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The document discusses industrial pharmacy and describes its objectives. Industrial pharmacy involves processes and procedures for converting raw materials into dosage forms and evaluating the products against requirements in pharmacopeias. The objectives of the course are to learn about the design and mechanisms of various pharmaceutical unit operations like mixing, milling, drying and their application in industry. Safety guidelines are important as hazardous chemicals and equipment are used.

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Practical Industrial Pharmacy I 4th Class, 2nd Semester University of Alkafeel College of Pharmacy Department of pharmaceutics Mustafa Al-Hamadani MSc Pharmaceutics Lab 1: Introduction in industrial pharmacy
industrial pharmacy Industrial Pharmacy is deal with processes and procedure that taken in order to conversion of raw material into certain dosage form. And evaluation of these products according to requirements described in the particular monograph. • These requirements and specification is described in the monograph of BP or USP etc. ‫ت‬ ‫ت‬ ‫ع‬ ‫ا‬ ‫م‬ ‫ل‬ ‫ا‬ ‫ل‬ ‫ص‬ ‫ي‬ ‫د‬ ‫ل‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ص‬ ‫ن‬ ‫ا‬ ‫ع‬ ‫ي‬ ‫ة‬ ‫م‬ ‫ع‬ ‫ا‬ ‫ل‬ ‫ع‬ ‫م‬ ‫ل‬ ‫ي‬ ‫ا‬ ‫ت‬ ‫و‬ ‫ا‬ ‫إل‬ ‫ج‬ ‫ر‬ ‫ا‬ ‫ء‬ ‫ا‬ ‫ت‬ ‫ا‬ ‫ل‬ ‫ت‬ ‫ي‬ ‫ي‬ ‫ت‬ ‫م‬ ‫ا‬ ‫ت‬ ‫خ‬ ‫ا‬ ‫ذ‬ ‫ه‬ ‫ا‬ ‫م‬ ‫ن‬ ‫أ‬ ‫ج‬ ‫ل‬ ‫ت‬ ‫ح‬ ‫و‬ ‫ي‬ ‫ل‬ ‫ا‬ ‫مل‬ ‫و‬ ‫ا‬ ‫د‬ ‫ا‬ ‫ل‬ ‫خ‬ ‫ا‬ ‫م‬ ‫إ‬ ‫ل‬ ‫ى‬ ‫ش‬ ‫ك‬ ‫ل‬ ‫ج‬ ‫ر‬ ‫ع‬ ‫ة‬ ‫م‬ ‫ع‬ ‫ي‬ ‫ن‬ ‫ة‬ . ‫و‬ ‫ت‬ ‫ق‬ ‫ي‬ ‫ي‬ ‫م‬ ‫ه‬ ‫ذ‬ ‫ه‬ ‫ا‬ ‫مل‬ ‫ن‬ ‫ت‬ ‫ج‬ ‫ا‬ ‫ت‬ ‫و‬ ‫ف‬ ‫ق‬ ‫ا‬ ‫ل‬ ‫ل‬ ‫م‬ ‫ت‬ ‫ط‬ ‫ل‬ ‫ب‬ ‫ا‬ ‫ت‬ ‫ا‬ ‫مل‬ ‫و‬ ‫ض‬ ‫ح‬ ‫ة‬ ‫ف‬ ‫ي‬ ‫ا‬ ‫ل‬ ‫د‬ ‫ر‬ ‫ا‬ ‫س‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫خ‬ ‫ا‬ ‫ص‬ ‫ة‬ . • ‫ي‬ ‫ت‬ ‫م‬ ‫و‬ ‫ص‬ ‫ف‬ ‫ه‬ ‫ذ‬ ‫ه‬ ‫ا‬ ‫مل‬ ‫ت‬ ‫ط‬ ‫ل‬ ‫ب‬ ‫ا‬ ‫ت‬ ‫و‬ ‫ا‬ ‫مل‬ ‫و‬ ‫ا‬ ‫ص‬ ‫ف‬ ‫ا‬ ‫ت‬ ‫ف‬ ‫ي‬ ‫د‬ ‫ر‬ ‫ا‬ ‫س‬ ‫ة‬ BP ‫أ‬ ‫و‬ USP ‫و‬ ‫م‬ ‫ا‬ ‫إ‬ ‫ل‬ ‫ى‬ ‫ذ‬ ‫ل‬ ‫ك‬ .
