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ORIGINAL PAPER - EXPLORATION GEOLOGY
Bimodal pore size behavior of the Shajara Formation Reservoirs
of the Permo-Carboniferous Unayzah Group, Saudi Arabia
K. E. Al-Khidir ā€¢ A. A. Al-Quraishi ā€¢
A. A. Al-Laboun ā€¢ M. S. Benzagouta
Received: 29 September 2010 / Accepted: 21 March 2011 / Published online: 5 April 2011
Ɠ The Author(s) 2011. This article is published with open access at Springerlink.com
Abstract The sandstones of the Permo-Carboniferous
Shajara Formation form the main part of the Unayzah
Reservoir in the Greater Arabian Basin. It is divided into
three reservoirs, namely from base to top Lower, Middle,
and Upper Shajara reservoirs. Mercury intrusion technique
was carried out on representative sandstone samples col-
lected from the type section and the three reservoirs are
generally characterized as heterogeneous megaporous res-
ervoirs. The best reservoir quality is assigned to the lower
sand unit of the Lower Shajara followed by the Middle
Shajara Reservoir. One sample collected from the upper
part of the Lower Shajara was described as low quality due
to its ļ¬ne grain characteristic and its proximity to the
unconformity surface. Reservoir quality is controlled to a
large extent by the depositional facies and speciļ¬cally by
rock texture illustrated by petrophysical description. The
quality of the three reservoirs of the Shajara Formation,
increases with the increase of grain size and grain sorting.
Keywords Shajara Reservoirs Ɓ Shajara Formation Ɓ
Unayzah Group Ɓ Pore size distribution
Introduction
The Permo-Carboniferous Unayzah Reservoirs are oil and
gas bearing in more than 30 oil and gas ļ¬elds in Saudi
Arabia. These reservoirs are partially represented in out-
crops by the Shajara, Safra, and Shiqqah sandstones of the
Unayzah Group. These formations are exposed as a thin
belt below the Khuff carbonates in central Arabia.
Fossil plants of the late Carboniferousā€“early Permian
age were ļ¬rst reported at the town of Unayzah by El-
Khayal et al. (1980). Later, the term Unazyah Formation
was informally introduced by Al-Laboun (1982) as sili-
ciclastics and minor carbonate section at the base of the
Khuff Formation. This deļ¬nition was adopted by Aramco
Stratigraphic Committee (1983) and formally deļ¬ned by
Al-Laboun (1987)in the American Association of Petro-
leum Geologist (AAPG). The Unayzah Formation was then
correlated with its equivalent units in different parts of the
Greater Arabian basin (Al-Laboun 1988) and its type
locality was established within Unayzah town with a ref-
erence section assigned at Wadi Ash-Shajara at the
Qusayba depression, Al-Qasim region (Fig. 1).
The subsurface informal reference section (Hawtah-1) of
the Unayzah Formation was studied by Ferguson and
Chambers (1991). The section consists of two sandstone
intervals separated by a coarsening upward siltstone unit.
Similarly, McGillivray and Husseini (1992) divided the
Unayzah Formation in the Hawtahā€“Hazmiyah ļ¬elds into
two informal sequences identiļ¬ed as Unayzah A and
Unayzah B members. The two members are separated by a
red-brown siltstone or ļ¬ne-grained silty sandstone. Senalp
and Al-Dauji (1995) studied the stratigraphy and sedimen-
tation of the Unayzah Reservoir in central Arabia. They
redeļ¬ned the Unayzah Formation at its type locality by
introducing the term ā€˜ā€˜basal Khuff clasticsā€™ā€™ (Ash-Shiqqah
K. E. Al-Khidir (&) Ɓ M. S. Benzagouta
Department of Petroleum and Natural Gas Engineering,
King Saud University, Riyadh, Saudi Arabia
e-mail: kalkhidir@ksu.edu.sa
A. A. Al-Quraishi
Oil and Gas Research Institute, King Abdulaziz City for Science
and Technology, Riyadh, Saudi Arabia
A. A. Al-Laboun
Department of Geology, King Saud University,
Riyadh, Saudi Arabia
123
J Petrol Explor Prod Technol (2011) 1:1ā€“9
DOI 10.1007/s13202-011-0007-5
member) of the Khuff Formation to be the upper contact of
the Unayzah Formation.
Evans et al. (1997) studied the stratigraphic trap in the
Permian Unayzah Formation, in Usaylah-1, central Arabia,
and they reported that the trap is an up dip pinch out. An oil
column 31 ft thick is encountered in the eolian sandstone
facies of the upper part of the Unayzah Formation. Later,
Wender et al. (1998) divided the Early Permian Unayzah
Formation into three units, the Unayzah-A Reservoir,
Unayzah Siltstone Member, and Unayzah-B Reservoir.
Melvin and Spraque (2006) studied origin and stratigraphic
architecture of glaciogenic sediments in Permianā€“Carbon-
iferous lower Unayzah sandstones in eastern central Saudi
Arabia. They subdivided the lower Unayzah sandstones
into three members, from base to top are: Unayzah C
Member, Unayzah B Member, and an un-named middle
Unayzah member.
Reservoir characteristics of the Permo-Carboniferous
Unayzah Formation, at Wadi Shajara was thoroughly
investigated through ļ¬eld and petrophysical examinations.
An exposed clastic sequence consisting of three sandstone
intervals separated by two mudstone units were observed
(Fig. 2). The clastic sequence is bounded from top and
bottom, by two regional unconformities, namely sub-Khuff
and sub-Unayzah unconformity, respectively. Based on
Saudi Stratigraphic Code (1983), a group is deļ¬ned as a
lithostratigraphic unit bounded by two regional unconfo-
rmities. Therefore, we propose raising the Permo-Carbon-
iferous Unayzah Formation to a group status and identify a
new formation named Shajara Formation (Al-Khidir 2007).
The term Unayzah Formation was restricted to the upper
unit of the group which is best represented in its original
type locality in Unayzah town, while the term Shajara
Formation was assigned to the Lower unit which is best
represented at Wadi Ash-Shajara (Laboun 2010). Depend-
ing on sub-Unayzah unconformity, sub-middle Shajara
local unconformity, the lower mudstone interval, and sub-
Khuff unconformity (Fig. 2), the Shajara Formation was
divided into three members, from base to top: the Lower
Shajara, the Middle Shajara, and the Upper Shajara
(Al-Khidir 2007).
