This document provides an overview of chemical engineering plant design. It discusses key aspects of the design process including general considerations, optimization, cost estimation, and factors affecting profitability. The document also outlines the stages of a typical plant design project and describes standards and guidelines for plant layout and piping design provided by organizations like ASME, CCPS, OSHA and NFPA. Skills needed for successful plant design include research, cost analysis, computer programming, and surveying.
Design and Simulation of Continuous Distillation ColumnsGerard B. Hawkins
Design and Simulation of Continuous Distillation Columns
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 FRACTIONAL DISTILLATION
5 ROUGH METHOD OF COLUMN DESIGN
5.1 Sharp Separations
5.2 Sloppy Separations
6 DETAIL DESIGN USING THE CHEMCAD DISTILLATION PROGRAM
6.1 Sharp Separations
6.2 Sloppy Separations
7 COMPLEX COLUMNS
7.1 Multiple Feeds
7.2 Sidestream Take-Offs
8 DESIGN USING A LABORATORY COLUMN
SIMULATION
9 DESIGN USING ACTUAL PLANT DATA
9.1 Uprating or Debottlenecking Exercises
10 REFERENCES
APPENDICES
A WORKED EXAMPLE
B SLOPPY SEPARATIONS
C SIMULATION USING PLANT DATA : CASE HISTORIES
TABLES
Batch Distillation
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 BACKGROUND TO THE DESIGN
4.1 General
4.2 Choice of batch/continuous operation
4.3 Boiling point curve and cut policy
4.4 Method of design
4.5 Scope of calculations required for design
5 SIMPLE BATCH DISTILLATION
6 FRACTIONAL BATCH DISTILLATION
6.1 General
6.2 Approximate methods
6.3 Rigorous design - use of a computer model
6.4 Other factors influencing the design
6.4.1 Occupation
6.4.2 Choice of Batch Rectification or Stripping
6.4.3 Batch size
6.4.4 Initial estimate of cut policy
6.4.5 Liquid Holdup
6.4.6 Total reflux operation and heating-up time
6.4.7 Column operating pressure
6.5 Optimum Design of the Batch Still
6.6 Special design problems
7 GENERAL ASPECTS OF EQUIPMENT DESIGN
7.1 Kettle reboilers
7.2 Column Internals
7.3 Condensers and reflux split boxes
8 PROCESS CONTROL AND INSTRUMENTATION IN
BATCH DISTILLATION
9 MECHANICAL DESIGN FEATURES
10 BIBLIOGRAPHY
APPENDICES
A McCABE - THIELE METHOD - TYPICAL EXAMPLE
Episode 60 : Pinch Diagram and Heat Integration
The optimal allocation of mass and energy within a unit operation, process and/or site.
Optimal allocation can be based on economic, environmental or other important objectives.
SAJJAD KHUDHUR ABBAS
Ceo , Founder & Head of SHacademy
Chemical Engineering , Al-Muthanna University, Iraq
Oil & Gas Safety and Health Professional – OSHACADEMY
Trainer of Trainers (TOT) - Canadian Center of Human
Development
Design and Simulation of Continuous Distillation ColumnsGerard B. Hawkins
Design and Simulation of Continuous Distillation Columns
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 FRACTIONAL DISTILLATION
5 ROUGH METHOD OF COLUMN DESIGN
5.1 Sharp Separations
5.2 Sloppy Separations
6 DETAIL DESIGN USING THE CHEMCAD DISTILLATION PROGRAM
6.1 Sharp Separations
6.2 Sloppy Separations
7 COMPLEX COLUMNS
7.1 Multiple Feeds
7.2 Sidestream Take-Offs
8 DESIGN USING A LABORATORY COLUMN
SIMULATION
9 DESIGN USING ACTUAL PLANT DATA
9.1 Uprating or Debottlenecking Exercises
10 REFERENCES
APPENDICES
A WORKED EXAMPLE
B SLOPPY SEPARATIONS
C SIMULATION USING PLANT DATA : CASE HISTORIES
TABLES
Batch Distillation
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 BACKGROUND TO THE DESIGN
4.1 General
4.2 Choice of batch/continuous operation
4.3 Boiling point curve and cut policy
4.4 Method of design
4.5 Scope of calculations required for design
5 SIMPLE BATCH DISTILLATION
6 FRACTIONAL BATCH DISTILLATION
6.1 General
6.2 Approximate methods
6.3 Rigorous design - use of a computer model
6.4 Other factors influencing the design
6.4.1 Occupation
6.4.2 Choice of Batch Rectification or Stripping
6.4.3 Batch size
6.4.4 Initial estimate of cut policy
6.4.5 Liquid Holdup
6.4.6 Total reflux operation and heating-up time
6.4.7 Column operating pressure
6.5 Optimum Design of the Batch Still
6.6 Special design problems
7 GENERAL ASPECTS OF EQUIPMENT DESIGN
7.1 Kettle reboilers
7.2 Column Internals
7.3 Condensers and reflux split boxes
8 PROCESS CONTROL AND INSTRUMENTATION IN
BATCH DISTILLATION
9 MECHANICAL DESIGN FEATURES
10 BIBLIOGRAPHY
APPENDICES
A McCABE - THIELE METHOD - TYPICAL EXAMPLE
Episode 60 : Pinch Diagram and Heat Integration
The optimal allocation of mass and energy within a unit operation, process and/or site.
