Utilization of rice husk ash in mix asphalt concrete as mineral fillar replac...rajatsikarwar
how to use rice husk as a replacement of cement in concrete
and conducting diifferent tests conducted to prove that it is satisfying the indian standards(IS).
A STUDY ON REPLACEMENT OF CEMENT WITH RICE HUSK ASHIAEME Publication
Objectives: This study is to identify the effect of parameter such as Activator ratio thataffects the properties of alkali activated fly ash
Methodology: To achieve the above objectives, the present investigation is adopted atechnology that is currently in use to manufacture and to test themain aim of this activity was to facilitate promotion of newmaterials later on to the concreteindustry. Research variable included activator ratio (1:2, 1:2.5, and 1:3). The trial mix isprepared for the molarity of 16 M. Concrete specimens were cured at roresponse variables are Flexural strength, Compressive strength and Split tensile strength.Findings: Test data are used to identify the variation ofGeopolymer concrete propertieswhich are affected by using of various activator ratios and curing period. At all ages, theactivator ratio 1:3 gives maximum strength and also economical when compared to otheractivator ratios. There is substantial gain incompressive strength of fly ash geopolymerconcrete with age.Improvements:Thisworkcan beenhancedforvariousmolaritiesundervarioustemperaturesandvariousactivator ratios.
Effectiveness of Use of Rice Husk Ash as Partial Replacement of Cement in Con...IJMER
India is a major rice producing country, and the husk generated during milling is mostly
used as a fuel in the boilers for processing paddy and producing energy through direct combustion.
About 21 million tones of Rice Husk Ash (RHA) is produced annually. This RHA is regarded as a waste
and has disposal problem because of the fact that it consumes a vast area for dumping. Lots of ways are
being thought of for disposing them by making commercial use of this RHA. RHA can be used as a
replacement for concrete (5 to 15%).This paper evaluates how different contents of Rice Husk Ash
added to concrete may influence its properties. In this study, cement was replaced by waste RHA as
5%,10% and 15% by weight for M-25 mix. The concrete specimens were tested for compressive
strength, durability (water absorption) and density at 28 days of age and the results obtained were
compared with those of normal concrete. The results concluded the permissibility of using waste RHA
as partial replacement of cement up to 10% by weight of cement
The influence of sintering temperature on the thermal conductivity of rice husk ash refractory is examined in this research. Cylindrical disk made from RHA whose chemical composition measured by XRF were sintered in the temperature range of 1000℃-1400℃. the crystalline phase transformation studied by XRD. The thermal conductivity of these Rice Husk Ash refractory was determined using the hot flux method and values calculated using Fourier’s equation for steady state heat conduction. Porosity and density test were also carried out Result showed that there was an increase in apparent density and conductivity with increasing sintering temperature though the values are still low and satisfactory for most insulation applications. Porosity of rice husk ash refractory decreases with increasing sintering temperature therefore the gains of higher strength from higher sintering temperature are not negated.
Use of Saw Dust Ash as Partial Replacement for Cement In Concreteinventionjournals
International Journal of Engineering and Science Invention (IJESI) is an international journal intended for professionals and researchers in all fields of computer science and electronics. IJESI publishes research articles and reviews within the whole field Engineering Science and Technology, new teaching methods, assessment, validation and the impact of new technologies and it will continue to provide information on the latest trends and developments in this ever-expanding subject. The publications of papers are selected through double peer reviewed to ensure originality, relevance, and readability. The articles published in our journal can be accessed online.
Utilization of rice husk ash in mix asphalt concrete as mineral fillar replac...rajatsikarwar
how to use rice husk as a replacement of cement in concrete
and conducting diifferent tests conducted to prove that it is satisfying the indian standards(IS).
A STUDY ON REPLACEMENT OF CEMENT WITH RICE HUSK ASHIAEME Publication
Objectives: This study is to identify the effect of parameter such as Activator ratio thataffects the properties of alkali activated fly ash
Methodology: To achieve the above objectives, the present investigation is adopted atechnology that is currently in use to manufacture and to test themain aim of this activity was to facilitate promotion of newmaterials later on to the concreteindustry. Research variable included activator ratio (1:2, 1:2.5, and 1:3). The trial mix isprepared for the molarity of 16 M. Concrete specimens were cured at roresponse variables are Flexural strength, Compressive strength and Split tensile strength.Findings: Test data are used to identify the variation ofGeopolymer concrete propertieswhich are affected by using of various activator ratios and curing period. At all ages, theactivator ratio 1:3 gives maximum strength and also economical when compared to otheractivator ratios. There is substantial gain incompressive strength of fly ash geopolymerconcrete with age.Improvements:Thisworkcan beenhancedforvariousmolaritiesundervarioustemperaturesandvariousactivator ratios.
Effectiveness of Use of Rice Husk Ash as Partial Replacement of Cement in Con...IJMER
India is a major rice producing country, and the husk generated during milling is mostly
used as a fuel in the boilers for processing paddy and producing energy through direct combustion.
