Reactor
Table 6 Reactor HAZOP Sheet
HAZOP STUDY RECORD
SHEET
PROJECT: TEREPHTHALIC ACID
MAJOR UNIT: REACTOR
Stream
System : TPA Production Study node: Inlet to Reactor
(Air + Acetic Acid + p-
Xylene)
Deviation
Parameter
Guide Word
Possible
consequences
Possible causes
Safeguard/ Action
required
Flow
More
1. Upsetting
process
2. Uncontrolled
reaction
3. Excessive heat
• Excess air
• Excess Air Valve
fully open
• Install high flow alarm
• Install dry air control
valve after compressor.
• Operator to
continuously monitor
pipe/valve condition
and manually change
valve position
no
• No reaction
• No product
• Pipe rupture
• Valve fully
closed
• Blockage
• Install feed flow meter
• To be included in
biweekly routine
checkup procedure by
Inspection Team
Less
• Less pressure
• Less favorable
product
• Pipe leakage
• Valve partially
closed
• Install low flow alarm
• Operator to
continuously monitor
pipe/valve condition
and manually change
valve position
Pressure
More
• High velocity
of reactant
• Overpressure
• High
temperature
• Valve failure
• Overheat
• High pressure alarm
• Install pressure safety
valve (PSV)
• Install high
temperature alarm
Less
• Less reaction
• Less favorable
product
• Leakage
• Compressor
failure
• Insert safety valve
• Install low pressure
alarm
Temperature
More
• Uncontrolled
reaction
• Mechanical
failure
• May cause
explosion
• Pressure increase
 Install temperature
sensor
Crystallizer
Table 7 Crystallizer HAZOP Sheet
Less
• Less pressure,
less favorable
product.
• Low pressure
• Install temperature
sensor
HAZOP STUDY
RECORD SHEET
PROJECT: TEREPHTHALIC ACID
MAJOR UNIT : CRYSTALLIZER
Stream
System : TPA
Production
Study node: Outlet of Reactor TPA mixture
Guide
Word
Deviation
Possible
Consequences
Possible Causes
Safeguard/Action
required
Flow
More
• Upsetting
process
• Increase
demand for
solvent
• Increase in
temperature
• Uncontrolled
reaction
• Install high flow alarm
• Regular monitoring by Control Team.
No  No product
• Pipe rupture,
valve fully
closed, blockage
• No reaction
• To be included in biweekly routine
checkup procedure by Inspection Team
• Regular monitoring by Control Team
• Operator to continuously monitor
pipe/valve condition and manually change
valve position
Less
• Less product
form
• Decrease in
temperature
• Low reaction rate
• Pipe leakage
• Valve partially
closed
• Install low flow alarm
• To be included in biweekly routine
checkup procedure by Inspection Team
• Regular monitoring by Control Team
Scrubber
Table 8 Scrubber HAZOP Sheet
Dryer
Table 9 Dryer HAZOP Sheet
Item Guide word Deviation Possible consequences Possible causes
Safeguard/ Action
required
S
C
R
U
B
B
E
R
Pressure
More
 Low absorption
rate
 Uncontrolled
reaction
 Install pressure safety
valve (PSV)
 Install high pressure
alarm
Less
 Less flow rate to
the absorber
 Agitate absorption
process
 Take longer time
 Low reaction
rate
 Pipe leakage
 Install low flow alarm
 Operator to monitor
pipe/valve condition
 Regular monitoring by
Control Team
Temperature
More
 Increase in utility
 Uncontrolled
process
conditions
 Install temperature
sensor
 Install auto-control
valve for utility
less
 Less pressure
 Take longer time
for absorption
process
 Low absorption
rate
 Install temperature
sensor
Item Guide Word Deviation Possible Consequences Possible Causes Safeguard/ Action required
D
R
Y
E
R
Pressure
More  Low drying rate
 Uncontrolled air
flowrate
 Install pressure safety
valve (PSV)
 Install high pressure
alarm
Less
 Less flow rate to the
dryer
 Improve steam
flowrate to the
process
 Take longer time
 Low drying rate
 Pipe leakage
 Install low flow alarm
 Operator to monitor
pipe/valve condition
 Regular monitoring by
Control Team
More
 Increase in utility  Uncontrolled
drying process
 Install temperature
sensor
Temperature
 Install auto-control
valve for utility
less
 Less pressure
 Longer time for
drying process
 Low flowrate
 Install temperature
sensor

Hazop Sample.pdf

  • 1.