Preface • Industrial Pharmacy is one of the foundations upon which the profession of pharmacy has been built. This laboratory has been designed to allow you to examine some of the basic physiochemical properties of some dosage forms. • There are many instructions and guidelines that complement working in a laboratory, as there are hazardous chemicals and heavy equipment that can be dangerous if handled improperly. • ‫ا‬ ‫ل‬ ‫ص‬ ‫ي‬ ‫د‬ ‫ل‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ص‬ ‫ن‬ ‫ا‬ ‫ع‬ ‫ي‬ ‫ة‬ ‫ه‬ ‫ي‬ ‫و‬ ‫ا‬ ‫ح‬ ‫د‬ ‫ة‬ ‫م‬ ‫ن‬ ‫ا‬ ‫أل‬ ‫س‬ ‫س‬ ‫ا‬ ‫ل‬ ‫ت‬ ‫ي‬ ‫ب‬ ‫ن‬ ‫ي‬ ‫ت‬ ‫ع‬ ‫ل‬ ‫ي‬ ‫ه‬ ‫ا‬ ‫م‬ ‫ه‬ ‫ن‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ص‬ ‫ي‬ ‫د‬ ‫ل‬ ‫ة‬ . ‫ت‬ ‫م‬ ‫ت‬ ‫ص‬ ‫م‬ ‫ي‬ ‫م‬ ‫ه‬ ‫ذ‬ ‫ا‬ ‫ا‬ ‫مل‬ ‫خ‬ ‫ت‬ ‫ب‬ ‫ر‬ ‫ل‬ ‫ل‬ ‫س‬ ‫م‬ ‫ا‬ ‫ح‬ ‫ل‬ ‫ك‬ ‫ب‬ ‫ف‬ ‫ح‬ ‫ص‬ ‫ب‬ ‫ع‬ ‫ض‬ ‫ا‬ ‫ل‬ ‫خ‬ ‫ص‬ ‫ا‬ ‫ئ‬ ‫ص‬ ‫ا‬ ‫ل‬ ‫ف‬ ‫ي‬ ‫ز‬ ‫ي‬ ‫ا‬ ‫ئ‬ ‫ي‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ك‬ ‫ي‬ ‫م‬ ‫ي‬ ‫ا‬ ‫ئ‬ ‫ي‬ ‫ة‬ ‫ا‬ ‫أل‬ ‫س‬ ‫ا‬ ‫س‬ ‫ي‬ ‫ة‬ ‫ل‬ ‫ب‬ ‫ع‬ ‫ض‬ ‫أ‬ ‫ش‬ ‫ك‬ ‫ا‬ ‫ل‬ ‫ا‬ ‫ل‬ ‫ج‬ ‫ر‬ ‫ع‬ ‫ة‬ . • ‫ه‬ ‫ن‬ ‫ا‬ ‫ك‬ ‫ا‬ ‫ل‬ ‫ع‬ ‫د‬ ‫ي‬ ‫د‬ ‫م‬ ‫ن‬ ‫ا‬ ‫ل‬ ‫ت‬ ‫ع‬ ‫ل‬ ‫ي‬ ‫م‬ ‫ا‬ ‫ت‬ ‫و‬ ‫ا‬ ‫مل‬ ‫ب‬ ‫ا‬ ‫د‬ ‫ئ‬ ‫ا‬ ‫ل‬ ‫ت‬ ‫و‬ ‫ج‬ ‫ي‬ ‫ه‬ ‫ي‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ت‬ ‫ي‬ ‫ت‬ ‫ك‬ ‫م‬ ‫ل‬ ‫ا‬ ‫ل‬ ‫ع‬ ‫م‬ ‫ل‬ ‫ف‬ ‫ي‬ ‫ا‬ ‫مل‬ ‫خ‬ ‫ت‬ ‫ب‬ ‫ر‬ ، ‫ح‬ ‫ي‬ ‫ث‬ ‫ت‬ ‫و‬ ‫ج‬ ‫د‬ ‫م‬ ‫و‬ ‫ا‬ ‫د‬ ‫ك‬ ‫ي‬ ‫م‬ ‫ي‬ ‫ا‬ ‫ئ‬ ‫ي‬ ‫ة‬ ‫خ‬ ‫ط‬ ‫ر‬ ‫ة‬ ‫و‬ ‫م‬ ‫ع‬ ‫د‬ ‫ا‬ ‫ت‬ ‫ث‬ ‫ق‬ ‫ي‬ ‫ل‬ ‫ة‬ ‫ي‬ ‫م‬ ‫ك‬ ‫ن‬ ‫أ‬ ‫ن‬ ‫ت‬ ‫ك‬ ‫و‬ ‫ن‬ ‫خ‬ ‫ط‬ ‫ي‬ ‫ر‬ ‫ة‬ ‫إ‬ ‫ذ‬ ‫ا‬ ‫ت‬ ‫م‬ ‫ا‬ ‫ل‬ ‫ت‬ ‫ع‬ ‫ا‬ ‫م‬ ‫ل‬ ‫م‬ ‫ع‬ ‫ه‬ ‫ا‬ ‫ب‬ ‫ش‬ ‫ك‬ ‫ل‬ ‫غ‬ ‫ي‬ ‫ر‬ ‫ص‬ ‫ح‬ ‫ي‬ ‫ح‬ .
