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ORIGINAL PAPER
Characterization of heterogeneity of the Shajara reservoirs
of the Shajara formation of the Permo-Carboniferous
Unayzah group
K. E. Al-Khidir & M. S. Benzagouta & A. A. Al-Qurishi &
A. A. Al-Laboun
Received: 8 January 2012 /Accepted: 10 August 2012 /Published online: 7 September 2012
# Saudi Society for Geosciences 2012
Abstract Representative sandstone samples were collected
from the surface-type section of the Shajara Formation of
the Permo-Carboniferous Unayzah Group for reservoir char-
acterization through fractal dimension investigation. Two
models based on mercury intrusion technique were
employed to represent the pores characteristics of these
sandstones. The results show that realistic dimensions and
outstanding fractal features of porous structures in Shajara
sandstones, when these materials are correlated by thermo-
dynamic model and 3-D fractal model of mercury intrusion.
On the basis of sub-Unayzah unconformity, sub-Middle
Shajara local unconformity, mudstone of the Middle Shajara
and sub-Khuff unconformity, the three porous and perme-
able sandstone units of Shajara Formation were treated
separately and classified here into three fractal dimension
units. The units from base to top are: Lower Shajara Fractal
Dimension Unit, Middle Shajara Fractal Dimension Unit,
and Upper Shajara Fractal Dimension Unit. The thermody-
namic model and 3-D fractal model were effectively used to
characterize the porous structures of Shajara sandstones in
logical and quantitative way.
Keywords Heterogeneity . Shajara formation . Shajara
fractal dimension units . Permeability
Introduction
The Unayzah Formation is hydrocarbon bearing in many oil
and gas fields in Saudi Arabia. It is composed of continental
siliciclastics of Permo-Carboniferous age. The formation
was formally defined by Al-Laboun (1987).
Lithologically, the clastic surface type section of the
Shajara Formation of the Permo-Carboniferous Unayzah
Group, that is exposed at Ash Shajara, Qusayba area, Al
Qassim district, Saudi Arabia, is classified into three mem-
bers: Lower Shajara Member, Middle Shajara Member, and
Upper Shajara Member (Al-Khidir 2007; Fig. 1). Local
unconformities were recognized within the Shajara Forma-
tion indicating minor stratigraphic break in sedimentation.
These local unconformities were interpreted as braided fluvial
channels. The clastic sequence starts with a red, porous,
permeable sandstone deposited unconformably on the Early
Devonian Tawail Formation.
On the other hand, the Middle Shajara Member is separated
from the Lower Shajara Member by a local unconformity.
Furthermore, a caliche surface (sub-Khuff unconformity) sep-
arates the Upper Shajara Member from the overlying Huqayl
Member of the Permo–Triassic Khuff Formation. Strongly
speaking, the sub-Unayzah unconformity, sub-Middle Shajara
unconformity, mudstone of the Middle Shajara Member, and
K. E. Al-Khidir (*) :M. S. Benzagouta
College of Engineering, Al Amoudi Research Chair in Petroleum,
EOR, Department of Petroleum Engineering and Natural Gas,
King Saud University,
Riyadh, Saudi Arabia
e-mail: kalkhidir@ksu.edu.sa
M. S. Benzagouta
e-mail: benz@ksu.edu.sa
A. A. Al-Qurishi
Petroleum and Natural Gas Research Institute,
King Abdulaziz City for Science and Technology,
Riyadh, Saudi Arabia
e-mail: aqurishi@kacst.edu.sa
A. A. Al-Laboun
College of Science Department of Geology, King Saud University,
Riyadh, Saudi Arabia
e-mail: ibnlaboun@yahoo.com
Arab J Geosci (2013) 6:3989–3995
DOI 10.1007/s12517-012-0656-9
sub-Khuff unconformity represent the backbone to classify
the Shajara Formation into three lithological units.
From the Petrophysical point of view, the sandstones of
the Shajara Formation were divided into three porous and
permeable zones: Lower Shajara Permeable Zone, Middle
Shajara Permeable Zone, and Upper Shajara Permeable
Zone (Al-Khidir 2007). Therefore, the three permeable
zones represent the backbone to study the fractal dimensions
of the porous structures of Shajara sandstones using mercury
intrusion technique with certain degree of accuracy.
Methodology and experimental work
Two models were used to characterize the fractal dimen-
sions of the sandstones of the Shajara Formation. These
models are: thermodynamic and 3-D fractal model of mercury
intrusion technique using autopore III. The term fractal was
first introduced by Mandelbrot (1977). It is defined as a
material that changes in size but not in geometrical shapes.
An important property of a fractal is self-similarity, which
refers to a characteristic of a form exhibited when substructure
Fig. 1 Surface type section of
the Shajara Formation of the
Permo-Carboniferous Unayzah
Group, showing the three
fractal dimension units,
N 26° 52 17.4, E 43° 36 18;
Al-Khidir et al. (2012)
3990 Arab J Geosci (2013) 6:3989–3995
resembles a superstructure in the same form. The fractal
dimension is used to study heterogeneity of a system. The
greater the fractal dimension, the greater the heterogeneous
system. Many authors have studied the fractal dimension,
among them Katz and Thompson (1985), Friesen and Mikula
(1987), Hansen and Skjeltrop (1988), Krohn (1988),
Lenormand (1990), Angulo and Gonzalez (1992), Toledo et
al. (1993), Shen and Li (1994, 1995), Li and Horne (2003), Li
(2004), and Kewen (2004). Mercury intrusion method was
used on samples representing the investigated area. This was
done by injecting mercury under pressure using Micromeritics
Autopore 111. The output of this experiment is construction of
capillary pressure curve as a function of mercury saturation.
