
Surface modification
Surface modificationSurface modification
Surface modification
 
Surface engineering
Surface engineeringSurface engineering
Surface engineering
 
Cvd & pvd by shreya
Cvd & pvd by shreyaCvd & pvd by shreya
Cvd & pvd by shreya
 
Ion implantation
Ion implantationIon implantation
Ion implantation
 
Epitaxy
EpitaxyEpitaxy
Epitaxy
 
Vapor deposition (CVD & PVD) on tools
Vapor deposition (CVD & PVD) on toolsVapor deposition (CVD & PVD) on tools
Vapor deposition (CVD & PVD) on tools
 
Sputtering process
Sputtering processSputtering process
Sputtering process
 
Thin film deposition using spray pyrolysis
Thin film deposition using spray pyrolysisThin film deposition using spray pyrolysis
Thin film deposition using spray pyrolysis
 
Superhydrophobic materials
Superhydrophobic materialsSuperhydrophobic materials
Superhydrophobic materials
 
Pulse laser depostion of thin film
Pulse laser depostion of thin filmPulse laser depostion of thin film
Pulse laser depostion of thin film
 
Chemical vapour deposition
Chemical vapour depositionChemical vapour deposition
Chemical vapour deposition
 

Viewers also liked

HHV Thin Films & Optics
HHV  Thin Films & OpticsHHV  Thin Films & Optics
HHV Thin Films & OpticsSuman
 
Presentation1
Presentation1Presentation1
Presentation1Rahul Das
 
Thin films in nano particles
Thin films in nano particlesThin films in nano particles
Thin films in nano particlesN.MANI KANDAN
 
Fabrication of abrasive belt grinder saravanan
Fabrication of abrasive belt grinder   saravananFabrication of abrasive belt grinder   saravanan
Fabrication of abrasive belt grinder saravanandinnusara
 
Foldable walker final project for Application in Mechanical Engineering
Foldable walker final project for Application in Mechanical Engineering Foldable walker final project for Application in Mechanical Engineering
Foldable walker final project for Application in Mechanical Engineering Jordan Tractor and Equipment Co.
 
DESIGN & FABRICATION OF FOUR WHEEL STEERED MULTI- UTILITY VEHICLE
DESIGN & FABRICATION OF FOUR WHEEL  STEERED MULTI- UTILITY VEHICLEDESIGN & FABRICATION OF FOUR WHEEL  STEERED MULTI- UTILITY VEHICLE
DESIGN & FABRICATION OF FOUR WHEEL STEERED MULTI- UTILITY VEHICLEDelwin CK
 
Design and fabrication of working model of abrasive jet machine
Design and fabrication of working model of abrasive jet machineDesign and fabrication of working model of abrasive jet machine
Design and fabrication of working model of abrasive jet machineNirmaljit Singh
 
Fire fighting robot remotely operated
Fire fighting robot remotely operatedFire fighting robot remotely operated
Fire fighting robot remotely operatedMohit Keshav
 
Automatic high speed bottle washing machine project mechanical engineering ...
Automatic high speed bottle washing machine project   mechanical engineering ...Automatic high speed bottle washing machine project   mechanical engineering ...
Automatic high speed bottle washing machine project mechanical engineering ...vasanth ravi
 
Pedal Powered Water Pump
Pedal Powered Water PumpPedal Powered Water Pump
Pedal Powered Water PumpNEERAJ KUMAR
 
Pneumatic Sheet Metal Shearing Machine - Project report
Pneumatic Sheet Metal Shearing Machine - Project reportPneumatic Sheet Metal Shearing Machine - Project report
Pneumatic Sheet Metal Shearing Machine - Project reportTejas Inamdar
 
Thin_Film_Technology_introduction[1]
Thin_Film_Technology_introduction[1]Thin_Film_Technology_introduction[1]
Thin_Film_Technology_introduction[1]Milan Van Bree
 
Mechanical Engineering project
Mechanical Engineering projectMechanical Engineering project
Mechanical Engineering projectManpreet Singh
 
CVD AND PVD THIN FILM TECHNIQUES
CVD AND PVD THIN FILM TECHNIQUESCVD AND PVD THIN FILM TECHNIQUES
CVD AND PVD THIN FILM TECHNIQUESHHV SOLAR Pvt Ltd
 
Fabrication of Automatic Guided Vehicle
Fabrication of Automatic Guided Vehicle Fabrication of Automatic Guided Vehicle
Fabrication of Automatic Guided Vehicle Ajith Aravind
 
Slideshare Powerpoint presentation
Slideshare Powerpoint presentationSlideshare Powerpoint presentation
Slideshare Powerpoint presentationelliehood
 

Viewers also liked (19)

HHV Thin Films & Optics
HHV  Thin Films & OpticsHHV  Thin Films & Optics
HHV Thin Films & Optics
 
Thin film coating
Thin film coatingThin film coating
Thin film coating
 
Presentation1
Presentation1Presentation1
Presentation1
 
Thin films in nano particles
Thin films in nano particlesThin films in nano particles
Thin films in nano particles
 
Fabrication of abrasive belt grinder saravanan
Fabrication of abrasive belt grinder   saravananFabrication of abrasive belt grinder   saravanan
Fabrication of abrasive belt grinder saravanan
 
Foldable walker final project for Application in Mechanical Engineering
Foldable walker final project for Application in Mechanical Engineering Foldable walker final project for Application in Mechanical Engineering
Foldable walker final project for Application in Mechanical Engineering
 
Thin films
Thin films Thin films
Thin films
 
DESIGN & FABRICATION OF FOUR WHEEL STEERED MULTI- UTILITY VEHICLE
DESIGN & FABRICATION OF FOUR WHEEL  STEERED MULTI- UTILITY VEHICLEDESIGN & FABRICATION OF FOUR WHEEL  STEERED MULTI- UTILITY VEHICLE
DESIGN & FABRICATION OF FOUR WHEEL STEERED MULTI- UTILITY VEHICLE
 
Design and fabrication of working model of abrasive jet machine
Design and fabrication of working model of abrasive jet machineDesign and fabrication of working model of abrasive jet machine
Design and fabrication of working model of abrasive jet machine
 
Fire fighting robot remotely operated
Fire fighting robot remotely operatedFire fighting robot remotely operated
Fire fighting robot remotely operated
 
Automatic high speed bottle washing machine project mechanical engineering ...
Automatic high speed bottle washing machine project   mechanical engineering ...Automatic high speed bottle washing machine project   mechanical engineering ...
Automatic high speed bottle washing machine project mechanical engineering ...
 