Optimal allocation can be based on economic, environmental or other important objectives.
SAJJAD KHUDHUR ABBAS
Ceo , Founder & Head of SHacademy
Chemical Engineering , Al-Muthanna University, Iraq
Oil & Gas Safety and Health Professional – OSHACADEMY
Trainer of Trainers (TOT) - Canadian Center of Human
Development
In the plant, ammonia is produced from synthesis gas containing hydrogen and nitrogen in the ratio of approximately 3:1. Besides these components, the synthesis gas contains inert gases such as argon and methane to a limited extent. The source of H2 is demineralized water and the hydrocarbons in the natural gas. The source of N2 is the atmospheric air. The source of CO2 is the hydrocarbons in the natural gas feed. Product ammonia and CO2 is sent to urea plant. The present article intended the description of ammonia plant for natural gas based plants and the possible material balance of some section.
Gas - Liquid Reactors
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 PRELIMINARY CONSIDERATIONS
4.1 Preliminary Equipment Selection
4.2 Equipment for Low Viscosity Liquids
4.3 Equipment for High Viscosity Liquids
5 REACTOR DESIGN
6 ESSENTIAL THEORY
6.1 Rate and Yield Determining Steps
6.2 Chemical and Physical Rates
6.3 Modification for Exothermic and Complex Reactions
6.4 Preliminary Selection of Reactor Type
7 EXPERIMENTAL DETERMINATION OF REGIME
7.1 Direct Measurement of Reaction Kinetics
7.2 Laboratory Gas-Liquid Reactor Experiments
8 EQUILIBRIUM AND DIFFUSIVITY DATA SOURCES
9 OVERALL EFFECTS
9.1 Liquid Flow Patterns
9.2 Scale of Mixing
9.3 Gas Flow Pattern : Mean Driving Force for Mass Transfer
9.4 Gas-Liquid Reactor Modeling
9.5 Heat Transfer
9.6 Materials of Construction
9.7 Foaming
10 FINAL CHOICE OF REACTOR TYPE
11 SCALE-UP AND SPECIFICATION OF GAS-LIQUID
REACTORS
11.1 Bubble Columns
11.2 Packed Columns
11.3 Trickle Beds
11.4 Plate or Tray Columns
11.5 Spray Columns
11.6 Wiped Film
11.7 Spinning Film Reactors
11.8 Stirred Vessels
11.9 Plunging Jet
11.10 Surface Aerator
11.11 Static Mixers
11.12 Ejectors, Venturis and Orifice Plates
11.13 3-Phase Fluidized Bed
12 BIBLIOGRAPHY
TABLES
1 REGIMES OF GAS-LIQUID MASS TRANSFER WITH ISOTHERMAL CHEMICAL REACTION
2 REGIMES OF GAS-LIQUID MASS TRANSFER IGNORING LARGE EXOTHERMS OR OTHER COMPLICATIONS
3 COMPARATIVE MASS TRANSFER PERFORMANCE OF CONTACTING DEVICES
4 COMPARATIVE MASS TRANSFER DATA
5 CHOICE OF GAS-LIQUID REACTOR TYPE
FIGURES
1 RATE AND YIELD DETERMINING STEPS
2 ENHANCEMENT FACTOR vs HATTA NUMBER
3 ENHANCEMENT FACTOR vs HATTA NUMBER : EFFECT OF THERMAL & OTHER FACTORS
4 REACTORS FOR LIQUID-PHASE KINETICS
MEASUREMENT
5 EXPERIMENTS TO DETERMINE THE OPERATING
REGIME
6 EXPERIMENTS DETERMINE THE OPERATING REGIME WHERE A SOLID CATALYST IS INVOLVED
7 THE MIXED ZONES IN LOOPS' MODEL FOR STIRRED REACTORS
Reactor and Catalyst Design
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 CATALYST DESIGN