About 21 million tones of Rice Husk Ash (RHA) is produced annually. This RHA is regarded as a waste
and has disposal problem because of the fact that it consumes a vast area for dumping. Lots of ways are
being thought of for disposing them by making commercial use of this RHA. RHA can be used as a
replacement for concrete (5 to 15%).This paper evaluates how different contents of Rice Husk Ash
added to concrete may influence its properties. In this study, cement was replaced by waste RHA as
5%,10% and 15% by weight for M-25 mix. The concrete specimens were tested for compressive
strength, durability (water absorption) and density at 28 days of age and the results obtained were
compared with those of normal concrete. The results concluded the permissibility of using waste RHA
as partial replacement of cement up to 10% by weight of cement
The influence of sintering temperature on the thermal conductivity of rice husk ash refractory is examined in this research. Cylindrical disk made from RHA whose chemical composition measured by XRF were sintered in the temperature range of 1000℃-1400℃. the crystalline phase transformation studied by XRD. The thermal conductivity of these Rice Husk Ash refractory was determined using the hot flux method and values calculated using Fourier’s equation for steady state heat conduction. Porosity and density test were also carried out Result showed that there was an increase in apparent density and conductivity with increasing sintering temperature though the values are still low and satisfactory for most insulation applications. Porosity of rice husk ash refractory decreases with increasing sintering temperature therefore the gains of higher strength from higher sintering temperature are not negated.
Use of Saw Dust Ash as Partial Replacement for Cement In Concreteinventionjournals
International Journal of Engineering and Science Invention (IJESI) is an international journal intended for professionals and researchers in all fields of computer science and electronics. IJESI publishes research articles and reviews within the whole field Engineering Science and Technology, new teaching methods, assessment, validation and the impact of new technologies and it will continue to provide information on the latest trends and developments in this ever-expanding subject. The publications of papers are selected through double peer reviewed to ensure originality, relevance, and readability. The articles published in our journal can be accessed online.
A REPORT ON PARTIAL SUBSTITUTE OF CEMENT IN CONCRETE USING RICE HUSK ASHIAEME Publication
Objectives: This research work is to examine the partial replacement of cement in concrete mistreatment rice husk ash. It involved the study of strength properties of the concrete with totally different proportions of rice husk ash as partial replacement in cement. Methods: The major problem sweet-faced by the globe nowadays is that the environmental pollution. In the industry, mainly the production of cement can cause the emission of pollutants that includes a nice impact on atmosphere. This can be reduced by the magnified usage of business by-products within the industry. Findings: In this present study, to produce the concrete, Portland cement is partially substituted with Rice husk ash. Different ratios of partial replacement is done like 1/3, 5%, 10%, 15%, 20%, and 25% is taken to prepare completely different mixes. The concrete specimens are tested for their compressive strength, split tensile strength take a look at and flexural strength test at the age of seven and twenty eight days.
The Effect of Rise Husk Ash on Strength and Permeability of ConcreteAkshay D Nicator
HA, produced after burning of Rice husks (RH) has high reactivity and pozzolanic property. Indian Standard code of practice for plain and reinforced concrete, IS 456- 2000, recommends use of RHA in concrete but does not specify quantities.
Mix Design of Grade M35 by Replacement of Cement with Rice Husk Ash in ConcreteDr. Amarjeet Singh
The optimized RHA, by controlled burn or
grinding, has been used as a pozzolanic material in cement
and concrete. Using it provides several advantages, such as
improved strength and durability properties, and
environmental benefits related to the disposal of waste
materials and to reduced carbon dioxide emissions. Up to
now, little research has been done to investigate the use of
RHA as supplementary material in cement and concrete
production .The main objective of this work is to study the
suitability of the rice husk ash as a pozzolanic material for
cement replacement in concrete. However it is expected that
the use of rice husk ash in concrete improve the strength
properties of concrete. Also it is an attempt made to develop
the concrete using rice husk ash as a source material for
partial replacement of cement, which satisfies the structural
properties of concrete like compressive strength.
A COMPREHENSIVE STUDY ON PARTIAL REPLACEMENT OF CEMENT WITH SUGARCANE BAGASSE...IAEME Publication
A Large quantities of waste materials and by-products are generated from manufacturing processes, service industries and municipal solid wastes, etc. As a result, solid waste management has become one of the major environmental concerns in the world. With the increasing awareness about the environment, scarcity of land-fill space and due to its ever increasing cost, waste materials and by-products utilization has become an attractive alternative to disposal. High consumption of natural sources, high amount production of industrial wastes and environmental pollution require obtaining new solutions for a sustainable development.Ordinary Portland cement is recognized as a major construction material throughout the world.
Experimental Study On Rice Husk As Fine Aggregates In Concretetheijes
The International Journal of Engineering & Science is aimed at providing a platform for researchers, engineers, scientists, or educators to publish their original research results, to exchange new ideas, to disseminate information in innovative designs, engineering experiences and technological skills. It is also the Journal's objective to promote engineering and technology education. All papers submitted to the Journal will be blind peer-reviewed. Only original articles will be published.
UTILIZATION OF SUGARCANE BAGASSE ASH AS A SUPPLEMENTARY CEMENTITIOUS MATERIAL...IAEME Publication
In developing countries, accumulation of unmanaged agricultural waste has resulted in an increased environmental concern. Recycling of such agricultural wastes is the viable solution not only to pollution problem, but also the problem of land filling. In view of utilization of agricultural waste in concrete and mortar, the present paper reviews, utilization of sugarcane bagasse ash (SCBA) in different compositions that were added to the raw material at different levels to develop
sustainable concrete and mortar. Various physico-mechanical properties of the concrete and mortar incorporating sugarcane bagasse ash are reviewed and recommendations are suggested as the outcome of the study.