The capillary pressure data was then used to calculate the pore
radius using Washburn's equation.
r ¼ 2 Â σ Â cos θ Pc= ð1Þ
r Pore radius in meter (m)
σ Mercury interfacial tension in Neuton per meter
(0.485 N/m)
θ Mercury contact angle measured in degrees (130°)
Pc Capillary pressure in Neuton per square meter (N/m2
)
With special reference to the thermodynamic model, log-
arithm of work done divided by the square of the pore radius
was plotted versus the logarithm of pore volume divided by
the pore radius, and the value of the slope of the straight line
is equivalent to the fractal dimension (Df). The thermody-
namic model equation is given below:
Log Pc  v r^2=ð Þ ¼ Df  Log v^0:3 r=ð Þ þ c ð2Þ
For the 3-D fractal model, the logarithm of mercury
saturation divided by average capillary pressure was plotted
versus logarithm of capillary pressure. and the slope was
determined from the straight line and its value was added to
4 to give the fractal dimension (Df).
Log dSHg dPc= Þ ¼ ðDf À 4Þ Â LogPc
À
ð3Þ
Results and discussion
The results of fractal dimensions of the porous structures in
sandstones of the Shajara Formation of the Permo-
Carboniferous Unayzah Group were shown in Table 1 Three
fractal dimension units were identified depending on ther-
modynamic model and 3-D fractal model of mercury intru-
sion technique. These fractal dimension units are: Lower
Shajara Fractal Dimension Unit, Middle Shajara Fractal
Dimension Unit, and Upper Shajara Fractal Dimension
Unit.
Concerning the Lower Shajara Fractal Dimension Unit, it
is represented by two sequences, namely lower and upper
(Fig. 1). The lower sequence is illustrated by three samples,
SJ1, SJ2, and SJ3 as shown in Fig. 1. Sample SJ1 is
described as medium-grained, moderately well-sorted, po-
rous, friable, red sandstone as shown in Fig. 1. The result of
thermodynamic model of sample SJ1 is demonstrated in
Fig. 2 and Table 1. The obtained straight line indicates a
porous system, while the value of the fractal dimension
(3.1332) assigns for sample heterogeneity. This anisotropy
is also confirmed in Fig. 2 which shows the 3-D fractal
model acquiring a fractal dimension of 2.8668. Regarding
sample SJ2, it is identified as medium-grained, well-sorted,
porous, friable, yellow sandstone (Fig. 1). Similarly, this
sample is characterized by straight line and a value of fractal
dimension equals to 3.1317 as demonstrated in Fig. 3 and
Table 1. This heterogeneity is also represented in Fig. 3 and
Table 1 revealing a value of fractal dimension equals to
2.8683.
Table 1 Thermodynamic model and 3-D fractal model of the Shajara Reservoirs of Shajara Formation of the Permo-Carboniferous Unayzah Group
showing the three fractal dimension units
Formation Units No. Thermodynamic 3-D fractal Φ % KmD
Shajara Formation Upper Shajara Fractal
Dimension Unit
SJ-13 3.1279 2.8721 25 973
SJ-12 3.1317 2.8683 28 1,440
SJ-11 3.1255 2.8745 36 1,197
Middle Shajara Fractal
Dimension Unit
SJ-9 3.1293 2.8907 31 1,394
SJ-8 3.1285 2.8715 32 1,344
SJ-7 3.1284 2.8716 35 1,472
Lower Shajara Fractal
Dimension Unit
SJ-5 3.0929 2.9071 31 55
SJ-4 3.1046 2.8954 30 176
SJ-3 3.0937 2.9063 34 56
SJ-2 3.1317 2.8683 35 1,955
SJ-1 3.1332 2.8668 29 1,680
Arab J Geosci (2013) 6:3989–3995 3991
On the other hand, decrease in grain size occurred as we
proceed from sample SJ2 to SJ3 in the same lower sequence
of the Lowe Shajara Fractal Dimension Unit. Lithologically,
the sample SJ3 consists mainly of white to pink, fine-
grained sandstone, hard and fair to good sorting. Such grain
size variability can lead to reservoir quality assessment of
the Lower Shajara Fractal Dimension Unit, through fractal
dimension and permeability investigation (Fig. 4). That is to
say, grain size is directly proportional to fractal dimension
obtained from thermodynamic model as well as permeabil-
ity. In other words, high values of fractal dimension and
permeability correspond to the medium-grained sandstone
facies of this lower sequence (Table 1). In the case of 3-D
fractal dimension model, grain size and permeability are
inversely proportional to the fractal dimension. That is to
say, high value of fractal dimension and low value of per-
meability consign to the fine-grained sandstone sequence
(sample SJ3, as shown in Table 1).
