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High Purity WaterHigh Purity Water
ProductionProduction
by Gary L Burgessby Gary L Burgess
April 16, 2007April 16, 2007
Fluidization /
Backwash prior
to Regeneration
Beginning
Separation in
Mixed Bed
Ion Exchanger
Start of
Separating of Ion
Exchange
Components
Separation of
Anion / Inert
Belt / Cation
Begins
Anion โ€“ Yellow
Blue โ€“ Inert
Navy - Cation
Compaction
Cation Bed
Formed
Anion Bed
Forming with
Fines / Lighter
Beads
Anion Resin
Compacting
Anion Fines
Mixed Bed
Ready for Acid
- HCl and
Caustic -
NaOH
Addition
Reverse Osmosis Pure Water Collected in Hollow Fiber โ€“ BioPharm
Diafiltration Flow is generally from Hollow Center Out
Spiral Wound Reverse Osmosis Element
RO note the Holes on Center Collector
Inlet End of Feed water to Spiral Wrappings with Center Collector
RO Spiral Windings Course Spacer, Membrane(s), Inner Spacer
RO Sealed Envelope with Feed Spacer / Mesh
RO with Inner Spacer โ€“ End is not sealed for Inner Spacer Illustration
Cavity โ€œDeadโ€ Area or Why Ball Valves are Generally not Acceptable
Diaphragm Valve โ€“ Weir Dam
Weir Dam not Fully Drainable in Vertical Orientation
Tip the Body on a 8 to 28 +/- Degree Angle depending on Size / Mfg & It is Drainable
Approximate Angle
for Free Draining
for Properly
Designed
Diaphragm Valve
Get โ€˜Rโ€™ Done โ€“ Welding Plastic Piping โ€“ ECTFE / Halar
Gaps or Contaminations and Bacterial Homes โ€“ Out of Round ECTFE
Polypropylene Butt Weld โ€“
Recess Areas & Horizontal
Dam
PVDF Butt Well
โ€“ Horizontal Dam
PVDF โ€“ Socket Weld โ€“ Smaller Dam โ€“ Less or No Recess Area
PP Electrical Current Weld โ€“ Note Bevel and Bacterial Contamination Potential
PVDF First Generation Seamless Weld
โ€“ some diameter variation
PFA โ€“ Perfluoroalkoxy Butt Weld
โ€“ Translucent Shows Internal Scratch
UHMW Polyethylene almost Seamless Butt-weld with Slight Damming
PVDF โ€“ Seamless Second Generation Weld โ€“ Internal Mandrel / Balloon
PVDF Weld โ€“ Note Fitting Different
Diameters & Rollover
or Curl Under of Weld
PVDF Butt-weld โ€“ Hot Plate Heats the Ends โ€“ then the Components are Pressed
Together
Lined Pipe โ€“ ECTFE Glass Like Smooth Bore โ€“ Flanging and Gaskets are less than
Ideal
Lined ECTFE Can Span Long Distances with Minimum Sagging
Timing and Temperature along with Cut and Pressure All
Critical for a Pure Weld
Perfection in Plastic Welding
Bronze โ€“ Tin Lined Pipe
- First in High Purity
Piping and Still Used
in Certain Applications
โ€“ Low Solubility
Tank Linings โ€“ Spray on PVCโ€™s
PVC Plate with Weld Rod Weld
PTFE Backing Weld โ€“ Large Dam in Horizontal in a Tank
PVDF Welding Rod โ€“ Raised Area on Both Sides โ€“ Potential Tank Separation
Better View of PVDF Weld
FEP Lining with Textile Bonding Backing to Tank Wall
FEP Smooth and Flat Weld
PVDF Plastic Sheets โ€“ Critical to Shipping Clean and Preventing Fabrication Scratching
Better View of Fabrication Bonding / Backing
Hose Barb in which 2 or 3 Barbs Have Corroded Away in a Few Months because of
Stray Currents in Water Cooled Rectifier

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