Bagasse ash as a partial replacement to cement. This replacement can improve the properties of cement as well as, it reduces the effects over the environment.
Utilization of Sugarcane Bagasse Ash in Concreteijsrd.com
Utilization of industrial and agricultural waste products in the industry has been the focus of research for economic, environmental, and technical reasons. Sugar-cane bagasse is a fibrous waste-product of the sugar refining industry, along with ethanol vapour. This waste-product is already causing serious environmental pollution which calls for urgent ways of handling the waste. In this paper, Bagasse ash has been chemically and physically characterized, in order to evaluate the possibility of their use in the industry. X-ray diffractometry determination of composition and presence of crystalline material, scanning electron microscopy/EDAX examination of morphology of particles, as well as physical properties and refractoriness of bagasse ash has been studied.
Utilization Of Sugarcane Bagasse Ash (SCBA) In Concrete By Partial Replacemen...iosrjce
IOSR Journal of Mechanical and Civil Engineering (IOSR-JMCE) is a double blind peer reviewed International Journal that provides rapid publication (within a month) of articles in all areas of mechanical and civil engineering and its applications. The journal welcomes publications of high quality papers on theoretical developments and practical applications in mechanical and civil engineering. Original research papers, state-of-the-art reviews, and high quality technical notes are invited for publications.
ALTERNATE AND LOW COST CONSTRUCTION MATERIAL: RICE HUSK ASH (RHA)AM Publications
Due to pozzolanic reactivity, Rice Husk Ash is used as a supplementary cementing material in concrete. It has
economical and technical advantages to be used in concrete. I am going to replace cement by the use of RHA by 5%,10% &
15% by weight of cement in three different experiment to find out the maximum strength and compare it with the strength of
normal concrete by using the grade of M20 at the days of 7 and 14. This research therefore is an investigation of the
performance of the concrete made of partially replacing OPC with RHA on the structural integrity and properties of RHA
concrete.
A REPORT ON PARTIAL SUBSTITUTE OF CEMENT IN CONCRETE USING RICE HUSK ASHIAEME Publication
Objectives: This research work is to examine the partial replacement of cement in concrete mistreatment rice husk ash. It involved the study of strength properties of the concrete with totally different proportions of rice husk ash as partial replacement in cement. Methods: The major problem sweet-faced by the globe nowadays is that the environmental pollution. In the industry, mainly the production of cement can cause the emission of pollutants that includes a nice impact on atmosphere. This can be reduced by the magnified usage of business by-products within the industry. Findings: In this present study, to produce the concrete, Portland cement is partially substituted with Rice husk ash. Different ratios of partial replacement is done like 1/3, 5%, 10%, 15%, 20%, and 25% is taken to prepare completely different mixes. The concrete specimens are tested for their compressive strength, split tensile strength take a look at and flexural strength test at the age of seven and twenty eight days.
The Effect of Rise Husk Ash on Strength and Permeability of ConcreteAkshay D Nicator
HA, produced after burning of Rice husks (RH) has high reactivity and pozzolanic property. Indian Standard code of practice for plain and reinforced concrete, IS 456- 2000, recommends use of RHA in concrete but does not specify quantities.
Mix Design of Grade M35 by Replacement of Cement with Rice Husk Ash in ConcreteDr. Amarjeet Singh
The optimized RHA, by controlled burn or
grinding, has been used as a pozzolanic material in cement
and concrete. Using it provides several advantages, such as
improved strength and durability properties, and
environmental benefits related to the disposal of waste
materials and to reduced carbon dioxide emissions. Up to
now, little research has been done to investigate the use of
RHA as supplementary material in cement and concrete
production .The main objective of this work is to study the
suitability of the rice husk ash as a pozzolanic material for
cement replacement in concrete. However it is expected that
the use of rice husk ash in concrete improve the strength
properties of concrete. Also it is an attempt made to develop
the concrete using rice husk ash as a source material for
partial replacement of cement, which satisfies the structural
properties of concrete like compressive strength.
A COMPREHENSIVE STUDY ON PARTIAL REPLACEMENT OF CEMENT WITH SUGARCANE BAGASSE...IAEME Publication
A Large quantities of waste materials and by-products are generated from manufacturing processes, service industries and municipal solid wastes, etc. As a result, solid waste management has become one of the major environmental concerns in the world. With the increasing awareness about the environment, scarcity of land-fill space and due to its ever increasing cost, waste materials and by-products utilization has become an attractive alternative to disposal. High consumption of natural sources, high amount production of industrial wastes and environmental pollution require obtaining new solutions for a sustainable development.Ordinary Portland cement is recognized as a major construction material throughout the world.
Experimental Study On Rice Husk As Fine Aggregates In Concretetheijes
The International Journal of Engineering & Science is aimed at providing a platform for researchers, engineers, scientists, or educators to publish their original research results, to exchange new ideas, to disseminate information in innovative designs, engineering experiences and technological skills. It is also the Journal's objective to promote engineering and technology education. All papers submitted to the Journal will be blind peer-reviewed. Only original articles will be published.
UTILIZATION OF SUGARCANE BAGASSE ASH AS A SUPPLEMENTARY CEMENTITIOUS MATERIAL...IAEME Publication
In developing countries, accumulation of unmanaged agricultural waste has resulted in an increased environmental concern. Recycling of such agricultural wastes is the viable solution not only to pollution problem, but also the problem of land filling. In view of utilization of agricultural waste in concrete and mortar, the present paper reviews, utilization of sugarcane bagasse ash (SCBA) in different compositions that were added to the raw material at different levels to develop
sustainable concrete and mortar. Various physico-mechanical properties of the concrete and mortar incorporating sugarcane bagasse ash are reviewed and recommendations are suggested as the outcome of the study.
