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International Journal of Advanced Engineering, Management and Science (IJAEMS) [Vol-3, Issue-5, May- 2017]
https://dx.doi.org/10.24001/ijaems.3.5.35 ISSN: 2454-1311
www.ijaems.com Page | 616
Wear Analysis on 410 Stainless Steel Material by
Hardening Process
Dr. Ram Subbiah1
, M. Harini2
, M. Maneesha3
, Md. Jahangeer4
, Dr. R. Rajavel5
1
Associate Professor, Mechanical Engineering, GRIET, Hyderabad
2, 3, 4
B.Tech - Mechanical Engineering, GRIET, Hyderabad
5
Professor & Head, Mechanical Engineering, AMET University, Chennai
Abstract— The wear conduct of 410 stainless steel has
been examined under a dry sliding contact at consistent
load. It was found that hardening procedure was successful
in enhancing the wear conduct of stainless steel material,
advancing the property of pliability. A low temperature
hardening has been completed for three distinct examples at
a hour, a hour and a half, 120 minutes. Untreated stainless
steel was utilized as a kind of perspective material and
experienced wear test for comparison with different
hardening samples. The hardening samples uncover that
hard layers that are shaped which enhances the surface
hardness. Small scale hardness estimations uncovered a
critical increment in hardness after treatment. The layers
were portrayed by optical magnifying lens and checking
electron magnifying lens investigation.
Keywords— Hardening, stainless steel, wear, hardness.
I. INTRODUCTION
Hardening is done to get high surface hardness, increment
wear resistance, enhance exhaustion life, and enhance
consumption resistance, high dimensional solidness.
Stainless steel is utilized in view of their high
imperviousness to oxidation and consumption resistance.
They discover applications broadly utilized as a part of
atomic reactors, car parts like cam shafts, cam adherents,
injectors, bio restorative inserts, synthetic and nourishment
ventures. Of the different warmth treatment methods
accessible, hardening offers the advantages of high
dimensional strength. The elevated amounts of substrate
add to incredible consumption resistance in stainless steel
materials.
Decided for this exploration work, on the premise of their
application and business accessibility, hardening produces
more uniform metallurgical framed case profundity. The
profundity and nature of case would be controlled by the
synthetic arrangement under which extinguishing is
finished. Solidifying is completed by taking steel to
austenizing temperature and extinguishing it all of a sudden.
The case solidifying medium utilized as a part of this
strategy is oil extinguishing.
II. MATERIALS USED
The material used in the present work was 410 stainless
steel material. The specimens were prepared in following
forms. (i) Polished cylindrical disc specimen measuring 50
mm diameter and 10 mm height were used. (ii) Pin
specimen with diameter 8 mm and height 30 mm were used
with taper edged surface.
III. TREATMENTS
Prior to all treatments, the specimens were cleaned
ultrasonically, rinsed and dried, with care taken to avoid
finger contact. Before hardening, the specimens were sand
blasted, pickled in 15% sulphuric acid for 20 minutes. The
samples were degreased using acetone and preheated in an
air circulated furnace for 15 minutes. The samples were
hardened for three different temperatures at 60 minutes, 90
minutes, 120 minutes respectively.
IV. WEAR MEASUREMENTS
Wear tests were carried out on a pin on disc machine. A
stationery pin was mounted horizontally against a vertically
rotating disc. The disc is rotated at a constant speed of 1000
rpm at a constant load of 2 Kg, which was applied
continuously for a fixed period of 2 minutes under dry
conditions. Wear test were conducted and the samples were
replaced one by one. The weights of the specimens were
measured using a standard caliberometer. The difference
between the specimen before and after testing gives the
wear loss.
V. RESULTS AND DISCUSSIONS
The hardened specimen results were compared with the
untreated specimen and it was found that, in hardened
specimen, the mixture of cementite and ferrite were
precipitated on the surface, to improve the hardness of
material. The wear rate of untreated specimen is specified to
International Journal of Advanced Engineering, Management and Science (IJAEMS) [Vol-3, Issue-5, May- 2017]
https://dx.doi.org/10.24001/ijaems.3.5.35 ISSN: 2454-1311
www.ijaems.com Page | 617
be lower that of hardened material. Hence good surface
hardness is obtained. Low temperature hardening results in
good wear performance to relative case depth, which
improves wear resistance. The ductility of material is
promoted in 410 stainless steel material. So by the process
of re - heat treatment of 410 stainless steel material, this
material can also be used for higher applications like power
plant turbine blades, nuclear reactors, marine applications
where components are subjected to sea water, automobile
applications.