The second sedimentary sequence of the Lower Shajara
Fractal Dimension Unit is isolated from the underlying
lower sequence by an intra lower Shajara unconformity as
delineated in Fig. 1. This sequence is illustrated by three
samples, namely SJ4, SJ5, and SJ6 as viewed in Fig. 1. With
regard to sample SJ4, it is described as coarse-grained, very
poorly sorted, white sandstone as mentioned in Fig. 1. This
sample possesses a fractal dimension value of about
3.1046.which is also account for heterogeneous system as
demonstrated in Fig. 5 and Table 1. This heterogeneity is
also documented by the value of the fractal dimension
(2.9954) obtained from the 3-D fractal model as shown in
Fig. 5. Again, reduction in grain size takes place as we
proceed from sample SJ4 to samples SJ5 and SJ6. Sample
SJ5 attained a fractal dimension value of about 3.0929
indicating a heterogeneous system as represented in Fig. 6.
Further verification of heterogeneity is shown in Fig. 6,
which displays a value of fractal dimension equals to
2.9071. No capillary pressure data available for sample SJ6,
but field observation demonstrates the presence of fine-
grained, compacted sandstone with yellow spots (Fig. 1).
Based on the obtained results of sample SJ4 and SJ5,
grain size is also directly proportional to the fractal dimen-
sion obtained from thermodynamic model, in addition to
Fig. 2 Thermodynamic and 3-D fractal model fractal for sample SJ-1
from Lower Shajara Fractal Shajar Dimension Unit
Fig. 3 Thermodynamic and 3-D model for sample SJ-2 from Lower
Fractal Dimension Unit
Fig. 4 Thermodynamic and 3-D fractal model for sample SJ-3 from
Lower Shajara Fractal Dimension Unit
Fig. 5 Thermodynamic and 3-D model for sample SJ-4 from Lower
Shajara Fractal Dimension Unit
3992 Arab J Geosci (2013) 6:3989–3995
permeability value. Furthermore high value of fractal di-
mension and permeability consign to sample SJ4 (coarse-
grained sequence) of this sequence as shown in sequence.
With regard to the fractal dimensions of sandstones from
Middle Shajara unit, their results were graphically repre-
sented in Figs.7, 8, and 9 and Table 1. This unit is separated
from the Lower Shajara Fractal Dimension Unit by sub-
middle Shajara local unconformity as shown in Fig. 1. This
unit is illustrated by four samples, namely SJ7, SJ8, SJ9, and
SJ10 as mentioned in Fig. 1. The Sample SJ7 consists
mainly of red sandstone is coarse-grained, moderately to
very well sorted, porous, and friable. This sample is also
characterized by straight line as shown in Fig. 7 which
accounts for a porous system. The result obtained from
thermodynamic model indicates the presence of a heteroge-
neous system (Df03.1284). Further pronouncement of het-
erogeneity is viewed by the 3-D fractal model (Fig. 7).
Based on this model, sample SJ7 acquired a value of fractal
dimension equals to 2.8716.
Similarly, reduction in grain size happened as we proceed
from sample SJ7 to SJ8 as illustrated in Fig. 1. Sample SJ8
is described as medium-grained, moderately well-sorted,
porous, friable, red sandstone (Fig. 1). This sample attained
a value of fractal dimension of about 3.1285 which also
delineates the presence of a heterogeneous system (Fig. 8
Table 1). The result displayed in Fig. 8 from 3-D fractal
model also announced for a heterogeneous system (Df0
2.8715). On the subject of sample SJ9, it is identified as
medium-grained, moderately well-sorted, porous, friable,
yellow sandstone (Fig. 1). As indicated in Fig. 9 and Table 1,
this sample has a value of fractal dimension equals to
3.1293, declaring the existence of a heterogeneous system.
Further verification of heterogeneity is shown in Fig. 9 and
Table 1.which reveals a value of fractal dimension corre-
sponds to 2.8707. On the topic of sample SJ10, it is recog-
nized as medium-grained, moderately sorted, porous,
friable, light brown sandstone (Fig. 1). This sample obtained
no capillary pressure data to determine its fractal dimension.
In and overall, concerning the fractal dimensions
obtained from thermodynamic model and the 3-D fractal
model for the Middle Shajara Fractal Dimension Unit, the
scenario is reversed. In the case of thermodynamic model,
Fig. 6 Thermodynamic and 3-D fractal model for sample SJ-5 from
Lower Shajara Fractal Dimension Unit
Fig. 7 Thermodynamic and 3-D model for sample SJ-7 from Middle
Shajara Fractal Dimension Unit
Fig. 8 Thermodynamic and 3-D fractal model for sample SJ-8 from
Middle Shajara Fractal Dimension Unit
Fig. 9 Thermodynamic and 3-D model for sample SJ-9 from Middle
Shajara Fractal Dimension Unit
Arab J Geosci (2013) 6:3989–3995 3993
the obtained fractal dimension enlarges upward with re-
duced grain size and permeability as shown in Table 1. On
the topic of the 3-D fractal model, the determined fractal
dimension decreases upward with reduction in grain size
and permeability as illustrated in Table 1.
With reference to the Upper Shajara fractal Dimension
Unit, it is represented by three samples, namely SJ11, SJ12,
and SJ13. Their results of fractal dimensions are shown in
Figs. 10, 11, and 12. The Sample SJ11 consists mainly of
medium grained-sandstone, fairly well to poorly sorted,
porous, friable, and yellow in color (Fig. 1). On the basis
of thermodynamic model, this sample acquiring a value of
fractal dimension equals to 3.1255 and straight line (Fig. 10)
delineates the occurrence of a heterogeneous porous system.