4.1 Equivalent Pellet Diameter
4.2 Voidage
4.3 Pellet Density
5 REACTOR DESIGN
6 CATALYST SUPPORT
6.1 Choice of Support
TABLES
1 CATALYST SUPPORT SHAPES
2 SECONDARY REFORMER SPREADSHEET
FIGURES
1 GRAPH OF EFFECTIVENESS v THIELE MODULUS
2 VARIATION OF COSTS WITH CATALYST SIZE
3 VARIATION OF COSTS WITH CATALYST BED VOIDAGE
4 VARIATION OF COSTS WITH VESSEL DIAMETER
Design and Rating of Packed Distillation Columns
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 DESIGN PHILOSOPHY
5 PERFORMANCE GUARANTEES
6 DESCRIPTION OF PACKED COLUMN INTERNALS
7. DESIGN CALCULATIONS
7.1 Selection of Packing Size
7.2 Rough Design
7.3 Detailed Design and Rating
8 LIQUID DISTRIBUTION AND REDISTRIBUTION
8.1 Basic Concepts
8.2 Pour Point Density
8.3 Peripheral Irrigation - the Wall Zone
8.4 Distributor Levelness
8.5 Maximum Bed Height and Liquid Redistribution
9 PRACTICAL ASPECTS OF PACKED COLUMN DESIGN
9.1 Packing
9.2 Support Grid
9.3 Liquid Collector
9.4 Liquid Distributor or Redistributor
9.5 Packing Hold-down Grid
9.6 Reflux or Feed Pipe
9.7 Reboil Return Pipe
9.8 Liquid Draw-offs
9.9 Vapor Draw-offs
10 BIBLIOGRAPHY
APPENDICES
A DEFINITIONS
A.1 INTRODUCTION
A.2 MECHANICAL DEFINITIONS
A.3 PERFORMANCE DEFINITIONS
B PACKING HYDRAULICS - THE NORTON METHOD
TABLES
1 PACKING FACTORS FOR THE MORE COMMON
RANDOM PACKINGS
An overview of distillation column design concepts and major design considerations. Explains distillation column design concepts, what you would provide to a professional distillation column designer, and what you can expect back from a distillation system design firm. To speak with an engineer about your distillation column project, call EPIC at 314-207-4250.
1. Introduction reasons for purification, types of poisons, and typical systems
2. Hydrogenation
3. Dechlorination
4. Sulfur Removal
5. Purification system start-up and shut-down
Natural Gas (from a natural reservoir or associated to a crude production) can contain acid gas (H2S and/or CO2)..
The Gas Sweetening Process aims to remove part or all of the acid gas.
Episode 53 : Computer Aided Process Engineering
Lecture notes and reading material
* A lecture note covering all the lectures has been prepared (see course home-page)
* Supplementary text-books are listed
* A course home-page has been created
* All lecture and tutorial material can be downloaded from the home-page
http://www.capec.kt.dtu.dk/Courses/MSc-level-Courses/
SAJJAD KHUDHUR ABBAS
Ceo , Founder & Head of SHacademy
Chemical Engineering , Al-Muthanna University, Iraq
Oil & Gas Safety and Health Professional – OSHACADEMY
Trainer of Trainers (TOT) - Canadian Center of Human
Development
Course by Chemical Engineering Guy
Check out full course:
http://www.chemicalengineeringguy.com/courses/aspen-plus-physical-properties-course/
Ask me for special discounts, or checkout "SURPIRSE" tab in my site for special discounts.
