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Module 1
With increasing stress on a material ,i.e. ,by applying load ,there
are possibilities that a material may fail before reaching the
desired stress value.
To improve the hardness of a substance so that it is able to sustain
more load in the elastic region process of strain hardening is done
Here ductility is compromised to get hardness and strength
 PRINCIPLE
The ability of a metal to plastically deform depends on the ability of
dislocation to move
If the concentration of the dislocation increases , the material resists their
further outflow by resisting further deformation or becoming more
harder.
2
• THEORY OF WORK HARDENING
• STAGES OF WORK HARDENING
• ADVANTAGES
• DISADVANTAGES
• ANNEALING
• INDUSTRIAL APPLICATIONS
• REFERENCES
• DEMONSTRATION
4
Before work hardening, the lattice of the material
exhibits a regular, nearly defect-free pattern
As the material is work hardened it becomes
increasingly saturated with new dislocations, and
more dislocations are prevented from nucleating (a
resistance to dislocation-formation develops).
This resistance to dislocation-formation manifests
itself as a resistance to plastic deformation; hence,
the observed strengthening.
5
6
7
• STAGE I : Easy Glide Region
• STAGE II : Linear Hardening Region
• STAGE III : Parabolic Hardening Region
9
• Shear stress is almost constant.
• Very low work hardening rate.
• BCC system do not exhibit an easy glide.
10
• Increase in degree of cross slip.
• Low hardening rate.
• Shape is parabolic.
12
No heating required.
Better surface finish.
Superior dimensional control.
Better reproducibility and interchange ability.
Directional properties can be imparted into the
metal.
Contamination problems are minimized.
13
Greater forces are required.
Heavier and more powerful equipment and
stronger tooling are required.
Metal is less ductile.
Intermediate anneals may be required to
compensate for loss of ductility that
accompanies strain hardening.
Undesirable residual stress may be produced.
14
Annealing is done when strain hardened materials are
exposed to heat above recrystallization temperature for
definite time and then it is cooled at room temperature.
 It has 3 basic stages :
RECOVERY
RECRYSTALLIZATION
GRAIN GROWTH
15
 The relief of some of the internal strain energy of a previously cold-
worked material.
 Relieves the stresses from cold working
 Recovery involves annihilation of point defects.
 Driving force for recovery is decrease in stored energy from cold work.
 During recovery, physical properties of the cold worked material
are restored without any observable change in microstructure.
 Recovery is first stage of annealing which takes place at low
temperatures of annealing.
 There is some reduction, though not substantial, in dislocation
density as well apart from formation of dislocation configurations
with low strain energies.
 Let us now examine the changes that occur when a
sample is heated from room temperature.
 At first, recovery occurs in which there is a change in the
stored energy without any obvious change in the optical
microstructure.
 Excess vacancies and interstitials anneal out giving a
drop in the electrical resistivity.
 Dislocations become mobile at a higher temperature,
eliminate and rearrange to give polygonization.
 Modest effects on mechanical behaviour
 This follows recovery during annealing of cold worked material.
Driving force is stored energy during cold work.
 It involves replacement of cold-worked structure by a new set of
strain-free, approximately equi-axed grains to replace all the
deformed crystals.
 This process ocurs above recrystallisation temperature which is
defined as the temperature at which 50% of material recrystallises
in one hour time.
 The recrystallization temperature is strongly dependent on the
purity of a material.
 Pure materials may recrystallize around 0.3Tm, while impure
materials may recrystallise around 0.4Tm, where Tm is absolute
melting temperature of the material.
 The nucleation of new grains happens in regions of
high dislocation density.
 Nucleation begins in a jumble of dislocations. The
recrystallised grain will essentially be free from
dislocations.
 A greater nucleation rate leads to a finer ultimate grain
size.
 There is a critical level of deformation below which there
will be no recrystallisation at all.
 A critical strain anneal can lead to a single crystal
recrystallisation.
 Grain growth follows complete crystallization if the material is
left at elevated temperatures.
 Grain growth does not need to be preceded by recovery
and recrystallization; it may occur in all polycrystalline
materials.
 In contrary to recovery and recrystallization, driving force for this
process is reduction in grain boundary energy.
