Presentation by Matthias Mersmann, General Manager Business Development New Products at LOESCHE GmbH, during the LOESCHE Symposium in Hanoi, Vietnam, in August 22, 2018.
A TEC Rocket Mill® at Wietersdorfer & Peggauer Cement, Austria, Case Study.
- Presented by Dr Stefan Kern at the LOESCHE Symposium in Hanoi, Vietnam. August 22, 2018.
Pyrolysis is a thermochemical treatment, which can be applied to any organic (carbon-based) product. It can be done on pure products as well as mixtures. In this treatment, material is exposed to high temperature, and in the absence of oxygen goes through chemical and physical separation into different molecules.
Theory of Carbon Formation in Steam Reforming
Contents
1 Introduction
2 Underpinning Theory
2.1 Conceptualization
2.2 Reforming Reactions
2.3 Carbon Formation Chemistry
2.3.1 Natural Gas
2.3.2 Carbon Formation for Naphtha Feeds
2.3.3 Carbon Gasification
2.4 Heat Transfer
3 Causes
3.1 Effects of Carbon Formation
3.2 Types of Carbon
4 What are the Effects of Carbon Formation?
4.1 Why does Carbon Formation Get Worse?
4.1.1 So what is the Next Step?
4.2 Consequences of Carbon Formation
4.3 Why does Carbon Form where it does?
4.3.1 Effect on Process Gas Temperature
4.4 Why does Carbon Formation Propagate Down the Tube?
4.4.1 Effect on Radiation on the Fluegas Side
4.5 Why does Carbon Formation propagate Up the Tube?
5 How do we Prevent Carbon Formation
5.1 The Role of Potash
5.2 Inclusion of Pre-reformer
5.3 Primary Reformer Catalyst Parameters
5.3.1 Activity
5.3.2 Heat Transfer
5.3.3 Increased Steam to Carbon Ratio
6 Steam Out
6.1 Why does increasing the Steam to Carbon Ratio Not Work?
6.2 Why does reducing the Feed Rate not help?
6.3 Fundamental Principles of Steam Outs
TABLES
1 Heat Transfer Coefficients in a Typical Reformer
2 Typical Catalyst Loading Options
FIGURES
1 Hot Bands
2 Conceptual Pellet
3 Naphtha Carbon Formation
4 Heat Transfer within an Reformer
5 Types of Carbon Formation
6 Effect of Carbon on Nickel Crystallites
7 Absorption of Heat
8 Comparison of "Base Case" v Carbon Forming Tube
9 Carbon Formation Vicious Circle
10 Temperature Profiles
11 Carbon Pinch Point
12 Carbon Formation
13 Effect on Process Gas Temperature
14 How does Carbon Propagate into an Unaffected Zone?
15 Movement of the Carbon Forming Region
16 Effect of Hot Bands on Radiative Heat Transfer
17 Effect of Potash on Carbon Formation
18 Application of a Pre-reformer
19 Effect of Activity on Carbon Formation
GE / Texaco Gasifier Feed to a Lurgi Methanol Plant and its Effect on Methano...Gerard B. Hawkins
GE / Texaco Gasifier Feed to a Lurgi Methanol Plant and its Effect on Methanol Production
CONTENTS
0 Methanol Synthesis Introduction
1 Executive Summary
2 Design Basis
2.1.1 Train I Design Basis
2.1.2 Train II Design Basis
2.1.3 Train III Design Basis
2.2 Design Philosophy
2.2.1 Operability Review
2.3 Assumptions
2.4 Train IV Flowsheet
2.4.1 CO2 Removal
3 Discussion
3.1 Natural Gas Consumption Figures
3.1.1 Base Case
3.1.2 Case 1 – Coal Gasification in Service
3.1.3 Case 2 – Coal Gasification in Service – No CO2 Export
3.2 Methanol Production Figures
3.2.1 Base Case
3.2.2 Case 1 – Coal Gasification in Service
3.2.3 Case 2 – Coal Gasification in Service – No CO2 Export
3.3 85% Natural Gas Availability
3.4 100% Natural Gas Availability
3.5 CO2 Emissions
3.5.1 Base Case
3.5.2 Case 1 – Coal Gasification in Service
3.5.3 Case 2 – Coal Gasification in Service – No CO2 Export
3.6 Specific Consumption Figures
3.6.1 Base Case
3.6.2 Case 1 – Coal Gasification and CO2 Import
3.6.3 Case 2 – Coal Gasification and No CO2 Import
3.7 Train IV Synthesis Gas Composition
4 Further Work
5 Conclusion
APPENDIX
Important Stream Data – Material Balance Stream Data
Texaco Gasifier with HP Steam Raising Boiler
CHARACTERISTICS OF COAL
Material Balance Considerations
A TEC Rocket Mill® at Wietersdorfer & Peggauer Cement, Austria, Case Study.