This is course on Process Simulation will show you how to model, manipulate and report thermodynamic, transport, physical and chemical properties of substances.
You will learn about:
Physical Property Environment
Physical Property Method & Method Assistant
Fluid and Property Packages
Physical property input, modeling, estimation and regression
Thermodynamic Properties (Material/Energy balances and Thermodynamic Processes)
Transport Properties for (Mass/Heat/Momentum Transfer)
Equilibrium Properties (Vapor-Liquid, Liquid-Liquid, etc...)
Getting Results (Plots, Graphs, Tables)
This is an excellent way to get started with Aspen Plus. Understanding the physical property environment will definitively help you in the simulation and flowsheet creation!
This is a "workshop-based" course, there is about 50% theory and about 50% practice!
In the plant, ammonia is produced from synthesis gas containing hydrogen and nitrogen in the ratio of approximately 3:1. Besides these components, the synthesis gas contains inert gases such as argon and methane to a limited extent. The source of H2 is demineralized water and the hydrocarbons in the natural gas. The source of N2 is the atmospheric air. The source of CO2 is the hydrocarbons in the natural gas feed. Product ammonia and CO2 is sent to urea plant. The present article intended the description of ammonia plant for natural gas based plants and the possible material balance of some section.
Gas - Liquid Reactors
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 PRELIMINARY CONSIDERATIONS
4.1 Preliminary Equipment Selection
4.2 Equipment for Low Viscosity Liquids
4.3 Equipment for High Viscosity Liquids
5 REACTOR DESIGN
6 ESSENTIAL THEORY
6.1 Rate and Yield Determining Steps
6.2 Chemical and Physical Rates
6.3 Modification for Exothermic and Complex Reactions
6.4 Preliminary Selection of Reactor Type
7 EXPERIMENTAL DETERMINATION OF REGIME
7.1 Direct Measurement of Reaction Kinetics
7.2 Laboratory Gas-Liquid Reactor Experiments
8 EQUILIBRIUM AND DIFFUSIVITY DATA SOURCES
9 OVERALL EFFECTS
9.1 Liquid Flow Patterns
9.2 Scale of Mixing
9.3 Gas Flow Pattern : Mean Driving Force for Mass Transfer
9.4 Gas-Liquid Reactor Modeling
9.5 Heat Transfer
9.6 Materials of Construction
9.7 Foaming
10 FINAL CHOICE OF REACTOR TYPE
11 SCALE-UP AND SPECIFICATION OF GAS-LIQUID
REACTORS
11.1 Bubble Columns
11.2 Packed Columns
11.3 Trickle Beds
11.4 Plate or Tray Columns
11.5 Spray Columns
11.6 Wiped Film
11.7 Spinning Film Reactors
11.8 Stirred Vessels
11.9 Plunging Jet
11.10 Surface Aerator
11.11 Static Mixers
11.12 Ejectors, Venturis and Orifice Plates
11.13 3-Phase Fluidized Bed
12 BIBLIOGRAPHY
TABLES
1 REGIMES OF GAS-LIQUID MASS TRANSFER WITH ISOTHERMAL CHEMICAL REACTION
2 REGIMES OF GAS-LIQUID MASS TRANSFER IGNORING LARGE EXOTHERMS OR OTHER COMPLICATIONS
3 COMPARATIVE MASS TRANSFER PERFORMANCE OF CONTACTING DEVICES
4 COMPARATIVE MASS TRANSFER DATA
5 CHOICE OF GAS-LIQUID REACTOR TYPE
FIGURES
1 RATE AND YIELD DETERMINING STEPS
2 ENHANCEMENT FACTOR vs HATTA NUMBER
3 ENHANCEMENT FACTOR vs HATTA NUMBER : EFFECT OF THERMAL & OTHER FACTORS
4 REACTORS FOR LIQUID-PHASE KINETICS
MEASUREMENT
5 EXPERIMENTS TO DETERMINE THE OPERATING
REGIME
6 EXPERIMENTS DETERMINE THE OPERATING REGIME WHERE A SOLID CATALYST IS INVOLVED
7 THE MIXED ZONES IN LOOPS' MODEL FOR STIRRED REACTORS
Reactor and Catalyst Design
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 CATALYST DESIGN
4.1 Equivalent Pellet Diameter
4.2 Voidage
4.3 Pellet Density
5 REACTOR DESIGN
6 CATALYST SUPPORT
