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ISSN No: 2456
International Journal of Trend in Scientific
Research and
International Conference on Advanced Engineering
and Information Technology
Experimental Analysis
Properties
Deepak T. J.1
, Senyange E. K.
1
Faculty of Engineering and Technology,
2
Faculty of Built Environment, Linton University College, Mantin, Negeri Sembilan, Malaysia
ABSTRACT
The current world is witnessing the construction of
challenging and innovative civil engineering
structures. It has been established that when fibers are
added in certain percentage to the concrete improves
the strength properties as well as crack resistance and
ductility. Fibers impart energy absorption, toughness
and impact resistance properties to fiber reinforced
concrete material and these characteristics in turn
improve the strength properties. In the present
experimental investigation the alkali resistant glass
fiber of diameter 14 micron, length 24mm, having an
aspect ratio of 855 was employed in percentage
varying from 0, 10%, 20%, 30%, 50%, 60% and 80%
to study the effect on compressive, split tensile and
flexural strength on M40 grade concrete. At early age
strength, the concrete with more than 20% of glass
fiber gain strength around 61% until 82% faster than
normal concrete. This implies that glass fibers assist
in increasing the Compressive strength of concrete.
The higher the glass fiber, in the mix the compressive
strength also increases.
Keywords: Glass fiber, fatigue, fracture, concrete,
toughness, impact and workability
1. INTRODUCTION
Glass fiber also known as fiberglass is a material
consist of numerous extremely fine fiber of glass.
Before, glass fiber was known as “glass wool” was
inverted in 1938 by Russell Games Slayter of Owen
Coming as the material to be used for insulation. Ever
since manufacturing, it has been used widely as an
insulating material; Glass fiber is also used as a
@ IJTSRD | Available Online @ www.ijtsrd.com | Special Issue Publication | November
ISSN No: 2456 - 6470 | www.ijtsrd.com | Special Issue
International Journal of Trend in Scientific
Research and Development (IJTSRD)
International Conference on Advanced Engineering
and Information Technology (ICAEIT-2017)
Experimental Analysis on Strength
Properties of Glass Fiber Concrete
, Senyange E. K.2
, Iman. F.2
, Nazrul Azmi A. Z.2
, Chakravarthy N.
Faculty of Engineering and Technology, Linton University College, Mantin, Negeri Sembilan, Malaysia
Faculty of Built Environment, Linton University College, Mantin, Negeri Sembilan, Malaysia
The current world is witnessing the construction of
and innovative civil engineering
structures. It has been established that when fibers are
added in certain percentage to the concrete improves
the strength properties as well as crack resistance and
ductility. Fibers impart energy absorption, toughness
d impact resistance properties to fiber reinforced
concrete material and these characteristics in turn
improve the strength properties. In the present
experimental investigation the alkali resistant glass
fiber of diameter 14 micron, length 24mm, having an
aspect ratio of 855 was employed in percentage
varying from 0, 10%, 20%, 30%, 50%, 60% and 80%
to study the effect on compressive, split tensile and
flexural strength on M40 grade concrete. At early age
strength, the concrete with more than 20% of glass
iber gain strength around 61% until 82% faster than
normal concrete. This implies that glass fibers assist
in increasing the Compressive strength of concrete.
The higher the glass fiber, in the mix the compressive
fiber, fatigue, fracture, concrete,
Glass fiber also known as fiberglass is a material
consist of numerous extremely fine fiber of glass.
was known as “glass wool” was
inverted in 1938 by Russell Games Slayter of Owen-
Coming as the material to be used for insulation. Ever
since manufacturing, it has been used widely as an
insulating material; Glass fiber is also used as a
reinforcing for many agents and polymeric products
or glass-reinforced plastic (GRP) (Cuevas, 2012).
Glass fibers are widely used for reinforcement due to
their mechanical properties such as high strength
(tensile strength of 3.40 GPa, tolerance to high
temperature, resistance to corrosive environment as
well as low cost, despite of low stiffness. The stiffness
for glass fiber range from approximately 70 to 90
GPa. Moreover, glass fibers are more sensitive to
moisture. Johnston and Colin (2000), suggested that
the strength of a glass fiber specimen decrease by
35% (769 – 499) when exposed to water at a room
temperature under constant load.
Production of glass fiber requires much energy and
fossil fuels. Glass processing is dusty, which make the
production of glass fibe
environmental pollution mostly air pollution (Daniel
and Negtegaal, 2001). Glass fibers also require high
temperature to manufacture like any fiber such as
carbon fiber. The amount of carbon emission and by
products produced as the resul
needs to be quantified for carbon fiber and all other
basic construction materials in order to assess the
sustainability of glass fiber (Johnston and Colin
2000).
Jain and Lee, (2012) highlighted that there are
significant environmental
sustainable fiber glass. First, no large smoke plumes
or other forms of environmental pollution produced
from GRP (Glass Reinforced Plastic) / FRP (Fiber
Reinforced Plastic) products. Unlike wood and metal
November 2018 P - 1
Special Issue Publication
International Conference on Advanced Engineering
, Chakravarthy N.2
Linton University College, Mantin, Negeri Sembilan, Malaysia
Faculty of Built Environment, Linton University College, Mantin, Negeri Sembilan, Malaysia
many agents and polymeric products
reinforced plastic (GRP) (Cuevas, 2012).
Glass fibers are widely used for reinforcement due to
their mechanical properties such as high strength
(tensile strength of 3.40 GPa, tolerance to high
sistance to corrosive environment as
well as low cost, despite of low stiffness. The stiffness
for glass fiber range from approximately 70 to 90
GPa. Moreover, glass fibers are more sensitive to
moisture. Johnston and Colin (2000), suggested that
gth of a glass fiber specimen decrease by
499) when exposed to water at a room
temperature under constant load.
