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Grease Sampling and Analysis of Offshore Wind Installations 
in Europe to Improve Asset Reliability 
Richard N. Wurzbach 
MRG Laboratories, York, Pennsylvania 
Reliability of current and installed wind turbine platforms is essential to 
future viability and growth of the windpower industry. Condition monitoring 
has been identified as an important tool in enhancing wind turbine 
reliability, and understanding dominant failure modes and root-causes. 
Grease lubrication is utilized for most drivetrain components, and proper 
lubrication is vital to reliable operation. Companies in the Danish wind 
industry, recognizing these concerns, created a project team to research 
methods and tools for obtaining grease samples from wind turbine main 
bearings. Utilizing the principles of the Theory of Sampling by Professor 
Pierre Gy, the team identified several tools and important methods in 
ensuring that analysis of greases from wind turbines provides accurate 
condition assessment and actionable data. Analysis methods utilizing 
small grease volumes (approximately 1 gram) were shown to be effective 
in differentiating bearing conditions, and providing accurate representation 
of bearing and grease condition. This poster outlines the methods for 
obtaining representative grease samples in wind turbines, and analysis 
methods performed on these samples. 
Objectives 
There is considerable difference between RDE and FdM-Fe results, and 
RDE significantly underestimates the amount of iron wear particles in all 
grease samples in this project. The explanation for this is most likely that a 
significant amount of wear particles in grease from main bearings in wind 
turbines are larger than 6-8 μm which is at the limit of sensitivity of the 
RDE instrument. A key to the success of the ferrous debris measurement 
is the configuration of the FdMPlus unit, in that the entire sample is 
introduced to the field of the Hall-effect sensor, thus cancelling any slight 
localized variations in ferrous debris distribution in the grease 
(heterogeneity), and providing an average value for trending and 
comparison. The project demonstrates that reliable measurement of 
ferrous wear in grease from wind turbine can only be achieved using the 
FdMPlus or similar measuring instruments. 
Generally, moisture has several negative effects in tribo-systems and 
moisture should be kept as low as possible. Similar to the above 
mentioned verification of FdM-Fe analysis in grease, it is documented that 
the combination of Grease Thief sampling and Karl Fischer (KF) Oven 
Method analysis of moisture is a very accurate and reliable method for 
assessment of water in main bearing greases. Trend analysis of moisture 
revealed some surprising variations. In Figure 4 trends for moisture in front 
and rear bearings in two units are shown. It is quite clear in these trends 
that these separate turbines are experiencing a similar change in moisture, 
increasing from March until June (moisture level triples) after which it is 
slightly decreased. The key point here to observe is that this is a tool for 
accurate tracking of moisture in grease. 
Conclusions 
References 
1. Grease sampling and analysis of wind turbine drivetrain components, R. 
Wurzbach, AWEA Poster Presentation, Chicago, Illinois, May 7, 2013 
2. Analysis of Grease in Wind Turbine bearing – a tool for condition monitoring, 
Part 2, H. Møller, et.al., LUBMAT Conference Proceedings, Manchester, UK, 
June 26, 2014 
Wind energy is foreseen to play a very important role in EU in the future, 
and many countries in Europe have launched ambitious investment plans. 
Vattenfall Renewable and DONG Energy are the major players in Off-shore 
wind farms and both companies operate a substantial number of wind 
farms in the North Sea. 
Maintenance and operation of off-shore wind farms is a great challenge as 
accessibility is limited and unplanned maintenance is very expensive. 
Condition monitoring of key components in a modern wind turbine is an 
absolute prerequisite. This research project evaluated sampling and 
analysis of grease in wind turbines as a tool to assess the condition of 
pitch-, yaw-, main- and generator bearings, with special focus on main 
bearings. 
The project was comprised of two parts. I) Development of methods for 
representative sampling of greases from bearings used in modern wind 
turbines; the present contribution describes the methodology to be 
developed and the results of the first research forays. II) Development of a 
comprehensive set of grease tests for condition monitoring as well as 
screening of a number of bearings in existing in turbines. 