This heterogeneity is confirmed in Fig. 10 and Table 1. That is
to say, fractal dimension equals to 2.8745. Concerning sample
SJ12 it is identified as very coarse-grained, moderately sorted,
porous, friable, yellow sandstone (Fig. 1). The fractal dimen-
sion obtained for this sample from thermodynamic model was
found to be 3.1317 assigning for heterogeneous system
(Fig. 11 and Table 1). Moreover, this heterogeneity is verified
in Fig. 11 which shows a value of fractal dimension identical
to 2.8683. Sample SJ13 is described as coarse-grained, mod-
erately sorted, porous, friable, light brown, cross bedded
sandstone as demonstrated (Fig. 1). This sample posses fractal
dimension value equivalent to 3.1279 pronouncing also for
heterogeneous system as indicated in Fig. 12. This heteroge-
neity is also affirmed in Fig. 12 which attains a value of fractal
dimension equals to 2.8721.
In and overall, such grain size variability can guide to
reservoir quality evaluation of the Upper Shajara Fractal
Dimension Unit, in the course of fractal dimension and
permeability examination. That is to say, grain size is di-
rectly proportional to fractal dimension determined from
thermodynamic model as well as permeability. On other
wards, high values of fractal dimension and permeability
correspond to the very coarse-grained sandstone sequence
(SJ12) as indicated in Fig. 11 and Table 1. Regarding the3-D
fractal dimension model, the value of fractal dimension
increases upward with decrease grain size and permeability
as shown in Table 1
An excellent correlation factor (1) was determined from
Fig. 13 to show the mathematical capability of the two
models and their permanence in calculating the fractal
dimensions of the porous structures of Shajara sandstones
with certain degree of precision. Figure 13 shows that fine-
Fig. 10 Thermodynamic and 3-D fractal model for sample SJ-11 from
Upper Shajara Fractal Dimension Unit
Fig. 11 Thermodynamic and 3-D model for sample SJ-12 from Upper
Shajara Fractal Dimension Unit
Fig. 12 Thermodynamic and 3-D fractal model for sample SJ-13 from
Upper Shajara Fractal Dimension Unit
Fig. 13 Thermodynamic model versus 3-D fractal model
3994 Arab J Geosci (2013) 6:3989–3995
grained facies of the Lower Shajara Fractal Dimension Unit
attained the lowest values of fractal dimensions obtained
from thermodynamic model. On the other hand, medium-
and coarse-grained facies of the Shajara Formation are char-
acterized by low values of fractal dimensions obtained from
3-D fractal model, compared to the fine-grained sequence
(Fig. 13).
Conclusion
& The thermodynamic model and 3-D fractal model of
mercury intrusion show their effectiveness, mathemati-
cal capabilities, and continuity in evaluating the fractal
dimension of the sandstones of the Shajara Formation of
the Permo-Carboniferous Unayzah Group.
& Three fractal dimension units were identified on the
basis of unconformities and mudstone of the Middle
Shajara unit.
& Excellent correlation factor (1) was obtained which as-
sign for the competency of the two models.
& The results of the fractal dimensions indicate the hetero-
geneity of the Shajara Reservoirs which account for a
wide range of pore sizes.
Acknowledgment The authors would like to thank Al Amoudi Re-
search Chair in Petroleum EOR, King Abdulaziz City for Science and
Technology and King Saud University, Depart of Petroleum Engineering
for the use of their laboratories.
References
Al-Khidir KE (2007) Reservoir Characteristics of the Unayzah Forma-
tion , Saudi Arabia, M.Sc. Thesis, King Saud University, Riyadh,
Kingdom of Saudi Arabia
Al-Khidir KE, Al-Laboun AA, Al-Qurishi AA (2012) M. S. Benzagouta
bimodal pore size behavior of the Shajara formation reservoirs of the
Permo-Carboniferous Unayzah Group, Saudi Arabia. J Petrol
Explor Prod Technol 1 (No.113202) (in press)
Al-Laboun AA (1987) Unayzah formation: a new Permo-Carboniferous
unit in Saudi Arabia. Am Assoc Pet Geol Bull 71(no. 1):29–38
Al-Laboun AA (2003) The Qusayba Depression: a window on the
influence of the Caledonian and Hercynian Orogenies in Central
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Angulo RF, Gonzalez H (1992) “Fractal Dimensions from Mercury
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Arab J Geosci (2013) 6:3989–3995 3995

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Characterization of heterogeneity of the shajara reservoirs of the shajara formation of the permo carboniferous