6.1 Choice of Support
TABLES
1 CATALYST SUPPORT SHAPES
2 SECONDARY REFORMER SPREADSHEET
FIGURES
1 GRAPH OF EFFECTIVENESS v THIELE MODULUS
2 VARIATION OF COSTS WITH CATALYST SIZE
3 VARIATION OF COSTS WITH CATALYST BED VOIDAGE
4 VARIATION OF COSTS WITH VESSEL DIAMETER
Design and Rating of Packed Distillation Columns
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 DESIGN PHILOSOPHY
5 PERFORMANCE GUARANTEES
6 DESCRIPTION OF PACKED COLUMN INTERNALS
7. DESIGN CALCULATIONS
7.1 Selection of Packing Size
7.2 Rough Design
7.3 Detailed Design and Rating
8 LIQUID DISTRIBUTION AND REDISTRIBUTION
8.1 Basic Concepts
8.2 Pour Point Density
8.3 Peripheral Irrigation - the Wall Zone
8.4 Distributor Levelness
8.5 Maximum Bed Height and Liquid Redistribution
9 PRACTICAL ASPECTS OF PACKED COLUMN DESIGN
9.1 Packing
9.2 Support Grid
9.3 Liquid Collector
9.4 Liquid Distributor or Redistributor
9.5 Packing Hold-down Grid
9.6 Reflux or Feed Pipe
9.7 Reboil Return Pipe
9.8 Liquid Draw-offs
9.9 Vapor Draw-offs
10 BIBLIOGRAPHY
APPENDICES
A DEFINITIONS
A.1 INTRODUCTION
A.2 MECHANICAL DEFINITIONS
A.3 PERFORMANCE DEFINITIONS
B PACKING HYDRAULICS - THE NORTON METHOD
TABLES
1 PACKING FACTORS FOR THE MORE COMMON
RANDOM PACKINGS
An overview of distillation column design concepts and major design considerations. Explains distillation column design concepts, what you would provide to a professional distillation column designer, and what you can expect back from a distillation system design firm. To speak with an engineer about your distillation column project, call EPIC at 314-207-4250.
1. Introduction reasons for purification, types of poisons, and typical systems
2. Hydrogenation
3. Dechlorination
4. Sulfur Removal
5. Purification system start-up and shut-down
Natural Gas (from a natural reservoir or associated to a crude production) can contain acid gas (H2S and/or CO2)..
The Gas Sweetening Process aims to remove part or all of the acid gas.
Episode 53 : Computer Aided Process Engineering
Lecture notes and reading material
* A lecture note covering all the lectures has been prepared (see course home-page)
* Supplementary text-books are listed
* A course home-page has been created
* All lecture and tutorial material can be downloaded from the home-page
http://www.capec.kt.dtu.dk/Courses/MSc-level-Courses/
SAJJAD KHUDHUR ABBAS
Ceo , Founder & Head of SHacademy
Chemical Engineering , Al-Muthanna University, Iraq
Oil & Gas Safety and Health Professional – OSHACADEMY
Trainer of Trainers (TOT) - Canadian Center of Human
Development
Course by Chemical Engineering Guy
Check out full course:
http://www.chemicalengineeringguy.com/courses/aspen-plus-physical-properties-course/
Ask me for special discounts, or checkout "SURPIRSE" tab in my site for special discounts.
This is course on Process Simulation will show you how to model, manipulate and report thermodynamic, transport, physical and chemical properties of substances.
You will learn about:
Physical Property Environment
Physical Property Method & Method Assistant
Fluid and Property Packages
Physical property input, modeling, estimation and regression
Thermodynamic Properties (Material/Energy balances and Thermodynamic Processes)
Transport Properties for (Mass/Heat/Momentum Transfer)
Equilibrium Properties (Vapor-Liquid, Liquid-Liquid, etc...)
Getting Results (Plots, Graphs, Tables)
This is an excellent way to get started with Aspen Plus. Understanding the physical property environment will definitively help you in the simulation and flowsheet creation!