Production of glass fiber requires much energy and
fossil fuels. Glass processing is dusty, which make the
production of glass fiber a contributor to
environmental pollution mostly air pollution (Daniel
and Negtegaal, 2001). Glass fibers also require high
temperature to manufacture like any fiber such as
carbon fiber. The amount of carbon emission and by-
products produced as the result of manufacturing
needs to be quantified for carbon fiber and all other
basic construction materials in order to assess the
sustainability of glass fiber (Johnston and Colin
Jain and Lee, (2012) highlighted that there are
benefits to choose
sustainable fiber glass. First, no large smoke plumes
or other forms of environmental pollution produced
from GRP (Glass Reinforced Plastic) / FRP (Fiber
Reinforced Plastic) products. Unlike wood and metal
International Journal of Trend in Scientific Research and Development (IJTSRD) | ISSN: 2456-647
@ IJTSRD | Available Online @ www.ijtsrd.com | Special Issue Publication | November 2018 P - 2
products, generally glass fibers are environmental
friendly, economical, highly resistant to corrosion and
more suitable than steel, aluminium and timber. Use
of fiberglass in lieu of steel, aluminium and timber
also means there will be less demand upon our natural
resources and a reduction of the environmental impact
resulting from the production of metals and the
disposal of their waste.
Alkali Resistant Glass Fiber is a recent introduction in
making fibrous concrete. Glass fiber which is
originally used in conjunction with cement was found
to be affected by alkaline condition of cement. Heurik
et al. (2004) has outlined the classification and
structural applications of composite materials.
Majumdar et al. (1991) has worked on the
development of fiber reinforced cements. Sivakumar
et al. (2007) has studied the properties of FRC using
high percentage dosages of hybrid fiber like steel,
glass and polypropylene. High strength concretes
were produced by using the above fibers. From the
various investigations studied it is clear that non
metallic fibers like glass and polypropylene can be
tried in FRC to derive benefits like more ductility,
impact resistance, crack resistance etc.
However, this paper presents the effect of glass fibers
on the compressive, split tensile and flexural strength
of the concrete.
2. Methodology
2.1 Materials used
Cement
The cement was of 53 grade, with specific gravity of
2.9 and fineness of 2800 cm2
/gm, prior preparation of
specimens it was stored in a humidity controlled room
to prevent it being exposed to the moisture.
Coarse aggregate
The coarse aggregate used for this research was well
graded angular granite machine crushed, passed
through 20mm sieve test, the specific gravity is 2.7,
flakiness index of 4.35% and elongation index of
3.64%. The aggregate was washed to be free from
dust, clay or any other organic matter.
Fine aggregate
Fine aggregate are normally obtained locally from
rivers or lakes. British Standards defined this material
as material passing 5.0 mm test sieve but retained on a
75 μm test sieve. The fine aggregate used for this
research having specific gravity of 2.4 passed through
5mm sieve test. The aggregate was kept in a dry place
prior mixed to ensure the moisture content is
controlled during mixing process.
Water
Portable water available in locality suitable for
drinking was used to prepare the concrete mix, the
main purpose of water as we have seen in literature
review is to set cement (to start chemical reaction
within cement pastes). The same type of water was
also used for curing concrete.
Glass Fiber
These are the main materials which were added to
reinforce the concrete. As stated in the literature
review glass fiber has high tensile strength of 2 –
4Gpa and elastic modulus of 70 – 80Gpa, brittle stress
strain characteristic from 2.4 – 4.8 elongation at break
and low creep at room temperature. Glass fiber also is
susceptible to alkali attack.
Type of glass fiber used was alkali resistance (AR-
Type) glass fiber having the following properties:-
 Aspect ratio of 857:1
 Density of 2.6t/m3
 Elastic modulus of 73GPa
 Tensile strength of 1.7GPa
 Density of 14micronon
 Length divided into 24mm
 Number of fiber 212million/kg
2.2 Mix design
The concrete mix design is based on the method
published by Department of the Environment (DOE)
in 1988 edition. The description provided in that
article illustrate the principle for methods, number of
design exercise were carried out in order to become
familiar with the design procedure. The DOE method
also provide information necessary to design concrete
for indirect tensile strength, containing entrained air
and using cement replacement but that was the focus.
The method is divided into five sections where by
section 1 is to deal with strength of concrete; section 2
is to deal with workability; section 3 is to deal with
cement content; section 4 is to deal with density of
fresh concrete; and finally section 5 is deal with
proportion of sand. Results were obtained from
various graphs and filled in the Table 1 provided by
DOE.
The aim was to design the concrete of characteristic
strength of 40 N/mm2
at 28 days by using Ordinary
International Journal of Trend in Scientific
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Portland Cement (OPC); The proportional defective
(percentage of failure) to be of 5 percent. The slump
range from 30 – 60 and the Vebe time within 3
seconds.
The relative density of aggregate was considered to be
2.7; the aggregates were well crushed with the
maximum size of 20mm. By using the DOE method
of mix design (1988 Edition) the quantities of cement,
water, sand and aggregate were obtained per cubic
meter. The amount of each quantity was divided by
the total volume for the specimens to acquire the
precise amount of each ingredient to be added in the
mix.
2.3 Casting and Curing of Concrete
After preparing the mix, cylindrical moulds of
diameter 100mm and height 200mm, cubes of 150 x
150 x 150mm and beam moulds of 110 x 110 x
5000mm were casted. Fresh concrete mix containing
Table 2: Compressive strength of concrete specimens at 7, 28, and 56 days of curing
Glass Fiber
(%)
Average 7 Days
Strength (N/mm
0 22.63
10 24.74
20 36.52
30 36.63
50 40.27
60 40.16
80 41.08
Figure 1: Graph of average compressive strength vs.
days of curing
The effect of Glass fiber on strength of concrete is
shown in Figure 1, which presents the substantial
increment compressive strength values of concrete
mixtures with different proportions of glass fiber
cured at 7 days, 28 days and 56 days. It is observed
International Journal of Trend in Scientific Research and Development (IJTSRD)
@ IJTSRD | Available Online @ www.ijtsrd.com | Special Issue Publication | November
Portland Cement (OPC); The proportional defective
(percentage of failure) to be of 5 percent. The slump
60 and the Vebe time within 3 – 6
The relative density of aggregate was considered to be
2.7; the aggregates were well crushed with the
maximum size of 20mm. By using the DOE method
of mix design (1988 Edition) the quantities of cement,
water, sand and aggregate were obtained per cubic
er. The amount of each quantity was divided by
the total volume for the specimens to acquire the
precise amount of each ingredient to be added in the
After preparing the mix, cylindrical moulds of
nd height 200mm, cubes of 150 x
150 x 150mm and beam moulds of 110 x 110 x
5000mm were casted. Fresh concrete mix containing
different percentages by volume of glass fiber was
casted into the moulds. The mix was casted carefully
to avoid segregation. The concrete was compacted by
using a steer bar to remove the voids. After 24 hours
the cement had set and hardened enough, the moulds
were removed. All the concrete cylinders, cubes and
beams were set into the curing tank for curing. The
curing was done at an average temperature of 27
the period of 7days, 28days and 56days.