  • 1. ORIGINAL PAPER Characterization of heterogeneity of the Shajara reservoirs of the Shajara formation of the Permo-Carboniferous Unayzah group K. E. Al-Khidir & M. S. Benzagouta & A. A. Al-Qurishi & A. A. Al-Laboun Received: 8 January 2012 /Accepted: 10 August 2012 /Published online: 7 September 2012 # Saudi Society for Geosciences 2012 Abstract Representative sandstone samples were collected from the surface-type section of the Shajara Formation of the Permo-Carboniferous Unayzah Group for reservoir char- acterization through fractal dimension investigation. Two models based on mercury intrusion technique were employed to represent the pores characteristics of these sandstones. The results show that realistic dimensions and outstanding fractal features of porous structures in Shajara sandstones, when these materials are correlated by thermo- dynamic model and 3-D fractal model of mercury intrusion. On the basis of sub-Unayzah unconformity, sub-Middle Shajara local unconformity, mudstone of the Middle Shajara and sub-Khuff unconformity, the three porous and perme- able sandstone units of Shajara Formation were treated separately and classified here into three fractal dimension units. The units from base to top are: Lower Shajara Fractal Dimension Unit, Middle Shajara Fractal Dimension Unit, and Upper Shajara Fractal Dimension Unit. The thermody- namic model and 3-D fractal model were effectively used to characterize the porous structures of Shajara sandstones in logical and quantitative way. Keywords Heterogeneity . Shajara formation . Shajara fractal dimension units . Permeability Introduction The Unayzah Formation is hydrocarbon bearing in many oil and gas fields in Saudi Arabia. It is composed of continental siliciclastics of Permo-Carboniferous age. The formation was formally defined by Al-Laboun (1987). Lithologically, the clastic surface type section of the Shajara Formation of the Permo-Carboniferous Unayzah Group, that is exposed at Ash Shajara, Qusayba area, Al Qassim district, Saudi Arabia, is classified into three mem- bers: Lower Shajara Member, Middle Shajara Member, and Upper Shajara Member (Al-Khidir 2007; Fig. 1). Local unconformities were recognized within the Shajara Forma- tion indicating minor stratigraphic break in sedimentation. These local unconformities were interpreted as braided fluvial channels. The clastic sequence starts with a red, porous, permeable sandstone deposited unconformably on the Early Devonian Tawail Formation. On the other hand, the Middle Shajara Member is separated from the Lower Shajara Member by a local unconformity. Furthermore, a caliche surface (sub-Khuff unconformity) sep- arates the Upper Shajara Member from the overlying Huqayl Member of the Permo–Triassic Khuff Formation. Strongly speaking, the sub-Unayzah unconformity, sub-Middle Shajara unconformity, mudstone of the Middle Shajara Member, and K. E. Al-Khidir (*) :M. S. Benzagouta College of Engineering, Al Amoudi Research Chair in Petroleum, EOR, Department of Petroleum Engineering and Natural Gas, King Saud University, Riyadh, Saudi Arabia e-mail: kalkhidir@ksu.edu.sa M. S. Benzagouta e-mail: benz@ksu.edu.sa A. A. Al-Qurishi Petroleum and Natural Gas Research Institute, King Abdulaziz City for Science and Technology, Riyadh, Saudi Arabia e-mail: aqurishi@kacst.edu.sa A. A. Al-Laboun College of Science Department of Geology, King Saud University, Riyadh, Saudi Arabia e-mail: ibnlaboun@yahoo.com Arab J Geosci (2013) 6:3989–3995 DOI 10.1007/s12517-012-0656-9
  • 2. sub-Khuff unconformity represent the backbone to classify the Shajara Formation into three lithological units. From the Petrophysical point of view, the sandstones of the Shajara Formation were divided into three porous and permeable zones: Lower Shajara Permeable Zone, Middle Shajara Permeable Zone, and Upper Shajara Permeable Zone (Al-Khidir 2007). Therefore, the three permeable zones represent the backbone to study the fractal dimensions of the porous structures of Shajara sandstones using mercury intrusion technique with certain degree of accuracy. Methodology and experimental work Two models were used to characterize the fractal dimen- sions of the sandstones of the Shajara Formation. These models are: thermodynamic and 3-D fractal model of mercury intrusion technique using autopore III. The term fractal was first introduced by Mandelbrot (1977). It is defined as a material that changes in size but not in geometrical shapes. An important property of a fractal is self-similarity, which refers to a characteristic of a form exhibited when substructure Fig. 1 Surface type section of the Shajara Formation of the Permo-Carboniferous Unayzah Group, showing the three fractal dimension units, N 26° 52 17.4, E 43° 36 18; Al-Khidir et al. (2012) 3990 Arab J Geosci (2013) 6:3989–3995
  • 3. resembles a superstructure in the same form. The fractal dimension is used to study heterogeneity of a system. The greater the fractal dimension, the greater the heterogeneous system. Many authors have studied the fractal dimension, among them Katz and Thompson (1985), Friesen and Mikula (1987), Hansen and Skjeltrop (1988), Krohn (1988), Lenormand (1990), Angulo and Gonzalez (1992), Toledo et al. (1993), Shen and Li (1994, 1995), Li and Horne (2003), Li (2004), and Kewen (2004). Mercury intrusion method was used on samples representing the investigated area. This was done by injecting mercury under pressure using Micromeritics Autopore 111. The output of this experiment is construction of capillary pressure curve as a function of mercury saturation. The capillary pressure data was then used to calculate the pore radius using Washburn's equation. r ¼ 2  σ  cos θ Pc= ð1Þ r Pore radius in meter (m) σ Mercury interfacial tension in Neuton per meter (0.485 N/m) θ Mercury contact angle measured in degrees (130°) Pc Capillary pressure in Neuton per square meter (N/m2 ) With special reference to the thermodynamic model, log- arithm of work done divided by the square of the pore radius was