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G R O U P M E M B E R S :
U M E R S H A H A B ( 2 0 1 4 4 4 3 )
T A L H A N A S I R K H A N L O D H I ( 2 0 1 4 3 8 3 )
M I A N M U H A M M A D H U S S A I N ( 2 0 1 4 1 6 9 )
A D V I S O R : D R . F A H D N A W A Z
C O - A D V I S O R : D R . I M R A N K H A N
Welding of Ti-5Al-2.5Sn
alloy and its characterization
1
Faculty of Materials and Chemical Engineering
Introduction
2
 Our work is focused primarily on Grade 6 Titanium
(Ti-5Al-2.5Sn)
 Good news: Only in-house testing remains, all
external processes have been carried out
Work Progress
3
Wire EDM
EBW
Wire EDM
Tensile
Testing
Impact testing
Optical
Microscopy
Scanning
Electron
Microscopy
Microhardness
Testing
Hole-drill
method
Welded Sample
4
Top view
Side view
Bottom view
Post EDM Plate
5
Overview of Samples
6
Impact
testing
Tensile testing Notch Tensile Testing
Tensile Testing
7
 ASTM standard E8M-04 was followed to prepare
the specimens for tensile testing
 Gage length: 25mm
 Conducted using the 30kN Instron machine
 Strain rate: 2.5mm/min
Graphs
8
Results of tensile testing
9
Max Load
(kN)
Energy at
break
(J)
Extension at
break
(mm)
Teanacity
(kg/den)
1 7.2 8.7 1.75 733
2 7.8 23.6 3.62 792
Impact Testing
10
 Charpy Impact tests were performed on the samples
 As per ASTM standard E-23, a V-notch with an angle
of 60 degrees and a depth of 2mm was used in the
test
Results
11
Sample
No.
Angle
(degrees)
Energy Absorbed
(J)
1 117 3.89
2 105 5.69
Angle: 117 degrees Angle: 105 degrees
Notch Tensile testing
12
 A specimen with notches of 45 degrees on both sides
as per ASTM standard E-8M-04 was used for this
test
 The test was conducted on the Instron tensile testing
machine
Results
13
Results
14
S no. Max Load
(kN)
Energy at
break
(J)
Extension at
break
(mm)
Tenacity
(kg/den)
1 8 4.86 1.00 817.8
2 9.4 6.34 1.12 955.2
Microstructural Analysis
15
 Grinding was performed on the samples to remove
any scratches
 Polishing was then performed on the sample for a
shiny appearance
 Kroll solution (6% Nitric acid, 2% Hydrofluoric acid
by volume) was used as an etchant
 Further etching was performed using 2% HF in order
to add colors to the microstructure
Results
16
Fusion zoneHeat affected zoneBase Metal
100 um
Results summary
17
 The microstructure of the heat affected zone changed
from equiaxed grains near the base metal to acicular
structure near the HAZ/FZ interface
 The cooling process was unidirectional which
resulted in columnar grains in the HAZ
Hole-drill method
18
 Performed as per ASTM standard E837
 Strain gages are placed at predetermined coordinates
 A hole is drilled at specified locations and the
resulting strain produces an electrical signal in the
strain gage
 The electrical signal is recorded by a strain recorder
 Since strain gages are placed at different coordinates
across the sample, this method gives us the residual
stress distribution
Strain gages
19
Strain indicator and recorder
20
Drill mounted on Tripod
21
References
22
1. Akman, Demir, T. C., and T.S 2009. “Laser Welding of Ti6Al4V Titanium Alloys.” Journal of
Materials Processing Technology 209(8):3705–13.
2. Bhargava P, et al. 2013 “Study on weld bead surface profile and angular distortion in 6 mm thick
butt weld joints of SS304 using fiber laser.” Optics and Lasers in Engineering 47(14):1231–41.
3. Xiao R, Zhang X. 2014. Problems and issues in laser beam welding of aluminum–lithium alloys. J
Manuf Process ;16:166–75.
4. Mats N., Ulf A., Håkan E., and Jukka L. 2015. “Surface Oxidation Behavior of Ti–6Al–4V
Manufactured by Electron Beam Melting (EBM®).” Journal of Manufacturing Processes 17:120–
26.
5. Luo, S.D. and Qian, 2016 “Microwave processing of titanium and titanium alloys for structural,
biomedical and shape memory applications: current status and challenges, Mater.”
Manufacturing Processes 1–15.
6. Khorev, A.I., 2016. “Development of titanium sheet alloys for welded structures working at high
temperatures”, Weld. International. 30:389–394
7. Junaid, M. et al. 2017. “Study of microstructure, mechanical properties and residual stresses in
full penetration electron beam welded Ti-5Al-2.5Sn alloy sheet.” Materials & Design. 139.