The Shajara Reservoirs of the Shajara Formation is oil
and gas bearing in many ļ¬elds in Saudi Arabia. In addition,
it is the principal Paleozoic clastic reservoir. To our
knowledge no petrophysical examination was conducted on
the surface samples of the Shajara Formation. The aim of
this work is to categorize the Shajara reservoirs by char-
acterizing the pore geometry and the pore aperture sizes of
the sandstones. This is done by integrating capillary pres-
sure obtained by the mercury injection porosimetry tech-
nique, petrofacies determination and lithofacies description
of outcrop samples collected.
Experimental work
The most obvious and straightforward measurements of
pore size are with geometric analysis of images of indi-
vidual pores. This can be done using various types of
microscopy on thin sections or other ļ¬‚at soil surfaces, or
tomography. Image-based techniques can be prohibitively
tedious because enough pores must be analyzed to give an
adequate statistical representation. Therefore, the determi-
nation of pore geometry and pore aperture size using
mercury injection technique is believed to be more helpful
in categorizing rocks by pore types (i.e. nanno, micro,
meso, macro or mega). Autopore III 9420 mercury intru-
sion unit was used to determine the capillary pressure,
porosity, pore throat accessibility, and pore level hetero-
geneity of the three reservoirs comprising the Shajara
Formation. This was conducted on nine outcrop sandstone
samples selected among 13 samples from the type section.
All samples except for one (SJ3) are friable sand and their
locations are presented in stratigraphic column illustrated
in Fig. 2.
Samplesā€™ permeability (k) was calculated utilizing Pur-
cellā€™s equation (1948) stated as:
K Ā¼ 14; 260 Ƃ k Ƃ / Ƃ
ZsĀ¼1
sĀ¼0
dSHg
Pc
ư1ƞ
where, k is a lithology factor (equal to 0.216), dSHg is
incremental mercury saturation and Pc is the capillary
pressure measured in psi.
The pore aperture size is calculated utilizing Washburn
equation expressed as:
Fig. 1 Location map of the studied area
2 J Petrol Explor Prod Technol (2011) 1:1ā€“9
123
r Ā¼
2 Ƃ r Ƃ cos h
Pc
ư2ƞ
where, r is the pore radius in micron, r is the surface tension
of mercury in Dynes/cm, h is the contact angle of mercury
in air and Pc is the capillary pressure in Dynes/cm2
.
To reveal the heterogeneity of the investigated reser-
voirs, the pore aperture distribution (PSD) was plotted as a
function of pore radius. The PSD function is deļ¬ned as the
rate of change of mercury intrusion volume with respect to
the difference of pore radius logarithm relative to the
maximum value of that term. To conļ¬rm the ļ¬ndings of the
PSD plots, the cumulative percent of mercury saturation
was plotted with respect to log pore radius.
On average, the pore throats entered by a non-wetting
ļ¬‚uid (mercury) at 35% saturation (R35) or less during a
capillary analysis, represent the pores that dominate ļ¬‚uid
ļ¬‚ow in a reservoir samples (Kolodzie 1980). The pore
throat corresponding to a mercury saturation of 35% was
evaluated using Winland equation expressed as:
LogR35 Ā¼ 0:732 Ć¾ 0:588 Ƃ log k ƀ 0:864 Ƃ log / Ć°3ƞ
Pittman (2001) reported that, pore throat radius
corresponding to the apex has the potential for delineating
Fig. 2 Stratigraphic column of
the type section of the Permo-
carboniferous Shajara
Formation of the Unayzah
Group, Wadi Shajara, Qusayba
area, al Qassim district, Saudi
Arabia, N 26Ā°52 17.4, E 43Ā°36
18
J Petrol Explor Prod Technol (2011) 1:1ā€“9 3
123
stratigraphic traps in the same manner as the pore aperture
corresponding to 35th percentile of a cumulative mercury
saturation curve, which was developed by Winland.
Therefore, the pore aperture size corresponding to the
apex (Rapex) was determined from Pittman equation stated
as follows:
LogRapex Ā¼ ƀ0:117 Ć¾ 0:475 Ƃ Logk ƀ 0:099 Ƃ Log/
ư4ƞ
Results and discussion
In order to determine the behavior of the pore geometry of
Shajara Reservoirs, samples capillary pressures were
measured and the measurements were used to determine
the pore size distribution. Figure 3 is the pore size distri-
bution of sample SJ1 representing the Lower Shajara
Reservoir. This sample is characterized as red in color,
medium grain size and moderately well sorted. The ļ¬gure
indicates a bimodal pore size distribution of two distinct
pore sizes, minor macro pores of sizes less than 10 lm and
major mega pores with size greater than 10 lm according
to Libny et al. classiļ¬cation (2001). Within the mega pores
there exist a variation in pore size. The sample is charac-
terized with maximum pore radius of 173.9 lm, and a
minimum radius of 0.01 lm, and an average pore size of
41.6 lm. Variation in pore size distribution demonstrates
the possibility of anisotropy. This anisotropy is well
deļ¬ned in Fig. 4 where three distinct tracks have been
obtained. The pore radii of the ļ¬rst track ranges from 60.2
to 173.9 lm. The second represents pore radii varying from
0.1 to 60.2 lm, whereas the third track is characterized by
very low pore radii ranging in size from 0.1 to 0.01 lm.
Sample SJ2 is the second sample representing the Lower
Shajara Reservoir. It is described as medium-grained, well
sorted sandstone. Figure 5 is the pore size distribution of
the sample indicating a bimodal pore size distribution with
Fig. 3 Incremental and cumulative PSD versus pore radius of sample
SJ1 from the Lower Shajara Reservoir
Fig. 4 Cumulative % SHg versus pore radius of sample SJ1 from the
Lower Shajara Reservoir
Fig. 5 Incremental and cumulative PSD versus pore radius of sample
SJ2 from the Lower Shajara Reservoir
Fig. 6 Cumulative % SHg versus pore radius of sample SJ2 from the
Lower Shajara Reservoir
4 J Petrol Explor Prod Technol (2011) 1:1ā€“9
123
a maximum pore radius of 173.9 lm, and an average pore
size of 25.4 lm. Again two distinct pore sizes exist with
majority of the sizes classiļ¬ed as megapores. Figure 6
conļ¬rms the heterogeneity of the sample as presented by
multiple tracks with distinctive pore radius ranges.