Learning objectives - Learning the design and mechanism of action of the instruments. - Learning the principles of each unite operation in pharmaceutical processes. - Learning define the physical principle of each unite operation in industrial pharmacy. - Learning review the use and application of each operation in relation to its advantages, disadvantages and mechanism of action. - Learning rationalize the use of the equipment for a specific application in pharmaceutical industry. - Learning predict the relationship between the equipment design and product characteristics. - Learning diagrammatically design the studied equipment for each operation
Course Outline • Section I: Pre-formulation - Physicochemical properties of drugs - Particle size - Surface area - Flow properties and rheology - Solubility - Hygroscopicity and wettability  Section II : Principle of pharmaceutical processing - Mixing - Milling and particle size analysis ((size reduction)) - Drying • ‫ا‬ ‫ل‬ ‫ق‬ ‫س‬ ‫م‬ ‫ا‬ ‫أل‬ ‫و‬ ‫ل‬ : ‫ا‬ ‫ل‬ ‫ص‬ ‫ي‬ ‫ا‬ ‫غ‬ ‫ة‬ ‫ا‬ ‫مل‬ ‫س‬ ‫ب‬ ‫ق‬ ‫ة‬ - ‫ا‬ ‫ل‬ ‫خ‬ ‫ص‬ ‫ا‬ ‫ئ‬ ‫ص‬ ‫ا‬ ‫ل‬ ‫ف‬ ‫ي‬ ‫ز‬ ‫ي‬ ‫ا‬ ‫ئ‬ ‫ي‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ك‬ ‫ي‬ ‫م‬ ‫ي‬ ‫ا‬ ‫ئ‬ ‫ي‬ ‫ة‬ ‫ل‬ ‫أل‬ ‫د‬ ‫و‬ ‫ي‬ ‫ة‬ - ‫ح‬ ‫ج‬ ‫م‬ ‫ا‬ ‫ل‬ ‫ج‬ ‫س‬ ‫ي‬ ‫م‬ ‫ا‬ ‫ت‬ - ‫م‬ ‫س‬ ‫ا‬ ‫ح‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫س‬ ‫ط‬ ‫ح‬ - ‫خ‬ ‫ص‬ ‫ا‬ ‫ئ‬ ‫ص‬ ‫ا‬ ‫ل‬ ‫ت‬ ‫د‬ ‫ف‬ ‫ق‬ ‫و‬ ‫ا‬ ‫ل‬ ‫ر‬ ‫ي‬ ‫و‬ ‫ل‬ ‫و‬ ‫ج‬ ‫ي‬ ‫ا‬ - ‫ا‬ ‫ل‬ ‫ذ‬ ‫و‬ ‫ب‬ ‫ا‬ ‫ن‬ ‫ي‬ ‫ة‬ - ‫ا‬ ‫س‬ ‫ت‬ ‫ر‬ ‫ط‬ ‫ا‬ ‫ب‬ ‫ي‬ ‫ة‬ ‫و‬ ‫ت‬ ‫ر‬ ‫ط‬ ‫ي‬ ‫ب‬ ‫ا‬ ‫ل‬ ‫ق‬ ‫س‬ ‫م‬ ‫ا‬ ‫ل‬ ‫ث‬ ‫ا‬ ‫ن‬ ‫ي‬ : ‫م‬ ‫ب‬ ‫د‬ ‫أ‬ ‫ا‬ ‫مل‬ ‫ع‬ ‫ا‬ ‫ل‬ ‫ج‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ص‬ ‫ي‬ ‫د‬ ‫ال‬ ‫ن‬ ‫ي‬ ‫ة‬ - ‫خ‬ ‫ل‬ ‫ط‬ - ‫ا‬ ‫ل‬ ‫ط‬ ‫ح‬ ‫ن‬ ‫و‬ ‫ت‬ ‫ح‬ ‫ل‬ ‫ي‬ ‫ل‬ ‫ح‬ ‫ج‬ ‫م‬ ‫ا‬ ‫ل‬ ‫ج‬ ‫س‬ ‫ي‬ ‫م‬ ‫ا‬ ‫ت‬ ) ) ‫ت‬ ‫خ‬ ‫ف‬ ‫ي‬ ‫ض‬ ‫ا‬ ‫ل‬ ‫ح‬ ‫ج‬ ‫م‬ ( ( - ‫ا‬ ‫ل‬ ‫ت‬ ‫ج‬ ‫ف‬ ‫ي‬ ‫ف‬