3. Results and Discussion
3.1 Compressive Strength
The most valuable property in concrete is the concrete
compressive strength because it gives the overall
definition of the quality concrete strength that relates
to the hydrated cement paste. Basically, the specimens
were being tests for three selected curing periods
namely: 7, 28, 56 days, detail test results are shown in
Table 2.
Table 2: Compressive strength of concrete specimens at 7, 28, and 56 days of curing
Average 7 Days
Strength (N/mm2
)
Average 28 Days
Strength (N/mm2
)
Average 56 Days
Strength (N/mm
22.63 38.52 42.21
24.74 40.63 46.2
36.52 43.8 48.43
36.63 48.54 49.64
40.27 49.24 50.02
40.16 49.04 50.67
41.08 52.45 51.53
compressive strength vs.
The effect of Glass fiber on strength of concrete is
shown in Figure 1, which presents the substantial
increment compressive strength values of concrete
mixtures with different proportions of glass fiber
cured at 7 days, 28 days and 56 days. It is observed
that the concrete with higher percentage of glass fiber
gain strength between 61% until 82% faster than
normal at early age. For instance the GFRC with 80%
fiber content was able to achieve the targe
after 7 days of curing. Once more it is observed that
there is an enormous 48% increment in strength
between GFRC with 10% and 20% of fiber. Concrete
with 20% of fiber is adequate to improves the bond
between cement and aggregates. The
also speeds up the hydration. During hydration
process water is absorbed by glass fiber results
strengthening of inter-molecule bond.
Apparently, addition of glass fiber contributing much
on strength of the concrete, as it is observed in the
graph at 7 days of curing, specimens with high
percentage of glass fiber (50% 60% and 80%) have
achieved compressive strength above the targeted
characteristics strength of 40 N/mm
the graph shows that at 56days of curing all the
| ISSN: 2456-647
November 2018 P - 3
different percentages by volume of glass fiber was
casted into the moulds. The mix was casted carefully
oncrete was compacted by
using a steer bar to remove the voids. After 24 hours
the cement had set and hardened enough, the moulds
were removed. All the concrete cylinders, cubes and
beams were set into the curing tank for curing. The
average temperature of 27°
C for
the period of 7days, 28days and 56days.
The most valuable property in concrete is the concrete
compressive strength because it gives the overall
concrete strength that relates
to the hydrated cement paste. Basically, the specimens
were being tests for three selected curing periods
namely: 7, 28, 56 days, detail test results are shown in
Table 2: Compressive strength of concrete specimens at 7, 28, and 56 days of curing
Average 56 Days
Strength (N/mm2
)
that the concrete with higher percentage of glass fiber
gain strength between 61% until 82% faster than
normal at early age. For instance the GFRC with 80%
fiber content was able to achieve the targeted strength
after 7 days of curing. Once more it is observed that
there is an enormous 48% increment in strength
between GFRC with 10% and 20% of fiber. Concrete
is adequate to improves the bond
between cement and aggregates. The presence of fiber
also speeds up the hydration. During hydration
process water is absorbed by glass fiber results
molecule bond.
Apparently, addition of glass fiber contributing much
on strength of the concrete, as it is observed in the
aph at 7 days of curing, specimens with high
percentage of glass fiber (50% 60% and 80%) have
achieved compressive strength above the targeted
characteristics strength of 40 N/mm2
. Nevertheless,
the graph shows that at 56days of curing all the
International Journal of Trend in Scientific
@ IJTSRD | Available Online @ www.ijtsrd.com
specimens where able to achieve strength above the
targeted strength.
3.2 Tensile Strength
The split tensile strength of the concrete specimens
was determined at 7, 28 and 56 days following BS EN
12390 part 6: 2009.
Table 3: Split Tensile strength of concrete speci
at 7, 28, and 56 days of curing
Glass
Fiber
(%)
Average 7
Days
Strength
(N/mm2
)
Average 28
Days
Strength
(N/mm2
)
0 3.42 4.24
10 3.52 4.5
20 3.83 5.15
30 4.12 4.92
50 4.16 5.3
60 4.29 5.59
80 4.58 6.84
Figure 2: Graph of average tensile strength vs. days of
curing
Figure 2 shows the tensile strength of GFRC against
days of curing. The figure illustrates the evidence that
the split tensile strength of GFRC increases with the
increase of curing days together with content of fiber
incorporated into the mix. The graph s
specimen with high percentage of glass fiber (80%)
have achieved extremely high split tensile strength at
all days of curing. Concrete with 80% of glass fiber
gain 60% and 61% of split tensile strength
respectively at 28 days and 56 days of curin
compared to the higher percentage strength of tensile
for the normal concrete. This implies that GFRC
achieves most of its split tensile strength after the age
of 28 days however the strength is slightly increasing
as the day of curing is increasing. Oth
samples with glass fiber have shown remarkable
International Journal of Trend in Scientific Research and Development (IJTSRD)
@ IJTSRD | Available Online @ www.ijtsrd.com | Special Issue Publication | November
ere able to achieve strength above the
The split tensile strength of the concrete specimens
was determined at 7, 28 and 56 days following BS EN
Table 3: Split Tensile strength of concrete specimens
at 7, 28, and 56 days of curing
Average 56
Days
Strength
(N/mm2
)
4.51
5.05
5.81
6.25
6.32
6.55
7.2
Figure 2: Graph of average tensile strength vs. days of
Figure 2 shows the tensile strength of GFRC against
days of curing. The figure illustrates the evidence that
the split tensile strength of GFRC increases with the
increase of curing days together with content of fiber
The graph shows that
specimen with high percentage of glass fiber (80%)
have achieved extremely high split tensile strength at
Concrete with 80% of glass fiber
gain 60% and 61% of split tensile strength
respectively at 28 days and 56 days of curing
compared to the higher percentage strength of tensile
for the normal concrete. This implies that GFRC
achieves most of its split tensile strength after the age
of 28 days however the strength is slightly increasing
as the day of curing is increasing. Other than that,
samples with glass fiber have shown remarkable
increase in split tensile strength with ages of curing
unlike the control samples (0%) glass fiber.