Pedal Powered Water Pump
Pedal Powered Water PumpPedal Powered Water Pump
Pedal Powered Water Pump
 
Pneumatic Sheet Metal Shearing Machine - Project report
Pneumatic Sheet Metal Shearing Machine - Project reportPneumatic Sheet Metal Shearing Machine - Project report
Pneumatic Sheet Metal Shearing Machine - Project report
 
Thin_Film_Technology_introduction[1]
Thin_Film_Technology_introduction[1]Thin_Film_Technology_introduction[1]
Thin_Film_Technology_introduction[1]
 
Mechanical Engineering project
Mechanical Engineering projectMechanical Engineering project
Mechanical Engineering project
 
Thin films
Thin filmsThin films
Thin films
 
CVD AND PVD THIN FILM TECHNIQUES
CVD AND PVD THIN FILM TECHNIQUESCVD AND PVD THIN FILM TECHNIQUES
CVD AND PVD THIN FILM TECHNIQUES
 
Fabrication of Automatic Guided Vehicle
Fabrication of Automatic Guided Vehicle Fabrication of Automatic Guided Vehicle
Fabrication of Automatic Guided Vehicle
 
Slideshare Powerpoint presentation
Slideshare Powerpoint presentationSlideshare Powerpoint presentation
Slideshare Powerpoint presentation
 

Similar to Design & Fabrication of a low cost spin coater

simulation and experimentation in feeder design_secure
simulation and experimentation in feeder   design_securesimulation and experimentation in feeder   design_secure
simulation and experimentation in feeder design_secureDhaval Sukhadia
 
Pile Design Using Wave Equation Analysis Program Application in Offshore Wind...
Pile Design Using Wave Equation Analysis Program Application in Offshore Wind...Pile Design Using Wave Equation Analysis Program Application in Offshore Wind...
Pile Design Using Wave Equation Analysis Program Application in Offshore Wind...khucmai
 
IRJET- Analytical Study of Solid Slab with Different Types of Cavity
IRJET- Analytical Study of Solid Slab with Different Types of CavityIRJET- Analytical Study of Solid Slab with Different Types of Cavity
IRJET- Analytical Study of Solid Slab with Different Types of CavityIRJET Journal
 
IRJET- Systematic Prevention and Repair of Potholes in Flexible Pavement
IRJET- Systematic Prevention and Repair of Potholes in Flexible PavementIRJET- Systematic Prevention and Repair of Potholes in Flexible Pavement
IRJET- Systematic Prevention and Repair of Potholes in Flexible PavementIRJET Journal
 
Anis rahman khokan's internship paper
Anis rahman khokan's internship paperAnis rahman khokan's internship paper
Anis rahman khokan's internship paperAnis Rahman Khokan
 
38785106 api-tank-design
38785106 api-tank-design38785106 api-tank-design
38785106 api-tank-design141jdf
 
FINAL YEAR PROJECT REPORT RANSA.0.pptx
FINAL YEAR PROJECT REPORT RANSA.0.pptxFINAL YEAR PROJECT REPORT RANSA.0.pptx
FINAL YEAR PROJECT REPORT RANSA.0.pptxRahulLodha11
 
A Project Report.pdf
A Project Report.pdfA Project Report.pdf
A Project Report.pdfRajKirar2
 
RESIDENTIAL CONSTRUCTION BUILDING
RESIDENTIAL CONSTRUCTION BUILDING RESIDENTIAL CONSTRUCTION BUILDING
RESIDENTIAL CONSTRUCTION BUILDING Vikas Sukhwal
 
General Estimation & Abstract Sheet of Royal City
General Estimation & Abstract Sheet of Royal CityGeneral Estimation & Abstract Sheet of Royal City
General Estimation & Abstract Sheet of Royal CityIRJET Journal
 
Product Development for Future using Rapid Prototyping Techniques
Product Development for Future using Rapid Prototyping TechniquesProduct Development for Future using Rapid Prototyping Techniques
Product Development for Future using Rapid Prototyping TechniquesIRJET Journal
 
Bps 5205 sustainability construction and maintainability velpandi & maria
Bps 5205  sustainability construction and maintainability  velpandi & mariaBps 5205  sustainability construction and maintainability  velpandi & maria
Bps 5205 sustainability construction and maintainability velpandi & mariaMaria Archana
 
SUMMER TRAINING REPORT BY VIJAY VERMA
SUMMER TRAINING REPORT BY VIJAY VERMASUMMER TRAINING REPORT BY VIJAY VERMA
SUMMER TRAINING REPORT BY VIJAY VERMAvjverma123
 
IRJET- Design and Fabrication of Manual Roller Bending Machine
IRJET-  	  Design and Fabrication of Manual Roller Bending MachineIRJET-  	  Design and Fabrication of Manual Roller Bending Machine
IRJET- Design and Fabrication of Manual Roller Bending MachineIRJET Journal
 
IRJET- Systematic Prevention and Repair of Potholes in Flexible Pavement
IRJET- Systematic Prevention and Repair of Potholes in Flexible PavementIRJET- Systematic Prevention and Repair of Potholes in Flexible Pavement
IRJET- Systematic Prevention and Repair of Potholes in Flexible PavementIRJET Journal
 
design engineering 2B report
design engineering 2B reportdesign engineering 2B report
design engineering 2B reporttirath prajapati
 
Vibration Table For Welding
Vibration Table For WeldingVibration Table For Welding
Vibration Table For WeldingHardik Solanki
 

Similar to Design & Fabrication of a low cost spin coater (20)

simulation and experimentation in feeder design_secure
simulation and experimentation in feeder   design_securesimulation and experimentation in feeder   design_secure
simulation and experimentation in feeder design_secure
 
Pile Design Using Wave Equation Analysis Program Application in Offshore Wind...
Pile Design Using Wave Equation Analysis Program Application in Offshore Wind...Pile Design Using Wave Equation Analysis Program Application in Offshore Wind...
Pile Design Using Wave Equation Analysis Program Application in Offshore Wind...
 
IRJET- Analytical Study of Solid Slab with Different Types of Cavity
IRJET- Analytical Study of Solid Slab with Different Types of CavityIRJET- Analytical Study of Solid Slab with Different Types of Cavity
IRJET- Analytical Study of Solid Slab with Different Types of Cavity
 
IRJET- Systematic Prevention and Repair of Potholes in Flexible Pavement
IRJET- Systematic Prevention and Repair of Potholes in Flexible PavementIRJET- Systematic Prevention and Repair of Potholes in Flexible Pavement
IRJET- Systematic Prevention and Repair of Potholes in Flexible Pavement
 
Anis rahman khokan's internship paper
Anis rahman khokan's internship paperAnis rahman khokan's internship paper
Anis rahman khokan's internship paper
 
38785106 api-tank-design
38785106 api-tank-design38785106 api-tank-design
38785106 api-tank-design
 
Final report
Final reportFinal report
Final report
 
FINAL YEAR PROJECT REPORT RANSA.0.pptx
FINAL YEAR PROJECT REPORT RANSA.0.pptxFINAL YEAR PROJECT REPORT RANSA.0.pptx
FINAL YEAR PROJECT REPORT RANSA.0.pptx
 
Siddharth Srivastava
Siddharth SrivastavaSiddharth Srivastava
Siddharth Srivastava
 
A Project Report.pdf
A Project Report.pdfA Project Report.pdf
A Project Report.pdf
 
RESIDENTIAL CONSTRUCTION BUILDING
RESIDENTIAL CONSTRUCTION BUILDING RESIDENTIAL CONSTRUCTION BUILDING
RESIDENTIAL CONSTRUCTION BUILDING
 
General Estimation & Abstract Sheet of Royal City
General Estimation & Abstract Sheet of Royal CityGeneral Estimation & Abstract Sheet of Royal City
General Estimation & Abstract Sheet of Royal City
 