Sample SJ3 of the Lower Shajara Reservoir is charac-
terized with ļ¬ner grain size when compared to samples SJ1
and SJ2. Such grain size variability as well as compaction
noticed through grains visual inspection is believed to be
due to the sample proximity to the unconformity surface.
This is reļ¬‚ected in a drastic drop in permeability of sample
SJ3 as stated in Table 1. The sample is also identiļ¬ed with
bimodal pore size distribution with skewness towards ļ¬ner
pore size as indicated in Fig. 7. The sample is characterized
with narrower range of pore radii variation and smaller
pore sizes compared to that of samples SJ1 and SJ2. Again,
Fig. 8 exhibits two tracks of pore radii ranging in size from
10 to 45 lm, and from 1 to 10 lm.
Grain size assessment, pore size distributions and calcu-
lated petrophysical properties of porosity and permeability
of samples SJ1, SJ2 and SJ3 can help assessing the Lower
Shajara Reservoir. This can be conļ¬rmed by the Winland
R35 and Pittman Rapex (Table 1). Based on the grain size
description and the obtained porosity and particularly per-
meability, it can likely be stated that the average pore size
decreases as the grain size gets ļ¬ner and as a consequence
ļ¬‚ow capacity declines. This is observed as we proceed
upward in the reservoir. Based on that and the reservoir
classiļ¬cation utilizing the Winland R35, the lower part of the
reservoir can be classiļ¬ed as megaporous (pore radius
greater than 10 lm), whereas the upper portion of the res-
ervoir represented by sample SJ3 is classiļ¬ed as macropo-
rous (pore radius between 2 and 10 lm) with lower ļ¬‚ow
capacity as stated by the low permeability value (Table 2).
Middle Shajara Reservoir were characterized using
samples SJ7, SJ8 and SJ9. Sample SJ7 is described as
coarse-grained, moderately well sorted sandstone. This
sample is characterized by bimodal pore size distribution as
shown in Fig. 9 with pore radii ranging from 1.2 to
180.8 lm with an average value of 46.15 lm. The sample
heterogeneity is revealed in Fig. 10, where two tracks of
pore radii exists. The ļ¬rst represents a pore radii ranging
from 10 to 180.8 lm, whereas the second represents pore
radii that vary from 1.2 to 10 lm.
Table 1 Petrophysical properties of samples tested
Petrophysical facies U (%) K (mD) R35 (lm) Rapex (lm) h (feet) U avg. (%) K avg. (mD) Reservoir
Sj-1 29.2 1,680 23 18.6 11.8 31.1 1,592 Lowe Shajara Reservoir
Sj-2 35.5 1,955 21.3 19.6 3.9
Sj-3 34.2 56 2.7 3.6 1.6
Sj-7 35.1 1,472 18.2 17.2 13.4 33.4 1,407 Middle Shajara Reservoir
Sj-8 31.9 1,344 18.7 16.8
Sj-9 31.5 1,395 19.3 16.9 0.9
Sj-11 36.2 1,197 15.7 15.5 13.1 29.9 1,204 Upper Shajara Reservoir
Sj-12 28.2 1,440 21.7 17.4
Sj-13 25.4 973 18.8 14.6 6.5
Fig. 7 Incremental and cumulative PSD versus pore radius of sample
SJ3 from the Lower Shajara Reservoir
Fig. 8 Cumulative % SHg versus pore radius of sample SJ3 from the
Lower Shajara Reservoir
J Petrol Explor Prod Technol (2011) 1:1ā€“9 5
123
Sample SJ8 is also identiļ¬ed as medium-grained, mod-
erately well sorted sandstone. This sample is characterized
with bimodal pore size distribution as shown in Fig. 11
with an average pore radius of 28.65 lm indicating smaller
average pore size than that of sample SJ7. The heteroge-
neity of this sample is afļ¬rmed in Fig. 12 which displays
Table 2 Lithofacies description of samples tested
Facies no. Color Grain size Sorting Hardness
SJ-1 Red Medium-grained Moderately well sorted Friable
SJ-2 Yellow Medium-grained Well sorted Friable
SJ-3 Whiteā€“pink Fine-grained Poorly sorted Hard
SJ-7 Red Coarse-grained Moderately well sorted Friable
SJ-8 Red Medium-grained Moderately well sorted Friable
SJ-9 Yellow Medium-grained Moderately well sorted Friable
Sj-11 Yellow Medium-grained Poorly sorted Friable
SJ-12 Yellow Very coarse-grained Moderately sorted Friable
SJ-13 Light brown Coarse-grained Moderately sorted Friable
Fig. 9 Incremental and cumulative PSD versus pore radius of sample
SJ7 from the Lower Shajara Reservoir
Fig. 10 Cumulative % SHg versus pore radius of sample SJ7 from the
Lower Shajara Reservoir
Fig. 11 Incremental and cumulative PSD versus pore radius of
sample SJ8 from the Lower Shajara Reservoir
Fig. 12 Cumulative % SHg versus pore radius of sample SJ8 from the
Lower Shajara Reservoir
6 J Petrol Explor Prod Technol (2011) 1:1ā€“9
123
two tracks of pore radii. The ļ¬rst is for a pore radii that
range in size from 37 to 180.8 lm, whereas the second is
characterized by pore radii varying in size from 1 to
10 lm.
Similar to the above two samples of the Middle Shajara
Reservoir, sample SJ9 is described as medium-grained,
moderately well sorted sandstone. This sample is charac-
terized with bimodal pore size distribution as indicated in
Fig. 13 with an average pore radius of 73.9 lm indicating
the largest mean pore size for this section of the reservoir.
Further veriļ¬cation of heterogeneity of this sample is
indicated in Fig. 14 which indicates two tracks of pore
radii, ranging in size from 10 to 164.4 lm and 1 to 10 lm.
Based on the outcomes obtained and the Winland R35 and
Pittman Rapex (Table 1), the whole Middle Shajara Reser-
voir is classiļ¬ed as megaporous reservoir with good ļ¬‚ow
capacity.