3.3 Flexural Strength
Flexural strength can be described as the capacity of a
beam or even a slab of concrete to resist failure due to
bending. This flexural strength is also known as
Modulus of Rupture. The effect of concrete with
various percentage of glass fiber on flexural
is shown on table 4. The flexural strength was tested
on 7, 28 and 56 days of curing.
Table 4: Flexural strength of concrete specimens at 7,
28, and 56 days of curing
Glass
Fiber
(%)
Average 7
Days
Strength
(N/mm2
)
Average 28
Days
Strength
(N/mm
0 2.76 4.11
10 3.76 4.5
20 4.09 4.81
30 4.37
50 4.55 5.28
60 4.8 5.3
80 4.82 5.65
Figure 3: Graph of average flexural strength vs. days
of curing
Based on the figure 3, the graph shows that concrete
with higher percentage of glass fiber have higher
flexural strength, also concrete of with lower
percentage of glass fiber have lower flexural strength.
In other words, the graph shows the evidence that
flexural strength increases with the increase in fiber
content.
The graph also shows that, the gain of flexural
strength is higher between 7 to 28 days than 28 to 56
days. This implies that at 28 days of curing GFRC
achieves sufficient strength. It is ob
| ISSN: 2456-647
November 2018 P - 4
increase in split tensile strength with ages of curing
unlike the control samples (0%) glass fiber.
Flexural strength can be described as the capacity of a
beam or even a slab of concrete to resist failure due to
bending. This flexural strength is also known as
. The effect of concrete with
various percentage of glass fiber on flexural strength
is shown on table 4. The flexural strength was tested
on 7, 28 and 56 days of curing.
Table 4: Flexural strength of concrete specimens at 7,
28, and 56 days of curing
Average 28
Days
Strength
(N/mm2
)
Average 56
Days
Strength
(N/mm2
)
4.11 4.31
4.5 4.92
4.81 5.32
5 5.72
5.28 6
5.3 6.18
5.65 7.3
Figure 3: Graph of average flexural strength vs. days
of curing
Based on the figure 3, the graph shows that concrete
with higher percentage of glass fiber have higher
flexural strength, also concrete of with lower
percentage of glass fiber have lower flexural strength.
In other words, the graph shows the evidence that
flexural strength increases with the increase in fiber
The graph also shows that, the gain of flexural
strength is higher between 7 to 28 days than 28 to 56
days. This implies that at 28 days of curing GFRC
achieves sufficient strength. It is observed that the
International Journal of Trend in Scientific Research and Development (IJTSRD) | ISSN: 2456-647
@ IJTSRD | Available Online @ www.ijtsrd.com | Special Issue Publication | November 2018 P - 5
flexural strength for the specimens having 80 percent
of fiber increased dramatic for 28 and 56 days while
for 7 days the increase is marginal.
4. Conclusions
Extensive experimentation was carried out with
various glass fiber percentages on concrete. For all
mixes, compressive strength, tensile strength and
flexural strength were determined at 7, 28 and 56
days. The following conclusions can be derived from
the investigation:
A. With minimum of 20% glass fiber is adequate to
improve the early age strength of the concrete.
This implies that glass fibers assist in increasing
the compressive strength of concrete. However,
the strength of the concrete at 56days are
relatively similar with the higher different of
strength only 22% for concrete with 80% glass
fiber.
B. The split tensile strength of “AR Glass fiber” for
M40 concrete is maximum when 80% of glass
fiber was incorporated into mix, this implies that
split tensile strength of Glass Fiber Reinforced
Concrete is high when the amount of fiber
incorporated into the concrete is also higher.
C. The flexural strength of “AR Glass fiber” for M40
concrete in this research is found to be maximum
at 80% glass fiber mix. This also implies that
flexural strength of Glass Fiber Reinforced
Concrete is high when the amount of fiber
incorporated into the concrete is also higher.
D. Fibers impart energy absorption, toughness and
impact resistance properties to fiber reinforced
concrete material and these characteristics in turn
improve the strength properties.
5. Acknowledgements
Authors would like to thank the Linton University
College and its group of institution’s Top
Management for their continuous support.
6. References
1. British Standards (BS), 1983, BS 1881: Part 110 -
Testing concrete. Method for making test
cylinders from fresh concrete. British Standard
Institute.
2. British Standards (BS), 1970, BS 1881: Part 3 -
Testing concrete. Method for curing concrete.
British Standard Institute.
3. British Standards (BS), 1983, BS 1881: Part 116 -
Testing concrete. Method for determination
compressive strength. British Standard Institute.
4. British Standards (BS), 1983, BS 1881: Part 118 -
Testing concrete. Method for determination
flexural strength. British Standard Institute.
5. British Standards (BS), 1983, BS 1881: Part 117 -
Testing concrete. Method for determination split
tensile strength. British Standard Institute.
6. British Standards (BS), EN 12390-6 2009, testing
hardened concrete Part 6: Split Tensile Strength of
concrete, European Committee for
Standardization.
7. Cuevas. Sherron, 2012, Fibre Material and
Technology: World Technologies.
8. Daniel R. A., Nagtegaal G., 2001, Pedestrain
bridge of pultruded sections as result of ecological
design. In: Proceedings of the EPTA seminar,
Roermond, Oct 2001.
9. Deepak T. J., Jalam A. A., Eric Loh, Siow Yun
Tong, Sudesh Nair, Panjehpour, 2015,
Prognostication of Concrete Characteristics with
Coconut Shell as Coarse Aggregate Partial
Percentile Replacement. International Journal of
Scientific Research in Science, Engineering and
Technology. Volume 1/Issue 4/456
10. Department of Environment (DOE), 1988, Design
of Normal Concrete mixes, 2nd Edition,
Construction Research Communications Ltd.
11. Heurik Strang, Victor C. Li. 2004. Classification
of Fiber Reinforced Cementitious Materials for
Structural Applications 6th Rilem symposium on
FRC, 20–22 Sep.Varenna, Italy, pp. 197–218.
12. Jain, R., and Lee, L., 2012, Fibre Reinforced
Polymer (FRP) Composites for Infrastructure
Applications: Focusing on Innovation,
Technology Implementation and Sustainability,
illustrated Ed., Springer.
13. Johnston, D. Colin, 2000, Fibre – Reinforced
Cements and Concrete: Advance in Concrete
Technology, Vol. 3, Taylor & Francis Ltd.
14. Majumdar, A. J., Laws, V. 1991. Building
Research Establishment book on Glass fiber
reinforced cement 2nd ed. Oxford; Boston: BSP
Professional.