Product Development for Future using Rapid Prototyping Techniques
Product Development for Future using Rapid Prototyping TechniquesProduct Development for Future using Rapid Prototyping Techniques
Product Development for Future using Rapid Prototyping Techniques
 
Bps 5205 sustainability construction and maintainability velpandi & maria
Bps 5205  sustainability construction and maintainability  velpandi & mariaBps 5205  sustainability construction and maintainability  velpandi & maria
Bps 5205 sustainability construction and maintainability velpandi & maria
 
SUMMER TRAINING REPORT BY VIJAY VERMA
SUMMER TRAINING REPORT BY VIJAY VERMASUMMER TRAINING REPORT BY VIJAY VERMA
SUMMER TRAINING REPORT BY VIJAY VERMA
 
IRJET- Design and Fabrication of Manual Roller Bending Machine
IRJET-  	  Design and Fabrication of Manual Roller Bending MachineIRJET-  	  Design and Fabrication of Manual Roller Bending Machine
IRJET- Design and Fabrication of Manual Roller Bending Machine
 
IRJET- Systematic Prevention and Repair of Potholes in Flexible Pavement
IRJET- Systematic Prevention and Repair of Potholes in Flexible PavementIRJET- Systematic Prevention and Repair of Potholes in Flexible Pavement
IRJET- Systematic Prevention and Repair of Potholes in Flexible Pavement
 
design engineering 2B report
design engineering 2B reportdesign engineering 2B report
design engineering 2B report
 
Vibration Table For Welding
Vibration Table For WeldingVibration Table For Welding
Vibration Table For Welding
 
THESIS FOR MAIL
THESIS FOR MAILTHESIS FOR MAIL
THESIS FOR MAIL
 

Recently uploaded

Revit Understanding Reference Planes and Reference lines in Revit for Family ...
Revit Understanding Reference Planes and Reference lines in Revit for Family ...Revit Understanding Reference Planes and Reference lines in Revit for Family ...
Revit Understanding Reference Planes and Reference lines in Revit for Family ...Narsimha murthy
 
CALL ON ➥8923113531 🔝Call Girls Aminabad Lucknow best Night Fun service
CALL ON ➥8923113531 🔝Call Girls Aminabad Lucknow best Night Fun serviceCALL ON ➥8923113531 🔝Call Girls Aminabad Lucknow best Night Fun service
CALL ON ➥8923113531 🔝Call Girls Aminabad Lucknow best Night Fun serviceanilsa9823
 
A level Digipak development Presentation
A level Digipak development PresentationA level Digipak development Presentation
A level Digipak development Presentationamedia6
 
The history of music videos a level presentation
The history of music videos a level presentationThe history of music videos a level presentation
The history of music videos a level presentationamedia6
 
Kala jadu for love marriage | Real amil baba | Famous amil baba | kala jadu n...
Kala jadu for love marriage | Real amil baba | Famous amil baba | kala jadu n...Kala jadu for love marriage | Real amil baba | Famous amil baba | kala jadu n...
Kala jadu for love marriage | Real amil baba | Famous amil baba | kala jadu n...babafaisel
 
NO1 Famous Amil Baba In Karachi Kala Jadu In Karachi Amil baba In Karachi Add...
NO1 Famous Amil Baba In Karachi Kala Jadu In Karachi Amil baba In Karachi Add...NO1 Famous Amil Baba In Karachi Kala Jadu In Karachi Amil baba In Karachi Add...
NO1 Famous Amil Baba In Karachi Kala Jadu In Karachi Amil baba In Karachi Add...Amil baba
 
如何办理(UVa毕业证书)弗吉尼亚大学毕业证毕业证(文凭)成绩单原版一比一定制
如何办理(UVa毕业证书)弗吉尼亚大学毕业证毕业证(文凭)成绩单原版一比一定制如何办理(UVa毕业证书)弗吉尼亚大学毕业证毕业证(文凭)成绩单原版一比一定制
如何办理(UVa毕业证书)弗吉尼亚大学毕业证毕业证(文凭)成绩单原版一比一定制didi bibo
 
Captivating Charm: Exploring Marseille's Hillside Villas with Our 3D Architec...
Captivating Charm: Exploring Marseille's Hillside Villas with Our 3D Architec...Captivating Charm: Exploring Marseille's Hillside Villas with Our 3D Architec...
Captivating Charm: Exploring Marseille's Hillside Villas with Our 3D Architec...Yantram Animation Studio Corporation
 
Call Girls In Safdarjung Enclave 24/7✡️9711147426✡️ Escorts Service
Call Girls In Safdarjung Enclave 24/7✡️9711147426✡️ Escorts ServiceCall Girls In Safdarjung Enclave 24/7✡️9711147426✡️ Escorts Service
Call Girls In Safdarjung Enclave 24/7✡️9711147426✡️ Escorts Servicejennyeacort
 
VVIP Pune Call Girls Hadapsar (7001035870) Pune Escorts Nearby with Complete ...
VVIP Pune Call Girls Hadapsar (7001035870) Pune Escorts Nearby with Complete ...VVIP Pune Call Girls Hadapsar (7001035870) Pune Escorts Nearby with Complete ...
VVIP Pune Call Girls Hadapsar (7001035870) Pune Escorts Nearby with Complete ...Call Girls in Nagpur High Profile
 
Dubai Call Girls Pro Domain O525547819 Call Girls Dubai Doux
Dubai Call Girls Pro Domain O525547819 Call Girls Dubai DouxDubai Call Girls Pro Domain O525547819 Call Girls Dubai Doux
Dubai Call Girls Pro Domain O525547819 Call Girls Dubai Douxkojalkojal131
 
3D Printing And Designing Final Report.pdf
3D Printing And Designing Final Report.pdf3D Printing And Designing Final Report.pdf
3D Printing And Designing Final Report.pdfSwaraliBorhade
 
ARt app | UX Case Study
ARt app | UX Case StudyARt app | UX Case Study
ARt app | UX Case StudySophia Viganò
 
VIP College Call Girls Gorakhpur Bhavna 8250192130 Independent Escort Service...
VIP College Call Girls Gorakhpur Bhavna 8250192130 Independent Escort Service...VIP College Call Girls Gorakhpur Bhavna 8250192130 Independent Escort Service...
VIP College Call Girls Gorakhpur Bhavna 8250192130 Independent Escort Service...Suhani Kapoor
 
VIP Call Girls Service Mehdipatnam Hyderabad Call +91-8250192130
VIP Call Girls Service Mehdipatnam Hyderabad Call +91-8250192130VIP Call Girls Service Mehdipatnam Hyderabad Call +91-8250192130
VIP Call Girls Service Mehdipatnam Hyderabad Call +91-8250192130Suhani Kapoor
 
VIP Russian Call Girls in Saharanpur Deepika 8250192130 Independent Escort Se...
VIP Russian Call Girls in Saharanpur Deepika 8250192130 Independent Escort Se...VIP Russian Call Girls in Saharanpur Deepika 8250192130 Independent Escort Se...
VIP Russian Call Girls in Saharanpur Deepika 8250192130 Independent Escort Se...Suhani Kapoor
 