Bagasse ash as a partial replacement to cement. This replacement can improve the properties of cement as well as, it reduces the effects over the environment.
Utilization of Sugarcane Bagasse Ash in Concreteijsrd.com
Utilization of industrial and agricultural waste products in the industry has been the focus of research for economic, environmental, and technical reasons. Sugar-cane bagasse is a fibrous waste-product of the sugar refining industry, along with ethanol vapour. This waste-product is already causing serious environmental pollution which calls for urgent ways of handling the waste. In this paper, Bagasse ash has been chemically and physically characterized, in order to evaluate the possibility of their use in the industry. X-ray diffractometry determination of composition and presence of crystalline material, scanning electron microscopy/EDAX examination of morphology of particles, as well as physical properties and refractoriness of bagasse ash has been studied.
Utilization Of Sugarcane Bagasse Ash (SCBA) In Concrete By Partial Replacemen...iosrjce
IOSR Journal of Mechanical and Civil Engineering (IOSR-JMCE) is a double blind peer reviewed International Journal that provides rapid publication (within a month) of articles in all areas of mechanical and civil engineering and its applications. The journal welcomes publications of high quality papers on theoretical developments and practical applications in mechanical and civil engineering. Original research papers, state-of-the-art reviews, and high quality technical notes are invited for publications.
ALTERNATE AND LOW COST CONSTRUCTION MATERIAL: RICE HUSK ASH (RHA)AM Publications
Due to pozzolanic reactivity, Rice Husk Ash is used as a supplementary cementing material in concrete. It has
economical and technical advantages to be used in concrete. I am going to replace cement by the use of RHA by 5%,10% &
15% by weight of cement in three different experiment to find out the maximum strength and compare it with the strength of
normal concrete by using the grade of M20 at the days of 7 and 14. This research therefore is an investigation of the
performance of the concrete made of partially replacing OPC with RHA on the structural integrity and properties of RHA
concrete.
Improvement of the Index and Compaction Characteristics of Black Cotton Soil ...Dr. Amarjeet Singh
The expansive soil obtained from Baure in Yamaltu Deba Local Government Area was rich in clay mineral (montmorillonite), unstable and difficult to use for construction purposes. The soil treated with up to 12% palm kernel shell ash (PKSA an agro – waste) by weight of dry soil to improve index properties and compaction characteristics of the soil using PKSA. Index tests were carried out to classify the natural soil, while the moisture-density relationships were determined by compaction tests on the natural and treated soils using three energy levels viz, British Standard light (BSL), West African Standard (WAS) and British Standard heavy (BSH). BCS used in the study was classified as A-7-5 (20) using the American Association of State Highway and Transportation Officials (AASHTO) and CH group in the Unified Soil Classification System (USCS). Tests results show that specific gravity of the soil increased from 2.29 for the natural to 2.34 at 12% treatment. Liquid limit decreased from 76.2% for natural to 73.4% at 10% PKSA content. Plastic limit increased from 40% for the natural soil to 47.1% at 12% PKSA content treatment. Maximum dry density (MDD) values decreased from 1.44Mg/m3, 1.5Mg/m3 and 1.65Mg/m3 for the natural soil to 1.38Mg/m3 at 10%, 1.45Mg/m3 at 10% and 1.56Mg/m3 at 6% PKSA content for BSL, WAS and BSH compaction energy levels respectively. On the other hand, optimum moisture content (OMC) value decreased from 28.5% and 22.4% for the natural soil to 22.4% and 21.0% at 12% PKSA content for BSL and WAS energies respectively while the value for BSH energy increased from 18.2% to 19.0% at 8% PKSA content. Results show that PKSA is suitable for the improvement of the index properties and compaction characteristics of BCS; and its beneficial use will reduce the attendant disposal problem on the environment.
Bonding Performance of Maltodextrin and Citric Acid for Particleboard Made Fr...UniversitasGadjahMada
Maltodextrin and citric acid are two types of natural materials with the potential as an eco-friendly binder. Maltodextrin is a natural substance rich in hydroxyl groups and can form hydrogen bonds with lignoselulosic
material, while citric acid is a polycarboxylic acid which can form an ester bond with a hydroxyl group at lignoselulosic material. The combination of maltodextrin and citric acid as a natural binder materials supposed
to be increase the ester bonds formed within the particleboard. This research determined to investigate the bonding properties of a new adhesive composed of maltodextrin/citric acid for nipa frond particleboard. Maltodextrin and citric acid were dissolved in distillated water at the ratios of 100/0, 87.5/12.5, 75/25 and 0/100, and the concentration of the solution was adjusted to 50% for maltodextrin and 60% citric acid (wt%). This adhesive solution was sprayed onto the particles at 20% resin content based on the weight of oven dried particles. Particleboards with a size of 25 × 25 × 1 cm, a target density 800 kg/m3 were prepared by hot-pressing at press temperatures of 180 degrees or 200 degrees, a press time of 10 minute and board pressure 3.6 MPa. Physical and mechanical properties of particleboard were tested by a standard method (JIS A 5908). The results showed that added citric acid level in maltodextrin/citric acid composition and hot-pressing temperature had affected to the properties of particleboard. The optimum properties of the board were achieved at a pressing temperature of 180 degrees and the addition of only 20% citric acid. The results also indicated that the peak intensity of C=O group increased and OH group decreased with the addition of citric acid and an increase in the pressing temperature, suggesting an interreaction between the hydroxyl groups from the lignocellulosic materials and carboxyl groups from citric acid to form the ester groups.