- Presented by Dr Stefan Kern at the LOESCHE Symposium in Hanoi, Vietnam. August 22, 2018.
Pyrolysis is a thermochemical treatment, which can be applied to any organic (carbon-based) product. It can be done on pure products as well as mixtures. In this treatment, material is exposed to high temperature, and in the absence of oxygen goes through chemical and physical separation into different molecules.
Theory of Carbon Formation in Steam Reforming
Contents
1 Introduction
2 Underpinning Theory
2.1 Conceptualization
2.2 Reforming Reactions
2.3 Carbon Formation Chemistry
2.3.1 Natural Gas
2.3.2 Carbon Formation for Naphtha Feeds
2.3.3 Carbon Gasification
2.4 Heat Transfer
3 Causes
3.1 Effects of Carbon Formation
3.2 Types of Carbon
4 What are the Effects of Carbon Formation?
4.1 Why does Carbon Formation Get Worse?
4.1.1 So what is the Next Step?
4.2 Consequences of Carbon Formation
4.3 Why does Carbon Form where it does?
4.3.1 Effect on Process Gas Temperature
4.4 Why does Carbon Formation Propagate Down the Tube?
4.4.1 Effect on Radiation on the Fluegas Side
4.5 Why does Carbon Formation propagate Up the Tube?
5 How do we Prevent Carbon Formation
5.1 The Role of Potash
5.2 Inclusion of Pre-reformer
5.3 Primary Reformer Catalyst Parameters
5.3.1 Activity
5.3.2 Heat Transfer
5.3.3 Increased Steam to Carbon Ratio
6 Steam Out
6.1 Why does increasing the Steam to Carbon Ratio Not Work?
6.2 Why does reducing the Feed Rate not help?
6.3 Fundamental Principles of Steam Outs
TABLES
1 Heat Transfer Coefficients in a Typical Reformer
2 Typical Catalyst Loading Options
FIGURES
1 Hot Bands
2 Conceptual Pellet
3 Naphtha Carbon Formation
4 Heat Transfer within an Reformer
5 Types of Carbon Formation
6 Effect of Carbon on Nickel Crystallites
7 Absorption of Heat
8 Comparison of "Base Case" v Carbon Forming Tube
9 Carbon Formation Vicious Circle
10 Temperature Profiles
11 Carbon Pinch Point
12 Carbon Formation
13 Effect on Process Gas Temperature
14 How does Carbon Propagate into an Unaffected Zone?
15 Movement of the Carbon Forming Region
16 Effect of Hot Bands on Radiative Heat Transfer
17 Effect of Potash on Carbon Formation
18 Application of a Pre-reformer
19 Effect of Activity on Carbon Formation
GE / Texaco Gasifier Feed to a Lurgi Methanol Plant and its Effect on Methano...Gerard B. Hawkins
GE / Texaco Gasifier Feed to a Lurgi Methanol Plant and its Effect on Methanol Production
CONTENTS
0 Methanol Synthesis Introduction
1 Executive Summary
2 Design Basis
2.1.1 Train I Design Basis
2.1.2 Train II Design Basis
2.1.3 Train III Design Basis
2.2 Design Philosophy
2.2.1 Operability Review
2.3 Assumptions
2.4 Train IV Flowsheet
2.4.1 CO2 Removal
3 Discussion
3.1 Natural Gas Consumption Figures
3.1.1 Base Case
3.1.2 Case 1 – Coal Gasification in Service
3.1.3 Case 2 – Coal Gasification in Service – No CO2 Export
3.2 Methanol Production Figures
3.2.1 Base Case
3.2.2 Case 1 – Coal Gasification in Service
3.2.3 Case 2 – Coal Gasification in Service – No CO2 Export
3.3 85% Natural Gas Availability
3.4 100% Natural Gas Availability
3.5 CO2 Emissions
3.5.1 Base Case
3.5.2 Case 1 – Coal Gasification in Service
3.5.3 Case 2 – Coal Gasification in Service – No CO2 Export
3.6 Specific Consumption Figures
3.6.1 Base Case
3.6.2 Case 1 – Coal Gasification and CO2 Import
3.6.3 Case 2 – Coal Gasification and No CO2 Import
3.7 Train IV Synthesis Gas Composition
4 Further Work
5 Conclusion
APPENDIX
Important Stream Data – Material Balance Stream Data
Texaco Gasifier with HP Steam Raising Boiler
CHARACTERISTICS OF COAL
Material Balance Considerations
Caldera inteligente: optimización de la combustión y reducción de emisionesAVEBIOM