Raj Nagar Extension Call Girls 9711199012 WhatsApp No, Delhi Escorts in Raj N...
Raj Nagar Extension Call Girls 9711199012 WhatsApp No, Delhi Escorts in Raj N...Raj Nagar Extension Call Girls 9711199012 WhatsApp No, Delhi Escorts in Raj N...
Raj Nagar Extension Call Girls 9711199012 WhatsApp No, Delhi Escorts in Raj N...ankitnayak356677
 
Abu Dhabi Call Girls O58993O4O2 Call Girls in Abu Dhabi`
Abu Dhabi Call Girls O58993O4O2 Call Girls in Abu Dhabi`Abu Dhabi Call Girls O58993O4O2 Call Girls in Abu Dhabi`
Abu Dhabi Call Girls O58993O4O2 Call Girls in Abu Dhabi`dajasot375
 
The_Canvas_of_Creative_Mastery_Newsletter_April_2024_Version.pdf
The_Canvas_of_Creative_Mastery_Newsletter_April_2024_Version.pdfThe_Canvas_of_Creative_Mastery_Newsletter_April_2024_Version.pdf
The_Canvas_of_Creative_Mastery_Newsletter_April_2024_Version.pdfAmirYakdi
 

Recently uploaded (20)

Revit Understanding Reference Planes and Reference lines in Revit for Family ...
Revit Understanding Reference Planes and Reference lines in Revit for Family ...Revit Understanding Reference Planes and Reference lines in Revit for Family ...
Revit Understanding Reference Planes and Reference lines in Revit for Family ...
 
CALL ON ➥8923113531 🔝Call Girls Aminabad Lucknow best Night Fun service
CALL ON ➥8923113531 🔝Call Girls Aminabad Lucknow best Night Fun serviceCALL ON ➥8923113531 🔝Call Girls Aminabad Lucknow best Night Fun service
CALL ON ➥8923113531 🔝Call Girls Aminabad Lucknow best Night Fun service
 
A level Digipak development Presentation
A level Digipak development PresentationA level Digipak development Presentation
A level Digipak development Presentation
 
The history of music videos a level presentation
The history of music videos a level presentationThe history of music videos a level presentation
The history of music videos a level presentation
 
Kala jadu for love marriage | Real amil baba | Famous amil baba | kala jadu n...
Kala jadu for love marriage | Real amil baba | Famous amil baba | kala jadu n...Kala jadu for love marriage | Real amil baba | Famous amil baba | kala jadu n...
Kala jadu for love marriage | Real amil baba | Famous amil baba | kala jadu n...
 
NO1 Famous Amil Baba In Karachi Kala Jadu In Karachi Amil baba In Karachi Add...
NO1 Famous Amil Baba In Karachi Kala Jadu In Karachi Amil baba In Karachi Add...NO1 Famous Amil Baba In Karachi Kala Jadu In Karachi Amil baba In Karachi Add...
NO1 Famous Amil Baba In Karachi Kala Jadu In Karachi Amil baba In Karachi Add...
 
如何办理(UVa毕业证书)弗吉尼亚大学毕业证毕业证(文凭)成绩单原版一比一定制
如何办理(UVa毕业证书)弗吉尼亚大学毕业证毕业证(文凭)成绩单原版一比一定制如何办理(UVa毕业证书)弗吉尼亚大学毕业证毕业证(文凭)成绩单原版一比一定制
如何办理(UVa毕业证书)弗吉尼亚大学毕业证毕业证(文凭)成绩单原版一比一定制
 
Captivating Charm: Exploring Marseille's Hillside Villas with Our 3D Architec...
Captivating Charm: Exploring Marseille's Hillside Villas with Our 3D Architec...Captivating Charm: Exploring Marseille's Hillside Villas with Our 3D Architec...
Captivating Charm: Exploring Marseille's Hillside Villas with Our 3D Architec...
 
Call Girls In Safdarjung Enclave 24/7✡️9711147426✡️ Escorts Service
Call Girls In Safdarjung Enclave 24/7✡️9711147426✡️ Escorts ServiceCall Girls In Safdarjung Enclave 24/7✡️9711147426✡️ Escorts Service
Call Girls In Safdarjung Enclave 24/7✡️9711147426✡️ Escorts Service
 
VVIP Pune Call Girls Hadapsar (7001035870) Pune Escorts Nearby with Complete ...
VVIP Pune Call Girls Hadapsar (7001035870) Pune Escorts Nearby with Complete ...VVIP Pune Call Girls Hadapsar (7001035870) Pune Escorts Nearby with Complete ...
VVIP Pune Call Girls Hadapsar (7001035870) Pune Escorts Nearby with Complete ...
 
Dubai Call Girls Pro Domain O525547819 Call Girls Dubai Doux
Dubai Call Girls Pro Domain O525547819 Call Girls Dubai DouxDubai Call Girls Pro Domain O525547819 Call Girls Dubai Doux
Dubai Call Girls Pro Domain O525547819 Call Girls Dubai Doux
 
young call girls in Vivek Vihar🔝 9953056974 🔝 Delhi escort Service
young call girls in Vivek Vihar🔝 9953056974 🔝 Delhi escort Serviceyoung call girls in Vivek Vihar🔝 9953056974 🔝 Delhi escort Service
young call girls in Vivek Vihar🔝 9953056974 🔝 Delhi escort Service
 
3D Printing And Designing Final Report.pdf
3D Printing And Designing Final Report.pdf3D Printing And Designing Final Report.pdf
3D Printing And Designing Final Report.pdf
 
ARt app | UX Case Study
ARt app | UX Case StudyARt app | UX Case Study
ARt app | UX Case Study
 
VIP College Call Girls Gorakhpur Bhavna 8250192130 Independent Escort Service...
VIP College Call Girls Gorakhpur Bhavna 8250192130 Independent Escort Service...VIP College Call Girls Gorakhpur Bhavna 8250192130 Independent Escort Service...
VIP College Call Girls Gorakhpur Bhavna 8250192130 Independent Escort Service...
 
VIP Call Girls Service Mehdipatnam Hyderabad Call +91-8250192130
VIP Call Girls Service Mehdipatnam Hyderabad Call +91-8250192130VIP Call Girls Service Mehdipatnam Hyderabad Call +91-8250192130
VIP Call Girls Service Mehdipatnam Hyderabad Call +91-8250192130
 
VIP Russian Call Girls in Saharanpur Deepika 8250192130 Independent Escort Se...
VIP Russian Call Girls in Saharanpur Deepika 8250192130 Independent Escort Se...VIP Russian Call Girls in Saharanpur Deepika 8250192130 Independent Escort Se...
VIP Russian Call Girls in Saharanpur Deepika 8250192130 Independent Escort Se...
 
Raj Nagar Extension Call Girls 9711199012 WhatsApp No, Delhi Escorts in Raj N...
Raj Nagar Extension Call Girls 9711199012 WhatsApp No, Delhi Escorts in Raj N...Raj Nagar Extension Call Girls 9711199012 WhatsApp No, Delhi Escorts in Raj N...
Raj Nagar Extension Call Girls 9711199012 WhatsApp No, Delhi Escorts in Raj N...
 