Biomass resources including wood and wood wastes, agricultural residues, municipal solid waste, animal wastes, wastes from food processing and aquatic plants and algae. They are renewable resources whose utilization has received great attention due to environmental consideration and the increasing demand of energy worldwide. (Bakat et. al., 2009; Tsai et.al., 2007). Biomass can be converted to energy via tgermochemical conversion processes such as direct combustion, pyrolysis and gasification. (Pattiya Suttibak, 2012). Fast pyrolysis or rapid pyrolysis is mostly applied to biomass so as to change it to less energy- dense solid form into liquid form which called Bio-oil. It is thermal decomposition occurring in the absent of Oxygen.
In fast pyrolysis, biomass decomposes very quickly to generate mostly vapourised quickly to generate mostly vapourised and some charcoal and non- considerable gas. After cooling and condensation, a dark brown homogeneous mobile liquid is formed which has heating value about half that of conventional fuel oil. A high yield of liquid is obtained with most biomass feed low in ash. (Bridgewater, 2012).
The lightweight and eco-friendly idea came up with new concept of using fly ash as filler in polymer composites because of their low density, good dispersion, globular particles fluidity, enhanced strength, and economical perspective. The infrastructures of industries, residential buildings as well as constructional materials, and materials used in different sectors in different ways worldwide demanding satisfaction with lightweight and eco-friendly materials having good physical properties, mechanical properties such as Compressive strength, Flexural strength, Impact Strength, Tensile strength, etc. and chemical properties via Fourier-Transform infrared spectroscopy (FTIR), Scanning electron microscopic (SEM), Thermal gravimetric analysis (TGA), etc. To get better properties numerous on going researches are going on to develop new materials which would be lightweight and eco-friendly. In the same way composites became more captivating materials and encountering with the traditionally available clay/ceramic materials and their conventional counterparts due to many compelling advantages.
A test on the production of pulp and paper from
durian hides has been carried out with cooking temperature of
135 OC for a duration of 1.5 hours in a liquid of 2% : 3% : 4%
NaOH with comparison of durian hide fragment : cooking liquid
1:6. Durian hides possesses grinding level of 180 CSF, cracking
index of 0.6 kPa.m2
/gr and low tension index namely 15 Nm/gr.
The composition of the mixture of durian hide pulp (3% NaOH)
with Old Currugated Carbon (OCC) is (100%:0); (90%:10%);
(80%:20%), (70%:30%). To the grinding level of 300 ml CSF,
starch of 1% and sizing agent (AKD) 1% is added. Physical
characteristics of the paper sheet possesses gramature of 54.5
gr/m2
, thickness 0.321 mm, tensile strength 1.13 kN/m, tearing
strength 253 mN, Porosity (Bensten) 2050 ml/minute and
roughness (Bensten) 1700 ml/minute. The paper grammage had
not fulfilled basic paper specification for plastic laminated
wrapping paper, SNI 14-6519-2001.
Similar to Preparation and characterization of rice husk ash as filler material in to (20)
Preparation and characterization of rice husk ash as filler material in to
1. Chemistry and Materials Research www.iiste.org
ISSN 2224- 3224 (Print) ISSN 2225- 0956 (Online)
Vol.6 No.7, 2014
14
Preparation and Characterization of Rice Husk Ash as Filler Material in to
Nanoparticles on Hdpe Thermoplastic Composites
Eva Marlina Ginting1*
, Basuki Wirjosentono2
, Nurdin Bukit3
, Harry Agusnar4
1,3
Departement of Physics Universitas Negeri Medan, Indonesia
2,4
Departement of Chemistry Universitas Sumatera Utara, Indonesia
*
E-mail: evamarlina67@yahoo.com ; nurdinbukit5@gmail.com
Abstract
The purpose of this research is to create nano particles rice rusk ash used as a filler in thermoplastic high density
poliethylen (HDPE) and nano-mechanical properties of the resulting composites. The method of rice husk ash
made way smoothed by ball mill PM 200 for 1 hour, the filter results in a ball mill with a sieve size of 200 mesh
(74 µm), rice husk ash is dissolved in 2.5M NaOH for 4 hours and then stirred with a magnetic stirrer, then at
Ball mill for 15 hours at a rate of 450 rpm, nano rice husk ash is used as filler in HDPE thermoplastic
composition (2,4,6,8,10) wt% were blends in an internal mixer at a temperature of 150 0
C laboplastomil at a rate
of 60 rpm for 10 minutes. Nano composite mechanical properties were analyzed with Universal Testing
Mechanic. The results obtained rice husk ash silica composition of 89.6 wt%, the particle size of 50.6 nm, the
results of the mechanical properties of tensile strength and elongation at break of an increase in the composition
of the mixture 2 to 4% by weight.
Keywords : Nano Particle Rice Husk Ash , XRF, XRD, SEM, Mechanic, Analysis
1. Introduction
Waste rice husk is being very abundant in Indonesia, but its use is traditionally limited. Rice husk has now been
developed as a raw material to produce ash that is known in the world as Rice Husk Ash (RHA). RHA is one of
the raw material to produce silica. Nano silica has now applied in various fields including science and industry.