Representative grease sampling from a tribo-system is a complex 
undertaking. The method and sampling equipment developed were 
evaluated against the Theory of Sampling (TOS) and for implementation 
testing of bias-free sampling tools for extraction of increments for analysis. 
An important aspect was the mapping of grease spatial heterogeneity in 
bearings. 
A key goal of these studies was to understand the critical considerations in 
obtaining grease samples to ensure that the results will inform the proper 
decisions regarding optimized maintenance of grease lubricated drivetrain 
components. Advanced notice of degraded lubrication conditions allows 
for proactive management of bearings and gears to ensure maximum life 
and performance. 
The sampling methods tested here met the requirements for 
representative sampling per the Theory of Sampling. In the first part of this 
project it was shown that extraction of grease increments from main 
bearings using the Grease Thief gave an unbiased sample. Comparison 
with microscopic evaluation of the particles and observation of the several 
bearings removed from service confirms that the precision is absolutely 
satisfactory and with a low overall uncertainty, and this sampling and 
analysis scheme for ferrous wear metals in greases is an effective tool for 
trend analysis. 
This research has significantly strengthened the position that grease 
analysis is a very important tool for conditioning monitoring of bearings in 
wind turbines and it can serve as an effective and important routine 
analysis in line with testing gear and hydraulic oils in wind turbines. This 
project has also documented that appropriate sampling procedures and an 
adequate test method should be used to provide correct values for level of 
wear metals and moisture in greases. 
Figure 2: Grease sampling from a damaged Main Bearing for 3- 
dimensional sampling (Photo courtesy of DONG Energy) 
Copyright 2013, York Laboratories, LLC 
Abstract 
Methods 
Results 
Sampling 
The focus of this project was to evaluate methods to obtain meaningful 
samples and apply analysis methods to those samples for wind turbine 
main bearings. The methodologies for sampling collection was the 
utilization of the active sampling devices described in ASTM D7718, 
Standard Practice for Obtaining In-Service Samples of Lubricating Grease. 
Two versions of these “grease thief” devices were used to produce an 
approximate 1 gram sample. The first, as seen in the image below, was 
inserted into an extension T-handle that allowed for remote actuation and 
gathering of the sample in the area directly adjacent to the surface of the 
moving bearing elements. 
The second method was used to sample grease from the partially 
disassembled main bearing for 3-dimensonal sampling. 3-dimensional 
sampling involves taking multiple samples from various locations around 
the bearing and comparing values to determine the distribution of the 
measured properties and particles in the grease. This was performed 
twice for this project, on two bearings that were removed from service after 
a time in service in North Sea offshore wind farms. These samples were 
obtained using a plastic spatula and syringe. The plastic spatula was used 
to gather a series of 1-gram samples, placing them inside the opened 
syringe, and then using the subsequently assembled syringe to inject the 
sample into the grease sampler body used in the first sampling exercise. 
This provided a uniform sample methodology in a standard sample 
geometry, allowing for multiple analyses with this small sample size. 
Analysis of Grease 
Analysis of these small sized samples was enabled by the sampling device 
itself, and the Die Extrusion process for grease consistency measurement 
and sample preparation. First, the sampling device was placed into a Hall- 
Effect sensor to measure the quantity of ferrous debris in the sample. This 
provided a quantification in parts per million (ppm) of ferrous debris. The 
sampling device was then threaded into a specially designed extrusion die, 
which provided a flow channel for the grease as it exited the sampling 
device. This extrusion was performed under controlled temperatures, and 
a precisely varying rate to produce a load profile for a given sample. The 
load profile, when compared to the new, fresh grease, provides an 
assessment of the consistency of the grease and its flow dynamics, 
important in ensuring proper lubrication. The extruded grease was 
deposited as a thin-film on a plastic substrate for subsequent analysis. 
The thin-film geometry allowed for multiple additional tests to be 
performed, including tests to evaluate wear, consistency, contamination 
and oxidation. The analysis methods included automated microscopic 
particle counting, differential scanning colorimetry, Fourier-transform 
infrared spectroscopy (FTIR), analytical ferrography, and colorimetric 
analysis, among others. 