 Tendency for larger grains to grow at the expense of smaller grains
is based on physics.
 In practical applications, grain growth is not desirable.
 Incorporation of impurity atoms and insoluble second phase
particles are effective in retarding grain growth.
 Grain growth is very strongly dependent on temperature
 Construction materials - High strength reduces
the need for material thickness which generally
saves weight and cost.
 Machine cutting tools (drill bits, taps, lathe tools)
need be much harder than the material they are
operating on in order to be effective.
 Knife blades – a high hardness blade keeps a
sharp edge.
 Anti-fatigue - Hardening can drastically improve
the service life of mechanical components with
repeated loading/unloading, such as axles and
cogs.
17
S.No. Cold working Hot working
1
It is done at a temperature below the
recrystallization temperature.
Hot working is done at a temperature above
recrystallization temperature.
2.
It is done below recrystallization temperature so
it is accomplished by strain hardening.
Hardening due to plastic deformation is
completely eliminated.
3.
Cold working decreases mechanical properties of
metal like elongation, reduction of area and
impact values.
It increases mechanical properties.
4. Crystallization does not take place. Crystallization takes place.
5. Material is not uniform after this working. Material is uniform thought.
6. There is more risk of cracks. There is less risk of cracks.
7.
Cold working increases ultimate tensile strength,
yield point hardness and fatigue strength but
decreases resistance to corrosion.
In hot working, ultimate tensile strength,
yield point, corrosion resistance are
unaffected.
S.No. Cold working Hot working
8. Internal and residual stresses are produced. Internal and residual stresses are not produced.
9. Cold working required more energy for
plastic deformation.
It requires less energy for plastic deformation
because at higher temperature metal become
more ductile and soft.
10. More stress is required. Less stress required.
11. It does not require pickling because no
oxidation of metal takes place.
Heavy oxidation occurs during hot working so
pickling is required to remove oxide.
12. Embrittlement does not occur in cold working
due to no reaction with oxygen at lower
temperature.
There is chance of embrittlement by oxygen in hot
working hence metal working is done at inert
atmosphere for reactive metals.
DEMONSTRATION
19

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Strain hardening.

  • 2. With increasing stress on a material ,i.e. ,by applying load ,there are possibilities that a material may fail before reaching the desired stress value. To improve the hardness of a substance so that it is able to sustain more load in the elastic region process of strain hardening is done Here ductility is compromised to get hardness and strength  PRINCIPLE The ability of a metal to plastically deform depends on the ability of dislocation to move If the concentration of the dislocation increases , the material resists their further outflow by resisting further deformation or becoming more harder. 2
  • 3. • THEORY OF WORK HARDENING • STAGES OF WORK HARDENING • ADVANTAGES • DISADVANTAGES • ANNEALING • INDUSTRIAL APPLICATIONS • REFERENCES • DEMONSTRATION 4
  • 4. Before work hardening, the lattice of the material exhibits a regular, nearly defect-free pattern As the material is work hardened it becomes increasingly saturated with new dislocations, and more dislocations are prevented from nucleating (a resistance to dislocation-formation develops). This resistance to dislocation-formation manifests itself as a resistance to plastic deformation; hence, the observed strengthening. 5
  • 5. 6
  • 6. 7
  • 7. • STAGE I : Easy Glide Region • STAGE II : Linear Hardening Region • STAGE III : Parabolic Hardening Region 9
  • 8. • Shear stress is almost constant. • Very low work hardening rate. • BCC system do not exhibit an easy glide. 10
  • 9. • Increase in degree of cross slip. • Low hardening rate. • Shape is parabolic. 12
  • 10. No heating required. Better surface finish. Superior dimensional control. Better reproducibility and interchange ability. Directional properties can be imparted into the metal. Contamination problems are minimized. 13
  • 11. Greater forces are required. Heavier and more powerful equipment and stronger tooling are required. Metal is less ductile. Intermediate anneals may be required to compensate for loss of ductility that accompanies strain hardening. Undesirable residual stress may be produced. 14
  • 12. Annealing is done when strain hardened materials are exposed to heat above recrystallization temperature for definite time and then it is cooled at room temperature.  It has 3 basic stages : RECOVERY RECRYSTALLIZATION GRAIN GROWTH 15
  • 13.