The Upper Shajara Reservoir is also represented by
three samples, namely from base to top SJ11, SJ12, and
SJ13. Sample SJ11 is identiļ¬ed as medium-grained, poorly
sorted sandstone. This sample is characterized with bimo-
dal pore size distribution as illustrated in Fig. 15. This
variation in pore size distribution is proved in Fig. 16
where three tracks of pore distribution are observed. The
ļ¬rst track is for pore radii varying in size from 30 to
173.9 lm. The second track represents distribution of pore
radii ranging in size from 0.1 to 30 lm. The third track
represents a very small pore radii range of 0.01ā€“0.1 lm.
This sample has a mean pore radius of 42.9 lm.
Sample SJ12 is identiļ¬ed as very coarse-grained, mod-
erately sorted sandstone. This sample is also characterized
with bimodal pore size distribution as illustrated in Fig. 17.
This sample possesses an average pore radius of 67.7 lm.
The pore heterogeneity is veriļ¬ed in Fig. 18 where two
Fig. 13 Incremental and cumulative PSD versus pore radius of
sample SJ9 from the Lower Shajara Reservoir
Fig. 14 Cumulative % SHg versus pore radius of sample SJ9 from the
Lower Shajara Reservoir
Fig. 15 Incremental and cumulative PSD versus pore radius of
sample SJ11 from the Lower Shajara Reservoir
Fig. 16 Cumulative % SHg versus pore radius of sample SJ11 from
the Lower Shajara Reservoir
J Petrol Explor Prod Technol (2011) 1:1ā€“9 7
123
tracks of pore size distribution exist. The ļ¬rst having pore
radii ranging in size from 36 to 173.9 lm, whereas the
second ranges from 3.6 to 36 lm.
Sample SJ13 represents the upper section of the reser-
voir. It is described as coarse-grained, moderately sorted
sandstone. Again it is characterized with bimodal pore size
distribution as illustrated in Fig. 19 with an average pore
radius of 25.2 lm. This sample is also considered hetero-
geneous as indicated in Fig. 20 where three distinct tracks
of pore radii are observed. Reservoir classiļ¬cation of the
Upper Shajara can be considered as megaporous.
In an overall view, and based on the relationship of R35
and Rapex presented in Fig. 21, the reservoir quality of the
Shajara Formation increases with the increase in mean pore
radius corresponding to the apex and to that corresponding
to 35% mercury saturation. Good correlation was obtained
Fig. 17 Incremental and cumulative PSD versus pore radius of
sample SJ12 from the Lower Shajara Reservoir
Fig. 18 Incremental and cumulative % SHg versus pore radius of
sample SJ12 from the Lower Shajara Reservoir
Fig. 19 Incremental and cumulative PSD versus pore radius of
sample SJ13 from the Lower Shajara Reservoir
Fig. 20 Cumulative % SHg versus pore radius of sample SJ13 from
the Lower Shajara Reservoir
Fig. 21 Winland R35 versus Pittman Rapex
8 J Petrol Explor Prod Technol (2011) 1:1ā€“9
123
for the R35 versus Rapex and all samples mean pore sizes are
grouped at megaporous category except for sample SJ3
which falls on macroporous category conļ¬rming the pre-
viously discussed pore size identiļ¬cation. In conclusion,
grain and pore size variability are the controlling factor on
the Shajara reservoir quality assessment.
Conclusions
ā€¢ The three reservoirs of the Shajara Formation are
characterized as heterogeneous reservoirs.
ā€¢ In general, the three Shajara Reservoirs are classiļ¬ed as
megaporous, with average pore size of 22, 49 and
45 lm for the Lower, Middle, and Upper Shajara
Reservoirs, respectively. However, the best reservoir
quality is assigned to the lower sand unit of the Lower
Shajara followed by the Middle Shajara Reservoir.
ā€¢ Pore radius corresponding to the apex and that corre-
sponding to the 35% mercury saturation conļ¬rms the
reservoir classiļ¬cation indicating megaporous reser-
voirs except for SJ3 of the Lower Shajara which has
low quality due to its ļ¬ne grain characteristic and its
proximity to the unconformity surface.
ā€¢ An excellent correlation factor of 0.93 was obtained
when Winland R35 was plotted versus Pittman Rapex.
ā€¢ Reservoir quality is controlled to a large extent by the
depositional facies and speciļ¬cally by rock texture
illustrated by petrophysical description. The quality of
the Shajara Formation reservoirs increases with the
increase in grain size and grain sorting.
Open Access This article is distributed under the terms of the
Creative Commons Attribution Noncommercial License which per-
mits any noncommercial use, distribution, and reproduction in any
medium, provided the original author(s) and source are credited.
References
Al-Khidir KE (2007) Reservoir characteristics of the Unayzah
formation. MSc thesis, King Saud University, Riyadh, Kingdom
of Saudi Arabia
Al-Laboun AA (1982) Subsurface stratigraphy of the Pre-Khuff
formations in central and northwestern Arabia. PhD thesis, King
Abdulaziz University, Jeddah, Kingdom of Saudi Arabia
Al-Laboun AA (1987) Unayzah Formation: a new Permo-Carboniferous
unit in Saudi Arabia. Am Assoc Petrol Geol Bull 71(1):29ā€“38
Al-Laboun AA (1988) The distribution of the Carboniferousā€“Permian
Siliciclastics in the Greater Arabian Basin. Geol Soc Am Bull
100(3):362ā€“373
El-Khayal AA, Chaloner WG, Hill CR (1980) Paleozoic plants from
Saudi Arabia. Nature 285:33ā€“34
Evans DS, Bahabri BH, Al-Qtaibi AM (1997) Stratigraphic trap in the
Permian Unayzah Formation, Central Saudi Arabia. GeoArabia
2:259ā€“278
Ferguson GS, Chambers TM (1991) Subsurface stratigraphy, depo-
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Permian Unayzah Formation in Central Saudi Arabia. In: Paper
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(1998) Paleozoic (Pre-Khuff) hydrocarbon geology of the
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Bimodal pore size behavior of the shajara formation reservoirs of the permo carboniferous unayzah group