Study of Samples 
The 3-dimensional sampling, as shown in the image above, involves 
collecting a spatially diverse set of samples from around the bearing 
geometry, and evaluating the spatial variability of the grease analytes. The 
purpose here was to note the heterogeneity of the grease in the housing. 
In the case of the wind turbine main bearing, it is important that any 
change in the grease or its constituents (wear particles, contaminants) 
should be represented in the sample that is routinely taken from the 
bearing. To evaluate this, two bearings were removed from service in off-shore 
applications. The first was a bearing with a known bearing defect 
as seen in the vibration signature for this bearing. The damage was 
advanced, and the bearing was scheduled for replacement. The 
opportunity was taken to carefully disassemble the bearing and 
methodically gather samples from various locations from within the 
housing. The second bearing was from a wind turbine that had suffered 
known gearbox damage, but had no indications of bearing faults. This 
bearing was sampled in a similar manner to obtain a 3-dimensional 
sample. In both cases, the visual appearance of the bearing was noted, 
and evidence of faults or damage on the bearing were recorded. It was 
found that the first bearing had significant raceway damage, while the 
second bearing had no appreciable fault or damage. 
Among the analysis tests performed, statistical analysis was used to 
evaluate trends and comparisons of values for both the ferrous debris 
levels and the moisture levels seen in the target bearings. Ferrous debris 
was compared by two methods, FdM (Hall-Effect), and Rotating Disk 
Electrode (RDE), an atomic emission method. This comparison allowed 
for insight into suitability of these common techniques used in liquid oil 
analysis, and evaluate suitability and issues pertaining specifically to 
grease. Moisture analysis is a difficult test for semi-solids like grease, yet 
potentially a very important parameter. To achieve meaningful analysis, 
the samples were extruded by a thin-film and exposed to a carrier gas in 
an elevated temperature chamber (Oven Method) to quantify in a precise 
and repeatable manner the moisture content in the analyzed grease 
samples. 
Acknowledgements 
This project was made possible by the support of DONG Energy and Vattenfall, 
and the participation of Hans Møller and Jan Ukonsaari of Vattenfall; Uffe Larsen, 
Trine Giselsson, & Jan Jacobsen of DONG Energy; and Kim Esbensen of GEUS. 
Figure 1: Grease sampling device and its use in extension T-handles to harvest 
targeted grease samples (Photo at lower left courtesy of Oelcheck, Gmbh) 
Figure 3: Comparison of FdM-Fe and RDE data. 
Figure 4: Moisture in main bearing greases, Vestas V80 2 MW 
(Grease: SKF LGWM 1)

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  • 1. Grease Sampling and Analysis of Offshore Wind Installations in Europe to Improve Asset Reliability Richard N. Wurzbach MRG Laboratories, York, Pennsylvania Reliability of current and installed wind turbine platforms is essential to future viability and growth of the windpower industry. Condition monitoring has been identified as an important tool in enhancing wind turbine reliability, and understanding dominant failure modes and root-causes. Grease lubrication is utilized for most drivetrain components, and proper lubrication is vital to reliable operation. Companies in the Danish wind industry, recognizing these concerns, created a project team to research methods and tools for obtaining grease samples from wind turbine main bearings. Utilizing the principles of the Theory of Sampling by Professor Pierre Gy, the team identified several tools and important methods in ensuring that analysis of greases from wind turbines provides accurate condition assessment and actionable data. Analysis methods utilizing small grease volumes (approximately 1 gram) were shown to be effective in differentiating bearing conditions, and providing accurate representation of bearing and grease condition. This poster outlines the methods for obtaining representative grease samples in wind turbines, and analysis methods performed on these samples. Objectives There is considerable difference between RDE and FdM-Fe results, and RDE significantly underestimates the amount of iron wear particles in all grease samples in this project. The explanation for this is most likely that a significant amount of wear particles in grease from main bearings in wind turbines are larger than 6-8 μm which is at the limit of sensitivity of the RDE instrument. A key to the success of the ferrous debris measurement is the configuration of the FdMPlus unit, in that the entire sample is introduced to the field of the Hall-effect sensor, thus cancelling any slight localized variations in ferrous debris distribution in the grease (heterogeneity), and providing an average value for trending and comparison. The project demonstrates that reliable measurement of ferrous wear in grease