5.1 Optical Microscope Results
Fig.1: Untreated Specimen
Fig.2: Hardening for 1 hour 11.5 microns
Fig.3: Hardening for 1.5 hour 13 microns
Fig.4: Hardening for 2 hour 14 microns
From the figure 1,2,3,4 it is seen that, as the time of
hardening increases, case depth also increases. Therefore
the case depth is increased from 11.5 to 14 microns
specimens respectively. The results are compared with
untreated specimen. Hence hardened specimen done for 120
minutes improves its wear resistance causing low wear loss
and wear rate.
5.2 Scanning Electron Microscope Results
Fig.5: Untreated Specimen SEM Image
Fig.6: SEM Image for 1 hour hardened specimen
Fig.7: SEM Image for 1.5 hour hardened specimen
International Journal of Advanced Engineering, Management and Science (IJAEMS) [Vol-3, Issue-5, May- 2017]
https://dx.doi.org/10.24001/ijaems.3.5.35 ISSN: 2454-1311
www.ijaems.com Page | 618
Fig.8: SEM Image for 2 hour hardened specimen
From the figure 5,6,7,8 the specimens were compared with
untreated specimen. The peel of material is very high in
untreated specimen. The wear of material is high. As the
case depth increases, wear loss of the material decreases. In
hardened specimen for 120 minutes, the wear loss of
material is less when compared to other hardened
specimens, which improves its wear resistance.
VI. CONCLUSION
The result of this work confirms that, hardening process
has effectively improved its wear resistance. As the time for
treatment increases, the case depth also increases. From the
wear studies, it is observed that hardened specimen for 120
minutes has a very good wear resistance. It is showed that,
as the time of treatment increases, weight loss decreases,
hence the life of the material is increased.
REFERENCES
[1] M.K. Lee, G.H. Kim, K.H. Kim, W.W. Kim, “Effects
of the surface temperature and cooling rate on the
residual stresses in a flame hardening of 12Cr steel”
Journal of Materials Processing Technology, Volume
176, Issues 1–3, 6 June 2006, Pages 140-145
[2] M.K. Lee, G.H. Kim, K.H. Kim, W.W. Kim, “Control
of surface hardnesses, hardening depths, and residual
stresses of low carbon 12Cr steel by flame hardening”
Surface and Coatings Technology, Volume 184, Issues
2–3, 22 June 2004, Pages 239-246
[3] C.F. Kuang, J. Li, S.G. Zhang, J. Wang, H.F. Liu,
A.A. Volinsky, “Effects of quenching and tempering
on the microstructure and bake hardening behavior of
ferrite and dual phase steels” Materials Science and
Engineering: A, Volume 613, 8 September 2014,
Pages 178-183.
[4] Lipeng Ding, Yaoyao Weng, Sainan Wu, Robert E.
Sanders, Zhihong Jia, Qing Liu, “Influence of
interrupted quenching and pre-aging on the bake
hardening of Al–Mg–Si Alloy” Materials Science and
Engineering: A, Volume 651, 10 January 2016, Pages
991-998
[5] K.O. Findley, J. Hidalgo, R.M. Huizenga, M.J.
Santofimia, “Controlling the work hardening of
martensite to increase the strength/ductility balance in
quenched and partitioned” Materials & Design,
Volume 117, 5 March 2017, Pages 248-256
[6] Jun Zhang, Hua Ding, R.D.K. Misra, Chao Wang,
“Enhanced stability of retained austenite and
consequent work hardening rate through pre-
quenching prior to quenching and partitioning in a Q–
P microalloyed steel” Materials Science and
Engineering: A, Volume 611, 12 August 2014, Pages
252-256
[7] Jun Zhang, Hua Ding, R.D.K. Misra, “Enhanced strain
hardening and microstructural characterization in a
low carbon quenching and partitioning steel with
partial austenization” Materials Science and
Engineering: A, Volume 636, 11 June 2015, Pages 53-
59.
[8] Ji Dong, Xiaosheng Zhou, Yongchang Liu, Chong Li,
Chenxi Liu, Huijun Li, “Effects of quenching-
partitioning-tempering treatment on microstructure
and mechanical performance of Nb-V-Ti microalloyed
ultra-high strength steel” Materials Science and
Engineering: A, Volume 690, 6 April 2017, Pages
283-293
[9] Qingguo Hao, Shengwei Qin, Yu Liu, Xunwei Zuo,
Nailu Chen, Yonghua Rong, “Relation between
microstructure and formability of quenching-
partitioning-tempering martensitic steel” Materials
Science and Engineering: A, Volume 671, 1 August
2016, Pages 135-146
[10]H. Rastegari, A. Kermanpur, A. Najafizadeh, “Effect
of initial microstructure on the work hardening
behavior of plain eutectoid steel” Materials Science
and Engineering: A, Volume 632, 24 April 2015,
Pages 103-109.