    Reactor Table 6 ReactorHAZOP Sheet HAZOP STUDY RECORD SHEET PROJECT: TEREPHTHALIC ACID MAJOR UNIT: REACTOR Stream System : TPA Production Study node: Inlet to Reactor (Air + Acetic Acid + p- Xylene) Deviation Parameter Guide Word Possible consequences Possible causes Safeguard/ Action required Flow More 1. Upsetting process 2. Uncontrolled reaction 3. Excessive heat • Excess air • Excess Air Valve fully open • Install high flow alarm • Install dry air control valve after compressor. • Operator to continuously monitor pipe/valve condition and manually change valve position no • No reaction • No product • Pipe rupture • Valve fully closed • Blockage • Install feed flow meter • To be included in biweekly routine checkup procedure by Inspection Team Less • Less pressure • Less favorable product • Pipe leakage • Valve partially closed • Install low flow alarm • Operator to continuously monitor pipe/valve condition and manually change valve position Pressure More • High velocity of reactant • Overpressure • High temperature • Valve failure • Overheat • High pressure alarm • Install pressure safety valve (PSV) • Install high temperature alarm Less • Less reaction • Less favorable product • Leakage • Compressor failure • Insert safety valve • Install low pressure alarm Temperature More • Uncontrolled reaction • Mechanical failure • May cause explosion • Pressure increase  Install temperature sensor
  • 2.
    Crystallizer Table 7 CrystallizerHAZOP Sheet Less • Less pressure, less favorable product. • Low pressure • Install temperature sensor HAZOP STUDY RECORD SHEET PROJECT: TEREPHTHALIC ACID MAJOR UNIT : CRYSTALLIZER Stream System : TPA Production Study node: Outlet of Reactor TPA mixture Guide Word Deviation Possible Consequences Possible Causes Safeguard/Action required Flow More • Upsetting process • Increase demand for solvent • Increase in temperature • Uncontrolled reaction • Install high flow alarm • Regular monitoring by Control Team. No  No product • Pipe rupture, valve fully closed, blockage • No reaction • To be included in biweekly routine checkup procedure by Inspection Team • Regular monitoring by Control Team • Operator to continuously monitor pipe/valve condition and manually change valve position Less • Less product form • Decrease in temperature • Low reaction rate • Pipe leakage • Valve partially closed • Install low flow alarm • To be included in biweekly routine checkup procedure by Inspection Team • Regular monitoring by Control Team
  • 3.
    Scrubber Table 8 ScrubberHAZOP Sheet Dryer Table 9 Dryer HAZOP Sheet Item Guide word Deviation Possible consequences Possible causes Safeguard/ Action required S C R U B B E R Pressure More  Low absorption rate  Uncontrolled reaction  Install pressure safety valve (PSV)  Install high pressure alarm Less  Less flow rate to the absorber  Agitate absorption process  Take longer time  Low reaction rate  Pipe leakage  Install low flow alarm  Operator to monitor pipe/valve condition  Regular monitoring by Control Team Temperature More  Increase in utility  Uncontrolled process conditions  Install temperature sensor  Install auto-control valve for utility less  Less pressure  Take longer time for absorption process  Low absorption rate  Install temperature sensor Item Guide Word Deviation Possible Consequences Possible Causes Safeguard/ Action required D R Y E R Pressure More  Low drying rate  Uncontrolled air flowrate  Install pressure safety valve (PSV)  Install high pressure alarm Less  Less flow rate to the dryer  Improve steam flowrate to the process  Take longer time  Low drying rate  Pipe leakage  Install low flow alarm  Operator to monitor pipe/valve condition  Regular monitoring by Control Team More  Increase in utility  Uncontrolled drying process  Install temperature sensor
  • 4.
    Temperature  Install auto-control valvefor utility less  Less pressure  Longer time for drying process  Low flowrate  Install temperature sensor