15. Sivakumar, A. and Santhanam Manu. 2007.
Mechanical Properties of High Strength Concrete
International Journal of Trend in Scientific Research and Development (IJTSRD) | ISSN: 2456-647
@ IJTSRD | Available Online @ www.ijtsrd.com | Special Issue Publication | November 2018 P - 6
Reinforced with Metallic and Non-Metallic
Fibers. Cement and Concrete Composites (29) pp.
603–608.
TABLE 1: CONCRETE MIX DESIGN BY DOE

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Experimental Analysis on Strength Properties of Glass Fiber Concrete

  • 1. @ IJTSRD | Available Online @ www.ijtsrd.com ISSN No: 2456 International Journal of Trend in Scientific Research and International Conference on Advanced Engineering and Information Technology Experimental Analysis Properties Deepak T. J.1 , Senyange E. K. 1 Faculty of Engineering and Technology, 2 Faculty of Built Environment, Linton University College, Mantin, Negeri Sembilan, Malaysia ABSTRACT The current world is witnessing the construction of challenging and innovative civil engineering structures. It has been established that when fibers are added in certain percentage to the concrete improves the strength properties as well as crack resistance and ductility. Fibers impart energy absorption, toughness and impact resistance properties to fiber reinforced concrete material and these characteristics in turn improve the strength properties. In the present experimental investigation the alkali resistant glass fiber of diameter 14 micron, length 24mm, having an aspect ratio of 855 was employed in percentage varying from 0, 10%, 20%, 30%, 50%, 60% and 80% to study the effect on compressive, split tensile and flexural strength on M40 grade concrete. At early age strength, the concrete with more than 20% of glass fiber gain strength around 61% until 82% faster than normal concrete. This implies that glass fibers assist in increasing the Compressive strength of concrete. The higher the glass fiber, in the mix the compressive strength also increases. Keywords: Glass fiber, fatigue, fracture, concrete, toughness, impact and workability 1. INTRODUCTION Glass fiber also known as fiberglass is a material consist of numerous extremely fine fiber of glass. Before, glass fiber was known as “glass wool” was inverted in 1938 by Russell Games Slayter of Owen Coming as the material to be used for insulation. Ever since manufacturing, it has been used widely as an insulating material; Glass fiber is also used as a @ IJTSRD | Available Online @ www.ijtsrd.com | Special Issue Publication | November ISSN No: 2456 - 6470 | www.ijtsrd.com | Special Issue International Journal of Trend in Scientific Research and Development (IJTSRD) International Conference on Advanced Engineering and Information Technology (ICAEIT-2017) Experimental Analysis on Strength Properties of Glass Fiber Concrete , Senyange E. K.2 , Iman. F.2 , Nazrul Azmi A. Z.2 , Chakravarthy N. Faculty of Engineering and Technology, Linton University College, Mantin, Negeri Sembilan, Malaysia Faculty of Built Environment, Linton University College, Mantin, Negeri Sembilan, Malaysia The current world is witnessing the construction of and innovative civil engineering structures. It has been established that when fibers are added in certain percentage to the concrete improves the strength properties as well as crack resistance and ductility. Fibers impart energy absorption, toughness d impact resistance properties to fiber reinforced concrete material and these characteristics in turn improve the strength properties. In the present experimental investigation the alkali resistant glass fiber of diameter 14 micron, length 24mm, having an aspect ratio of 855 was employed in percentage varying from 0, 10%, 20%, 30%, 50%, 60% and 80% to study the effect on compressive, split tensile and flexural strength on M40 grade concrete. At early age strength, the concrete with more than 20% of glass iber gain strength around 61% until 82% faster than normal concrete. This implies that glass fibers assist in increasing the Compressive strength of concrete. The higher the glass fiber, in the mix the compressive fiber, fatigue, fracture, concrete, Glass fiber also known as fiberglass is a material consist of numerous extremely fine fiber of glass. was known as “glass wool” was inverted in 1938 by Russell Games Slayter of Owen- Coming as the material to be used for insulation. Ever since manufacturing, it has been used widely as an insulating material; Glass fiber is also used as a reinforcing for many agents and polymeric products or glass-reinforced plastic (GRP) (Cuevas, 2012). Glass fibers are widely used for reinforcement due to their mechanical properties such as high strength (tensile strength of 3.40 GPa, tolerance to high temperature, resistance to corrosive environment as well as low cost, despite of low stiffness. The stiffness for glass fiber range from approximately 70 to 90 GPa. Moreover, glass fibers are more sensitive to moisture. Johnston and Colin (2000), suggested that the strength of a glass fiber specimen decrease by 35% (769 – 499) when exposed to water at a room temperature under constant load. Production of glass fiber requires much energy and fossil fuels. Glass processing is dusty, which make the production of glass fibe environmental pollution mostly air pollution (Daniel and Negtegaal, 2001). Glass fibers also require high temperature to manufacture like any fiber such as carbon fiber. The amount of carbon emission and by products produced as the resul needs to be quantified for carbon fiber and all other basic construction materials in order to assess the sustainability of glass fiber (Johnston and Colin 2000). Jain and Lee, (2012) highlighted that there are significant environmental sustainable fiber glass. First, no large smoke plumes or other forms of environmental pollution produced from GRP (Glass Reinforced Plastic) / FRP (Fiber Reinforced Plastic) products. Unlike wood and metal November 2018 P - 1 Special Issue Publication International Conference on Advanced Engineering , Chakravarthy N.2 Linton University College, Mantin, Negeri Sembilan, Malaysia Faculty of Built Environment, Linton University College, Mantin, Negeri Sembilan, Malaysia many agents and polymeric products reinforced plastic (GRP) (Cuevas, 2012). Glass fibers are widely used for reinforcement due to their mechanical properties such as high strength (tensile strength of 3.40 GPa, tolerance to high sistance to corrosive environment as well as low cost, despite of low stiffness. The stiffness for glass fiber range from approximately 70 to 90 GPa. Moreover, glass fibers are more sensitive to moisture. Johnston and Colin (2000), suggested that gth of a glass fiber specimen decrease by 499) when exposed to water at a room temperature under constant load. Production of glass fiber requires much energy and fossil fuels. Glass processing is dusty, which make the production of glass fiber a contributor to environmental pollution mostly air pollution (Daniel and Negtegaal, 2001). Glass fibers also require high temperature to manufacture like any fiber such as carbon fiber. The amount of carbon emission and by- products produced as the result of manufacturing needs to be quantified for carbon fiber and all other basic construction materials in order to assess the sustainability of glass fiber (Johnston and Colin Jain and Lee, (2012) highlighted that there are benefits to choose sustainable fiber glass. First, no large smoke plumes or other forms of environmental pollution produced from GRP (Glass Reinforced Plastic) / FRP (Fiber Reinforced Plastic) products. Unlike wood and metal