Course Outline • Section III: Formulation and Evaluation of pharmaceutical dosage forms - Powder and Granules  Effervescent granules: Preparation and characterization. - Tablet dosage form: Preparation and characterization.  Preparation of tablets  Formulation of Tablets  Evaluation of Tablets • ‫ا‬ ‫ل‬ ‫ق‬ ‫س‬ ‫م‬ ‫ا‬ ‫ل‬ ‫ث‬ ‫ا‬ ‫ل‬ ‫ث‬ : ‫ص‬ ‫ي‬ ‫ا‬ ‫غ‬ ‫ة‬ ‫و‬ ‫ت‬ ‫ق‬ ‫ي‬ ‫ي‬ ‫م‬ ‫أ‬ ‫ش‬ ‫ك‬ ‫ا‬ ‫ل‬ ‫ا‬ ‫ل‬ ‫ج‬ ‫ر‬ ‫ع‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ص‬ ‫ي‬ ‫د‬ ‫ال‬ ‫ن‬ ‫ي‬ ‫ة‬ - ‫م‬ ‫س‬ ‫ح‬ ‫و‬ ‫ق‬ ‫و‬ ‫ح‬ ‫ب‬ ‫ي‬ ‫ب‬ ‫ا‬ ‫ت‬ ‫ا‬ ‫ل‬ ‫ح‬ ‫ب‬ ‫ي‬ ‫ب‬ ‫ا‬ ‫ت‬ ‫ا‬ ‫ل‬ ‫ف‬ ‫و‬ ‫ا‬ ‫ر‬ ‫ة‬ : ‫ا‬ ‫ل‬ ‫ت‬ ‫ح‬ ‫ض‬ ‫ي‬ ‫ر‬ ‫و‬ ‫ا‬ ‫ل‬ ‫ت‬ ‫و‬ ‫ص‬ ‫ي‬ ‫ف‬ . - ‫ش‬ ‫ك‬ ‫ل‬ ‫ج‬ ‫ر‬ ‫ع‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ج‬ ‫ه‬ ‫ا‬ ‫ز‬ ‫ا‬ ‫ل‬ ‫ل‬ ‫و‬ ‫ح‬ ‫ي‬ : ‫ا‬ ‫ل‬ ‫ت‬ ‫ح‬ ‫ض‬ ‫ي‬ ‫ر‬ ‫و‬ ‫ا‬ ‫ل‬ ‫ت‬ ‫و‬ ‫ص‬ ‫ي‬ ‫ف‬ . ‫إ‬ ‫ع‬ ‫د‬ ‫ا‬ ‫د‬ ‫ا‬ ‫أل‬ ‫ق‬ ‫ر‬ ‫ا‬ ‫ص‬ ‫ص‬ ‫ي‬ ‫ا‬ ‫غ‬ ‫ة‬ ‫ا‬ ‫أل‬ ‫ج‬ ‫ه‬ ‫ز‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ل‬ ‫و‬ ‫ح‬ ‫ي‬ ‫ة‬ ‫ت‬ ‫ق‬ ‫ي‬ ‫ي‬ ‫م‬ ‫ا‬ ‫أل‬ ‫ج‬ ‫ه‬ ‫ز‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ل‬ ‫و‬ ‫ح‬ ‫ي‬ ‫ة‬
Laboratory Safety • Dress Code • For your protection, you are required to wear the following protective stuff, at all times during the lab:  A lab coat  Closed-Toed Shoes (no sandals or open-toed shoes)  Do not wear contact lenses • The following special protective equipment is available for specific tasks, or on your request: - Latex (and non-allergenic neoprene) gloves - Masks - Protective hair covers • ‫ق‬ ‫و‬ ‫ا‬ ‫ع‬ ‫د‬ ‫ا‬ ‫ل‬ ‫ل‬ ‫ب‬ ‫ا‬ ‫س‬ • ‫ل‬ ‫ح‬ ‫م‬ ‫ا‬ ‫ي‬ ‫ت‬ ‫ك‬ ، ‫ي‬ ‫ط‬ ‫ل‬ ‫ب‬ ‫م‬ ‫ن‬ ‫ك‬ ‫ا‬ ‫ر‬ ‫ت‬ ‫د‬ ‫ا‬ ‫ء‬ ‫ا‬ ‫ل‬ ‫ح‬ ‫م‬ ‫ا‬ ‫ي‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ت‬ ‫ا‬ ‫ل‬ ‫ي‬ ‫ة‬ ‫ا‬ ‫أل‬ ‫ش‬ ‫ي‬ ‫ا‬ ‫ء‬ ، ‫ف‬ ‫ي‬ ‫ج‬ ‫م‬ ‫ي‬ ‫ع‬ ‫ا‬ ‫أل‬ ‫و‬ ‫ق‬ ‫ا‬ ‫ت‬ ‫أ‬ ‫ث‬ ‫ن‬ ‫ا‬ ‫ء‬ ‫ا‬ ‫مل‬ ‫خ‬ ‫ت‬ ‫ب‬ ‫ر‬ : ‫م‬ ‫ع‬ ‫ط‬ ‫ف‬ ‫م‬ ‫خ‬ ‫ت‬ ‫ب‬ ‫ر‬ ‫أ‬ ‫ح‬ ‫ذ‬ ‫ي‬ ‫ة‬ ‫م‬ ‫غ‬ ‫ل‬ ‫ق‬ ‫ة‬ ‫ا‬ ‫أل‬ ‫ص‬ ‫ا‬ ‫ب‬ ‫ع‬ ) ‫ب‬ ‫د‬ ‫و‬ ‫ن‬ ‫ص‬ ‫ن‬ ‫د‬ ‫ل‬ ‫أ‬ ‫و‬ ‫أ‬ ‫ح‬ ‫ذ‬ ‫ي‬ ‫ة‬ ‫م‬ ‫ف‬ ‫ت‬ ‫و‬ ‫ح‬ ‫ة‬ ‫ا‬ ‫أل‬ ‫ص‬ ‫ا‬ ‫ب‬ ‫ع‬ ( ‫ال‬ ‫ت‬ ‫ر‬ ‫ت‬ ‫د‬ ‫ي‬ ‫ا‬ ‫ل‬ ‫ع‬ ‫د‬ ‫س‬ ‫ا‬ ‫ت‬ ‫ا‬ ‫ل‬ ‫ال‬ ‫ص‬ ‫ق‬ ‫ة‬ • ‫ت‬ ‫ت‬ ‫و‬ ‫ف‬ ‫ر‬ ‫م‬ ‫ع‬ ‫د‬ ‫ا‬ ‫ت‬ ‫ا‬ ‫ل‬ ‫ح‬ ‫م‬ ‫ا‬ ‫ي‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫خ‬ ‫ا‬ ‫ص‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ت‬ ‫ا‬ ‫ل‬ ‫ي‬ ‫ة‬ ‫مل‬ ‫ه‬ ‫ا‬ ‫م‬ ‫م‬ ‫ح‬ ‫د‬ ‫د‬ ‫ة‬ ، ‫أ‬ ‫و‬ ‫ب‬ ‫ن‬ ‫ا‬ ‫ء‬ ‫ع‬ ‫ل‬ ‫ى‬ ‫ط‬ ‫ل‬ ‫ب‬ ‫ك‬ : - ‫ق‬ ‫ف‬ ‫ا‬ ‫ز‬ ‫ا‬ ‫ت‬ ‫ا‬ ‫ل‬ ‫ال‬ ‫ت‬ ‫ك‬ ‫س‬ ) ‫و‬ ‫ا‬ ‫ل‬ ‫ن‬ ‫ي‬ ‫و‬ ‫ب‬ ‫ر‬ ‫ي‬ ‫ن‬ ‫غ‬ ‫ي‬ ‫ر‬ ‫ا‬ ‫مل‬ ‫س‬ ‫ب‬ ‫ب‬ ‫ة‬ ‫ل‬ ‫ل‬ ‫ح‬ ‫س‬ ‫ا‬ ‫س‬ ‫ي‬ ‫ة‬ ( - ‫ا‬ ‫أل‬ ‫ق‬ ‫ن‬ ‫ع‬ ‫ة‬ - ‫أ‬ ‫غ‬ ‫ط‬ ‫ي‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ش‬ ‫ع‬ ‫ر‬ ‫ا‬ ‫ل‬ ‫و‬ ‫ا‬ ‫ق‬ ‫ي‬ ‫ة‬
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  • 1. Practical Industrial Pharmacy I 4th Class, 2nd Semester University of Alkafeel College of Pharmacy Department of pharmaceutics Mustafa Al-Hamadani MSc Pharmaceutics Lab 1: Introduction in industrial pharmacy
  • 2. industrial pharmacy Industrial Pharmacy is deal with processes and procedure that taken in order to conversion of raw material into certain dosage form. And evaluation of these products according to requirements described in the particular monograph. • These requirements and specification is described in the monograph of BP or USP etc. ‫ت‬ ‫ت‬ ‫ع‬ ‫ا‬ ‫م‬ ‫ل‬ ‫ا‬ ‫ل‬ ‫ص‬ ‫ي‬ ‫د‬ ‫ل‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ص‬ ‫ن‬ ‫ا‬ ‫ع‬ ‫ي‬ ‫ة‬ ‫م‬ ‫ع‬ ‫ا‬ ‫ل‬ ‫ع‬ ‫م‬ ‫ل‬ ‫ي‬ ‫ا‬ ‫ت‬ ‫و‬ ‫ا‬ ‫إل‬ ‫ج‬ ‫ر‬ ‫ا‬ ‫ء‬ ‫ا‬ ‫ت‬ ‫ا‬ ‫ل‬ ‫ت‬ ‫ي‬ ‫ي‬ ‫ت‬ ‫م‬ ‫ا‬ ‫ت‬ ‫خ‬ ‫ا‬ ‫ذ‬ ‫ه‬ ‫ا‬ ‫م‬ ‫ن‬ ‫أ‬ ‫ج‬ ‫ل‬ ‫ت‬ ‫ح‬ ‫و‬ ‫ي‬ ‫ل‬ ‫ا‬ ‫مل‬ ‫و‬ ‫ا‬ ‫د‬ ‫ا‬ ‫ل‬ ‫خ‬ ‫ا‬ ‫م‬ ‫إ‬ ‫ل‬ ‫ى‬ ‫ش‬ ‫ك‬ ‫ل‬ ‫ج‬ ‫ر‬ ‫ع‬ ‫ة‬ ‫م‬ ‫ع‬ ‫ي‬ ‫ن‬ ‫ة‬ . ‫و‬ ‫ت‬ ‫ق‬ ‫ي‬ ‫ي‬ ‫م‬ ‫ه‬ ‫ذ‬ ‫ه‬ ‫ا‬ ‫مل‬ ‫ن‬ ‫ت‬ ‫ج‬ ‫ا‬ ‫ت‬ ‫و‬ ‫ف‬ ‫ق‬ ‫ا‬ ‫ل‬ ‫ل‬ ‫م‬ ‫ت‬ ‫ط‬ ‫ل‬ ‫ب‬ ‫ا‬ ‫ت‬ ‫ا‬ ‫مل‬ ‫و‬ ‫ض‬ ‫ح‬ ‫ة‬ ‫ف‬ ‫ي‬ ‫ا‬ ‫ل‬ ‫د‬ ‫ر‬ ‫ا‬ ‫س‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫خ‬ ‫ا‬ ‫ص‬ ‫ة‬ . • ‫ي‬ ‫ت‬ ‫م‬ ‫و‬ ‫ص‬ ‫ف‬ ‫ه‬ ‫ذ‬ ‫ه‬ ‫ا‬ ‫مل‬ ‫ت‬ ‫ط‬ ‫ل‬ ‫ب‬ ‫ا‬ ‫ت‬ ‫و‬ ‫ا‬ ‫مل‬ ‫و‬ ‫ا‬ ‫ص‬ ‫ف‬ ‫ا‬ ‫ت‬ ‫ف‬ ‫ي‬ ‫د‬ ‫ر‬ ‫ا‬ ‫س‬ ‫ة‬ BP ‫أ‬ ‫و‬ USP ‫و‬ ‫م‬ ‫ا‬ ‫إ‬ ‫ل‬ ‫ى‬ ‫ذ‬ ‫ل‬ ‫ك‬ .