Abu Dhabi Call Girls O58993O4O2 Call Girls in Abu Dhabi`
Abu Dhabi Call Girls O58993O4O2 Call Girls in Abu Dhabi`Abu Dhabi Call Girls O58993O4O2 Call Girls in Abu Dhabi`
Abu Dhabi Call Girls O58993O4O2 Call Girls in Abu Dhabi`
 
The_Canvas_of_Creative_Mastery_Newsletter_April_2024_Version.pdf
The_Canvas_of_Creative_Mastery_Newsletter_April_2024_Version.pdfThe_Canvas_of_Creative_Mastery_Newsletter_April_2024_Version.pdf
The_Canvas_of_Creative_Mastery_Newsletter_April_2024_Version.pdf
 

Design & Fabrication of a low cost spin coater

  • 1. i | P a g e SCHOOL OF MECHANICAL ENGINEERING REPORT ON CAPSTON PROJECT TITLE: DESIGN & FABRICATION OF A LOW COST SPIN COATER Submitted to Lovely Professional University In partial fulfillment of the requirement for the award of “DEGREE OF BACHELOR OF TECHNOLOGY [MECHANICAL ENGINEERING]” Submitted By Name Registration No.  SAURABH PANDEY 11102793  KAPIL RAGHUWANSHI 11105326  SUDHIR YADAV 11108007  PUNEET KUMAR 11111389 Research Supervisor Mr. Sumit shoor UID. 14602 Assistant Professor School Of Mechanical Engineering
  • 2. ii | P a g e CERTIFICATE This is certified that Saurabh Pandey, Kapil Raghuwanshi, Sudhir Yadav, Puneet Kumar have complete this capstone project of – Design & Fabrication of Low Cost Spin Coater under my guidance. During this project they have done most efforts to study and understand the subject in detail. In addition to the books mentioned in the bibliography they have referred various study material, magazine, websites, research papers and notes to complete this project. During this project they have been very much curious and enthusiast to understand the spirit of the expert documentation and procedures. We wish them best of luck. Research Supervisor Mr. Sumit Shoor 14602 Asst. Professor School Of Mechanical Engg. Signature of Supervisor
  • 3. iii | P a g e DECLARATION This is to certify that we are the student of School Of Mechanical Engineering, pursuing Bachelor of Technology(Mechanical Engineering) have completed capstone project on topic “Design & Fabrication of Low Cost Spin Coater” for partial fulfillment of degree of Bachelor of Technology to Lovely professional University, Phagwara (PUNJAB).We solemnly declare that the work done by us is original and no copy of it has been submitted to Lovely Professional University or any other university for award of any other degree/fellowship. Name Registration Number Signature  Saurabh Pandey 11102793  Kapil Raghuwanshi 11105326  Sudhir Yadav 11108007  Puneet Kumar 11111389
  • 4. iv | P a g e Acknowledgement Itakethis opportunitytopresent myvotes ofthanks toallthoseguidepost whoreallyactedas lightening pillars to enlighten our way throughout this project that has led to successful and satisfactorycompletion of this study. We are really grateful to our teacher for providing us with an opportunity to undertake this project in this university and providing us with all the facilities. We are highly thankful to Mr. Sumit Shoor(Asst. Professor) for his active support, valuable time and advice, whole- hearted guidance, sincere cooperation and pains-taking involvement during the study and in completing the assignment of preparing the said project within the time stipulated. Lastly, we are thankful to all those particularly the various friends who have been instrumental in creating proper, healthy and conductive environment and including new and fresh innovative ideas for us during the project, their help, it would have been extremely difficult for us to prepare the project in a time bound framework.
  • 5. v | P a g e ABSTRACT The goal of this capstone project was designing a low cost spin coater which works economically. With the help of this spin coater we can create a thin film on the flat surface of any work piece. This process is basically follows the principle of Centrifugal Force which draws a rotating body away from the centre of rotation. The thickness of film depends on different factors which are as follows:  Concentration of the Solution  Rotational Speed  Rotation Time So these above are some factors which can affect the thickness of the film. By taking care of these above said factors we can get the desired thickness of film of any substrate. Spin Coating is a fast and easy method to generate thin and homogeneous films out of solutions.
  • 6. vi | P a g e TABLE OF CONTENTS Title Page Cover Page i Certificate ii Declaration iii Acknowledgement iv Abstract v Table of Contents vi – vii List of figures viii List of Graph ix List of Tables x CHAPTER 1 Introduction 1 - 4 1.1 Definition and brief history of Spin Coating 1 1.2 Physics of Spin Coating 2 1.3 Industrial uses of spin Coating technology 2 1.4 Common spin coating defects 2 -3 1.5 The Spinning Coating Process 4 1.6 Objective of Project 4 CHAPTER 2 Literature Review 5 - 8 2.1 Introduction 5 2.1.1 Spin Coater with a touch screen interface 5 2.1.2 Cost effective home-made Spin Coater 6 - 7 for depositing thin films 2.1.3 Design & Fabrication of a Low cost effective 7 Spin Coater for deposition of thin films 2.1.4 A comprehensive study of spin coating as a 8 thin film deposition technique and coating Equipment
  • 7. vii | P a g e CHAPTER 3 Material and Modeling 9-16 3.1 Introduction 9 3.2 Materials/Parts used in the making of the project 9 3.3 Specification of Materials/Equipments 10-12 3.4 Modeling of spin coater 12-15 3.4.1 Key stages of spin coating 13-15 3.6 Cost Analysis 16 CHAPTER 4 Results & Discussion 17 - 20 4.1 Introduction 17 4.2 Result 17 - 19 4.2.1 Graph between film thickness Vs spin time 18 4.2.2 Graph between film thickness Vs spin speed 18- 19 4.3 Spin coating troubleshooting process 19- 20 CHAPTER 5 Conclusion & Future scope 20 - 21 5.1 Conclusion 21 - 22 5.1.1 Advantage 21 5.1.2 Disadvantage 21 - 22 5.2 Future scope 22 References 23- 24
  • 8. viii | P a g e LIST OF FIGUERS FIGURE 1.1 Spin Coating using Centrifugal force Page No. 1 FIGURE 1.2 Defects occurs from spin coating Page No. 3 FIGURE 1.3 Defects occurs from spin coating Page No. 3 FIGURE 1.4 Dispense of coating fluid at the centre Page No. 4 FIGURE 2.1 Touch screen interface Page No. 5 FIGURE 2.2 Chuck with adjustable Clamps Page No. 6 FIGURE 3.1 Front View of outer cabinet Page No. 10 FIGURE 3.2 High speed sewing machine motor Page No. 11 FIGURE 3.3 Front & Rear view of the Disk with Clamping arrangement Page No. 12 FIGURE 3.4 Final design of spin coater Page No. 13 FIGURE 3.5 Key stages of spin coating process Page No. 14 FIGURE 4.1 First experiment Page No. 17
  • 9. ix | P a g e LIST OF GRAPHS GRAPH 4.1 Relationship between film thickness and spinning time Page No. 18 GRAPH 4.2 Relationship between film thickness and spinning time Page No. 19
  • 10. x | P a g e LIST OF TABLE TABLE 3.1 Cost analysis Page No. 16 TABLE 4.1 Troubleshooting Page No. 20 TABLE 4.2 Troubleshooting Page No. 20
  • 11. 1 | P a g e CHAPTER 01 INTRODUCTION Spin Coating is basically a procedure which is used to deposit uniform thin films to any flat surface of work piece. Usually a small amount of coating material is applied on the centre of the work piece’s surface when the disk is spinning at very low speed. Here in this process we are using the basic principle of centrifugal force. This is applied due to the spinning of Disk. FIG. 1.1 Spin Coating using Centrifugal force [1] 1.1 Definition and brief history of Spin Coating  A process in which solution is spread evenly over a surface using centripetal force when the disk is rotating.  Spin Coating will result in a relatively uniform thin film of a specific thickness.  Spin Coating is an important way of creating thin films in the microelectronics industry where we need thin films coating.  Spin Coating was first used to apply coatings of paints and pitch around seventy years ago.  In 1958 Emsile et. Al. developed the first spin coating model.  This model has been used as a basis for future more specific or complicated models.