This is a "workshop-based" course, there is about 50% theory and about 50% practice!
Review of Hooke and Jeeves Direct Search Solution Method Analysis Applicable ...ijiert bestjournal
Role of optimization in engineering design is prominent one with the a dvent of computers. Optimization has become a part of computer aided design methodology. It is primarily being used in those design activities in which the goal is not only to achieve a feasible design,but als o a design objective. The paper reviews the optimization in detail followed by the literature review and b rief discussion of Hooks and Jeeves Method Analysis with an example.
Episode 55 : Conceptual Process Synthesis-Design
Process Flowsheet Synthesis: Method to determine a process flowsheet that satisfies all product, operational and other requirements
SAJJAD KHUDHUR ABBAS
Ceo , Founder & Head of SHacademy
Chemical Engineering , Al-Muthanna University, Iraq
Oil & Gas Safety and Health Professional – OSHACADEMY
Trainer of Trainers (TOT) - Canadian Center of Human
Development
Value Engineering is a technique for determining the manufacturing requirements of a
product/service; it is concerned with its evaluation and finally the selection of less costly
conditions. VE is a process for achieving the optimal result in a way that quality, safety, reliability
and convertibility of every monetary unit are improved.
Here theory of Value Engineering along with case study of UTM is presented.
Welcome to WIPAC Monthly the magazine brought to you by the LinkedIn Group Water Industry Process Automation & Control.
In this month's edition, along with this month's industry news to celebrate the 13 years since the group was created we have articles including
A case study of the used of Advanced Process Control at the Wastewater Treatment works at Lleida in Spain
A look back on an article on smart wastewater networks in order to see how the industry has measured up in the interim around the adoption of Digital Transformation in the Water Industry.
Saudi Arabia stands as a titan in the global energy landscape, renowned for its abundant oil and gas resources. It's the largest exporter of petroleum and holds some of the world's most significant reserves. Let's delve into the top 10 oil and gas projects shaping Saudi Arabia's energy future in 2024.
Water scarcity is the lack of fresh water resources to meet the standard water demand. There are two type of water scarcity. One is physical. The other is economic water scarcity.
Overview of the fundamental roles in Hydropower generation and the components involved in wider Electrical Engineering.
This paper presents the design and construction of hydroelectric dams from the hydrologist’s survey of the valley before construction, all aspects and involved disciplines, fluid dynamics, structural engineering, generation and mains frequency regulation to the very transmission of power through the network in the United Kingdom.
Author: Robbie Edward Sayers
Collaborators and co editors: Charlie Sims and Connor Healey.
(C) 2024 Robbie E. Sayers
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3. Course Learning Outcomes (CLOs)
• CLOs are the skills learnt by the students at
the end of each course in the program.
• The three (3) learning domains characterize by
Bloom’s Taxonomy and their respective levels
of learning are
1. Cognitive (Knowledge) (6 levels)
2. Psychomotor (Skill) (7 levels)
3. Affective (Attitude) (5 levels)
4.
5. Program learning outcomes (Total=12)
1) Engineering Knowledge
2) Problem Analysis
3) Design/Development of Solutions
4) Investigation
5) Modern Tool Usage
6) The Engineer and Society
7) Environment and Sustainability
8) Ethics
9) Individual and Team Work
10) Communication
11) Project Management
12) Lifelong Learning
6. MEASURABLE STUDENT LEARNING OUTCOMES
CLOs Description PLOs Domain
Domain
Level
CLO-1
Create, design and evaluate alternate processes
and equipment for a chemical process and
assess various societal, environmental, and
safety issues associated with such design
PLO-4 Cognitive 6. Create
CLO-2
Apply knowledge acquired in core Chemical
Engineering courses (e.g., Stoichiometry,
Reaction Engineering, Thermodynamics, and
Unit Operations) for selection and design of
materials handling, heat transfer, and
separation process equipment.