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Wear Analysis on 410 Stainless Steel Material by Hardening Process

  • 1. International Journal of Advanced Engineering, Management and Science (IJAEMS) [Vol-3, Issue-5, May- 2017] https://dx.doi.org/10.24001/ijaems.3.5.35 ISSN: 2454-1311 www.ijaems.com Page | 616 Wear Analysis on 410 Stainless Steel Material by Hardening Process Dr. Ram Subbiah1 , M. Harini2 , M. Maneesha3 , Md. Jahangeer4 , Dr. R. Rajavel5 1 Associate Professor, Mechanical Engineering, GRIET, Hyderabad 2, 3, 4 B.Tech - Mechanical Engineering, GRIET, Hyderabad 5 Professor & Head, Mechanical Engineering, AMET University, Chennai Abstract— The wear conduct of 410 stainless steel has been examined under a dry sliding contact at consistent load. It was found that hardening procedure was successful in enhancing the wear conduct of stainless steel material, advancing the property of pliability. A low temperature hardening has been completed for three distinct examples at a hour, a hour and a half, 120 minutes. Untreated stainless steel was utilized as a kind of perspective material and experienced wear test for comparison with different hardening samples. The hardening samples uncover that hard layers that are shaped which enhances the surface hardness. Small scale hardness estimations uncovered a critical increment in hardness after treatment. The layers were portrayed by optical magnifying lens and checking electron magnifying lens investigation. Keywords— Hardening, stainless steel, wear, hardness. I. INTRODUCTION Hardening is done to get high surface hardness, increment wear resistance, enhance exhaustion life, and enhance consumption resistance, high dimensional solidness. Stainless steel is utilized in view of their high imperviousness to oxidation and consumption resistance. They discover applications broadly utilized as a part of atomic reactors, car parts like cam shafts, cam adherents, injectors, bio restorative inserts, synthetic and nourishment ventures. Of the different warmth treatment methods accessible, hardening offers the advantages of high dimensional strength. The elevated amounts of substrate add to incredible consumption resistance in stainless steel materials. Decided for this exploration work, on the premise of their application and business accessibility, hardening produces more uniform metallurgical framed case profundity. The profundity and nature of case would be controlled by the synthetic arrangement under which extinguishing is finished. Solidifying is completed by taking steel to austenizing temperature and extinguishing it all of a sudden. The case solidifying medium utilized as a part of this strategy is oil extinguishing. II. MATERIALS USED The material used in the present work was 410 stainless steel material. The specimens were prepared in following forms. (i) Polished cylindrical disc specimen measuring 50 mm diameter and 10 mm height were used. (ii) Pin specimen with diameter 8 mm and height 30 mm were used with taper edged surface. III. TREATMENTS Prior to all treatments, the specimens were cleaned ultrasonically, rinsed and dried, with care taken to avoid finger contact. Before hardening, the specimens were sand blasted, pickled in 15% sulphuric acid for 20 minutes. The samples were degreased using acetone and preheated in an air circulated furnace for 15 minutes. The samples were hardened for three different temperatures at 60 minutes, 90 minutes, 120 minutes respectively. IV. WEAR MEASUREMENTS Wear tests were carried out on a pin on disc machine. A stationery pin was mounted horizontally against a vertically rotating disc. The disc is rotated at a constant speed of 1000 rpm at a constant load of 2 Kg, which was applied continuously for a fixed period of 2 minutes under dry conditions. Wear test were conducted and the samples were replaced one by one. The weights of the specimens were measured using a standard caliberometer. The difference between the specimen before and after testing gives the wear loss. V. RESULTS AND DISCUSSIONS The hardened specimen results were compared with the untreated specimen and it was found that, in hardened specimen, the mixture of cementite and ferrite were precipitated on the surface, to improve the hardness of material. The wear rate of untreated specimen is specified to
