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POWDER
METALLURGY
1
PowderMetallurgy-AdityaDeshpande
POWDER METALLURGY
PowderMetallurgy-AdityaDeshpande
2
1. POWDER PRODUCTION
2. BLENDING OR MIXING
3. COMPACTION
4. SINTERING
5. FINISHING(SIZING OR IMPREGNATION)
6. TESTING OR INSPECTION
PowderMetallurgy-AdityaDeshpande
3
PowderMetallurgy-AdityaDeshpande
4
PowderMetallurgy-AdityaDeshpande
5
 Atomization the most
common
 Others
 Chemical reduction of
oxides
 Electrolytic deposition
 Different shapes
produced
 Will affect compaction
process significantly
Powder Metallurgy- Aditya
Deshpande
6
•This method involves mainly milling action in which ball mills, eddy
mills, roll crusher mills are used.
•In ball milling method material to be disintegrated is tumbled together
with
a large number of hard wear resistant solid balls which by hitting the
material, cause to break it down to fine particles
PowderMetallurgy-AdityaDeshpande
7
Atomization consist of mechanically
disintegrating a stream of molten metal
into fine particles by means of a jet of
compressed air, inert gas or water, the
powder so formed being collected in
dust collector
Water and gas Atomising
PowderMetallurgy-AdityaDeshpande
8
 Used to production of copper powders used in oil less bronze
bearings
 Electrolysis copper sulphate solution in which copper anode and
aluminum cathode used.
PowderMetallurgy-AdityaDeshpande
9
 MIXING: mixing is used to
produce uniform distribution
of powder.
 BLENDING : Blending is an
operation of through mixing
of powder with different
composition
Double cone mixer
Y shape mixer
PowderMetallurgy-AdityaDeshpande
10
 Can use master alloys, (most commonly) or
elemental powders that are used to build up the
alloys
 Master alloys are with the normal alloy ingredients
 Elemental or pre-alloyed metal powders are first
mixed with lubricants or other alloy additions to
produce a homogeneous mixture of ingredients
 The initial mixing may be done by either the metal
powder producer or the P/M parts manufacturer
 When the particles are blended:
 Desire to produce a homogenous blend
 Over-mixing will work-harden the particles and produce
variability in the sintering process
PowderMetallurgy-AdityaDeshpande
11
Various
blenders
PowderMetallurgy-AdityaDeshpande
12
 During compacting the volume of the powder is reduced and voids
are reduced
 When clean metallic particles are pressed together cold welding
occurs. The compact generally has 70% of its density at this stage.
 Compacting can be done to different shapes such as circular,
square,hollow circular
 Compacting pressures of some metal powders:
METAL POWDER PRESSURE(Mpa)
Al 75-275
Al2O3 100-150
BRASS 400-700
W 75-150
Fe 400-800
PowderMetallurgy-AdityaDeshpande
13
 Usually gravity filled
cavity at room
temperature
 Pressed at 60-100 ksi
 Produces a “Green”
compact
 Size and shape of finished
part (almost)
 Not as strong as finished
part – handling concern
 Friction between
particles is a major
factor
Powder Metallurgy- Aditya
Deshpande
14
FIG : Press for PM
PowderMetallurgy-AdityaDeshpande
15
PowderMetallurgy-AdityaDeshpande
16
 Bonding common surfaces of adjacent particles touching each others
in a mass of powder or compact by heating is called sintering
 Sintering is usually carried out in electric resistance furnace , gas or
oil fired furnace.
 Types of sintering:
A. Solid phase sintering
B. Liquid phase sintering
PowderMetallurgy-AdityaDeshpande
17
 Parts are heated to ~80%
of melting temperature
 Transforms compacted
mechanical bonds to
much stronger metal
bonds
 Many parts are done at
this stage. Some will
require additional
processing
18
Powder Metallurgy- Aditya
Deshpande
SOLID PHASE SINTERING
In this process the reen compacts are
heated usually above recrystallization
temperature of low melting metal
LIQUID PHASE SINTERING
The liquid phase sintering is carried out above the melting point
of one of the alloy constituting or above meltin point of alloy
formed during sintering
PowderMetallurgy-AdityaDeshpande
19
 the sintered component have slightly different size from the desired
size due to sintering distortion this can be correct by sizing
operation.