PLO-3 Cognitive 3. Apply
CLO-3
Understand the concept of heat integration for
minimization of overall energy footprint of a
chemical process
PLO-5 Cognitive 3. Apply
7. Course description
(1) Introduction to process design and development
(2) General design considerations
(3) Optimal design
(4) Materials of fabrication and their selection
(5) Material transfer handling and equipment design
(6) Heat transfer equipment design
(7) Mass transfer equipment design
(8) Application of computer aided design software
8. WEEK-WISE LECTURE PLAN
Week Topics CLO’s
Week 1
Introduction: General overall design considerations: Process design and flowsheet development, optimum design; practical
consideration and engineering ethics in design
CLO-1
Week 2
General design considerations: Health and safety hazards, importance and objectives of safety, safety measures in equipment design:
Fire and explosion hazards and prevention, Chemical, toxic, electrical hazards, control, precautions and prevention, personnel safety,
loss prevention and safety audit.
CLO-1
Week 3
Environmental protection and development of pollution control systems. Thermal pollution control, toxicological studies, industrial
hygiene, radiation hazards.
CLO-1
Week 4 Plant site location and layout of chemical plant, piping layout, plant operation and control, plant considerations and exercise problems. CLO-1
Week 5
Process design development: Process selection/creation, synthesis and design: equipment design and specifications. Preliminary process
design: screening of process alternatives; economic decision making.
CLO-1
Week 6
Flow sheet synthesis and development: Process information, input-output structure; function and operation diagrams; analysis and
development of process flow sheet.
CLO-2
Week 7
Optimum design and design strategy: defining the optimum problems, programming optimization problems; optimization solution
methodologies; optimization applications and cost analysis.
CLO-2
Week 8
Pinch technology an overview, key steps of pinch technology: Targeting of heat exchanger network: Designing of HEN: Pinch design
methods, Heuristic rules, stream splitting, design of maximum energy recovery (MER)
CLO-3
MID TERM EXAMINATION
Week 10
Materials selection and fabrication: Corrosion and factors contributing to corrosion; corrosion prevention; material properties;
economics involved in materials selection.
CLO-2
Week 11
Materials handling equipment design and cost: Basic concept of fluid transport, frictional losses, selection of piping material, design of
piping system.
CLO-2
Week 12
Computer aided design, cost estimation and profitability analysis of investments, Transport of fluids: selection, design and cost analysis
for pumping, compression, expansion, agitation and mixing of fluids, flow measurement and storage of fluids.
CLO-4
Week 13 Heat transfer equipment design and cost: Basic theory of heat transfer in exchanger, heat exchanger selection criterion. CLO-2
Week 14 General methods for the design of heat exchangers: Design of key heat exchangers CLO-1
Week 15 Separation equipment design and costs: Introduction, selection, general design and cost of equipment for separation process. CLO-1
Week 16
Design and cost for multi-component distillation: Absorption, adsorption membrane separation. Selection and design of filtration
equipment.
CLO-1
FINAL TERM EXAMINATION
9. 1- “Plant Design and Economics for Chemical Engineers” by M. S. Peters, K. D.
Timmerhaus, and R. E. West
2- Coulson and Richardson’s Chemical Engineering — Volume 6: Chemical
Engineering
Text Books:
10. 1- An Applied Guide to process and Plant Design by Sean Moran
2- Process Equipment and Plant Design by Subhabrata Ray
3- Ullmann’s Chemical Engineering and Plant Design
Reference Books:
11. Reference Books:
1. “Ludwig’s Applied Process Design for Chemical and Petrochemical Plants” by A. K. Coker
2. “Chemical Engineering Desgin-Volume 6” by R. Sinnott & Cavin Towler
3. “Chemical Process Equipment: Selection and Design” by J. R. Couper, W. R. Penney, J. R.
Fair, and S. M. Walas
4. “Equipment Design Handbook: For Refineries and Chemical Engineers” by F. L. Evans
5. “Chemical Process: Design and Integration” by R. Smith
6. “The Art of Chemical Process Design” by G. L. Wells, and L. M. Rose
12. The general term plant design includes all
engineering aspects involved in the
development of either a new, modified, or
expanded industrial plant. In this development,
the chemical engineer will be making economic
evaluations of new processes, designing
individual pieces of equipment, or developing a
plant layout. Because of these many design
duties, the chemical engineer is many times
referred to as a design engineer.
Chemical Engineering Plant Design
13. On the other hand, a chemical engineer
specializing in the economic aspects of the
design is often referred to as a cost engineer.