  • 3. Preface • Industrial Pharmacy is one of the foundations upon which the profession of pharmacy has been built. This laboratory has been designed to allow you to examine some of the basic physiochemical properties of some dosage forms. • There are many instructions and guidelines that complement working in a laboratory, as there are hazardous chemicals and heavy equipment that can be dangerous if handled improperly. • ‫ا‬ ‫ل‬ ‫ص‬ ‫ي‬ ‫د‬ ‫ل‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ص‬ ‫ن‬ ‫ا‬ ‫ع‬ ‫ي‬ ‫ة‬ ‫ه‬ ‫ي‬ ‫و‬ ‫ا‬ ‫ح‬ ‫د‬ ‫ة‬ ‫م‬ ‫ن‬ ‫ا‬ ‫أل‬ ‫س‬ ‫س‬ ‫ا‬ ‫ل‬ ‫ت‬ ‫ي‬ ‫ب‬ ‫ن‬ ‫ي‬ ‫ت‬ ‫ع‬ ‫ل‬ ‫ي‬ ‫ه‬ ‫ا‬ ‫م‬ ‫ه‬ ‫ن‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ص‬ ‫ي‬ ‫د‬ ‫ل‬ ‫ة‬ . ‫ت‬ ‫م‬ ‫ت‬ ‫ص‬ ‫م‬ ‫ي‬ ‫م‬ ‫ه‬ ‫ذ‬ ‫ا‬ ‫ا‬ ‫مل‬ ‫خ‬ ‫ت‬ ‫ب‬ ‫ر‬ ‫ل‬ ‫ل‬ ‫س‬ ‫م‬ ‫ا‬ ‫ح‬ ‫ل‬ ‫ك‬ ‫ب‬ ‫ف‬ ‫ح‬ ‫ص‬ ‫ب‬ ‫ع‬ ‫ض‬ ‫ا‬ ‫ل‬ ‫خ‬ ‫ص‬ ‫ا‬ ‫ئ‬ ‫ص‬ ‫ا‬ ‫ل‬ ‫ف‬ ‫ي‬ ‫ز‬ ‫ي‬ ‫ا‬ ‫ئ‬ ‫ي‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ك‬ ‫ي‬ ‫م‬ ‫ي‬ ‫ا‬ ‫ئ‬ ‫ي‬ ‫ة‬ ‫ا‬ ‫أل‬ ‫س‬ ‫ا‬ ‫س‬ ‫ي‬ ‫ة‬ ‫ل‬ ‫ب‬ ‫ع‬ ‫ض‬ ‫أ‬ ‫ش‬ ‫ك‬ ‫ا‬ ‫ل‬ ‫ا‬ ‫ل‬ ‫ج‬ ‫ر‬ ‫ع‬ ‫ة‬ . • ‫ه‬ ‫ن‬ ‫ا‬ ‫ك‬ ‫ا‬ ‫ل‬ ‫ع‬ ‫د‬ ‫ي‬ ‫د‬ ‫م‬ ‫ن‬ ‫ا‬ ‫ل‬ ‫ت‬ ‫ع‬ ‫ل‬ ‫ي‬ ‫م‬ ‫ا‬ ‫ت‬ ‫و‬ ‫ا‬ ‫مل‬ ‫ب‬ ‫ا‬ ‫د‬ ‫ئ‬ ‫ا‬ ‫ل‬ ‫ت‬ ‫و‬ ‫ج‬ ‫ي‬ ‫ه‬ ‫ي‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ت‬ ‫ي‬ ‫ت‬ ‫ك‬ ‫م‬ ‫ل‬ ‫ا‬ ‫ل‬ ‫ع‬ ‫م‬ ‫ل‬ ‫ف‬ ‫ي‬ ‫ا‬ ‫مل‬ ‫خ‬ ‫ت‬ ‫ب‬ ‫ر‬ ، ‫ح‬ ‫ي‬ ‫ث‬ ‫ت‬ ‫و‬ ‫ج‬ ‫د‬ ‫م‬ ‫و‬ ‫ا‬ ‫د‬ ‫ك‬ ‫ي‬ ‫م‬ ‫ي‬ ‫ا‬ ‫ئ‬ ‫ي‬ ‫ة‬ ‫خ‬ ‫ط‬ ‫ر‬ ‫ة‬ ‫و‬ ‫م‬ ‫ع‬ ‫د‬ ‫ا‬ ‫ت‬ ‫ث‬ ‫ق‬ ‫ي‬ ‫ل‬ ‫ة‬ ‫ي‬ ‫م‬ ‫ك‬ ‫ن‬ ‫أ‬ ‫ن‬ ‫ت‬ ‫ك‬ ‫و‬ ‫ن‬ ‫خ‬ ‫ط‬ ‫ي‬ ‫ر‬ ‫ة‬ ‫إ‬ ‫ذ‬ ‫ا‬ ‫ت‬ ‫م‬ ‫ا‬ ‫ل‬ ‫ت‬ ‫ع‬ ‫ا‬ ‫م‬ ‫ل‬ ‫م‬ ‫ع‬ ‫ه‬ ‫ا‬ ‫ب‬ ‫ش‬ ‫ك‬ ‫ل‬ ‫غ‬ ‫ي‬ ‫ر‬ ‫ص‬ ‫ح‬ ‫ي‬ ‫ح‬ .
  • 4. Learning objectives - Learning the design and mechanism of action of the instruments. - Learning the principles of each unite operation in pharmaceutical processes. - Learning define the physical principle of each unite operation in industrial pharmacy. - Learning review the use and application of each operation in relation to its advantages, disadvantages and mechanism of action. - Learning rationalize the use of the equipment for a specific application in pharmaceutical industry. - Learning predict the relationship between the equipment design and product characteristics. - Learning diagrammatically design the studied equipment for each operation