  • 2. International Journal of Advanced Engineering, Management and Science (IJAEMS) [Vol-3, Issue-5, May- 2017] https://dx.doi.org/10.24001/ijaems.3.5.35 ISSN: 2454-1311 www.ijaems.com Page | 617 be lower that of hardened material. Hence good surface hardness is obtained. Low temperature hardening results in good wear performance to relative case depth, which improves wear resistance. The ductility of material is promoted in 410 stainless steel material. So by the process of re - heat treatment of 410 stainless steel material, this material can also be used for higher applications like power plant turbine blades, nuclear reactors, marine applications where components are subjected to sea water, automobile applications. 5.1 Optical Microscope Results Fig.1: Untreated Specimen Fig.2: Hardening for 1 hour 11.5 microns Fig.3: Hardening for 1.5 hour 13 microns Fig.4: Hardening for 2 hour 14 microns From the figure 1,2,3,4 it is seen that, as the time of hardening increases, case depth also increases. Therefore the case depth is increased from 11.5 to 14 microns specimens respectively. The results are compared with untreated specimen. Hence hardened specimen done for 120 minutes improves its wear resistance causing low wear loss and wear rate. 5.2 Scanning Electron Microscope Results Fig.5: Untreated Specimen SEM Image Fig.6: SEM Image for 1 hour hardened specimen Fig.7: SEM Image for 1.5 hour hardened specimen
  • 3. International Journal of Advanced Engineering, Management and Science (IJAEMS) [Vol-3, Issue-5, May- 2017] https://dx.doi.org/10.24001/ijaems.3.5.35 ISSN: 2454-1311 www.ijaems.com Page | 618 Fig.8: SEM Image for 2 hour hardened specimen From the figure 5,6,7,8 the specimens were compared with untreated specimen. The peel of material is very high in untreated specimen. The wear of material is high. As the case depth increases, wear loss of the material decreases. In hardened specimen for 120 minutes, the wear loss of material is less when compared to other hardened specimens, which improves its wear resistance. VI. CONCLUSION The result of this work confirms that, hardening process has effectively improved its wear resistance. As the time for treatment increases, the case depth also increases. From the wear studies, it is observed that hardened specimen for 120 minutes has a very good wear resistance. It is showed that, as the time of treatment increases, weight loss decreases, hence the life of the material is increased. REFERENCES [1] M.K. Lee, G.H. Kim, K.H. Kim, W.W. Kim, “Effects of the surface temperature and cooling rate on the residual stresses in a flame hardening of 12Cr steel” Journal of Materials Processing Technology, Volume 176, Issues 1–3, 6 June 2006, Pages 140-145 [2] M.K. Lee, G.H. Kim, K.H. Kim, W.W. Kim, “Control of surface hardnesses, hardening depths, and residual stresses of low carbon 12Cr steel by flame hardening” Surface and Coatings Technology, Volume 184, Issues 2–3, 22 June 2004, Pages 239-246 [3] C.F. Kuang, J. Li, S.G. Zhang, J. Wang, H.F. Liu, A.A. Volinsky, “Effects of quenching and tempering on the microstructure and bake hardening behavior of ferrite and dual phase steels” Materials Science and Engineering: A, Volume 613, 8 September 2014, Pages 178-183. [4] Lipeng Ding, Yaoyao Weng, Sainan Wu, Robert E. Sanders, Zhihong Jia, Qing Liu, “Influence of interrupted quenching and pre-aging on the bake hardening of Al–Mg–Si Alloy” Materials Science and Engineering: A, Volume 651, 10 January 2016, Pages 991-998 [5] K.O. Findley, J. Hidalgo, R.M. Huizenga, M.J. Santofimia, “Controlling the work hardening of martensite to increase the strength/ductility balance in quenched and partitioned” Materials & Design, Volume 117, 5 March 2017, Pages 248-256 [6] Jun Zhang, Hua Ding, R.D.K. Misra, Chao Wang, “Enhanced stability of retained austenite and consequent work hardening rate through pre- quenching prior to quenching and partitioning in a Q– P microalloyed steel” Materials Science and Engineering: A, Volume 611, 12 August 2014, Pages 252-256 [7] Jun Zhang, Hua Ding, R.D.K. Misra, “Enhanced strain hardening and microstructural characterization in a low carbon quenching and partitioning steel with partial austenization” Materials Science and Engineering: A, Volume 636, 11 June 2015, Pages 53- 59. [8] Ji Dong, Xiaosheng Zhou, Yongchang Liu, Chong Li, Chenxi Liu, Huijun Li, “Effects of quenching- partitioning-tempering treatment on microstructure and mechanical performance of Nb-V-Ti microalloyed ultra-high strength steel” Materials Science and Engineering: A, Volume 690, 6 April 2017, Pages 283-293 [9] Qingguo Hao, Shengwei Qin, Yu Liu, Xunwei Zuo, Nailu Chen, Yonghua Rong, “Relation between microstructure and formability of quenching- partitioning-tempering martensitic steel” Materials Science and Engineering: A, Volume 671, 1 August 2016, Pages 135-146 [10]H. Rastegari, A. Kermanpur, A. Najafizadeh, “Effect of initial microstructure on the work hardening behavior of plain eutectoid steel” Materials Science and Engineering: A, Volume 632, 24 April 2015, Pages 103-109.