Waste rice husk is being very abundant in Indonesia is an agricultural country. During this limited use of
traditional rice husk, which is for organic materials and for burning bricks. Rice husk is an agricultural residue
from rice milling process. Central Statistics Agency reported that rice production in 2011 is estimated at 67.31
million tons of milled rice rose 895.86 thousand tons (1.35 percent) than in 2010 amounted to 66.41 million tons
of paddy. This means that Indonesia produced 13.462 tons of rice husk in 2011. Material rice husk ash has been
used as a filler material.
Silica has been widely used as catalysts, and various kinds of organic-inorganic composite materials (Sun. L et
al, 2001). In addition in the form of processed products, silica has also been used directly for purification of oil,
as an additive in pharmaceutical products and detergents, as a stationary phase in chromatography columns,
fillers and as an adsorbent polymer (Kamath and Proctor, 1998; Sun L, et al, 2001).
There has been much research on the preparation of nano silica from rice husk ash by way of synthesis, among
others, (Thuadaij.N. Et al, 2008), (Supakorn Pukird, et al, 2009), as well as (Ezzat Rafiee, et al, 2012). From the
results of previous studies have reported that approximately 20% of the weight of the rice is rice husk, and varies
from 13 to 29% of the composition husk ash which is always generated whenever the chaff burned
(Krishnarao.R, et al., 2000).
Rice husk has now been developed as a raw material to produce ash that is known in the world as RHA (Rice
Husk Ask). RHA is one of the most raw materials rich in silica containing about 90-98% silica after complete
combustion (Thuadaij, N et. al., 2008).Waste is often defined as waste material/waste materials from the
processing of agricultural products. Waste destruction process naturally progresses slowly, so that the waste does
not only interfere with the surrounding environment but also interfere with human health. At each rice mill will
always we see that the chaff pile mountains even higher and higher. Currently the use of rice husk is still very
little, so husks remain a waste material that is disturbing the environment.
The most common value content of silica (SiO2) in the rice husk ash is 94-96% and if its value is close to or
below 90% may be caused by chaff samples that have been contaminated by other substances that lower the
silica content (Prasad. CS, et al., 2001 ). Rice husk ash when burned in a controlled manner at high temperatures
(500 - 600 0
C) will produce silica ash that can be used for a variety of chemical processes.
2. Chemistry and Materials Research www.iiste.org
ISSN 2224- 3224 (Print) ISSN 2225- 0956 (Online)
Vol.6 No.7, 2014
15
The rice milling process is usually obtained about 20-30% husk, bran between 8-12% and milled rice from 50 to
63.5% between the initial weights of the data of grain. Husk with a high percentage of these can cause
environmental problems. Therefore, today a lot of rice husk ash is used as an adjunct to construction materials.
Rice husk is a biomass material such other berlignosellulosa but siliceous high. Amorphous silica is formed
when silicon is thermally oxidized. Usually the amorphous silica has a density of 2:21 g/cm3, (Harsono, 2002).
Rice husk silica in crystalline form (quartz ) and amorphous concentrated on the outer surface and a little on the
inside of the husk (Jauberthie. R, et al., 2000).
There has been much research on the preparation of nano silica from rice husk ash by way of synthesis, among
others, (Thuadaij.N. et al , 2008), particle size 50 nm was obtained, (Supakorn Pukird , et al , 2009), particle size
obtained 40 - 200 nm, as well as (Rafiee, E., et al , 2012).
Material of this nature generally have hydrophilic properties, then the material is generally not compatible with
most polymer materials. Therefore, must be chemically modified to make the surface more hidrofobis, it is
necessary for a material that is compatible with the polymer matrix , (Jacob, S., et al , 2010).
Nano-sized fillers, better known as nano filler material can be applied to the polymer nano- composite material
that results in the improvement of some of the basic properties of polymers, such as thermal resistance
properties, mechanical properties, chemical resistance and fuel properties (flammability). Preparation of polymer
composites made by combining two different materials so as to enhance the mechanical properties of the
material. The materials technology can be made in the nanoscale size, from a few studies mention that
preparation composite with nano-sized fillers can improve the mechanical properties.
Results of some studies suggest that the properties of a filler material will be compatible with the polymer
matrix, is influenced by several factors, among others, the size of the filler particles, wherein the particle size of
a small filler can improve the degree of reinforcement of polymers compared to the larger size, (Leblance, J,
2002), as well as the smaller the particle size the higher the bonding between the filler with the polymer matrix,
(Khols J, et al, 2002), the amount of surface area can be increased by the presence of a porous surface on the
surface of the filler as well as with the addition of nano can improve the thermal and mechanical properties of
nano-composites, (Bukit.N, 2012), as well as with adding bentonite nano filer on HDPE (Bukit. N, et al, 2013).
Nano CaCO3 to HDPE, (Zebarjad, S. M, et, al. 2006), nano carbon with HDPE, (Fouad, H., et al, 2011).
The use of rice husk ash in the composite can provide several advantages such as increased strength and
endurance, reduce the cost of materials, reducing the environmental impact of waste materials, and reduce CO2
emissions.