plotted versus the logarithm of pore volume divided by the pore radius, and the value of the slope of the straight line is equivalent to the fractal dimension (Df). The thermody- namic model equation is given below: Log Pc  v r^2=ð Þ ¼ Df  Log v^0:3 r=ð Þ þ c ð2Þ For the 3-D fractal model, the logarithm of mercury saturation divided by average capillary pressure was plotted versus logarithm of capillary pressure. and the slope was determined from the straight line and its value was added to 4 to give the fractal dimension (Df). Log dSHg dPc= Þ ¼ ðDf À 4Þ Â LogPc À ð3Þ Results and discussion The results of fractal dimensions of the porous structures in sandstones of the Shajara Formation of the Permo- Carboniferous Unayzah Group were shown in Table 1 Three fractal dimension units were identified depending on ther- modynamic model and 3-D fractal model of mercury intru- sion technique. These fractal dimension units are: Lower Shajara Fractal Dimension Unit, Middle Shajara Fractal Dimension Unit, and Upper Shajara Fractal Dimension Unit. Concerning the Lower Shajara Fractal Dimension Unit, it is represented by two sequences, namely lower and upper (Fig. 1). The lower sequence is illustrated by three samples, SJ1, SJ2, and SJ3 as shown in Fig. 1. Sample SJ1 is described as medium-grained, moderately well-sorted, po- rous, friable, red sandstone as shown in Fig. 1. The result of thermodynamic model of sample SJ1 is demonstrated in Fig. 2 and Table 1. The obtained straight line indicates a porous system, while the value of the fractal dimension (3.1332) assigns for sample heterogeneity. This anisotropy is also confirmed in Fig. 2 which shows the 3-D fractal model acquiring a fractal dimension of 2.8668. Regarding sample SJ2, it is identified as medium-grained, well-sorted, porous, friable, yellow sandstone (Fig. 1). Similarly, this sample is characterized by straight line and a value of fractal dimension equals to 3.1317 as demonstrated in Fig. 3 and Table 1. This heterogeneity is also represented in Fig. 3 and Table 1 revealing a value of fractal dimension equals to 2.8683. Table 1 Thermodynamic model and 3-D fractal model of the Shajara Reservoirs of Shajara Formation of the Permo-Carboniferous Unayzah Group showing the three fractal dimension units Formation Units No. Thermodynamic 3-D fractal Φ % KmD Shajara Formation Upper Shajara Fractal Dimension Unit SJ-13 3.1279 2.8721 25 973 SJ-12 3.1317 2.8683 28 1,440 SJ-11 3.1255 2.8745 36 1,197 Middle Shajara Fractal Dimension Unit SJ-9 3.1293 2.8907 31 1,394 SJ-8 3.1285 2.8715 32 1,344 SJ-7 3.1284 2.8716 35 1,472 Lower Shajara Fractal Dimension Unit SJ-5 3.0929 2.9071 31 55 SJ-4 3.1046 2.8954 30 176 SJ-3 3.0937 2.9063 34 56 SJ-2 3.1317 2.8683 35 1,955 SJ-1 3.1332 2.8668 29 1,680 Arab J Geosci (2013) 6:3989–3995 3991
  • 4. On the other hand, decrease in grain size occurred as we proceed from sample SJ2 to SJ3 in the same lower sequence of the Lowe Shajara Fractal Dimension Unit. Lithologically, the sample SJ3 consists mainly of white to pink, fine- grained sandstone, hard and fair to good sorting. Such grain size variability can lead to reservoir quality assessment of the Lower Shajara Fractal Dimension Unit, through fractal dimension and permeability investigation (Fig. 4). That is to say, grain size is directly proportional to fractal dimension obtained from thermodynamic model as well as permeabil- ity. In other words, high values of fractal dimension and permeability correspond to the medium-grained sandstone facies of this lower sequence (Table 1). In the case of 3-D fractal dimension model, grain size and permeability are inversely proportional to the fractal dimension. That is to say, high value of fractal dimension and low value of per- meability consign to the fine-grained sandstone sequence (sample SJ3, as shown in Table 1). The second sedimentary sequence of the Lower Shajara Fractal Dimension Unit is isolated from the underlying lower sequence by an intra lower Shajara unconformity as delineated in Fig. 1. This sequence is illustrated by three samples, namely SJ4, SJ5, and SJ6 as viewed in Fig. 1. With regard to sample SJ4, it is described as coarse-grained, very poorly sorted, white sandstone as mentioned in Fig. 1. This sample possesses a fractal dimension value of about 3.1046.which is also account for heterogeneous system as demonstrated in Fig. 5 and Table 1. This heterogeneity is also documented by the value of the fractal dimension (2.9954) obtained from the 3-D fractal model as shown in Fig. 5. Again, reduction in grain size takes place as we proceed from sample SJ4 to samples SJ5 and SJ6. Sample SJ5 attained a fractal dimension value of about 3.0929 indicating a heterogeneous system as represented in Fig. 6. Further verification of heterogeneity is shown in Fig. 6, which displays a value of fractal dimension equals to 2.9071. No capillary pressure data available for sample SJ6, but field observation demonstrates the presence of fine- grained, compacted sandstone with yellow spots (Fig. 1). Based on the obtained results of sample SJ4 and SJ5, grain size is also directly proportional to the fractal dimen- sion obtained from thermodynamic model, in addition to Fig. 2 Thermodynamic and 3-D fractal model fractal for sample SJ-1 from Lower Shajara Fractal Shajar Dimension Unit Fig. 3 Thermodynamic and 3-D model for sample SJ-2 from Lower Fractal Dimension Unit Fig. 4 Thermodynamic and 3-D fractal model for sample SJ-3 from Lower Shajara Fractal Dimension Unit Fig. 5 Thermodynamic and 3-D model for sample SJ-4 from Lower Shajara Fractal Dimension Unit 3992 Arab J Geosci (2013) 6:3989–3995