  • 1. ORIGINAL PAPER - EXPLORATION GEOLOGY Bimodal pore size behavior of the Shajara Formation Reservoirs of the Permo-Carboniferous Unayzah Group, Saudi Arabia K. E. Al-Khidir ā€¢ A. A. Al-Quraishi ā€¢ A. A. Al-Laboun ā€¢ M. S. Benzagouta Received: 29 September 2010 / Accepted: 21 March 2011 / Published online: 5 April 2011 Ɠ The Author(s) 2011. This article is published with open access at Springerlink.com Abstract The sandstones of the Permo-Carboniferous Shajara Formation form the main part of the Unayzah Reservoir in the Greater Arabian Basin. It is divided into three reservoirs, namely from base to top Lower, Middle, and Upper Shajara reservoirs. Mercury intrusion technique was carried out on representative sandstone samples col- lected from the type section and the three reservoirs are generally characterized as heterogeneous megaporous res- ervoirs. The best reservoir quality is assigned to the lower sand unit of the Lower Shajara followed by the Middle Shajara Reservoir. One sample collected from the upper part of the Lower Shajara was described as low quality due to its ļ¬ne grain characteristic and its proximity to the unconformity surface. Reservoir quality is controlled to a large extent by the depositional facies and speciļ¬cally by rock texture illustrated by petrophysical description. The quality of the three reservoirs of the Shajara Formation, increases with the increase of grain size and grain sorting. Keywords Shajara Reservoirs Ɓ Shajara Formation Ɓ Unayzah Group Ɓ Pore size distribution Introduction The Permo-Carboniferous Unayzah Reservoirs are oil and gas bearing in more than 30 oil and gas ļ¬elds in Saudi Arabia. These reservoirs are partially represented in out- crops by the Shajara, Safra, and Shiqqah sandstones of the Unayzah Group. These formations are exposed as a thin belt below the Khuff carbonates in central Arabia. Fossil plants of the late Carboniferousā€“early Permian age were ļ¬rst reported at the town of Unayzah by El- Khayal et al. (1980). Later, the term Unazyah Formation was informally introduced by Al-Laboun (1982) as sili- ciclastics and minor carbonate section at the base of the Khuff Formation. This deļ¬nition was adopted by Aramco Stratigraphic Committee (1983) and formally deļ¬ned by Al-Laboun (1987)in the American Association of Petro- leum Geologist (AAPG). The Unayzah Formation was then correlated with its equivalent units in different parts of the Greater Arabian basin (Al-Laboun 1988) and its type locality was established within Unayzah town with a ref- erence section assigned at Wadi Ash-Shajara at the Qusayba depression, Al-Qasim region (Fig. 1). The subsurface informal reference section (Hawtah-1) of the Unayzah Formation was studied by Ferguson and Chambers (1991). The section consists of two sandstone intervals separated by a coarsening upward siltstone unit. Similarly, McGillivray and Husseini (1992) divided the Unayzah Formation in the Hawtahā€“Hazmiyah ļ¬elds into two informal sequences identiļ¬ed as Unayzah A and Unayzah B members. The two members are separated by a red-brown siltstone or ļ¬ne-grained silty sandstone. Senalp and Al-Dauji (1995) studied the stratigraphy and sedimen- tation of the Unayzah Reservoir in central Arabia. They redeļ¬ned the Unayzah Formation at its type locality by introducing the term ā€˜ā€˜basal Khuff clasticsā€™ā€™ (Ash-Shiqqah K. E. Al-Khidir (&) Ɓ M. S. Benzagouta Department of Petroleum and Natural Gas Engineering, King Saud University, Riyadh, Saudi Arabia e-mail: kalkhidir@ksu.edu.sa A. A. Al-Quraishi Oil and Gas Research Institute, King Abdulaziz City for Science and Technology, Riyadh, Saudi Arabia A. A. Al-Laboun Department of Geology, King Saud University, Riyadh, Saudi Arabia 123 J Petrol Explor Prod Technol (2011) 1:1ā€“9 DOI 10.1007/s13202-011-0007-5
  • 2. member) of the Khuff Formation to be the upper contact of the Unayzah Formation. Evans et al. (1997) studied the stratigraphic trap in the Permian Unayzah Formation, in Usaylah-1, central Arabia, and they reported that the trap is an up dip pinch out. An oil column 31 ft thick is encountered in the eolian sandstone facies of the upper part of the Unayzah Formation. Later, Wender et al. (1998) divided the Early Permian Unayzah Formation into three units, the Unayzah-A Reservoir, Unayzah Siltstone Member, and Unayzah-B Reservoir. Melvin and Spraque (2006) studied origin and stratigraphic architecture of glaciogenic sediments in Permianā€“Carbon- iferous lower Unayzah sandstones in eastern central Saudi Arabia. They subdivided the lower Unayzah sandstones into three members, from base to top are: Unayzah C Member, Unayzah B Member, and an un-named middle Unayzah member. Reservoir characteristics of the Permo-Carboniferous Unayzah Formation, at Wadi Shajara was thoroughly investigated through ļ¬eld and petrophysical examinations. An exposed clastic sequence consisting of three sandstone intervals separated by two mudstone units were observed (Fig. 2). The clastic sequence is bounded from top and bottom, by two regional unconformities, namely sub-Khuff and sub-Unayzah unconformity, respectively. Based on Saudi Stratigraphic Code (1983), a group is deļ¬ned as a lithostratigraphic unit bounded by two regional unconfo- rmities. Therefore, we propose raising the Permo-Carbon- iferous Unayzah Formation to a group status and identify a new formation named Shajara Formation (Al-Khidir 2007). The term Unayzah Formation was restricted to the upper unit of the group which is best represented in its original type locality in Unayzah town, while the term Shajara Formation was assigned to the Lower unit which is best represented at Wadi Ash-Shajara (Laboun 2010). Depend- ing on sub-Unayzah unconformity, sub-middle Shajara local unconformity, the lower mudstone interval, and sub- Khuff unconformity (Fig. 2), the Shajara Formation was divided into three members, from base to top: the Lower Shajara, the Middle Shajara, and the Upper Shajara (Al-Khidir 2007). The Shajara Reservoirs of the Shajara Formation is oil and gas bearing in many ļ¬elds in Saudi Arabia. In addition, it is the principal Paleozoic clastic reservoir. To our knowledge no petrophysical examination was conducted on the surface samples of the Shajara Formation. The aim of this work is to categorize