  • 12. 2 | P a g e 1.2 Physics of Spin Coating Spin Coating process basically uses the principle of Centrifugal force. When the disk is rotating in any direction, a centrifugal force generates which draws rotating body away from the centre of rotation. We will further discuss about the centrifugal force here: Centrifugal Force Centrifugal force is the apparent force that draws a rotating body away from the centre of rotation. It is caused by the inertia of the body.[2] 1.3 Industrial uses of Spin Coating technology  Photo resists for patterning wafers in micro circuit production.  Insulating layers for micro circuit fabrication such as polymers.  Flat screen display coatings.  Antireflection coatings and conductive oxides.  DVD & CD ROM.  Television tube antireflection coatings. 1.4 Common Spin Coating Defects There occur lots of defects after completing the coating processes. Some of them are as follows:  Bubbles on the surface of the Coated substrate.  These bubbles occurs when fluid is deposited as the wafer is spinning, and may be caused by a faulty dispense tip.  A swirling pattern may be observed.
  • 13. 3 | P a g e FIG. 1.2 Defects occurs from spin coating[3]  Causes :-  Fluid deposited off centre.  Acceleration too high.  Spin time too short.  Exhaust rate too high.  A mark or circle in the centre of the wafer could indicate a chuck mark. FIG. 1.3 Defects occurs from spin coating[3]  If a Chuck mark occurs the type of chuck should be changed.  Uncoated areas on substrate occur when to little fluid is deposited on the substrate.  Pinhole defects can be caused by 1) Air Bubbles 2) particles in fluid/ Substrate .
  • 14. 4 | P a g e 1.5 Spin Coating process A typical Spin Coating Process basically consist of four steps which consist of a Dispense step in which the coating fluid material is deposited onto the surface of work piece, a high speed spin step to thin the fluid, and a drying step eliminate excess coating fluid from the resulting film.  Loading Of Substrate FIG. 1.4 Dispense of coating fluid at the centre  Dispense of Coating fluid on Substrate  Film Casting And Drying  Process Complete This method was first described by Emslie et al. (1958) and Meyerhofer Et al. (1978) using several simplifications.[4] 1.6 Objective of Project The basic object of this project is to Design a low cost spin Coater which will effective as well as economical. We tried here to Design a Spin Coater which is of low cost but fully functional.
  • 15. 5 | P a g e CHAPTER 2 LITRATURE REVIEW 2.1 Introduction In very simple words spin coating is a method used to apply a layer of uniform thickness of thin films to any work piece of flat surface. And the mechanism used for spin coating is known as spin coater. So for getting some knowledge about above said project we need some basic knowledge about the project which we got from some research papers, magazines, books etc. & some of here as follows : 2.1.1 Spin Coater with a touch screen interface Here according to Mr. Gurucharan V. Karnad(Dept. of Physics, Indian institute of science, Bangalore), et. Al. Spin Coating is one of the coating technique used to apply thin uniform films to flat surface of work piece. A spin coater is a machine used for spin coating , and is one of the most ubiquitous instrument in any laboratory dealing with micro fluidic devices. Run Time Setting Menu Display Screen RPM Setting FIG. 2.1 [5] They made a spin coater with a touch screen panel interface which cost about 350USD. The user input is through the touch screen panel interface, where parameters like duration of spin and spin speed can be entered. Real time speed is also displayed alongside.
  • 16. 6 | P a g e In these spin coater the substrate is mounted either using a double- side tape or a set of clamps. Improvements with the help of vacuums chuck, computer interfacing etc. can be done as per necessity. FIG. 2.2 Chuck with adjustable Clamps So here talking about our project we are using manual holding device over chuck for the mounting of substrate. We studied in an article that there is a problem of entering fuid into the vacuum pipe occurs when we are using vacuum chuck so we decide here not to use vacuum chuck.[6] 2.1.2 Cost effective home-made Spin Coater for depositing thin films Writer : Mohua Fardousi et. Al. A simple low cost spin coater design has been described in this paper. This low cost coating system is used to deposit thin films. The system can be easily built with the basic knowledge of machine and electronics. According to them this project can be done using a DC motor and electronic circuit , Designed to control the spinning speed. The spinning speed varies from 350- 3800 rpm.
  • 17. 7 | P a g e Talking about our project we used 230 volts regulator for controlling the speed of Motor. We want to make a low cost project which are having very less complications so we did not used any electronic circuit to avoid complications.[7] 2.1.3 Design & Fabrication of a Low cost effective Spin Coater for deposition of thin films Writer : Mohammad Meftahul Ferdaus et. Al. According to authors this paper tells us about the design and fabrication of a low cost spin coater for depositing thin films on any flat substrate. In simple words spin coater is a machine that can dispense a liquid fluid onto a substrate equally. Some unique desirable properties of Spin coating machine such as ability to make defect free and uniform thickness of thin film, accuracy when talking about rotation control together with a closed optimized process chamber etc. are maintained in this prototype spin coater. The materials used for making thin film liquefied in a volatile solvent. Here the system is fabricated by using a dc motor and simple electronics circuit, in which the spinning speed can be controlled very easily. In this design the spinning speed is up to 3,000 rpm that can be controlled step by step manually. Thin film deposition by this cost effective spin coater is a very simple technique and can be used widely for preparing films of uniform thickness.[8] So as we said above we were trying to reduce complication from the project so we used regulator for controlling the speed of motor. We can regulate motor from 300 rpm to 9000 rpm.
  • 18. 8 | P a g e 2.1.4 A comprehensive study of spin coating as a thin film deposition technique and coating Equipment Writer : M. D. Tyona, Advances in Material Research, Vol. 2, No. 4(2013) 181 – 193 et. Al. According to the author spin coating machine designed and fabricated using affordable components. The system was easily built with the knowledge of mechanics, fluid mechanics and basics of electronics. This equipment employs majorly three basic components and two circuit units in its operation. These includes a high speed Dc motor, a proximity sensor mounted at a distance of about 15mm from a reflective metal attached to the spindle of the motor to detect every passage of reflective metal at its front and generate pulses. Talking about our project we are neither using any kind of sensor here nor any electronic circuit for reducing or controlling the speed of motor. In the process of making our project we are focusing on making a low cost Spin Coater. That’s why here we used a 230 volt Regulator for controlling the speed of motor.[9]