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The weakness of reservoir simulations is the lack of quantity and quality of the required input; their strength is the ability to vary one parameter at a time. Therefore, reservoir simulations are an appropriate tool to evaluate relative uncertainty but absolute forecasts can be misleading, leading to poor business decisions. As recovery processes increase in complexity, the impact of such decisions may have a major impact on the project viability. A responsible use of reservoir simulations is discussed, addressing both technical users and decision makers. The danger of creating a false confidence in forecasts and the value of simulating complex processes are demonstrated with examples. This is a call for the return of the reservoir engineer who is in control of the simulations and not controlled by them, and the decision maker who appreciates a black & white graph of a forecast with realistic uncertainties over a 3-D hologram in colour.
An exclusive, in-depth look at the latest natural refrigerants-based technology trends in different applications around the globe with Prof. Dr.-Ing. Armin Hafner, NTNU (Norwegian University of Science and Technology).
The weakness of reservoir simulations is the lack of quantity and quality of the required input; their strength is the ability to vary one parameter at a time. Therefore, reservoir simulations are an appropriate tool to evaluate relative uncertainty but absolute forecasts can be misleading, leading to poor business decisions. As recovery processes increase in complexity, the impact of such decisions may have a major impact on the project viability. A responsible use of reservoir simulations is discussed, addressing both technical users and decision makers. The danger of creating a false confidence in forecasts and the value of simulating complex processes are demonstrated with examples. This is a call for the return of the reservoir engineer who is in control of the simulations and not controlled by them, and the decision maker who appreciates a black & white graph of a forecast with realistic uncertainties over a 3-D hologram in colour.
The Support Scheme for Renewable Heat is a government funded initiative. It is designed to increase the energy generated from renewable sources in the heat sector.
The scheme is open to:
commercial,
industrial,
agricultural,
district heating,
public sector
and other non-domestic heat users not covered by the emissions trading system.
This scheme will contribute to meeting Ireland’s renewable energy targets. It will also reduce greenhouse gas emissions.
The government funded scheme offers two alternative support options;
a grant for heat pump systems, or
ongoing operational aid for biomass or biogas heating systems
This workshop will explain the SSRH, how it could work for you and how to apply to SEAI for support. It will also allow time for questions and discussion on any aspect of the scheme. The workshop is relevant to any non-domestic fossil fuel user and any business in the renewable heat supply chain.
IMPROVEMENT OF PRODUCTIVITY AND QUALITY IN THE WIND ENERGY INDUSTRY THROUGH THE USE OF AN ADVANCED SENSOR SYSTEM , presented at SAMPE-Europe Conference 2017,
Stuttgart, November 15th 2017
Creatnet Technology is at the forefront of the Emulsified Fuel Revolution in the India. Using Technology developed by RADE Initiative, we are now servicing various industries by providing them with Emulsified Fuel Oil and providing on-site Fuel Emulsification services to large consumers.
Representing Industrial decarbonization Options in TIMES Belgium modelIEA-ETSAP
Representing Industrial decarbonization Options in TIMES Belgium model
Dr. Partha Das, VITO NV (The Flemish institute for technological research), Belgium.
The cement industry is worldwide one of the main contributors to man-made CO2 emissions, estimated at 7% of global emissions.
To keep pace with the demand and pressure to reduce CO2 emissions, a shift to sustainable building materials for housing and infrastructure must still be continued.
Cement manufacturers can make significant progress toward sustainability goals with alternative fuels and efficiency projects by reducing clinker content through cementitious additives (SCM).