the Shajara reservoirs by char- acterizing the pore geometry and the pore aperture sizes of the sandstones. This is done by integrating capillary pres- sure obtained by the mercury injection porosimetry tech- nique, petrofacies determination and lithofacies description of outcrop samples collected. Experimental work The most obvious and straightforward measurements of pore size are with geometric analysis of images of indi- vidual pores. This can be done using various types of microscopy on thin sections or other ļ¬‚at soil surfaces, or tomography. Image-based techniques can be prohibitively tedious because enough pores must be analyzed to give an adequate statistical representation. Therefore, the determi- nation of pore geometry and pore aperture size using mercury injection technique is believed to be more helpful in categorizing rocks by pore types (i.e. nanno, micro, meso, macro or mega). Autopore III 9420 mercury intru- sion unit was used to determine the capillary pressure, porosity, pore throat accessibility, and pore level hetero- geneity of the three reservoirs comprising the Shajara Formation. This was conducted on nine outcrop sandstone samples selected among 13 samples from the type section. All samples except for one (SJ3) are friable sand and their locations are presented in stratigraphic column illustrated in Fig. 2. Samplesā€™ permeability (k) was calculated utilizing Pur- cellā€™s equation (1948) stated as: K Ā¼ 14; 260 Ƃ k Ƃ / Ƃ ZsĀ¼1 sĀ¼0 dSHg Pc Ć°1ƞ where, k is a lithology factor (equal to 0.216), dSHg is incremental mercury saturation and Pc is the capillary pressure measured in psi. The pore aperture size is calculated utilizing Washburn equation expressed as: Fig. 1 Location map of the studied area 2 J Petrol Explor Prod Technol (2011) 1:1ā€“9 123
  • 3. r Ā¼ 2 Ƃ r Ƃ cos h Pc Ć°2ƞ where, r is the pore radius in micron, r is the surface tension of mercury in Dynes/cm, h is the contact angle of mercury in air and Pc is the capillary pressure in Dynes/cm2 . To reveal the heterogeneity of the investigated reser- voirs, the pore aperture distribution (PSD) was plotted as a function of pore radius. The PSD function is deļ¬ned as the rate of change of mercury intrusion volume with respect to the difference of pore radius logarithm relative to the maximum value of that term. To conļ¬rm the ļ¬ndings of the PSD plots, the cumulative percent of mercury saturation was plotted with respect to log pore radius. On average, the pore throats entered by a non-wetting ļ¬‚uid (mercury) at 35% saturation (R35) or less during a capillary analysis, represent the pores that dominate ļ¬‚uid ļ¬‚ow in a reservoir samples (Kolodzie 1980). The pore throat corresponding to a mercury saturation of 35% was evaluated using Winland equation expressed as: LogR35 Ā¼ 0:732 Ć¾ 0:588 Ƃ log k ƀ 0:864 Ƃ log / Ć°3ƞ Pittman (2001) reported that, pore throat radius corresponding to the apex has the potential for delineating Fig. 2 Stratigraphic column of the type section of the Permo- carboniferous Shajara Formation of the Unayzah Group, Wadi Shajara, Qusayba area, al Qassim district, Saudi Arabia, N 26Ā°52 17.4, E 43Ā°36 18 J Petrol Explor Prod Technol (2011) 1:1ā€“9 3 123
  • 4. stratigraphic traps in the same manner as the pore aperture corresponding to 35th percentile of a cumulative mercury saturation curve, which was developed by Winland. Therefore, the pore aperture size corresponding to the apex (Rapex) was determined from Pittman equation stated as follows: LogRapex Ā¼ ƀ0:117 Ć¾ 0:475 Ƃ Logk ƀ 0:099 Ƃ Log/ Ć°4ƞ Results and discussion In order to determine the behavior of the pore geometry of Shajara Reservoirs, samples capillary pressures were measured and the measurements were used to determine the pore size distribution. Figure 3 is the pore size distri- bution of sample SJ1 representing the Lower Shajara Reservoir. This sample is characterized as red in color, medium grain size and moderately well sorted. The ļ¬gure indicates a bimodal pore size distribution of two distinct pore sizes, minor macro pores of sizes less than 10 lm and major mega pores with size greater than 10 lm according to Libny et al. classiļ¬cation (2001). Within the mega pores there exist a variation in pore size. The sample is charac- terized with maximum pore radius of 173.9 lm, and a minimum radius of 0.01 lm, and an average pore size of 41.6 lm. Variation in pore size distribution demonstrates the possibility of anisotropy. This anisotropy is well deļ¬ned in Fig. 4 where three distinct tracks have been obtained. The pore radii of the ļ¬rst track ranges from 60.2 to 173.9 lm. The second represents pore radii varying from 0.1 to 60.2 lm, whereas the third track is characterized by very low pore radii ranging in size from 0.1 to 0.01 lm. Sample SJ2 is the second sample representing the Lower Shajara Reservoir. It is described as medium-grained, well sorted sandstone. Figure 5 is the pore size distribution of the sample indicating a bimodal pore size distribution with Fig. 3 Incremental and cumulative PSD versus pore radius of sample SJ1 from the Lower Shajara Reservoir Fig. 4 Cumulative % SHg versus pore radius of sample SJ1 from the Lower Shajara Reservoir Fig. 5 Incremental and cumulative PSD versus pore radius of sample SJ2 from the Lower Shajara Reservoir Fig. 6 Cumulative % SHg versus pore radius of sample SJ2 from the Lower Shajara Reservoir 4 J Petrol Explor Prod Technol (2011) 1:1ā€“9 123