from wind turbine can only be achieved using the FdMPlus or similar measuring instruments. Generally, moisture has several negative effects in tribo-systems and moisture should be kept as low as possible. Similar to the above mentioned verification of FdM-Fe analysis in grease, it is documented that the combination of Grease Thief sampling and Karl Fischer (KF) Oven Method analysis of moisture is a very accurate and reliable method for assessment of water in main bearing greases. Trend analysis of moisture revealed some surprising variations. In Figure 4 trends for moisture in front and rear bearings in two units are shown. It is quite clear in these trends that these separate turbines are experiencing a similar change in moisture, increasing from March until June (moisture level triples) after which it is slightly decreased. The key point here to observe is that this is a tool for accurate tracking of moisture in grease. Conclusions References 1. Grease sampling and analysis of wind turbine drivetrain components, R. Wurzbach, AWEA Poster Presentation, Chicago, Illinois, May 7, 2013 2. Analysis of Grease in Wind Turbine bearing – a tool for condition monitoring, Part 2, H. Møller, et.al., LUBMAT Conference Proceedings, Manchester, UK, June 26, 2014 Wind energy is foreseen to play a very important role in EU in the future, and many countries in Europe have launched ambitious investment plans. Vattenfall Renewable and DONG Energy are the major players in Off-shore wind farms and both companies operate a substantial number of wind farms in the North Sea. Maintenance and operation of off-shore wind farms is a great challenge as accessibility is limited and unplanned maintenance is very expensive. Condition monitoring of key components in a modern wind turbine is an absolute prerequisite. This research project evaluated sampling and analysis of grease in wind turbines as a tool to assess the condition of pitch-, yaw-, main- and generator bearings, with special focus on main bearings. The project was comprised of two parts. I) Development of methods for representative sampling of greases from bearings used in modern wind turbines; the present contribution describes the methodology to be developed and the results of the first research forays. II) Development of a comprehensive set of grease tests for condition monitoring as well as screening of a number of bearings in existing in turbines. Representative grease sampling from a tribo-system is a complex undertaking. The method and sampling equipment developed were evaluated against the Theory of Sampling (TOS) and for implementation testing of bias-free sampling tools for extraction of increments for analysis. An important aspect was the mapping of grease spatial heterogeneity in bearings. A key goal of these studies was to understand the critical considerations in obtaining grease samples to ensure that the results will inform the proper decisions regarding optimized maintenance of grease lubricated drivetrain components. Advanced notice of degraded lubrication conditions allows for proactive management of bearings and gears to ensure maximum life and performance. The sampling methods tested here met the requirements for representative sampling per the Theory of Sampling. In the first part of this project it was shown that extraction of grease increments from main bearings using the Grease Thief gave an unbiased sample. Comparison with microscopic evaluation of the particles and observation of the several bearings removed from service confirms that the precision is absolutely satisfactory and with a low overall uncertainty, and this sampling and analysis scheme for ferrous wear metals in greases is an effective tool for trend analysis. This research has significantly strengthened the position that grease analysis is a very important tool for conditioning monitoring of bearings in wind turbines and it can serve as an effective and important routine analysis in line with testing gear and hydraulic oils in wind turbines. This project has also documented that appropriate sampling procedures and an adequate test method should be used to provide correct values for level of wear metals and moisture in greases. Figure 2: Grease sampling from a damaged Main Bearing for 3- dimensional sampling (Photo courtesy of DONG Energy) Copyright 2013, York Laboratories, LLC Abstract Methods Results Sampling The focus of this project was to evaluate methods to obtain meaningful samples and apply analysis methods to those samples for wind turbine main bearings. The methodologies for sampling collection was the utilization of the active sampling devices described in ASTM D7718, Standard Practice for Obtaining In-Service Samples of Lubricating Grease. Two versions of these “grease thief” devices were used to produce an approximate 1 gram sample. The first, as seen in the image below, was inserted into an extension T-handle that allowed for remote actuation and gathering of the sample in the area directly adjacent to the surface of the moving bearing elements. The second method was used to sample grease from the partially disassembled main bearing for 3-dimensonal sampling. 