 This is done by placing component in master dye and applying
pressure on it
PowderMetallurgy-AdityaDeshpande
20
 This term is used when oil or other fluid is permitted in the pores of
sintered materials
 Application : oil impregnated bearings, gears and similar
components
PowderMetallurgy-AdityaDeshpande
21
 An operation in which the pores of PM part filled with molten
metals . The melting point of filler material is below that of PM part.
 It gives:
 Improved strength
 Improved toughness
 Less porosity
PowderMetallurgy-AdityaDeshpande
22
1. Controlled porosity for self lubrication or filtration
uses
2. Can be very economical at large run sizes (100,000
parts)
3. Close control over the dimensions
4. So no or minimum machining after process. So
scrap – minimum(yield up to 99%)
5. No necessity of skilled person
6. Production of components of any desired
composition
PowderMetallurgy-AdityaDeshpande
23
1. Controlled porosity can be obtained.
2. P/M parts can be welded, machined, heat treated.
3. Production of refractory material is possible without
melting.
4. Production of components of metal which are
completely insoluble in liquid state(layer type
systems)
5. Mfg- cemented carbide cutting tool only by P/M.
6. Components of properties similar to parent metal can
be produced.
PowderMetallurgy-AdityaDeshpande
24
1. Problem of the material powder handling.
2. Limitation of size of components.
3. High initial cost so not suitable for small production.
4. Parts having poor corrosion resistance due to
porosity.
5. As stated above- hardness, ductility, toughness,
strength are poor as compared to conventional
manufacturing.
6. Components with theoretical density are not
manufactured.
7. Specialty machines
PowderMetallurgy-AdityaDeshpande
25
1. Automotive field
2. Defence field
3. High temperature applications
4. Aerospace field
5. Atomic energy field
6. others
PowderMetallurgy-AdityaDeshpande
26
PowderMetallurgy-AdityaDeshpande
27
PowderMetallurgy-AdityaDeshpande
28
PowderMetallurgy-AdityaDeshpande
29
PowderMetallurgy-AdityaDeshpande
30
PowderMetallurgy-AdityaDeshpande
31
Self lubricating bearings
PowderMetallurgy-AdityaDeshpande
32
PowderMetallurgy-AdityaDeshpande
33
Carbide tips for cutting tools
PowderMetallurgy-AdityaDeshpande
34
a) Tungsten filaments in
electric bulb
b) Filament in X- ray tubeFig. a)
Fig. b)
PowderMetallurgy-AdityaDeshpande
35
Solid
fuel in
rockets,
space
launch
vehicles
PowderMetallurgy-AdityaDeshpande
36
Bullets and
cartridge cases
PowderMetallurgy-AdityaDeshpande
37

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Powder Metallurgy

  • 3. 1. POWDER PRODUCTION 2. BLENDING OR MIXING 3. COMPACTION 4. SINTERING 5. FINISHING(SIZING OR IMPREGNATION) 6. TESTING OR INSPECTION PowderMetallurgy-AdityaDeshpande 3
  • 6.  Atomization the most common  Others  Chemical reduction of oxides  Electrolytic deposition  Different shapes produced  Will affect compaction process significantly Powder Metallurgy- Aditya Deshpande 6
  • 7. •This method involves mainly milling action in which ball mills, eddy mills, roll crusher mills are used. •In ball milling method material to be disintegrated is tumbled together with a large number of hard wear resistant solid balls which by hitting the material, cause to break it down to fine particles PowderMetallurgy-AdityaDeshpande 7
  • 8. Atomization consist of mechanically disintegrating a stream of molten metal into fine particles by means of a jet of compressed air, inert gas or water, the powder so formed being collected in dust collector Water and gas Atomising PowderMetallurgy-AdityaDeshpande 8
  • 9.  Used to production of copper powders used in oil less bronze bearings  Electrolysis copper sulphate solution in which copper anode and aluminum cathode used. PowderMetallurgy-AdityaDeshpande 9
  • 10.  MIXING: mixing is used to produce uniform distribution of powder.  BLENDING : Blending is an operation of through mixing of powder with different composition Double cone mixer Y shape mixer PowderMetallurgy-AdityaDeshpande 10
  • 11.  Can use master alloys, (most commonly) or elemental powders that are used to build up the alloys  Master alloys are with the normal alloy ingredients  Elemental or pre-alloyed metal powders are first mixed with lubricants or other alloy additions to produce a homogeneous mixture of ingredients  The initial mixing may be done by either the metal powder producer or the P/M parts manufacturer  When the particles are blended:  Desire to produce a homogenous blend  Over-mixing will work-harden the particles and produce variability in the sintering process PowderMetallurgy-AdityaDeshpande 11