  • 5. a maximum pore radius of 173.9 lm, and an average pore size of 25.4 lm. Again two distinct pore sizes exist with majority of the sizes classiļ¬ed as megapores. Figure 6 conļ¬rms the heterogeneity of the sample as presented by multiple tracks with distinctive pore radius ranges. Sample SJ3 of the Lower Shajara Reservoir is charac- terized with ļ¬ner grain size when compared to samples SJ1 and SJ2. Such grain size variability as well as compaction noticed through grains visual inspection is believed to be due to the sample proximity to the unconformity surface. This is reļ¬‚ected in a drastic drop in permeability of sample SJ3 as stated in Table 1. The sample is also identiļ¬ed with bimodal pore size distribution with skewness towards ļ¬ner pore size as indicated in Fig. 7. The sample is characterized with narrower range of pore radii variation and smaller pore sizes compared to that of samples SJ1 and SJ2. Again, Fig. 8 exhibits two tracks of pore radii ranging in size from 10 to 45 lm, and from 1 to 10 lm. Grain size assessment, pore size distributions and calcu- lated petrophysical properties of porosity and permeability of samples SJ1, SJ2 and SJ3 can help assessing the Lower Shajara Reservoir. This can be conļ¬rmed by the Winland R35 and Pittman Rapex (Table 1). Based on the grain size description and the obtained porosity and particularly per- meability, it can likely be stated that the average pore size decreases as the grain size gets ļ¬ner and as a consequence ļ¬‚ow capacity declines. This is observed as we proceed upward in the reservoir. Based on that and the reservoir classiļ¬cation utilizing the Winland R35, the lower part of the reservoir can be classiļ¬ed as megaporous (pore radius greater than 10 lm), whereas the upper portion of the res- ervoir represented by sample SJ3 is classiļ¬ed as macropo- rous (pore radius between 2 and 10 lm) with lower ļ¬‚ow capacity as stated by the low permeability value (Table 2). Middle Shajara Reservoir were characterized using samples SJ7, SJ8 and SJ9. Sample SJ7 is described as coarse-grained, moderately well sorted sandstone. This sample is characterized by bimodal pore size distribution as shown in Fig. 9 with pore radii ranging from 1.2 to 180.8 lm with an average value of 46.15 lm. The sample heterogeneity is revealed in Fig. 10, where two tracks of pore radii exists. The ļ¬rst represents a pore radii ranging from 10 to 180.8 lm, whereas the second represents pore radii that vary from 1.2 to 10 lm. Table 1 Petrophysical properties of samples tested Petrophysical facies U (%) K (mD) R35 (lm) Rapex (lm) h (feet) U avg. (%) K avg. (mD) Reservoir Sj-1 29.2 1,680 23 18.6 11.8 31.1 1,592 Lowe Shajara Reservoir Sj-2 35.5 1,955 21.3 19.6 3.9 Sj-3 34.2 56 2.7 3.6 1.6 Sj-7 35.1 1,472 18.2 17.2 13.4 33.4 1,407 Middle Shajara Reservoir Sj-8 31.9 1,344 18.7 16.8 Sj-9 31.5 1,395 19.3 16.9 0.9 Sj-11 36.2 1,197 15.7 15.5 13.1 29.9 1,204 Upper Shajara Reservoir Sj-12 28.2 1,440 21.7 17.4 Sj-13 25.4 973 18.8 14.6 6.5 Fig. 7 Incremental and cumulative PSD versus pore radius of sample SJ3 from the Lower Shajara Reservoir Fig. 8 Cumulative % SHg versus pore radius of sample SJ3 from the Lower Shajara Reservoir J Petrol Explor Prod Technol (2011) 1:1ā€“9 5 123
  • 6. Sample SJ8 is also identiļ¬ed as medium-grained, mod- erately well sorted sandstone. This sample is characterized with bimodal pore size distribution as shown in Fig. 11 with an average pore radius of 28.65 lm indicating smaller average pore size than that of sample SJ7. The heteroge- neity of this sample is afļ¬rmed in Fig. 12 which displays Table 2 Lithofacies description of samples tested Facies no. Color Grain size Sorting Hardness SJ-1 Red Medium-grained Moderately well sorted Friable SJ-2 Yellow Medium-grained Well sorted Friable SJ-3 Whiteā€“pink Fine-grained Poorly sorted Hard SJ-7 Red Coarse-grained Moderately well sorted Friable SJ-8 Red Medium-grained Moderately well sorted Friable SJ-9 Yellow Medium-grained Moderately well sorted Friable Sj-11 Yellow Medium-grained Poorly sorted Friable SJ-12 Yellow Very coarse-grained Moderately sorted Friable SJ-13 Light brown Coarse-grained Moderately sorted Friable Fig. 9 Incremental and cumulative PSD versus pore radius of sample SJ7 from the Lower Shajara Reservoir Fig. 10 Cumulative % SHg versus pore radius of sample SJ7 from the Lower Shajara Reservoir Fig. 11 Incremental and cumulative PSD versus pore radius of sample SJ8 from the Lower Shajara Reservoir Fig. 12 Cumulative % SHg versus pore radius of sample SJ8 from the Lower Shajara Reservoir 6 J Petrol Explor Prod Technol (2011) 1:1ā€“9 123
  • 7. two tracks of pore radii. The ļ¬rst is for a pore radii that range in size from 37 to 180.8 lm, whereas the second is characterized by pore radii varying in size from 1 to 10 lm. Similar to the above two samples of the Middle Shajara Reservoir, sample SJ9 is described as medium-grained, moderately well sorted sandstone. This sample is charac- terized with bimodal pore size distribution as indicated in Fig. 13 with an average pore radius of 73.9 lm indicating the largest mean pore size for this section of the reservoir. Further veriļ¬cation of heterogeneity of this sample is indicated in Fig. 14 which indicates two tracks of pore radii, ranging in size from 10 to 164.4 lm and 1 to 10 lm. Based on the outcomes obtained and the Winland R35 and Pittman Rapex (Table 1), the whole Middle Shajara Reser- voir is classiļ¬ed as megaporous reservoir with good ļ¬‚ow capacity. The Upper Shajara Reservoir is also represented by three samples, namely from base to top SJ11, SJ12, and SJ13. Sample SJ11 is identiļ¬ed as medium-grained, poorly sorted sandstone. This sample is characterized with bimo- dal pore size distribution as illustrated in Fig. 15. This variation in pore size distribution is proved in Fig. 16 where three tracks of pore distribution are observed. The ļ¬rst track is for pore radii varying in size from 30 to 173.9 lm. The second track represents distribution of pore radii ranging in size from 0.1 to 30 lm. The third track represents a very small pore radii range of 0.01ā€“0.1 lm. This sample has a mean pore radius of 42.9 lm. Sample SJ12 is identiļ¬ed as very coarse-grained, mod- erately sorted sandstone. This sample is also characterized with bimodal pore size distribution as illustrated in Fig. 17. This sample possesses an average pore radius of 67.7 lm. The pore heterogeneity is veriļ¬ed in Fig. 18 where two Fig. 13 Incremental and cumulative PSD versus pore radius of sample SJ9 from the Lower Shajara Reservoir Fig. 14 Cumulative % SHg versus pore radius of sample SJ9 from the Lower Shajara Reservoir Fig. 15 Incremental and cumulative PSD versus pore radius of sample SJ11 from the Lower Shajara Reservoir Fig. 16 Cumulative % SHg versus pore radius of sample SJ11 from the Lower Shajara Reservoir J Petrol Explor Prod Technol (2011) 1:1ā€“9 7 123