  • 5. Course Outline • Section I: Pre-formulation - Physicochemical properties of drugs - Particle size - Surface area - Flow properties and rheology - Solubility - Hygroscopicity and wettability  Section II : Principle of pharmaceutical processing - Mixing - Milling and particle size analysis ((size reduction)) - Drying • ‫ا‬ ‫ل‬ ‫ق‬ ‫س‬ ‫م‬ ‫ا‬ ‫أل‬ ‫و‬ ‫ل‬ : ‫ا‬ ‫ل‬ ‫ص‬ ‫ي‬ ‫ا‬ ‫غ‬ ‫ة‬ ‫ا‬ ‫مل‬ ‫س‬ ‫ب‬ ‫ق‬ ‫ة‬ - ‫ا‬ ‫ل‬ ‫خ‬ ‫ص‬ ‫ا‬ ‫ئ‬ ‫ص‬ ‫ا‬ ‫ل‬ ‫ف‬ ‫ي‬ ‫ز‬ ‫ي‬ ‫ا‬ ‫ئ‬ ‫ي‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ك‬ ‫ي‬ ‫م‬ ‫ي‬ ‫ا‬ ‫ئ‬ ‫ي‬ ‫ة‬ ‫ل‬ ‫أل‬ ‫د‬ ‫و‬ ‫ي‬ ‫ة‬ - ‫ح‬ ‫ج‬ ‫م‬ ‫ا‬ ‫ل‬ ‫ج‬ ‫س‬ ‫ي‬ ‫م‬ ‫ا‬ ‫ت‬ - ‫م‬ ‫س‬ ‫ا‬ ‫ح‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫س‬ ‫ط‬ ‫ح‬ - ‫خ‬ ‫ص‬ ‫ا‬ ‫ئ‬ ‫ص‬ ‫ا‬ ‫ل‬ ‫ت‬ ‫د‬ ‫ف‬ ‫ق‬ ‫و‬ ‫ا‬ ‫ل‬ ‫ر‬ ‫ي‬ ‫و‬ ‫ل‬ ‫و‬ ‫ج‬ ‫ي‬ ‫ا‬ - ‫ا‬ ‫ل‬ ‫ذ‬ ‫و‬ ‫ب‬ ‫ا‬ ‫ن‬ ‫ي‬ ‫ة‬ - ‫ا‬ ‫س‬ ‫ت‬ ‫ر‬ ‫ط‬ ‫ا‬ ‫ب‬ ‫ي‬ ‫ة‬ ‫و‬ ‫ت‬ ‫ر‬ ‫ط‬ ‫ي‬ ‫ب‬ ‫ا‬ ‫ل‬ ‫ق‬ ‫س‬ ‫م‬ ‫ا‬ ‫ل‬ ‫ث‬ ‫ا‬ ‫ن‬ ‫ي‬ : ‫م‬ ‫ب‬ ‫د‬ ‫أ‬ ‫ا‬ ‫مل‬ ‫ع‬ ‫ا‬ ‫ل‬ ‫ج‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ص‬ ‫ي‬ ‫د‬ ‫ال‬ ‫ن‬ ‫ي‬ ‫ة‬ - ‫خ‬ ‫ل‬ ‫ط‬ - ‫ا‬ ‫ل‬ ‫ط‬ ‫ح‬ ‫ن‬ ‫و‬ ‫ت‬ ‫ح‬ ‫ل‬ ‫ي‬ ‫ل‬ ‫ح‬ ‫ج‬ ‫م‬ ‫ا‬ ‫ل‬ ‫ج‬ ‫س‬ ‫ي‬ ‫م‬ ‫ا‬ ‫ت‬ ) ) ‫ت‬ ‫خ‬ ‫ف‬ ‫ي‬ ‫ض‬ ‫ا‬ ‫ل‬ ‫ح‬ ‫ج‬ ‫م‬ ( ( - ‫ا‬ ‫ل‬ ‫ت‬ ‫ج‬ ‫ف‬ ‫ي‬ ‫ف‬
  • 6. Course Outline • Section III: Formulation and Evaluation of pharmaceutical dosage forms - Powder and Granules  Effervescent granules: Preparation and characterization. - Tablet dosage form: Preparation and characterization.  Preparation of tablets  Formulation of Tablets  Evaluation of Tablets • ‫ا‬ ‫ل‬ ‫ق‬ ‫س‬ ‫م‬ ‫ا‬ ‫ل‬ ‫ث‬ ‫ا‬ ‫ل‬ ‫ث‬ : ‫ص‬ ‫ي‬ ‫ا‬ ‫غ‬ ‫ة‬ ‫و‬ ‫ت‬ ‫ق‬ ‫ي‬ ‫ي‬ ‫م‬ ‫أ‬ ‫ش‬ ‫ك‬ ‫ا‬ ‫ل‬ ‫ا‬ ‫ل‬ ‫ج‬ ‫ر‬ ‫ع‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ص‬ ‫ي‬ ‫د‬ ‫ال‬ ‫ن‬ ‫ي‬ ‫ة‬ - ‫م‬ ‫س‬ ‫ح‬ ‫و‬ ‫ق‬ ‫و‬ ‫ح‬ ‫ب‬ ‫ي‬ ‫ب‬ ‫ا‬ ‫ت‬ ‫ا‬ ‫ل‬ ‫ح‬ ‫ب‬ ‫ي‬ ‫ب‬ ‫ا‬ ‫ت‬ ‫ا‬ ‫ل‬ ‫ف‬ ‫و‬ ‫ا‬ ‫ر‬ ‫ة‬ : ‫ا‬ ‫ل‬ ‫ت‬ ‫ح‬ ‫ض‬ ‫ي‬ ‫ر‬ ‫و‬ ‫ا‬ ‫ل‬ ‫ت‬ ‫و‬ ‫ص‬ ‫ي‬ ‫ف‬ . - ‫ش‬ ‫ك‬ ‫ل‬ ‫ج‬ ‫ر‬ ‫ع‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ج‬ ‫ه‬ ‫ا‬ ‫ز‬ ‫ا‬ ‫ل‬ ‫ل‬ ‫و‬ ‫ح‬ ‫ي‬ : ‫ا‬ ‫ل‬ ‫ت‬ ‫ح‬ ‫ض‬ ‫ي‬ ‫ر‬ ‫و‬ ‫ا‬ ‫ل‬ ‫ت‬ ‫و‬ ‫ص‬ ‫ي‬ ‫ف‬ . ‫إ‬ ‫ع‬ ‫د‬ ‫ا‬ ‫د‬ ‫ا‬ ‫أل‬ ‫ق‬ ‫ر‬ ‫ا‬ ‫ص‬ ‫ص‬ ‫ي‬ ‫ا‬ ‫غ‬ ‫ة‬ ‫ا‬ ‫أل‬ ‫ج‬ ‫ه‬ ‫ز‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ل‬ ‫و‬ ‫ح‬ ‫ي‬ ‫ة‬ ‫ت‬ ‫ق‬ ‫ي‬ ‫ي‬ ‫م‬ ‫ا‬ ‫أل‬ ‫ج‬ ‫ه‬ ‫ز‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ل‬ ‫و‬ ‫ح‬ ‫ي‬ ‫ة‬
  • 7. Laboratory Safety • Dress Code • For your protection, you are required to wear the following protective stuff, at all times during the lab:  A lab coat  Closed-Toed Shoes (no sandals or open-toed shoes)  Do not wear contact lenses • The following special protective equipment is available for specific tasks, or on your request: - Latex (and non-allergenic neoprene) gloves - Masks - Protective hair covers • ‫ق‬ ‫و‬ ‫ا‬ ‫ع‬ ‫د‬ ‫ا‬ ‫ل‬ ‫ل‬ ‫ب‬ ‫ا‬ ‫س‬ • ‫ل‬ ‫ح‬ ‫م‬ ‫ا‬ ‫ي‬ ‫ت‬ ‫ك‬ ، ‫ي‬ ‫ط‬ ‫ل‬ ‫ب‬ ‫م‬ ‫ن‬ ‫ك‬ ‫ا‬ ‫ر‬ ‫ت‬ ‫د‬ ‫ا‬ ‫ء‬ ‫ا‬ ‫ل‬ ‫ح‬ ‫م‬ ‫ا‬ ‫ي‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ت‬ ‫ا‬ ‫ل‬ ‫ي‬ ‫ة‬ ‫ا‬ ‫أل‬ ‫ش‬ ‫ي‬ ‫ا‬ ‫ء‬ ، ‫ف‬ ‫ي‬ ‫ج‬ ‫م‬ ‫ي‬ ‫ع‬ ‫ا‬ ‫أل‬ ‫و‬ ‫ق‬ ‫ا‬ ‫ت‬ ‫أ‬ ‫ث‬ ‫ن‬ ‫ا‬ ‫ء‬ ‫ا‬ ‫مل‬ ‫خ‬ ‫ت‬ ‫ب‬ ‫ر‬ : ‫م‬ ‫ع‬ ‫ط‬ ‫ف‬ ‫م‬ ‫خ‬ ‫ت‬ ‫ب‬ ‫ر‬ ‫أ‬ ‫ح‬ ‫ذ‬ ‫ي‬ ‫ة‬ ‫م‬ ‫غ‬ ‫ل‬ ‫ق‬ ‫ة‬ ‫ا‬ ‫أل‬ ‫ص‬ ‫ا‬ ‫ب‬ ‫ع‬ ) ‫ب‬ ‫د‬ ‫و‬ ‫ن‬ ‫ص‬ ‫ن‬ ‫د‬ ‫ل‬ ‫أ‬ ‫و‬ ‫أ‬ ‫ح‬ ‫ذ‬ ‫ي‬ ‫ة‬ ‫م‬ ‫ف‬ ‫ت‬ ‫و‬ ‫ح‬ ‫ة‬ ‫ا‬ ‫أل‬ ‫ص‬ ‫ا‬ ‫ب‬ ‫ع‬ ( ‫ال‬ ‫ت‬ ‫ر‬ ‫ت‬ ‫د‬ ‫ي‬ ‫ا‬ ‫ل‬ ‫ع‬ ‫د‬ ‫س‬ ‫ا‬ ‫ت‬ ‫ا‬ ‫ل‬ ‫ال‬ ‫ص‬ ‫ق‬ ‫ة‬ • ‫ت‬ ‫ت‬ ‫و‬ ‫ف‬ ‫ر‬ ‫م‬ ‫ع‬ ‫د‬ ‫ا‬ ‫ت‬ ‫ا‬ ‫ل‬ ‫ح‬ ‫م‬ ‫ا‬ ‫ي‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫خ‬ ‫ا‬ ‫ص‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ت‬ ‫ا‬ ‫ل‬ ‫ي‬ ‫ة‬ ‫مل‬ ‫ه‬ ‫ا‬ ‫م‬ ‫م‬ ‫ح‬ ‫د‬ ‫د‬ ‫ة‬ ، ‫أ‬ ‫و‬ ‫ب‬ ‫ن‬ ‫ا‬ ‫ء‬ ‫ع‬ ‫ل‬ ‫ى‬ ‫ط‬ ‫ل‬ ‫ب‬ ‫ك‬ : - ‫ق‬ ‫ف‬ ‫ا‬ ‫ز‬ ‫ا‬ ‫ت‬ ‫ا‬ ‫ل‬ ‫ال‬ ‫ت‬ ‫ك‬ ‫س‬ ) ‫و‬ ‫ا‬ ‫ل‬ ‫ن‬ ‫ي‬ ‫و‬ ‫ب‬ ‫ر‬ ‫ي‬ ‫ن‬ ‫غ‬ ‫ي‬ ‫ر‬ ‫ا‬ ‫مل‬ ‫س‬ ‫ب‬ ‫ب‬ ‫ة‬ ‫ل‬ ‫ل‬ ‫ح‬ ‫س‬ ‫ا‬ ‫س‬ ‫ي‬ ‫ة‬ ( - ‫ا‬ ‫أل‬ ‫ق‬ ‫ن‬ ‫ع‬ ‫ة‬ - ‫أ‬ ‫غ‬ ‫ط‬ ‫ي‬ ‫ة‬ ‫ا‬ ‫ل‬ ‫ش‬ ‫ع‬ ‫ر‬ ‫ا‬ ‫ل‬ ‫و‬ ‫ا‬ ‫ق‬ ‫ي‬ ‫ة‬