  • 2. International Journal of Trend in Scientific Research and Development (IJTSRD) | ISSN: 2456-647 @ IJTSRD | Available Online @ www.ijtsrd.com | Special Issue Publication | November 2018 P - 2 products, generally glass fibers are environmental friendly, economical, highly resistant to corrosion and more suitable than steel, aluminium and timber. Use of fiberglass in lieu of steel, aluminium and timber also means there will be less demand upon our natural resources and a reduction of the environmental impact resulting from the production of metals and the disposal of their waste. Alkali Resistant Glass Fiber is a recent introduction in making fibrous concrete. Glass fiber which is originally used in conjunction with cement was found to be affected by alkaline condition of cement. Heurik et al. (2004) has outlined the classification and structural applications of composite materials. Majumdar et al. (1991) has worked on the development of fiber reinforced cements. Sivakumar et al. (2007) has studied the properties of FRC using high percentage dosages of hybrid fiber like steel, glass and polypropylene. High strength concretes were produced by using the above fibers. From the various investigations studied it is clear that non metallic fibers like glass and polypropylene can be tried in FRC to derive benefits like more ductility, impact resistance, crack resistance etc. However, this paper presents the effect of glass fibers on the compressive, split tensile and flexural strength of the concrete. 2. Methodology 2.1 Materials used Cement The cement was of 53 grade, with specific gravity of 2.9 and fineness of 2800 cm2 /gm, prior preparation of specimens it was stored in a humidity controlled room to prevent it being exposed to the moisture. Coarse aggregate The coarse aggregate used for this research was well graded angular granite machine crushed, passed through 20mm sieve test, the specific gravity is 2.7, flakiness index of 4.35% and elongation index of 3.64%. The aggregate was washed to be free from dust, clay or any other organic matter. Fine aggregate Fine aggregate are normally obtained locally from rivers or lakes. British Standards defined this material as material passing 5.0 mm test sieve but retained on a 75 μm test sieve. The fine aggregate used for this research having specific gravity of 2.4 passed through 5mm sieve test. The aggregate was kept in a dry place prior mixed to ensure the moisture content is controlled during mixing process. Water Portable water available in locality suitable for drinking was used to prepare the concrete mix, the main purpose of water as we have seen in literature review is to set cement (to start chemical reaction within cement pastes). The same type of water was also used for curing concrete. Glass Fiber These are the main materials which were added to reinforce the concrete. As stated in the literature review glass fiber has high tensile strength of 2 – 4Gpa and elastic modulus of 70 – 80Gpa, brittle stress strain characteristic from 2.4 – 4.8 elongation at break and low creep at room temperature. Glass fiber also is susceptible to alkali attack. Type of glass fiber used was alkali resistance (AR- Type) glass fiber having the following properties:-  Aspect ratio of 857:1  Density of 2.6t/m3  Elastic modulus of 73GPa  Tensile strength of 1.7GPa  Density of 14micronon  Length divided into 24mm  Number of fiber 212million/kg 2.2 Mix design The concrete mix design is based on the method published by Department of the Environment (DOE) in 1988 edition. The description provided in that article illustrate the principle for methods, number of design exercise were carried out in order to become familiar with the design procedure. The DOE method also provide information necessary to design concrete for indirect tensile strength, containing entrained air and using cement replacement but that was the focus. The method is divided into five sections where by section 1 is to deal with strength of concrete; section 2 is to deal with workability; section 3 is to deal with cement content; section 4 is to deal with density of fresh concrete; and finally section 5 is deal with proportion of sand. Results were obtained from various graphs and filled in the Table 1 provided by DOE. The aim was to design the concrete of characteristic strength of 40 N/mm2 at 28 days by using Ordinary
  • 3. International Journal of Trend in Scientific @ IJTSRD | Available Online @ www.ijtsrd.com Portland Cement (OPC); The proportional defective (percentage of failure) to be of 5 percent. The slump range from 30 – 60 and the Vebe time within 3 seconds. The relative density of aggregate was considered to be 2.7; the aggregates were well crushed with the maximum size of 20mm. By using the DOE method of mix design (1988 Edition) the quantities of cement, water, sand and aggregate were obtained per cubic meter. The amount of each quantity was divided by the total volume for the specimens to acquire the precise amount of each ingredient to be added in the mix. 2.3 Casting and Curing of Concrete After preparing the mix, cylindrical moulds of diameter 100mm and height 200mm, cubes of 150 x 150 x 150mm and beam moulds of 110 x 110 x 5000mm were casted. Fresh concrete mix containing Table 2: Compressive strength of concrete specimens at 7, 28, and 56 days of curing Glass Fiber (%) Average 7 Days Strength (N/mm 0 22.63 10 24.74 20 36.52 30 36.63 50 40.27 60 40.16 80 41.08 Figure 1: Graph of average compressive strength vs. days of curing The effect of Glass fiber on strength of concrete is shown in Figure 1, which presents the substantial increment compressive strength values of concrete mixtures with different proportions of glass fiber cured at 7 days, 28 days and 56 days. It is observed International Journal of Trend in Scientific Research and Development (IJTSRD) @ IJTSRD | Available Online @ www.ijtsrd.com | Special Issue Publication | November Portland Cement (OPC); The proportional defective (percentage of failure) to be of 5 percent. The slump 60 and the Vebe time within 3 – 6 The relative density of aggregate was considered to be 2.7; the aggregates were well crushed with the maximum size of 20mm. By using the DOE method of mix design (1988 Edition) the quantities of cement, water, sand and aggregate were obtained per cubic er. The amount of each quantity was divided by the total volume for the specimens to acquire the precise amount