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Failure of Flexible PVC Hose in
Underground Applications
Presented at “Plastics in Underground Pipes 2011”
Houston, TX / November 1 & 2, 2011

Duane Priddy, Ph.D.
President/Plastic Failure Labs

Plastics in Underground Pipes – Houston DP 11/1/11

1
Benefits of PVC Hose
‱ Semi-flexible PVC hose combines the
attributes of rigid PVC (high modulus) with
flexible PVC (high flexibility) to yield a product
that has the benefits of PVC pipe (easy to
install using standard glued PVC fittings) yet it
is semi-flexible allowing it to be installed with
flexing around underground obstructions

Plastics in Underground Pipes – Houston DP 11/1/11

2
Manufacturing Process
‱ The hose is manufactured using a co-extrusion
process where the rigid PVC formulation is
extruded into a strand along side of the
flexible PVC formulation which is extruded
into a narrow sheet. As the strand and the
sheet co-extrude from the die, they are
wound around a mandrel to form the hose.
The rigid PVC strand ends up embedded in the
wall of the hose as a helical coil.
Plastics in Underground Pipes – Houston DP 11/1/11

3
Plastics in Underground Pipes – Houston DP 11/1/11

4
Example Failures: Swimming Pools

These failure occurred after 1 – 2
years of service

Plastics in Underground Pipes – Houston DP 11/1/11

5
Exterior Cracking is Most Common but also may
Occur on Either the Interior Wall

Plastics in Underground Pipes – Houston DP 11/1/11

6
Microscope Views of Cracks
Close-up view of failed region in outside hose wall

View of fractures surface shows repeating diagonal void
pattern in flexible PVC portion

7
Plastics in Underground Pipes – Houston DP 11/1/11
Fracture surface analysis
Closer view of the voids

Plastics in Underground Pipes – Houston DP 11/1/11

8
Views of Fracture Surface

Plastics in Underground Pipes – Houston DP 11/1/11

9
SEM Analysis of Fracture Surface

Plastics in Underground Pipes – Houston DP 11/1/11

10
SEM of Fracture Surface

Plastics in Underground Pipes – Houston DP 11/1/11

11
SEM Analysis of Fracture Surface

Plastics in Underground Pipes – Houston DP 11/1/11

12
FTIR Spectra of Flexible & Rigid Components in Failed Samples

Flexible
DOP plasticizer

Rigid

Plastics in Underground Pipes – Houston DP 11/1/11

13
Conclusions
‱ Some pipe samples contain voids in the
fracture surface and fracture propagation
follows the voids = manufacturing defect
‱ Most fractures show evidence of ESC failure of
the rigid strands
‱ Flex hoses that use flexible PVC containing a
migrating plasticizer are inherently defective
because the plasticizer migrates into the rigid
PVC strands causing them to stress-crack.
Plastics in Underground Pipes – Houston DP 11/1/11

14
Concluding Remarks
‱ Flex hose manufactures should use only flexible PVC
made using non-migrating plasticizer.
‱ IAPMO needs to include a requirement in the PVC
flex hose standard requiring only the use of nonmigrating plasticizers.

Plastics in Underground Pipes – Houston DP 11/1/11

15
Possible Technical Solutions
‱ Use a rigid plastic component that is
compatible with flexible PVC; e.g., PP
‱ Place a barrier layer between the rigid and
flexible components to stop the DOP
migration
‱ Develop a low cost non-migrating plasticizer

Plastics in Underground Pipes – Houston DP 11/1/11

16

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Flexible pvc hose for underground applications

  • 1. Failure of Flexible PVC Hose in Underground Applications Presented at “Plastics in Underground Pipes 2011” Houston, TX / November 1 & 2, 2011 Duane Priddy, Ph.D. President/Plastic Failure Labs Plastics in Underground Pipes – Houston DP 11/1/11 1
  • 2. Benefits of PVC Hose ‱ Semi-flexible PVC hose combines the attributes of rigid PVC (high modulus) with flexible PVC (high flexibility) to yield a product that has the benefits of PVC pipe (easy to install using standard glued PVC fittings) yet it is semi-flexible allowing it to be installed with flexing around underground obstructions Plastics in Underground Pipes – Houston DP 11/1/11 2
  • 3. Manufacturing Process ‱ The hose is manufactured using a co-extrusion process where the rigid PVC formulation is extruded into a strand along side of the flexible PVC formulation which is extruded into a narrow sheet. As the strand and the sheet co-extrude from the die, they are wound around a mandrel to form the hose. The rigid PVC strand ends up embedded in the wall of the hose as a helical coil. Plastics in Underground Pipes – Houston DP 11/1/11 3
  • 4. Plastics in Underground Pipes – Houston DP 11/1/11 4
  • 5. Example Failures: Swimming Pools These failure occurred after 1 – 2 years of service Plastics in Underground Pipes – Houston DP 11/1/11 5
  • 6. Exterior Cracking is Most Common but also may Occur on Either the Interior Wall Plastics in Underground Pipes – Houston DP 11/1/11 6
  • 7. Microscope Views of Cracks Close-up view of failed region in outside hose wall View of fractures surface shows repeating diagonal void pattern in flexible PVC portion 7 Plastics in Underground Pipes – Houston DP 11/1/11
  • 8. Fracture surface analysis Closer view of the voids Plastics in Underground Pipes – Houston DP 11/1/11 8
  • 9. Views of Fracture Surface Plastics in Underground Pipes – Houston DP 11/1/11 9
  • 10. SEM Analysis of Fracture Surface Plastics in Underground Pipes – Houston DP 11/1/11 10
  • 11. SEM of Fracture Surface Plastics in Underground Pipes – Houston DP 11/1/11 11
  • 12. SEM Analysis of Fracture Surface Plastics in Underground Pipes – Houston DP 11/1/11 12
  • 13. FTIR Spectra of Flexible & Rigid Components in Failed Samples Flexible DOP plasticizer Rigid Plastics in Underground Pipes – Houston DP 11/1/11 13
  • 14. Conclusions ‱ Some pipe samples contain voids in the fracture surface and fracture propagation follows the voids = manufacturing defect ‱ Most fractures show evidence of ESC failure of the rigid strands ‱ Flex hoses that use flexible PVC containing a migrating plasticizer are inherently defective because the plasticizer migrates into the rigid PVC strands causing them to stress-crack. Plastics in Underground Pipes – Houston DP 11/1/11 14
  • 15. Concluding Remarks ‱ Flex hose manufactures should use only flexible PVC made using non-migrating plasticizer. ‱ IAPMO needs to include a requirement in the PVC flex hose standard requiring only the use of nonmigrating plasticizers. Plastics in Underground Pipes – Houston DP 11/1/11 15
  • 16. Possible Technical Solutions ‱ Use a rigid plastic component that is compatible with flexible PVC; e.g., PP ‱ Place a barrier layer between the rigid and flexible components to stop the DOP migration ‱ Develop a low cost non-migrating plasticizer Plastics in Underground Pipes – Houston DP 11/1/11 16