The term process engineering is used in
connection with economic evaluation and
general economic analyses of industrial
processes, while process design refers to the
actual design of the equipment and facilities
necessary for carrying out the process.
Similarly, the meaning of plant design is limited
by some engineers to items related directly to
the complete plant, such as plant layout,
general service facilities, and plant location.
Chemical Engineering Plant Design Cont’d
22. A plant-design project moves to completion through a
series of stages
1. Inception
2. Preliminary evaluation of economics and market
3. Development of data necessary for final design
4. Final economic evaluation
5. Detailed engineering design
6. Procurement
7. Erection
8. Startup and trial runs
9. Production
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24. PROCESS DESIGN DEVELOPMENT
• Inception of the basic idea.
• Originate new process or
modify an existing process.
• The process-research phase.
• Pilot plant or a commercial
development plant.
• Complete market analysis.
• Complete cost-and-profit
analysis.
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27. COST ESTIMATION
• Fixed costs
• Raw materials costs
• Labor charges
• Maintenance
• Power
• Utilities
• Costs for plant and administrative overhead
• Distribution of the final products
• Other miscellaneous items
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28. Special Techniques for Cost
Estimation
1. Order of magnitude estimate:(ratio estimate) accuracy typically
+30%, usually based on the costs of similar processes and requiring no
design information.
2. Preliminary estimates (budget authorization/scope estimate):
accuracy typically +20%, They are based on limited cost data and
design detail.
3. Study estimates (factored estimate): based on knowledge of major
items of equipment, accuracy of estimate upto +30%
4. Detailed estimates (contractor’s estimate): accuracy +5%, Complete
specifications, drawings, and site surveys for the plant construction are
required
5. Definitive estimates (project control estimate): accuracy +10%,
Based on complete data but before completion of drawings &
specifications.
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29. FACTORS AFFECTING PROFITABILITY
OF INVESTMENTS
• Interest
• Insurance
• Taxes
• Depreciation
• Manufacturing costs
• Time value of money
• Rate of return
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30. OPTIMUM DESIGN
There are several alternative methods which
can be used for any given process or operation,
optimization is to choose the best process and to
incorporate into designing the equipment and
methods which will give the best results.
If there are two or more methods for obtaining
exactly equivalent final results, the preferred
method would be the one involving the least total
cost.
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32. Optimum Operation Design
Many processes require definite conditions
of temperature, pressure, contact time, or other
variables if the best results are to be obtained. It
is often possible to make a partial separation of
these optimum conditions from direct economic
considerations. In cases of this type, the best
design is designated as the optimum operation
design.
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34. THE DESIGN APPROACH
• Profitable plant design
• Generally overdesign and safety factors
• Optimization of the design by using high-
speed computers
• Make necessary assumptions
• Economic conditions and limitations
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48. Skills needed for Plant design project
• Research
• Market analysis
• Design of individual pieces of equipment
• Cost estimation
• Computer programming
• Plant-location surveys
49.
50. Organizations involved in providing standards
and guidelines for plant layout and piping design
• American Society for Mechanical Engineers (ASME): Publishes and updates codes
for piping design. The code relevant to the design of piping systems is ASME B31.3
– 2016 Process Piping. (www.asme.org)
• Center for Chemical Process Safety (CCPS): Publishes documents and guidelines
related to process safety. The focus is on preventing or mitigating catastrophic
releases of chemicals, hydrocarbons, and other hazardous materials. CCPS has
published guidelines for “Facility Siting and Layout”. (www.aiche.org/ccps)
• Construction Industry Institute (CII): Provides guidelines for cost effective and safe
construction methods and has several publications on constructability.
(www.construction-institute.org)
• Society of Piping Engineers and Designers (SPED): Promotes excellence and quality
in the practice of piping engineering and design. SPED emphasizes education and
training and has certification programs for piping designers. (www.spedweb.org)
• Occupational Safety and Health Administration (OSHA): Provides regulations and
safety standards for the operation of process plants. (www.osha.gov)
• National Fire Protection Association (NFPA): Provides fire protection standards for
process plants and for gas storage and handling. (www.nfpa.org)
Editor's Notes
On the other hand,
a chemical engineer specializing in the economic aspects of the design is often
referred to as a cost engineer.