  • 19. 9 | P a g e CHAPTER 03 MATERIAL AND MODELING 3.1 Introduction Material and Modeling is an important part of the project report. In which we will discuss here about the materials, equipments etc. what we used during making of our project as well as the modeling of spin coater and spin coating process. Here also we will discuss about the design of the project as well as we will do cost analysis of the project. 3.2 Materials/Equipments used in the making of the project Materials and equipments are the base for making of any project. Here in the making of our project we used Tin for the outer covering inside which we will assemble all the other equipments like motor, shafts, pulley, belt, other electronic parts etc. We used here Pewter for making clamps because of its several properties like it is very less in their weight comparing to other metals or any things. We used here a plastic pot for the upper covering of Disk as it is very less in weight. As we were trying to reduce the weight of our project. We also used a syringe for deposition of fluid exactly at the centre in exact measurement.[10] We used here hard board for making the disk because of its light weight. Another reason for using of hard board’s disk is its ease of cleaning as after every deposition of fluid some fluid may be shown there on the disk.
  • 20. 10 | P a g e 3.3 Specification of Materials/Equipment As we said that we used here Tin for making the outer covering of body. So the specification/Size of the Tin part was as given below: We used 2 Parts of Tin here both are of same size 23” * 9” & after that we gave them a design as shown below here: Below shown is the front view of the outer cabinet: FIG 3.1 Front View of outer cabinet Another important equipment used here is motor. Which plays a very important role is working of project. Specification of motor is as given below: Basically we need here a motor which is having very high speed as well as that speed can controlled by any external means. So we used here High speed sewing machine motor here as it has speed about 9000 revolution per minute. Which is comparatively very high than other spin motors etc.[11] Talking about our requirement we need a motor here which can work in between 300 to 6500 Rpm and that can be controlled by any external means like regulator etc.
  • 21. 11 | P a g e Specification of Motor: AMPS 0.5 HORSE POWER 1/12 CYCLE 50. Hz VOLTS 220/230 V R.P.M. 9000 FIG. 3.2 High speed sewing machine motor We also used here a syringe of 10ml for the depositing of coating fluid in exact volume at the centre. We fitted the syringe at the centre of the top cover. Talking about the disk we used hard board for making the disk because of its different properties as we explained before in the report. We also used here pewter for making of the holding arrangement and then we assemble those pewter with the disk which is as shown below in the figure:
  • 22. 12 | P a g e FIG. 3.3 Front & Rear view of the Disk with Clamping arrangement Then there are some other things which we use here in the making of our projects are as follows: A shaft of Dia. 6 mm 2 nos. pulley of Internal Dia. 6mm 1 plastic pot with cover for top cover Some screw bolts etc. 3.4 Modeling of spin coater As already spin coating has been continuously used in the different industry long before, hardly even a single theoretical study has been initiated. An exact theory of spin coating would allow better understanding of design and control of the process in its various applications. Several years of industrial production operations have shown that the depositions of thin films, which constitute the main utilization of the spin coating process, are quasi perfectly controlled. However, any progress in developing mathematical models should be probably more helpful in the case of heat resistant dielectric insulating films (polyamides or other materials).[12]
  • 23. 13 | P a g e FIG. 3.4 Final design of spin coater 3.4.1 Key stages of spin coating The operation of spin coating can be effectively modeled by dividing the whole process into four stages sketched in Figure 10, which are deposition, spin-up (increase in rpm), spin-off (decrease in rpm) and evaporation of solvents. The first three are commonly sequential, but spin-off and evaporation usually overlap. Stage 3 and stage 4 are the two stages that have the most impact on final coating thickness. Deposition: During the first stage, solution is provided to fall on rotating substrates from syringes and the substrate is accelerated to the desired speed. Spreading of the solution takes place due to centrifugal force and height is reduced to critical height. This is the stage of delivering an excess
  • 24. 14 | P a g e of the liquid to be coated to the surface of the substrate a portion of which’s immediately covered or “wetted”. FIG. 3.5 Key stages of spin coating process[13] Spin-up: The second stage is when the substrate is accelerated up to its final, desired, rotation speed. This stage is usually characterized by aggressive fluid expulsion from the wafer surface by the rotational motion. Because of the initial depth of fluid on the wafer surface, spiral vortices may briefly be present during this stage; these would form as a result of the twisting motion caused by the inertia that the top of the fluid layer exerts while the wafer below rotates faster and faster. Eventually, the fluid is thin enough to be completely co-rotating with the wafer and any evidence of fluid thickness differences is gone. Ultimately, the wafer reaches its desired speed and the fluid is thin enough that the viscous shear drag exactly balances the rotational accelerations.[14]
  • 25. 15 | P a g e Stable fluid outflow: This stage is also known as spin down process in which the speed of rotating of disk will get decrease slowly. The third stage is when the substrate is spinning at a constant rate and fluid viscous forces dominate fluid thinning behavior. This stage is characterized by gradual fluid thinning. Evaporation: When spin-off stage ends the film drying stage begins. During this stage centrifugal out flow stops and further shrinkage is due to solvent loss. This results in the formation of thin film on the substrate. The fourth stage is when the substrate is spinning at a constant rate and solvent evaporation dominates the coating thinning behavior. In this, the rate of evaporation depends on two factors (a) the difference in partial pressure (actually chemical potential) of each solvent species between the free surface of the liquid layer and the bulk of the gas flowing nearby. During the evaporation stage the suspended or dissolved solids may grow so concentrated at the liquid surface as to form a high viscosity, low diffusivity layer or solid skin.[15]
  • 26. 16 | P a g e 3.5 Cost Analysis Cost analysis is the portion where we will discuss about the cost of different used products, materials as well as cost of the equipments etc. The cost of every product/material/equipments is as shown below in the table: TABLE: Materials/Equipments Names Cost Motor 1300 Tin for outer covering 700 Plastic pot 130 Syringe 10 Disk 200 Clamp 100 Shaft 50 Belt 10 Screw Bolts 50 Wires 20 Regulator 25 Plugs 25 Pulley 200 Welding Charges 200 TOTAL COST 3000 TABLE 3.1 Cost analysis
  • 27. 17 | P a g e CHAPTER 04 RESULT & DISCUSSION 4.1 Introduction Here, we will discuss about different factors which affects coating as well as we will perform our experiment and will put the result here. We will also discuss here the troubleshooting of spin coating process. 4.2 Result We perform on our project by taking a glass lid and the coating solution is the mixture of color and water. Fill that solution in syringe and place the glass lid on disk and tighten by the clamps. Place the top cover on its position. After that start the machine and control the speed of motor with the help of the regulator. The speed should be about 300 rpm at the time of starting the at the same speed press the syringe so that deposition of the coating fluid can be occurs at the centre of glass lid. Then slowly increase the speed of motor up to 6500 rpm. This is the second process of spin coating leave as it is for 60 seconds and then slowly decreases the speed and bring it to around 1000 rpm so that evaporation can be occurs. As we said before we perform a demonstration and what we got is as shown below: FIG. 4.1 First experiment