  • 8. tracks of pore size distribution exist. The ļ¬rst having pore radii ranging in size from 36 to 173.9 lm, whereas the second ranges from 3.6 to 36 lm. Sample SJ13 represents the upper section of the reser- voir. It is described as coarse-grained, moderately sorted sandstone. Again it is characterized with bimodal pore size distribution as illustrated in Fig. 19 with an average pore radius of 25.2 lm. This sample is also considered hetero- geneous as indicated in Fig. 20 where three distinct tracks of pore radii are observed. Reservoir classiļ¬cation of the Upper Shajara can be considered as megaporous. In an overall view, and based on the relationship of R35 and Rapex presented in Fig. 21, the reservoir quality of the Shajara Formation increases with the increase in mean pore radius corresponding to the apex and to that corresponding to 35% mercury saturation. Good correlation was obtained Fig. 17 Incremental and cumulative PSD versus pore radius of sample SJ12 from the Lower Shajara Reservoir Fig. 18 Incremental and cumulative % SHg versus pore radius of sample SJ12 from the Lower Shajara Reservoir Fig. 19 Incremental and cumulative PSD versus pore radius of sample SJ13 from the Lower Shajara Reservoir Fig. 20 Cumulative % SHg versus pore radius of sample SJ13 from the Lower Shajara Reservoir Fig. 21 Winland R35 versus Pittman Rapex 8 J Petrol Explor Prod Technol (2011) 1:1ā€“9 123
  • 9. for the R35 versus Rapex and all samples mean pore sizes are grouped at megaporous category except for sample SJ3 which falls on macroporous category conļ¬rming the pre- viously discussed pore size identiļ¬cation. In conclusion, grain and pore size variability are the controlling factor on the Shajara reservoir quality assessment. Conclusions ā€¢ The three reservoirs of the Shajara Formation are characterized as heterogeneous reservoirs. ā€¢ In general, the three Shajara Reservoirs are classiļ¬ed as megaporous, with average pore size of 22, 49 and 45 lm for the Lower, Middle, and Upper Shajara Reservoirs, respectively. However, the best reservoir quality is assigned to the lower sand unit of the Lower Shajara followed by the Middle Shajara Reservoir. ā€¢ Pore radius corresponding to the apex and that corre- sponding to the 35% mercury saturation conļ¬rms the reservoir classiļ¬cation indicating megaporous reser- voirs except for SJ3 of the Lower Shajara which has low quality due to its ļ¬ne grain characteristic and its proximity to the unconformity surface. ā€¢ An excellent correlation factor of 0.93 was obtained when Winland R35 was plotted versus Pittman Rapex. ā€¢ Reservoir quality is controlled to a large extent by the depositional facies and speciļ¬cally by rock texture illustrated by petrophysical description. The quality of the Shajara Formation reservoirs increases with the increase in grain size and grain sorting. Open Access This article is distributed under the terms of the Creative Commons Attribution Noncommercial License which per- mits any noncommercial use, distribution, and reproduction in any medium, provided the original author(s) and source are credited. References Al-Khidir KE (2007) Reservoir characteristics of the Unayzah formation. MSc thesis, King Saud University, Riyadh, Kingdom of Saudi Arabia Al-Laboun AA (1982) Subsurface stratigraphy of the Pre-Khuff formations in central and northwestern Arabia. PhD thesis, King Abdulaziz University, Jeddah, Kingdom of Saudi Arabia Al-Laboun AA (1987) Unayzah Formation: a new Permo-Carboniferous unit in Saudi Arabia. Am Assoc Petrol Geol Bull 71(1):29ā€“38 Al-Laboun AA (1988) The distribution of the Carboniferousā€“Permian Siliciclastics in the Greater Arabian Basin. Geol Soc Am Bull 100(3):362ā€“373 El-Khayal AA, Chaloner WG, Hill CR (1980) Paleozoic plants from Saudi Arabia. Nature 285:33ā€“34 Evans DS, Bahabri BH, Al-Qtaibi AM (1997) Stratigraphic trap in the Permian Unayzah Formation, Central Saudi Arabia. GeoArabia 2:259ā€“278 Ferguson GS, Chambers TM (1991) Subsurface stratigraphy, depo- sitional history, and reservoir development of the early-to-late Permian Unayzah Formation in Central Saudi Arabia. In: Paper SPE 21394 presented at the middle east oil show held in Bahrain, Nov. 16ā€“19 Kolodzie SJ (1980) Analysis of pore throat size and use of the Waxmanā€“Smits equation to determine OOIP in spindle ļ¬eld. In: Paper SPE 9382, 55th annual fall technical conference, Colorado Libny L, Roberto R, Quaglia A, Porras JC, and Lazarde H (2001) Bimodal behavior of mercury injection capillary pressure curve and its relationship to pore geometry, rock quality and produc- tion performance in a laminated and heterogeneous reservoir. In: SPE 69457 presented at Latin America and Caribbean Petroleum Engineering Conference, Argentina, March 25ā€“28 McGillivray JG, Husseini MI (1992) The Paleozoic petroleum geology of central Arabia. Am Assoc Petrol Geol Bull 76(10): 1473ā€“1490 Melvin J, Sprague A (2006) Origin and stratigraphic architecture of galciogenic sediments in Permian-Carboniferous Lower Unay- zah Sandstones, Eastern Central Saudi Arabia. GeoArabia 11(4):105ā€“152 Pittman ED (2001) Estimating pore throat size in sandstones from routine core analysis data Purcell WR (1948) Capillary pressuresā€”their measurement using mercury and the calculation of the permeability therefrom, AIME, T.P.2544 Senalp M, Al-Dauji A (1995) Stratigraphy and sedimentation of the Unayzah Reservoir, Central Saudi Arabia. In: Husseini MI (ed) The middle east petroleum geosciences, Geo 94, Gulf Petrolink, Bahrain, vol 2, pp 837ā€“847 Wender LE, Bryant JW, Dicken MF, Neville AS, Al-Moqbel AM (1998) Paleozoic (Pre-Khuff) hydrocarbon geology of the Ghawar area, Eastern Saudi Arabia. GeoArabia 3(2):273ā€“302 J Petrol Explor Prod Technol (2011) 1:1ā€“9 9 123