  • 5. permeability value. Furthermore high value of fractal di- mension and permeability consign to sample SJ4 (coarse- grained sequence) of this sequence as shown in sequence. With regard to the fractal dimensions of sandstones from Middle Shajara unit, their results were graphically repre- sented in Figs.7, 8, and 9 and Table 1. This unit is separated from the Lower Shajara Fractal Dimension Unit by sub- middle Shajara local unconformity as shown in Fig. 1. This unit is illustrated by four samples, namely SJ7, SJ8, SJ9, and SJ10 as mentioned in Fig. 1. The Sample SJ7 consists mainly of red sandstone is coarse-grained, moderately to very well sorted, porous, and friable. This sample is also characterized by straight line as shown in Fig. 7 which accounts for a porous system. The result obtained from thermodynamic model indicates the presence of a heteroge- neous system (Df03.1284). Further pronouncement of het- erogeneity is viewed by the 3-D fractal model (Fig. 7). Based on this model, sample SJ7 acquired a value of fractal dimension equals to 2.8716. Similarly, reduction in grain size happened as we proceed from sample SJ7 to SJ8 as illustrated in Fig. 1. Sample SJ8 is described as medium-grained, moderately well-sorted, porous, friable, red sandstone (Fig. 1). This sample attained a value of fractal dimension of about 3.1285 which also delineates the presence of a heterogeneous system (Fig. 8 Table 1). The result displayed in Fig. 8 from 3-D fractal model also announced for a heterogeneous system (Df0 2.8715). On the subject of sample SJ9, it is identified as medium-grained, moderately well-sorted, porous, friable, yellow sandstone (Fig. 1). As indicated in Fig. 9 and Table 1, this sample has a value of fractal dimension equals to 3.1293, declaring the existence of a heterogeneous system. Further verification of heterogeneity is shown in Fig. 9 and Table 1.which reveals a value of fractal dimension corre- sponds to 2.8707. On the topic of sample SJ10, it is recog- nized as medium-grained, moderately sorted, porous, friable, light brown sandstone (Fig. 1). This sample obtained no capillary pressure data to determine its fractal dimension. In and overall, concerning the fractal dimensions obtained from thermodynamic model and the 3-D fractal model for the Middle Shajara Fractal Dimension Unit, the scenario is reversed. In the case of thermodynamic model, Fig. 6 Thermodynamic and 3-D fractal model for sample SJ-5 from Lower Shajara Fractal Dimension Unit Fig. 7 Thermodynamic and 3-D model for sample SJ-7 from Middle Shajara Fractal Dimension Unit Fig. 8 Thermodynamic and 3-D fractal model for sample SJ-8 from Middle Shajara Fractal Dimension Unit Fig. 9 Thermodynamic and 3-D model for sample SJ-9 from Middle Shajara Fractal Dimension Unit Arab J Geosci (2013) 6:3989–3995 3993
  • 6. the obtained fractal dimension enlarges upward with re- duced grain size and permeability as shown in Table 1. On the topic of the 3-D fractal model, the determined fractal dimension decreases upward with reduction in grain size and permeability as illustrated in Table 1. With reference to the Upper Shajara fractal Dimension Unit, it is represented by three samples, namely SJ11, SJ12, and SJ13. Their results of fractal dimensions are shown in Figs. 10, 11, and 12. The Sample SJ11 consists mainly of medium grained-sandstone, fairly well to poorly sorted, porous, friable, and yellow in color (Fig. 1). On the basis of thermodynamic model, this sample acquiring a value of fractal dimension equals to 3.1255 and straight line (Fig. 10) delineates the occurrence of a heterogeneous porous system. This heterogeneity is confirmed in Fig. 10 and Table 1. That is to say, fractal dimension equals to 2.8745. Concerning sample SJ12 it is identified as very coarse-grained, moderately sorted, porous, friable, yellow sandstone (Fig. 1). The fractal dimen- sion obtained for this sample from thermodynamic model was found to be 3.1317 assigning for heterogeneous system (Fig. 11 and Table 1). Moreover, this heterogeneity is verified in Fig. 11 which shows a value of fractal dimension identical to 2.8683. Sample SJ13 is described as coarse-grained, mod- erately sorted, porous, friable, light brown, cross bedded sandstone as demonstrated (Fig. 1). This sample posses fractal dimension value equivalent to 3.1279 pronouncing also for heterogeneous system as indicated in Fig. 12. This heteroge- neity is also affirmed in Fig. 12 which attains a value of fractal dimension equals to 2.8721. In and overall, such grain size variability can guide to reservoir quality evaluation of the Upper Shajara Fractal Dimension Unit, in the course of fractal dimension and permeability examination. That is to say, grain size is di- rectly proportional to fractal dimension determined from thermodynamic model as well as permeability. On other