Alternative Fuel Market After Covid-19 – Focus on Efficiency and QualityLOESCHE
Covid-19 has changed the way people interact with each other and the way business is done. Now is the time to change the paradigm regarding alternative fuel projects towards a more holistic approach in order to ensure investment efficiency. Simple and cheap (at first) shall give way to smart, flexible, and sustainable concepts. Suppliers shall give way to partners.
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Presentación realizada por Morten Gotlieb, Jefe sección Biomasa y Tecnología Combustión en el Instituto Tecnológico Danés, en el 11 Congreso Internacional de Bioenergía "Bioenergía 4.0: Retos y Oportunidades" www.congresobioenergia.org
The weakness of reservoir simulations is the lack of quantity and quality of the required input; their strength is the ability to vary one parameter at a time. Therefore, reservoir simulations are an appropriate tool to evaluate relative uncertainty but absolute forecasts can be misleading, leading to poor business decisions. As recovery processes increase in complexity, the impact of such decisions may have a major impact on the project viability. A responsible use of reservoir simulations is discussed, addressing both technical users and decision makers. The danger of creating a false confidence in forecasts and the value of simulating complex processes are demonstrated with examples. This is a call for the return of the reservoir engineer who is in control of the simulations and not controlled by them, and the decision maker who appreciates a black & white graph of a forecast with realistic uncertainties over a 3-D hologram in colour.
An exclusive, in-depth look at the latest natural refrigerants-based technology trends in different applications around the globe with Prof. Dr.-Ing. Armin Hafner, NTNU (Norwegian University of Science and Technology).
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district heating,
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and other non-domestic heat users not covered by the emissions trading system.
This scheme will contribute to meeting Ireland’s renewable energy targets. It will also reduce greenhouse gas emissions.
The government funded scheme offers two alternative support options;
a grant for heat pump systems, or
ongoing operational aid for biomass or biogas heating systems
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Stuttgart, November 15th 2017
Creatnet Technology is at the forefront of the Emulsified Fuel Revolution in the India. Using Technology developed by RADE Initiative, we are now servicing various industries by providing them with Emulsified Fuel Oil and providing on-site Fuel Emulsification services to large consumers.
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Optimal Alternative Fuel Burning Starts with Computer Simulation
1. Optimal Alternative Fuel Burning Starts With
Computer Simulation
Matthias Mersmann, 22nd August 2018
2. LOESCHE Symposium Hanoi 2018 22.08.2018
Optimal alternative fuel burning
starts with computer simulation
What happens if…
Why alternative fuels change the production process
What needs to be done to get it right
How to optimize the process for alternative fuel firing
01
04
03
02
3. LOESCHE Symposium Hanoi 2018 22.08.2018
Optimal alternative fuel burning starts with computer
simulation
3
What
Happens
if…
▪ … you have signed contracts to get the waste streams to burn alternative
fuels.
▪ … you have set up and invested in the logistics to get the waste to your plant.
▪ … you have worked for years to get the permissions to burn alternative fuel.
▪ … you have invested in new equipment to process the waste to fuel.
▪ … you have invested in pyro-process equipment to burn the alternative fuel.
4. LOESCHE Symposium Hanoi 2018 22.08.2018
Optimal alternative fuel burning starts with computer
simulation
4
And
then …
▪ … your kiln production goes down.
▪ … your kiln availability goes down.
▪ … you can burn only half the alternative fuel as you have planned for.
▪ … make sure your plant delivers what your have in mind!
▪ … make sure you master the process!
5. LOESCHE Symposium Hanoi 2018 22.08.2018
Optimal alternative fuel burning starts with computer
simulation
5
Make
sure
to…
▪ … understand what is happening during AF combustion.
▪ … transfer the complexity of the process into simulation models.
▪ … optimize the design of equipment & process prior to installation.
▪ … rely on aixergee‘s ‘Real-Physics’ Virtual Reality models.