  • 13.  During compacting the volume of the powder is reduced and voids are reduced  When clean metallic particles are pressed together cold welding occurs. The compact generally has 70% of its density at this stage.  Compacting can be done to different shapes such as circular, square,hollow circular  Compacting pressures of some metal powders: METAL POWDER PRESSURE(Mpa) Al 75-275 Al2O3 100-150 BRASS 400-700 W 75-150 Fe 400-800 PowderMetallurgy-AdityaDeshpande 13
  • 14.  Usually gravity filled cavity at room temperature  Pressed at 60-100 ksi  Produces a “Green” compact  Size and shape of finished part (almost)  Not as strong as finished part – handling concern  Friction between particles is a major factor Powder Metallurgy- Aditya Deshpande 14
  • 15. FIG : Press for PM PowderMetallurgy-AdityaDeshpande 15
  • 17.  Bonding common surfaces of adjacent particles touching each others in a mass of powder or compact by heating is called sintering  Sintering is usually carried out in electric resistance furnace , gas or oil fired furnace.  Types of sintering: A. Solid phase sintering B. Liquid phase sintering PowderMetallurgy-AdityaDeshpande 17
  • 18.  Parts are heated to ~80% of melting temperature  Transforms compacted mechanical bonds to much stronger metal bonds  Many parts are done at this stage. Some will require additional processing 18 Powder Metallurgy- Aditya Deshpande
  • 19. SOLID PHASE SINTERING In this process the reen compacts are heated usually above recrystallization temperature of low melting metal LIQUID PHASE SINTERING The liquid phase sintering is carried out above the melting point of one of the alloy constituting or above meltin point of alloy formed during sintering PowderMetallurgy-AdityaDeshpande 19
  • 20.  the sintered component have slightly different size from the desired size due to sintering distortion this can be correct by sizing operation.  This is done by placing component in master dye and applying pressure on it PowderMetallurgy-AdityaDeshpande 20
  • 21.  This term is used when oil or other fluid is permitted in the pores of sintered materials  Application : oil impregnated bearings, gears and similar components PowderMetallurgy-AdityaDeshpande 21
  • 22.  An operation in which the pores of PM part filled with molten metals . The melting point of filler material is below that of PM part.  It gives:  Improved strength  Improved toughness  Less porosity PowderMetallurgy-AdityaDeshpande 22
  • 23. 1. Controlled porosity for self lubrication or filtration uses 2. Can be very economical at large run sizes (100,000 parts) 3. Close control over the dimensions 4. So no or minimum machining after process. So scrap – minimum(yield up to 99%) 5. No necessity of skilled person 6. Production of components of any desired composition PowderMetallurgy-AdityaDeshpande 23
  • 24. 1. Controlled porosity can be obtained. 2. P/M parts can be welded, machined, heat treated. 3. Production of refractory material is possible without melting. 4. Production of components of metal which are completely insoluble in liquid state(layer type systems) 5. Mfg- cemented carbide cutting tool only by P/M. 6. Components of properties similar to parent metal can be produced. PowderMetallurgy-AdityaDeshpande 24
  • 25. 1. Problem of the material powder handling. 2. Limitation of size of components. 3. High initial cost so not suitable for small production. 4. Parts having poor corrosion resistance due to porosity. 5. As stated above- hardness, ductility, toughness, strength are poor as compared to conventional manufacturing. 6. Components with theoretical density are not manufactured. 7. Specialty machines PowderMetallurgy-AdityaDeshpande 25
  • 26. 1. Automotive field 2. Defence field 3. High temperature applications 4. Aerospace field 5. Atomic energy field 6. others PowderMetallurgy-AdityaDeshpande 26
  • 34. Carbide tips for cutting tools PowderMetallurgy-AdityaDeshpande 34
  • 35. a) Tungsten filaments in electric bulb b) Filament in X- ray tubeFig. a) Fig. b) PowderMetallurgy-AdityaDeshpande 35