wards, high values of fractal dimension and permeability correspond to the very coarse-grained sandstone sequence (SJ12) as indicated in Fig. 11 and Table 1. Regarding the3-D fractal dimension model, the value of fractal dimension increases upward with decrease grain size and permeability as shown in Table 1 An excellent correlation factor (1) was determined from Fig. 13 to show the mathematical capability of the two models and their permanence in calculating the fractal dimensions of the porous structures of Shajara sandstones with certain degree of precision. Figure 13 shows that fine- Fig. 10 Thermodynamic and 3-D fractal model for sample SJ-11 from Upper Shajara Fractal Dimension Unit Fig. 11 Thermodynamic and 3-D model for sample SJ-12 from Upper Shajara Fractal Dimension Unit Fig. 12 Thermodynamic and 3-D fractal model for sample SJ-13 from Upper Shajara Fractal Dimension Unit Fig. 13 Thermodynamic model versus 3-D fractal model 3994 Arab J Geosci (2013) 6:3989–3995
  • 7. grained facies of the Lower Shajara Fractal Dimension Unit attained the lowest values of fractal dimensions obtained from thermodynamic model. On the other hand, medium- and coarse-grained facies of the Shajara Formation are char- acterized by low values of fractal dimensions obtained from 3-D fractal model, compared to the fine-grained sequence (Fig. 13). Conclusion & The thermodynamic model and 3-D fractal model of mercury intrusion show their effectiveness, mathemati- cal capabilities, and continuity in evaluating the fractal dimension of the sandstones of the Shajara Formation of the Permo-Carboniferous Unayzah Group. & Three fractal dimension units were identified on the basis of unconformities and mudstone of the Middle Shajara unit. & Excellent correlation factor (1) was obtained which as- sign for the competency of the two models. & The results of the fractal dimensions indicate the hetero- geneity of the Shajara Reservoirs which account for a wide range of pore sizes. Acknowledgment The authors would like to thank Al Amoudi Re- search Chair in Petroleum EOR, King Abdulaziz City for Science and Technology and King Saud University, Depart of Petroleum Engineering for the use of their laboratories. References Al-Khidir KE (2007) Reservoir Characteristics of the Unayzah Forma- tion , Saudi Arabia, M.Sc. Thesis, King Saud University, Riyadh, Kingdom of Saudi Arabia Al-Khidir KE, Al-Laboun AA, Al-Qurishi AA (2012) M. S. Benzagouta bimodal pore size behavior of the Shajara formation reservoirs of the Permo-Carboniferous Unayzah Group, Saudi Arabia. J Petrol Explor Prod Technol 1 (No.113202) (in press) Al-Laboun AA (1987) Unayzah formation: a new Permo-Carboniferous unit in Saudi Arabia. Am Assoc Pet Geol Bull 71(no. 1):29–38 Al-Laboun AA (2003) The Qusayba Depression: a window on the influence of the Caledonian and Hercynian Orogenies in Central Arabia, The Eighth Arab conference on Mineral Resources, 13– 16 October, Sana, Yemen Angulo RF, Gonzalez H (1992) “Fractal Dimensions from Mercury Intrusion Capillary Tests,” SPE 23695, presented at the 2nd Latin American Petroleum Engineering Conf. of SPE held in Caracas, Venezuela, March 8–11 Friesen WI, Mikula RJ (1987) Fractal dimensions of coal particles. J Colloid Interf Sci 120(1):263–271 Hansen JP, Skjeltorp AT (1988) Fractal pore space and rock perme- ability implications. Phys Rev B 38(4):2635–2638 Katz AJ, Thompson AH (1985) Fractal sandstone pores: implications for conductivity and pore formation. Phys Rev Lett 54:1325– 1328 Kewen Li (2004) Theoretical development of the Brooks-Corey Cap- illary Pressure Model from Fractal Modeling of Porous Media. SPE 89429, Stanford University for presentation at the 2004 SPE/ DOE Fourteenth Symposium on Improved Oil Recovery held in Tulsa, Oklahoma, U.S.A., 17–21, April Krohn CE (1988) Fractal measurements of sandstones, shales, and carbonates. J Geophys Res 93(B4):3297–3305 Lenormand R (1990) Gravity-assisted inert gas injection: micromodel experiments and model based on fractal roughness. The European Oil and Gas Conference, Altavilla Milica, Palermo, Sicily, October 9–12 Li K (2004) Characterization of rock heterogeneity using fractal ge- ometry. SPE 86975, Proceedings of the 2004 SPE Western Region Meeting, Bakersfield, CA, USA, March 16–18 Li K, Horne RN (2003) Fractal characterization of the Geysers rock. Presented at the GRC 2003 annual meeting, October 12–15, 2003. GRC Trans, Morelia p 27 Mandelbrot, BB (1977) Fractals: form, chance, and dimensions. W. H. Freeman and Company, San Francisco Shen P, Li K (1995) Quantitative description for the heterogeneity of pore structure by using mercury capillary pressure curves. SPE 29996, Proceedings of the SPE International Meeting held in Beijing, China, November 14–17 Shen P, Li K (1994) A new method for determining the fractal dimension of pore structures and its application. Proceedings of the 10th Offshore South East Asia Conference, Singapore, December 6-9 Toledo PG, Novy RA, Davis HT, Scriven LE (1993) Capillary pres- sure, water relative permeability, electrical conductivity and cap- illary dispersion coefficient of fractal porous media at low wetting phase saturations. SPE Adv Technol Ser 2(1):136–141 Arab J Geosci (2013) 6:3989–3995 3995