of each ingredient to be added in the After preparing the mix, cylindrical moulds of nd height 200mm, cubes of 150 x 150 x 150mm and beam moulds of 110 x 110 x 5000mm were casted. Fresh concrete mix containing different percentages by volume of glass fiber was casted into the moulds. The mix was casted carefully to avoid segregation. The concrete was compacted by using a steer bar to remove the voids. After 24 hours the cement had set and hardened enough, the moulds were removed. All the concrete cylinders, cubes and beams were set into the curing tank for curing. The curing was done at an average temperature of 27 the period of 7days, 28days and 56days. 3. Results and Discussion 3.1 Compressive Strength The most valuable property in concrete is the concrete compressive strength because it gives the overall definition of the quality concrete strength that relates to the hydrated cement paste. Basically, the specimens were being tests for three selected curing periods namely: 7, 28, 56 days, detail test results are shown in Table 2. Table 2: Compressive strength of concrete specimens at 7, 28, and 56 days of curing Average 7 Days Strength (N/mm2 ) Average 28 Days Strength (N/mm2 ) Average 56 Days Strength (N/mm 22.63 38.52 42.21 24.74 40.63 46.2 36.52 43.8 48.43 36.63 48.54 49.64 40.27 49.24 50.02 40.16 49.04 50.67 41.08 52.45 51.53 compressive strength vs. The effect of Glass fiber on strength of concrete is shown in Figure 1, which presents the substantial increment compressive strength values of concrete mixtures with different proportions of glass fiber cured at 7 days, 28 days and 56 days. It is observed that the concrete with higher percentage of glass fiber gain strength between 61% until 82% faster than normal at early age. For instance the GFRC with 80% fiber content was able to achieve the targe after 7 days of curing. Once more it is observed that there is an enormous 48% increment in strength between GFRC with 10% and 20% of fiber. Concrete with 20% of fiber is adequate to improves the bond between cement and aggregates. The also speeds up the hydration. During hydration process water is absorbed by glass fiber results strengthening of inter-molecule bond. Apparently, addition of glass fiber contributing much on strength of the concrete, as it is observed in the graph at 7 days of curing, specimens with high percentage of glass fiber (50% 60% and 80%) have achieved compressive strength above the targeted characteristics strength of 40 N/mm the graph shows that at 56days of curing all the | ISSN: 2456-647 November 2018 P - 3 different percentages by volume of glass fiber was casted into the moulds. The mix was casted carefully oncrete was compacted by using a steer bar to remove the voids. After 24 hours the cement had set and hardened enough, the moulds were removed. All the concrete cylinders, cubes and beams were set into the curing tank for curing. The average temperature of 27° C for the period of 7days, 28days and 56days. The most valuable property in concrete is the concrete compressive strength because it gives the overall concrete strength that relates to the hydrated cement paste. Basically, the specimens were being tests for three selected curing periods namely: 7, 28, 56 days, detail test results are shown in Table 2: Compressive strength of concrete specimens at 7, 28, and 56 days of curing Average 56 Days Strength (N/mm2 ) that the concrete with higher percentage of glass fiber gain strength between 61% until 82% faster than normal at early age. For instance the GFRC with 80% fiber content was able to achieve the targeted strength after 7 days of curing. Once more it is observed that there is an enormous 48% increment in strength between GFRC with 10% and 20% of fiber. Concrete is adequate to improves the bond between cement and aggregates. The presence of fiber also speeds up the hydration. During hydration process water is absorbed by glass fiber results molecule bond. Apparently, addition of glass fiber contributing much on strength of the concrete, as it is observed in the aph at 7 days of curing, specimens with high percentage of glass fiber (50% 60% and 80%) have achieved compressive strength above the targeted characteristics strength of 40 N/mm2 . Nevertheless, the graph shows that at 56days of curing all the
  • 4. International Journal of Trend in Scientific @ IJTSRD | Available Online @ www.ijtsrd.com specimens where able to achieve strength above the targeted strength. 3.2 Tensile Strength The split tensile strength of the concrete specimens was determined at 7, 28 and 56 days following BS EN 12390 part 6: 2009. Table 3: Split Tensile strength of concrete speci at 7, 28, and 56 days of curing Glass Fiber (%) Average 7 Days Strength (N/mm2 ) Average 28 Days Strength (N/mm2 ) 0 3.42 4.24 10 3.52 4.5 20 3.83 5.15 30 4.12 4.92 50 4.16 5.3 60 4.29 5.59 80 4.58 6.84 Figure 2: Graph of average tensile strength vs. days of curing Figure 2 shows the tensile strength of GFRC against days of curing. The figure illustrates the evidence that the split tensile strength of GFRC increases with the increase of curing days together with content of fiber incorporated into the mix. The graph s specimen with high percentage of glass fiber (80%) have achieved extremely high split tensile strength at all days of curing. Concrete with 80% of glass fiber gain 60% and 61% of split tensile strength respectively at 28 days and 56 days of curin compared to the higher percentage strength of tensile for the normal concrete. This implies that GFRC achieves most of its split tensile strength after the age of 28 days however the strength is slightly increasing as the day of curing is increasing. Oth samples with glass fiber have shown remarkable International Journal of Trend in Scientific Research and Development (IJTSRD) @ IJTSRD | Available Online @ www.ijtsrd.com | Special Issue Publication | November ere able to achieve strength above the The split tensile strength of the concrete specimens was determined at 7, 28 and 56 days following BS EN Table 3: Split Tensile strength of concrete specimens at 7, 28, and 56 days of curing Average 56 Days Strength (N/mm2 ) 4.51 5.05 5.81 6.25 6.32 6.55 7.2 Figure 2: Graph of average tensile strength vs. days of Figure 2 shows the tensile strength of GFRC against days of curing. The figure illustrates the evidence that the split tensile strength of GFRC increases with the increase of curing days together with content of fiber The graph shows that specimen with high percentage of glass fiber (80%) have achieved extremely high split tensile strength at Concrete with 80% of glass fiber gain 60% and 61% of split tensile strength respectively at 28 days and 56 days of curing compared to the higher percentage strength of tensile for the normal concrete. This implies that GFRC achieves most of its split tensile strength after the age of 28 days however the strength is slightly increasing as the day of curing is increasing. Other than that, samples with glass fiber have shown remarkable increase in split tensile strength with ages of curing unlike the control samples (0%) glass fiber. 