  • 14.  The relief of some of the internal strain energy of a previously cold- worked material.  Relieves the stresses from cold working  Recovery involves annihilation of point defects.  Driving force for recovery is decrease in stored energy from cold work.  During recovery, physical properties of the cold worked material are restored without any observable change in microstructure.  Recovery is first stage of annealing which takes place at low temperatures of annealing.  There is some reduction, though not substantial, in dislocation density as well apart from formation of dislocation configurations with low strain energies.
  • 15.  Let us now examine the changes that occur when a sample is heated from room temperature.  At first, recovery occurs in which there is a change in the stored energy without any obvious change in the optical microstructure.  Excess vacancies and interstitials anneal out giving a drop in the electrical resistivity.  Dislocations become mobile at a higher temperature, eliminate and rearrange to give polygonization.  Modest effects on mechanical behaviour
  • 16.  This follows recovery during annealing of cold worked material. Driving force is stored energy during cold work.  It involves replacement of cold-worked structure by a new set of strain-free, approximately equi-axed grains to replace all the deformed crystals.  This process ocurs above recrystallisation temperature which is defined as the temperature at which 50% of material recrystallises in one hour time.  The recrystallization temperature is strongly dependent on the purity of a material.  Pure materials may recrystallize around 0.3Tm, while impure materials may recrystallise around 0.4Tm, where Tm is absolute melting temperature of the material.
  • 17.  The nucleation of new grains happens in regions of high dislocation density.  Nucleation begins in a jumble of dislocations. The recrystallised grain will essentially be free from dislocations.  A greater nucleation rate leads to a finer ultimate grain size.  There is a critical level of deformation below which there will be no recrystallisation at all.  A critical strain anneal can lead to a single crystal recrystallisation.
  • 18.  Grain growth follows complete crystallization if the material is left at elevated temperatures.  Grain growth does not need to be preceded by recovery and recrystallization; it may occur in all polycrystalline materials.  In contrary to recovery and recrystallization, driving force for this process is reduction in grain boundary energy.  Tendency for larger grains to grow at the expense of smaller grains is based on physics.  In practical applications, grain growth is not desirable.  Incorporation of impurity atoms and insoluble second phase particles are effective in retarding grain growth.  Grain growth is very strongly dependent on temperature
  • 19.  Construction materials - High strength reduces the need for material thickness which generally saves weight and cost.  Machine cutting tools (drill bits, taps, lathe tools) need be much harder than the material they are operating on in order to be effective.  Knife blades – a high hardness blade keeps a sharp edge.  Anti-fatigue - Hardening can drastically improve the service life of mechanical components with repeated loading/unloading, such as axles and cogs. 17
  • 20. S.No. Cold working Hot working 1 It is done at a temperature below the recrystallization temperature. Hot working is done at a temperature above recrystallization temperature. 2. It is done below recrystallization temperature so it is accomplished by strain hardening. Hardening due to plastic deformation is completely eliminated. 3. Cold working decreases mechanical properties of metal like elongation, reduction of area and impact values. It increases mechanical properties. 4. Crystallization does not take place. Crystallization takes place. 5. Material is not uniform after this working. Material is uniform thought. 6. There is more risk of cracks. There is less risk of cracks. 7. Cold working increases ultimate tensile strength, yield point hardness and fatigue strength but decreases resistance to corrosion. In hot working, ultimate tensile strength, yield point, corrosion resistance are unaffected.
  • 21. S.No. Cold working Hot working 8. Internal and residual stresses are produced. Internal and residual stresses are not produced. 9. Cold working required more energy for plastic deformation. It requires less energy for plastic deformation because at higher temperature metal become more ductile and soft. 10. More stress is required. Less stress required. 11. It does not require pickling because no oxidation of metal takes place. Heavy oxidation occurs during hot working so pickling is required to remove oxide. 12. Embrittlement does not occur in cold working due to no reaction with oxygen at lower temperature. There is chance of embrittlement by oxygen in hot working hence metal working is done at inert atmosphere for reactive metals.