The use of silica in the composite layer can enhance the material properties (changes in cationic capacity, high
surface broad, large aspect ratio), (Tjong, 2006), (Utracki, 2007), is essential to improve the physical and
mechanical properties, strength tensile, modulus tensile, flexural strength, thermal stability, thermal properties,
for some thermoset nanocomposite thermoplastic material and the amount of silica filler is not too much, (Koo,
et. al, 2002; Wu, et. al, 2007; Lei, et. al, 2007; Kord, et. al, 2010; Samal, et. Al, 2008).
In this study the process of making nano-particles made of rice husk ash making process that results from the
burning of white rice husk in rice plant then milled with a ball mill for one hours, then filtered with a 200 mesh
size, equivalent to 74 µm then soaking with a solution 2.5 N NaOH for 4 hours preparation results do the ball
mill for 15 hours at a rate of 450 rpm to obtain nano-meter size is used as a filler in thermoplastic HDPE.
2. Experimental
2.1 Matrials and Methods
Materials used in the study of rice husk ash, Copolimer HDPE Production of PT Titan Petrokimia Nusantara
Indonesia, melting temperature of 136°C, density 0.941 g/cm3, filter paper, Polietilene grafted Maleic
Anhidride (PE-g-MA) production sigma aldrich USA, NaOH.
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2.2 Instrumentation
Internal Mixer Laboplastomil Model 30 R150, Hydraulic Hot Press, Cold Press of 37 ton from Genno Japan,
Universal Testing Mechanic (UTM), X- Ray Difraction (XRD), Scanning Electron Microscop (SEM), X-Ray
Flurosensi (XRF).
2.3 Nano Particles Preparation Process Rice Husk Ash
The procedure of this study conducted by rice husk ash white color from the burning of the rice plant, is
processed with rice husk ash manner in ball mill, for 1 hour, strain the results in the ball mill with a sieve size of
200 mesh (74 µm), the ash dissolved in 2.5M NaOH for 4 hours and then stirred with a magnetic stirrer, after
filtering with filter paper and vacum pump, the residue was washed with distilled water hasi then the rice husk
ash in the warm up with a 1000
C oven for 2 hours, method (Dominic, M., et al .2013), rice husk ash, the results
of treatment are both included in a planetary ball mill P 200 for 15 hours at a rate of 450 rpm, according to the
method (Bukit. N et al 2013); (Nikmatin. S, 2013).
2.4 Blends of HDPE-PE-g-MA / Nano Particle Rice Husk Ash
HDPE-rice husk ash composites were prepared by mixing HDPE, nano Particle rice husk ash and PE-g-MA,
with the composition as presented in Table 1. The mixture was placed in the internal mixer laboplastomill, and
mixed at a temperature of 150°C, which is the melting point of HDPE, at a rate of 60 rpm for 10 minutes.
Table. 1 Composition Blends HDPE /Nano Particle Rice Husk Ash
With Compatibelizer PE-g-MA in Internal Mixer
Materials Blends Composition ( wt %)
HDPE Sabsp.1 S absp.2 S absp.3 S absp.4 S absp.5
HDPE 100 95 93 91 89 87
PE-g-MA 0 3 3 3 3 3
Nano Particle
Rice Ash
0 2 4 6 8 10
2.5 Mechanical Properties Measurement
Tensile strength measurement was performed according to JIS K 6781 standard using Universal Testing
Machine, at crosshead speed of 50 mm min-1
. Young’s modulus (E), ultimate tensile strength (σmax), and
elongation at break (εb) were determined from the stress-strain curves.
2.6. X-Ray Difraction (XRD) Analysis.
The XRD analysis was conducted at room temperature using X-ray difractometer type Shimadzu XRD 6000.
The operating conditions used were CuKλ radiation (λ = 0.15418 Å, produced at 40 kV and 30 mA). Pattern was
recorded over goniometer (2θ) ranging from 5°
to 60°
. The interlayer distance of rice ash in nanocomposite was
derived from the peak position (d001 = reflection) in XRD diffractograms according to the Bragg equation: d = λ
/2sin θ.
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3.Result and Discussion
3.1 Analysis Composition Rice Husk Ash
Table 2. Rice Husk Ash XRF Synthesis with Solutions NaOH
Components Composition (%wt)
SiO2 89,49
MgO 3,84
P2O5 2,19
CaO 1,08
Al2O3 1,07
Fe2O3 0,72
K2O 0,52
Cl 0,34
MnO 0,30
SO3 0,26
Cr2O3 0,06
ZnO 0,06
MnO 0,04
3.2. Analisys XRD Rice Husk Ash
From the results of X-ray Diffraction seen rice husk ash has shown this is due to the crystal pattern combustion
temperatures reached above 9000
C seen from Figure 1 the diffraction patterns did not differn significantly, but
there is a shift in the peak of the diffraction peaks in the preparation of rice husk ash before seen the peak
maximum at 21.8779 with 2 theta angles , spacing distance d = 4.05928Å and FWHM = 0.26180 and 4784 while
the peak intensity after the preparation process of dissolution with NaOH and Ball mill for 15 hours maximum
peak at 2 theta angles 21.8748 at a distance d = 4.05984 Å and FWHM = 0.27420, and the peak intensity of
4451. This shows the difference FWHM rice husk ash particles get smaller. In Table 3. Shows the maximum
difference between the three peaks of pure rice husk ash with rice husk ash dissolved with NaOH and the ball
mill for 15 hours. Crystalline sample size was calculated by Scherrer method analysis of x-ray diffraction
pattern.