3.3 Flexural Strength Flexural strength can be described as the capacity of a beam or even a slab of concrete to resist failure due to bending. This flexural strength is also known as Modulus of Rupture. The effect of concrete with various percentage of glass fiber on flexural is shown on table 4. The flexural strength was tested on 7, 28 and 56 days of curing. Table 4: Flexural strength of concrete specimens at 7, 28, and 56 days of curing Glass Fiber (%) Average 7 Days Strength (N/mm2 ) Average 28 Days Strength (N/mm 0 2.76 4.11 10 3.76 4.5 20 4.09 4.81 30 4.37 50 4.55 5.28 60 4.8 5.3 80 4.82 5.65 Figure 3: Graph of average flexural strength vs. days of curing Based on the figure 3, the graph shows that concrete with higher percentage of glass fiber have higher flexural strength, also concrete of with lower percentage of glass fiber have lower flexural strength. In other words, the graph shows the evidence that flexural strength increases with the increase in fiber content. The graph also shows that, the gain of flexural strength is higher between 7 to 28 days than 28 to 56 days. This implies that at 28 days of curing GFRC achieves sufficient strength. It is ob | ISSN: 2456-647 November 2018 P - 4 increase in split tensile strength with ages of curing unlike the control samples (0%) glass fiber. Flexural strength can be described as the capacity of a beam or even a slab of concrete to resist failure due to bending. This flexural strength is also known as . The effect of concrete with various percentage of glass fiber on flexural strength is shown on table 4. The flexural strength was tested on 7, 28 and 56 days of curing. Table 4: Flexural strength of concrete specimens at 7, 28, and 56 days of curing Average 28 Days Strength (N/mm2 ) Average 56 Days Strength (N/mm2 ) 4.11 4.31 4.5 4.92 4.81 5.32 5 5.72 5.28 6 5.3 6.18 5.65 7.3 Figure 3: Graph of average flexural strength vs. days of curing Based on the figure 3, the graph shows that concrete with higher percentage of glass fiber have higher flexural strength, also concrete of with lower percentage of glass fiber have lower flexural strength. In other words, the graph shows the evidence that flexural strength increases with the increase in fiber The graph also shows that, the gain of flexural strength is higher between 7 to 28 days than 28 to 56 days. This implies that at 28 days of curing GFRC achieves sufficient strength. It is observed that the
  • 5. International Journal of Trend in Scientific Research and Development (IJTSRD) | ISSN: 2456-647 @ IJTSRD | Available Online @ www.ijtsrd.com | Special Issue Publication | November 2018 P - 5 flexural strength for the specimens having 80 percent of fiber increased dramatic for 28 and 56 days while for 7 days the increase is marginal. 4. Conclusions Extensive experimentation was carried out with various glass fiber percentages on concrete. For all mixes, compressive strength, tensile strength and flexural strength were determined at 7, 28 and 56 days. The following conclusions can be derived from the investigation: A. With minimum of 20% glass fiber is adequate to improve the early age strength of the concrete. This implies that glass fibers assist in increasing the compressive strength of concrete. However, the strength of the concrete at 56days are relatively similar with the higher different of strength only 22% for concrete with 80% glass fiber. B. The split tensile strength of “AR Glass fiber” for M40 concrete is maximum when 80% of glass fiber was incorporated into mix, this implies that split tensile strength of Glass Fiber Reinforced Concrete is high when the amount of fiber incorporated into the concrete is also higher. C. The flexural strength of “AR Glass fiber” for M40 concrete in this research is found to be maximum at 80% glass fiber mix. This also implies that flexural strength of Glass Fiber Reinforced Concrete is high when the amount of fiber incorporated into the concrete is also higher. D. Fibers impart energy absorption, toughness and impact resistance properties to fiber reinforced concrete material and these characteristics in turn improve the strength properties. 5. Acknowledgements Authors would like to thank the Linton University College and its group of institution’s Top Management for their continuous support. 6. References 1. British Standards (BS), 1983, BS 1881: Part 110 - Testing concrete. Method for making test cylinders from fresh concrete. British Standard Institute. 2. British Standards (BS), 1970, BS 1881: Part 3 - Testing concrete. Method for curing concrete. British Standard Institute. 3. British Standards (BS), 1983, BS 1881: Part 116 - Testing concrete. Method for determination compressive strength. British Standard Institute. 4. British Standards (BS), 1983, BS 1881: Part 118 - Testing concrete. Method for determination flexural strength. British Standard Institute. 5. British Standards (BS), 1983, BS 1881: Part 117 - Testing concrete. Method for determination split tensile strength. British Standard Institute. 6. British Standards (BS), EN 12390-6 2009, testing hardened concrete Part 6: Split Tensile Strength of concrete, European Committee for Standardization. 7. Cuevas. Sherron, 2012, Fibre Material and Technology: World Technologies. 8. Daniel R. A., Nagtegaal G., 2001, Pedestrain bridge of pultruded sections as result of ecological design. In: Proceedings of the EPTA seminar, Roermond, Oct 2001. 9. Deepak T. J., Jalam A. A., Eric Loh, Siow Yun Tong, Sudesh Nair, Panjehpour, 2015, Prognostication of Concrete Characteristics with Coconut Shell as Coarse Aggregate Partial Percentile Replacement. International Journal of Scientific Research in Science, Engineering and Technology. Volume 1/Issue 4/456 10. Department of Environment (DOE), 1988, Design of Normal Concrete mixes, 2nd Edition, Construction Research Communications Ltd. 11. Heurik Strang, Victor C. Li. 2004. Classification of Fiber Reinforced Cementitious Materials for Structural Applications 6th Rilem symposium on FRC, 20–22 Sep.Varenna, Italy, pp. 197–218. 12. Jain, R., and Lee, L., 2012, Fibre Reinforced Polymer (FRP) Composites for Infrastructure Applications: Focusing on Innovation, Technology Implementation and Sustainability, illustrated Ed., Springer. 13. Johnston, D. Colin, 2000, Fibre – Reinforced Cements and Concrete: Advance in Concrete Technology, Vol. 3, Taylor & Francis Ltd. 14. Majumdar, A. J., Laws, V. 1991. Building Research Establishment book on Glass fiber reinforced cement 2nd ed. Oxford; Boston: BSP Professional. 15. Sivakumar, A. and Santhanam Manu. 2007. Mechanical Properties of High Strength Concrete
  • 6. International Journal of Trend in Scientific Research and Development (IJTSRD) | ISSN: 2456-647 @ IJTSRD | Available Online @ www.ijtsrd.com | Special Issue Publication | November 2018 P - 6 Reinforced with Metallic and Non-Metallic Fibers. Cement and Concrete Composites (29) pp. 603–608. TABLE 1: CONCRETE MIX DESIGN BY DOE