  • 28. 18 | P a g e 4.2.1 Graph between film thickness Vs spin time There are several factors which affect the thickness of film. Basic Initial conditions that can be recommended for a good film deposition are the following:  1) The spinning disk should be perfectly leveled horizontally. 2) The deposited solution should wet the substrate. 3) The substrate must be clean and free from any kind of dust particles. 4) The solution should be homogeneous and uniform. The relationship of film thickness with spinning time is as shown in graph below: GRAPH 4.1 Relationship between film thickness and spinning time So here above is the graph showing the relationship between film thicknesses Vs. spinning time As its shown here by increasing the spin time we can reduce the thickness of film. 4.2.2 Graph between film thickness Vs spin speed Another factor which affects the film thickness is spin speed. So the relationship between film thickness and spin speed is as shown in graph below: We can get from the below graph that we can reduce the film thickness by increase in spin speed.
  • 29. 19 | P a g e GRAPH 4.2 Relationship Between film thickness and spin speed There are several methods for the thin film deposition. Among all the advantages of spin-coating methods are: available equipments, no time-consuming delays, fast operating and low cost. The important factors are: • Fluid viscosity. • Solution concentration • Angular speed. • Spin Time. • Evaporation rate of solvent. Applications: In insulating layers for microcircuit fabrication (like: polymers, SOG), microcircuit production, flat screen display coatings, antireflection coatings, in dielectric application and microelectronic industries for the fabrication of integrated circuits. 4.3 Spin coating troubleshooting process As already explained, there are number of major factors which affect the coating process. Some of them are these as follows spin speed, acceleration, spin time and exhaust. Following is a list of issues to consider for specific process problems.
  • 30. 20 | P a g e Film too thin Reason Solution Spin speed too high Select lower speed Spin time too long Decrease time during high speed step TABLE 4.1 Troubleshooting Film too thick Spin speed too low Select higher speed Spin time too short Increase time during high speed step TABLE 4.2 Troubleshooting Air bubbles on wafer surface 1) Air bubbles in dispensed fluid (resin) 2) Dispense tip is cut unevenly or has burrs or defects Comets, streaks, or flares 1) Fluid velocity (dispense rate) is too high 2) Spin bowl exhaust rate is too high 3) Resist sits on wafer too long prior to spin 4) Spin speed and acceleration setting is too high 5) Particles exist on substrate surface prior to dispense 6) Fluid is not being dispensed at the center of the substrate surface Swirl pattern 1) Spin bowl exhaust rate is too high 2) Fluid is striking substrate surface off center 3) Spin speed and acceleration setting is too high 4) Spin time too short
  • 31. 21 | P a g e CHAPTER 05 Conclusion & Future scope 5.1 Conclusion A cost effective spin-coater was successfully designed and fabricated. The total system is very simple. Spin coaters are ideal tools for the preparation of thin films. In this work, thin films are successfully prepared by spin-coating method. This spin coater can also be used for film deposition of different types of precursor solution. From this review we conclude that one can understand the basic physics behind the spin coating process. And establish the relationship between film thickness Vs. time and speed. . 5.1.1 Advantages As evidenced by its maturity, spin coating has many advantages in coating operations with its biggest advantage being the absence of coupled process variables. Film thickness is easily changed by changing spin speed, or switching to a different viscosity photo resist. But among the alternative coating techniques, many have multiple coupled parameters, making coating control more complex. Another advantage of spin coating is the ability of the film to get progressively more uniform as it thins, and if the film ever becomes completely uniform during the coating process, it will remain so for the duration of the process. It is low cost and fast operating system. The maturity of spin coating implies many of the issues involved in spin coating have been studied and a lot of information exists on the subject. 5.1.2 Disadvantages The disadvantages of spin coating are few, but they are becoming more important as substrate size increases and photo resist costs rise. Large substrates cannot be spun at a sufficiently high rate in order to allow the film to thin. The biggest disadvantage of spin coating is its lack of material efficiency. Typical spin coating processes utilize only 2–5% of the material dispensed
  • 32. 22 | P a g e onto the substrate, while the remaining 95–98% is flung off in to the coating bowl and disposed. Not only are the prices of the photo resist increasing substantially, but disposal costs increasing as well. If economically feasible manufacturing costs are to be maintained, a method for improving this material utilization is of primary importance, especially in the flat panel display area. 5.2 Future scope By including microprocessor in the main circuit we can include the auto on/off system. We also can add a digital display to know the speed, time and other necessary readings.
  • 33. 23 | P a g e REFERENCE [1] A G Emsile, F T Bonner and L G Peek J. Appl. Phys. 29 858 (1958) [2] D Meyerhofer J. Appl. Phys. A9 3993 (1978) [3] D E Bornside, C W Macosko et al, J. Imaging Tech. 13 122 (1987) [4] R K Yonkoski and D S Soane J. Appl. Phys. 72 725 (1992) [5] C J Lawrence and W Zhou Journal of Non-Newtonian Fluid Mechanics 39 137 (1991) [6] S Middleman An Introduction to Fluid Dynamics (New York : John Wiley and Sons) (1998) [7] O Omar, A K Ray, A K Hassan and F Davis Supramolecular Science 4 417 (1997) [8] W W Flack, D S Soong, A T Bell and D W Hess J. Appl. Phys. 56 1199 (1983) [9] http://www.cise.columbia.edu/clean/process/spintheory.pdf [10] http://www.mse.arizona.edu/faculty/birnie/Coatings [11] Ohring, M. (1992), ‘The Materials Science of Thin Films’, Academic Press limited, 24-28 Oval Road, London, NW1, 7DX, UK, pp. XIII. Moshfegh, A. Z. Känel, H.V., Kashyap, S.C., and Wuttig, M. (2003), ‘Proceedings of the International Workshop on Physics And Technology Of Thin Films’, World Scientific Publishing Co. Pvt Ltd. 5 Toh Tuck Link, Singapore, 596224 Tehran, Iran, pp. IX. [12] Seshan, K. (2002), ‘Handbook of thin-film Deposition processes and techniques: Principles, Methods, Equipment and Applications’, 2nd ed, Norwich, New York, U.S.A.: Noyes publications, William andrew publishing.
  • 34. 24 | P a g e [13] Aguilar, R.G., and López, J.O. (2011), ‘Low cost instrumentation for spin-coating deposition of thin films in an undergraduate laboratory’, Latin American Journal of Physics Education, 5 (2), 368-373. [14] Smirnov, M.A., Rambu, P., Baban, C., and Rusu, G.I. (2010), ‘Electronic Transport Properties in Polycrystalline ZnO Thin Films’, Journal of Advanced Research in Physics, 1 (2), 021011. [15] Sevvanthi, P. Claude, A., Jayanthi, C., and Poiyamozhi, A. (2012), ‘Instrumentation for fabricating an indigenous spin coating apparatus and growth of zinc oxide thin films and their characterizations’, Advances in Applied Science Research, 3 (6), 3573-3580.