With Br, K, λ and D, respectively half peak width (FWHM) in radians, Scherrer constant (0.9), x-rays
wavelength (1.5406 Å), and the crystal diameter (nm). From the XRD data using the equation obtained Scerrer
rice husk ash particle size after ball mill for 15 hours at a rate of 450 rpm gained an average of 50.6 nm.
Table 3. Three Largest Difference Peaks of the XRD Results from Rice Husk Ash
Material 1 Theta
(deg)
d (Å) I/I1 FWHM(deg) Intensity(Counts)
Rice Husk Ash
Micro Size
Rice Husk Ash
Nano Size
21.8779 4.05928 100 0.26180 4784
36.0582 2.48885 16 0.26360 771
20.6000 4.30811 10 0.33480 500
21.8748 4.05984 100 0.27420 4451
36.0545 2.48910 16 0.28220 690
31.3507 2.85100 8 0.30750 335
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Figure 1. X-Ray Difraction Rice Husk Ash Micro and Nano Size
Figure 2. Diffraction patterns dhkl Rice Husk Ash Nano
From the analysis of X-ray Diffraction nano rice husk ash obtained maximum peak d hkl 0 01 with d spacing
3.1274 Å while the d hkl 0 12 d spacing 2.1593 with densities 3.2500 g/cm³ type Quartz crystal with cell
parameters a = 4.5350 Å c = 5.1700 Å system hexagonal crystal.
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3.3 Analysis Morphology Rice Husk Ash
Figure 3. Morphology Rice Husk Ash Figure 4. Morphology Rice Husk Ash
Ball Mill 1 hours with NaOH
Figure 5. Morphology Rice Rusk Ash Nano Particle Ball Mill 15 hours with NaOH
3.4 Mechanical Characteristics.
In this study, mechanical properties of the samples include tensile strength, elongation at break, and Young’s
modulus, are measured in order to evaluate of nano Particle rice rusk ash Table 4. On Figure 6 until 8 shows the
tensile strengths, elongation at break and Young’s Modulus of the samples filled with nano particle rice rusk ash
with PE-g-MA .
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Figure 7. Elongation at Break of the Samples Filler Rice Rusk Ash Nano
Figure 8. Young,s Modulus of the Samples Filler Rice Rusk Ash Nano
From the data on the mechanical properties of tensile strength increased compared to pure HDPE nano-particles
in a mixture of rice husk ash with compatibilizer PE-g-MA on the composition of 2% to 4% and a decrease in
maximum tensile strength at 6 to 10%, this is because clumping occurs at a certain composition of rice husk ash,
thereby reducing the tensile strength of this can be seen from the results of morphological, as well as the
elongation at break and Young's modulus decreased with increasing nano rice husk ash. The increase in tensile
strength due to an increase in covalent bonding and hydrogen bonding with the OH group and the oxygen of
each of the goup carboxil add bonding between the filler with the matrix which is in line with studies (Bhat, et.
al, 2011) .Improved mechanical properties depend on many factors including the aspect ratio of the filler
material, the degree disperse and orientation in the matrix, and adhesion at the interface matrix – filler.
The particle size is small filler increases the degree of polymer reinforcement versus large particle size (Leblanc,
2002). Particle size has a direct relationship to the surface area of the filler material. Thus, the small particle size
provides a large surface area for interaction between the polymer matrix and filler so improve reinforcement of
polymeric materials.
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This is probably due to the silicate layer of rice husk ash can be dispersed nanometer-sized randomly and evenly
providing exfoliation in nanocomposite structure. Silicate layers that exist on rice husk ash scattered individuals
have extensive contacts a large surface that can bind strongly to the HDPE matrix which further gives effect to
the increase in tensile strength. The incorporation of rice husk ash with nano compatibilizer PE-g-MA is more
than 6% wt contrary negative effects which would lower the tensile strength. This is probably due to the decrease
in the degree of spread of exfoliation of silicate layers in the nanocomposite rice husk ash with nano-particle
content of rice husk ash high (> 6 wt%). In addition, the nano-particle agglomeration rice husk ash as shown in
the SEM image also led to a decrease in tensile strength. Rice husk ash agglomeration is believed to be a stress
concentration and the beginning of the crack so that the power will go down. The same thing from the study
(Kusmono, et. al, 2010).
This is due to the increasing number of content of silica resulted in a drop in tensile strength, which is in line
with the research, (Koo, et. al, 2002; Wu, et. al, 2007; Lei, et. al, 2007; Kord, et. al, 2010; Samal, et. al 2008).
Figure 9 morphology of HDPE with a mixture of rice husk ash nano on the composition of 2 to 10% by weight,
the greater the visible content of silica, there will be algomerat which in turn reduces the tensile strength and
elongation at breaks.
a b
c d
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Figure 9. Morphology HDPE/PE-g- MA/Rice Rusk Ash Nano Blends (a) (2 wt%); (b) (4 wt%); (c) (6 wt );
(d) (8 wt%); (e) (10 wt%); (f) (HDPE)
4. Conclusion
The results obtained rice husk ash silica composition of 89.6 wt%, the particle size of 50.6 nm, analysis of X-ray
Diffraction nano rice husk ash obtained densities 3.2500 g/cm³ type Quartz crystal with cell parameters a =
4.5350 Å c = 5.1700 Å system hexagonal crystal. The results of the mechanical properties of tensile strength and
elongation at break of an increase in the composition of the mixture 2 to 4% by weight.
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