3-dimensional sampling involves taking multiple samples from various locations around the bearing and comparing values to determine the distribution of the measured properties and particles in the grease. This was performed twice for this project, on two bearings that were removed from service after a time in service in North Sea offshore wind farms. These samples were obtained using a plastic spatula and syringe. The plastic spatula was used to gather a series of 1-gram samples, placing them inside the opened syringe, and then using the subsequently assembled syringe to inject the sample into the grease sampler body used in the first sampling exercise. This provided a uniform sample methodology in a standard sample geometry, allowing for multiple analyses with this small sample size. Analysis of Grease Analysis of these small sized samples was enabled by the sampling device itself, and the Die Extrusion process for grease consistency measurement and sample preparation. First, the sampling device was placed into a Hall- Effect sensor to measure the quantity of ferrous debris in the sample. This provided a quantification in parts per million (ppm) of ferrous debris. The sampling device was then threaded into a specially designed extrusion die, which provided a flow channel for the grease as it exited the sampling device. This extrusion was performed under controlled temperatures, and a precisely varying rate to produce a load profile for a given sample. The load profile, when compared to the new, fresh grease, provides an assessment of the consistency of the grease and its flow dynamics, important in ensuring proper lubrication. The extruded grease was deposited as a thin-film on a plastic substrate for subsequent analysis. The thin-film geometry allowed for multiple additional tests to be performed, including tests to evaluate wear, consistency, contamination and oxidation. The analysis methods included automated microscopic particle counting, differential scanning colorimetry, Fourier-transform infrared spectroscopy (FTIR), analytical ferrography, and colorimetric analysis, among others. Study of Samples The 3-dimensional sampling, as shown in the image above, involves collecting a spatially diverse set of samples from around the bearing geometry, and evaluating the spatial variability of the grease analytes. The purpose here was to note the heterogeneity of the grease in the housing. In the case of the wind turbine main bearing, it is important that any change in the grease or its constituents (wear particles, contaminants) should be represented in the sample that is routinely taken from the bearing. To evaluate this, two bearings were removed from service in off-shore applications. The first was a bearing with a known bearing defect as seen in the vibration signature for this bearing. The damage was advanced, and the bearing was scheduled for replacement. The opportunity was taken to carefully disassemble the bearing and methodically gather samples from various locations from within the housing. The second bearing was from a wind turbine that had suffered known gearbox damage, but had no indications of bearing faults. This bearing was sampled in a similar manner to obtain a 3-dimensional sample. In both cases, the visual appearance of the bearing was noted, and evidence of faults or damage on the bearing were recorded. It was found that the first bearing had significant raceway damage, while the second bearing had no appreciable fault or damage. Among the analysis tests performed, statistical analysis was used to evaluate trends and comparisons of values for both the ferrous debris levels and the moisture levels seen in the target bearings. Ferrous debris was compared by two methods, FdM (Hall-Effect), and Rotating Disk Electrode (RDE), an atomic emission method. This comparison allowed for insight into suitability of these common techniques used in liquid oil analysis, and evaluate suitability and issues pertaining specifically to grease. Moisture analysis is a difficult test for semi-solids like grease, yet potentially a very important parameter. To achieve meaningful analysis, the samples were extruded by a thin-film and exposed to a carrier gas in an elevated temperature chamber (Oven Method) to quantify in a precise and repeatable manner the moisture content in the analyzed grease samples. Acknowledgements This project was made possible by the support of DONG Energy and Vattenfall, and the participation of Hans Møller and Jan Ukonsaari of Vattenfall; Uffe Larsen, Trine Giselsson, & Jan Jacobsen of DONG Energy; and Kim Esbensen of GEUS. Figure 1: Grease sampling device and its use in extension T-handles to harvest targeted grease samples (Photo at lower left courtesy of Oelcheck, Gmbh) Figure 3: Comparison of FdM-Fe and RDE data. Figure 4: Moisture in main bearing greases, Vestas V80 2 MW (Grease: SKF LGWM 1)