6. LOESCHE Symposium Hanoi 2018 22.08.2018
Optimal alternative fuel burning starts with computer
simulation
6
▪ Transfer of the real plant into virtual reality
▪ ‘Look inside the running process’
▪ Evaluate ALL process parameters:
− Gas flows
− Particle movement
− Temperatures
− Burnout
− Calcination
▪ …
▪ Optimize on the basis of knowledge
7. LOESCHE Symposium Hanoi 2018 22.08.2018
Optimal alternative fuel burning
starts with computer simulation
What happens if…
Why alternative fuels change the production process
What needs to be done to get it right
How to optimize the process for alternative fuel firing
01
04
03
02
8. LOESCHE Symposium Hanoi 2018 22.08.2018
Why alternative fuels change the production process
8
Do you see the difference?
Noble fuels (primary
fuels) are produced
with the objective be
used as fuels. They
are finely ground and
optimized for being
fired.
Alternative fuels
(secondary fuels) are
made of wasted
material which was
not intended to be
fired initially. They are
processed to be able
to be burned.
They differ in:
▪ Combustion
properties
▪ Pneumatic
properties
Noble(primary)fuels Alternative(secondary)fuels
9. LOESCHE Symposium Hanoi 2018 22.08.2018
Why alternative fuels change the production process
9
Pneumatic behavior of secondary fuels
10. LOESCHE Symposium Hanoi 2018 22.08.2018
Why alternative fuels change the production process
10
Combustion of noble fuels
Noble fuels (primary fuels) are produced with the
objective be used as fuels. They are finely ground
and optimized for being fired.
▪ Coal dust ignites spontaneously
▪ Coal dust burns with a short stiff flame
11. LOESCHE Symposium Hanoi 2018 22.08.2018
Why alternative fuels change the production process
11
Combustion of secondary fuels
Alternative fuels (secondary fuels) are made of
wasted material which was not intended to be fired
initially. They are processed to be able to be burned.
▪ Lumpy particles fall or fly.
▪ It takes long to ignite the AF particles.
▪ It takes long to burn out the AF-particles.
12. LOESCHE Symposium Hanoi 2018 22.08.2018
Optimal alternative fuel burning starts with computer
simulation
12
▪ Transfer of the real plant into virtual reality
▪ ‘Look inside the running process’
▪ Evaluate ALL process parameters:
− Gas flows
− Particle movement
− Temperatures
− Burnout
− Calcination
▪ …
▪ Optimize on the basis of knowledge
13. LOESCHE Symposium Hanoi 2018 22.08.2018
Why alternative fuels change the production process
13
The production process of cement clinker is depending on energy induction at specific locations.
▪ The sintering zone needs a stiff flame of limited length.
▪ The calciner needs a heat release within the riser duct and sufficient burnout without drop out.
Secondary fuels must be prepared appropriately.
▪ Small particles and high specific surface for fast ignition
The plant equipment must be adapted appropriately.
▪ Burners and calciners must allow sufficient retention time for the particles, transport and burn-out.
Alternativefuels flowand burndifferently
14. LOESCHE Symposium Hanoi 2018 22.08.2018
Optimal alternative fuel burning
starts with computer simulation
What happens if…
Why alternative fuels change the production process
What needs to be done to get it right
How to optimize the process for alternative fuel firing
01
04
03
02
15. LOESCHE Symposium Hanoi 2018 22.08.2018
What needs to be done to get it right
15
Kiln burner
Challenge:
▪ Short flight time of particles
▪ Insufficient oxygen availability in
the center of the flame
Solution:
▪ Fine ground RDF (Rocket Mill®)
▪ Specific burner
− Flexiflame ECOPRO
− Satellite burner
RDF
through
central
pipe
RDF
through
satellite
burner
16. LOESCHE Symposium Hanoi 2018 22.08.2018
What needs to be done to get it right
16
Kiln burner simulation features
aixergee ‘Real Physics’ simulation
▪ Full heat transfer (radiation,
convection, conduction)
▪ Fully coupled impulse transfer
▪ Full combustion model
▪ Lumpy & shaped particle flow
▪ Heat transfer into clinker bed
▪ Mineralization of material bed
▪ Ultrasonic flow at burner tip
▪ NOx model
▪ …
RDF flame contribution
Coal flame contribution
RDF trajectories colored by particle size [m] Oxygen concentration profile [m³/m³]
17. LOESCHE Symposium Hanoi 2018 22.08.2018
What needs to be done to get it right
17
Calciner
Challenge:
▪ Keep the lumpy secondary fuel particles in
suspension until they burn out
▪ Drop out fuel is lost and creates problems
in the kiln
Solution:
▪ Find the best injection point
▪ Design the calciner geometry appropriately
Bad fuel suspension: Good fuel suspension:
18. LOESCHE Symposium Hanoi 2018 22.08.2018
What needs to be done to get it right
18
Calciner simulation features
aixergee ‘Real Physics’
simulation
▪ Full heat transfer (radiation,
convection, conduction)
▪ Fully coupled impulse transfer
▪ Full combustion model
▪ Lumpy & shaped particle flow
▪ Individual particle
identification
▪ calcination
▪ NOx model
▪ …
RDF (pelletized & partially desagglomerated):
1 Cylinder dense
2 Ball dense
3 Ball med. dense
4 Flat thick dense fluff
5 Flat fluff
6 Flat thin light fluff
19. LOESCHE Symposium Hanoi 2018 22.08.2018
What needs to be done to get it right
19
Calciner simulation features
goodbad
aixergee ‘Real Physics’ Simulation
▪ Full heat transfer (radiation,
convection, conduction)
▪ Fully coupled impulse transfer
▪ Full combustion model
▪ Lumpy & shaped particle flow
▪ Individual particle identification
▪ calcination
▪ NOx model
▪ …
20. LOESCHE Symposium Hanoi 2018 22.08.2018
Optimal alternative fuel burning
starts with computer simulation
What happens if…
Why alternative fuels change the production process
What needs to be done to get it right
How to optimize the process for alternative fuel firing
01
04
03
02
21. LOESCHE Symposium Hanoi 2018 22.08.2018
How to optimize the process for alternative fuel firing
21
▪ Cement plant equipment is originally designed for noble fuel combustion.
▪ As alternative fuels differ extremely in flow and combustion behavior, the equipment needs to be adapted.
▪ Adaptation must be based on understanding how the alternative fuel behaves in the process.
▪ Computer simulation is the only method to investigate and predict this behavior.
▪ Design should be based on these findings and not on simple guessing!
▪ aixergee commands on computer models which have proven their realistic prediction in > 250 projects.
Knowingwhat to doinstead of expensive guessing
22. LOESCHE Symposium Hanoi 2018 22.08.2018
How to optimize the process for alternative fuel firing
22
Design process from general understanding to the perfect plant equipment
AF specification
Physical and
chemical
parameters
Simulation of the PRocess
Realistic prediction and
general design of the
equipment
Plantdesign and engineering
Transfer of general design into
steel and machines
Planttechnology
Existing equipment
or new design
23. LOESCHE Symposium Hanoi 2018 22.08.2018
How to optimize the process for alternative fuel firing
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Example: Calciner modification Aalborg Cement
SLC Calciner with massive problems in
pneumatic transport stability
▪ Cyclical loading and unloading of meal clouds
(mass fluctuation +/- 20%!)
▪ Fall through of meal into the tertiary air duct
▪ Disturbance of combustion and calcination
process
▪ Limitation of AF-firing rate
▪ Occasional CO-peaks indicating AF-firing
overload
24. LOESCHE Symposium Hanoi 2018 22.08.2018
How to optimize the process for alternative fuel firing
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Example: Calciner modification Aalborg Cement
Steeper cone Steeper cone
− Slim shaft
Steeper cone
− Slim shaft
− Elongation
− Mixing chamber
Retrofit proposals
25. LOESCHE Symposium Hanoi 2018 22.08.2018
How to optimize the process for alternative fuel firing
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Example: Calciner modification Aalborg Cement
Prove of improvement by computer
simulation
▪ Modified calciner
▪ Increase of production rate from 4500
t/d to 4700 t/d
▪ AF-firing 100 % TSR
▪ Much more constant combustion
process
▪ Much less CO as a proof for better
combustion despite higher firing rate
CO generation ‘modified’CO generation ‘As is’
26. LOESCHE Symposium Hanoi 2018 22.08.2018
How to optimize the process for alternative fuel firing
26
LOESCHE can supply everything out of one hand!
Your
alternative fuel
project
your AF
designs your
winning process
provides
tailor-made
engineering &
supply
ensures reliable
partnership
Your success
27. THANK YOU
for your attention
A company of
LOESCHE Group
Hansaallee 243
D-40549 Düsseldorf
Tel.: +49 211 5353 - 0
Email: loesche@loesche.de