.10.1016/j.matdes.2017.11.009.
8. https://www.twmperformance.com/index.php?route=common/home
9. http://www.dsweldingfabrication.com/ds-welding-welding_types.html
23
Thank You

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Presentation

  • 1. G R O U P M E M B E R S : U M E R S H A H A B ( 2 0 1 4 4 4 3 ) T A L H A N A S I R K H A N L O D H I ( 2 0 1 4 3 8 3 ) M I A N M U H A M M A D H U S S A I N ( 2 0 1 4 1 6 9 ) A D V I S O R : D R . F A H D N A W A Z C O - A D V I S O R : D R . I M R A N K H A N Welding of Ti-5Al-2.5Sn alloy and its characterization 1 Faculty of Materials and Chemical Engineering
  • 2. Introduction 2  Our work is focused primarily on Grade 6 Titanium (Ti-5Al-2.5Sn)  Good news: Only in-house testing remains, all external processes have been carried out
  • 3. Work Progress 3 Wire EDM EBW Wire EDM Tensile Testing Impact testing Optical Microscopy Scanning Electron Microscopy Microhardness Testing Hole-drill method
  • 4. Welded Sample 4 Top view Side view Bottom view
  • 6. Overview of Samples 6 Impact testing Tensile testing Notch Tensile Testing
  • 7. Tensile Testing 7  ASTM standard E8M-04 was followed to prepare the specimens for tensile testing  Gage length: 25mm  Conducted using the 30kN Instron machine  Strain rate: 2.5mm/min
  • 9. Results of tensile testing 9 Max Load (kN) Energy at break (J) Extension at break (mm) Teanacity (kg/den) 1 7.2 8.7 1.75 733 2 7.8 23.6 3.62 792
  • 10. Impact Testing 10  Charpy Impact tests were performed on the samples  As per ASTM standard E-23, a V-notch with an angle of 60 degrees and a depth of 2mm was used in the test
  • 11. Results 11 Sample No. Angle (degrees) Energy Absorbed (J) 1 117 3.89 2 105 5.69 Angle: 117 degrees Angle: 105 degrees
  • 12. Notch Tensile testing 12  A specimen with notches of 45 degrees on both sides as per ASTM standard E-8M-04 was used for this test  The test was conducted on the Instron tensile testing machine
  • 14. Results 14 S no. Max Load (kN) Energy at break (J) Extension at break (mm) Tenacity (kg/den) 1 8 4.86 1.00 817.8 2 9.4 6.34 1.12 955.2
  • 15. Microstructural Analysis 15  Grinding was performed on the samples to remove any scratches  Polishing was then performed on the sample for a shiny appearance  Kroll solution (6% Nitric acid, 2% Hydrofluoric acid by volume) was used as an etchant  Further etching was performed using 2% HF in order to add colors to the microstructure
  • 16. Results 16 Fusion zoneHeat affected zoneBase Metal 100 um
  • 17. Results summary 17  The microstructure of the heat affected zone changed from equiaxed grains near the base metal to acicular structure near the HAZ/FZ interface  The cooling process was unidirectional which resulted in columnar grains in the HAZ
  • 18. Hole-drill method 18  Performed as per ASTM standard E837  Strain gages are placed at predetermined coordinates  A hole is drilled at specified locations and the resulting strain produces an electrical signal in the strain gage  The electrical signal is recorded by a strain recorder  Since strain gages are placed at different coordinates across the sample, this method gives us the residual stress distribution
  • 20. Strain indicator and recorder 20
  • 21. Drill mounted on Tripod 21
  • 22. References 22 1. Akman, Demir, T. C., and T.S 2009. “Laser Welding of Ti6Al4V Titanium Alloys.” Journal of Materials Processing Technology 209(8):3705–13. 2. Bhargava P, et al. 2013 “Study on weld bead surface profile and angular distortion in 6 mm thick butt weld joints of SS304 using fiber laser.” Optics and Lasers in Engineering 47(14):1231–41. 3. Xiao R, Zhang X. 2014. Problems and issues in laser beam welding of aluminum–lithium alloys. J Manuf Process ;16:166–75. 4. Mats N., Ulf A., Håkan E., and Jukka L. 2015. “Surface Oxidation Behavior of Ti–6Al–4V Manufactured by Electron Beam Melting (EBM®).” Journal of Manufacturing Processes 17:120– 26. 5. Luo, S.D. and Qian, 2016 “Microwave processing of titanium and titanium alloys for structural, biomedical and shape memory applications: current status and challenges, Mater.” Manufacturing Processes 1–15. 6. Khorev, A.I., 2016. “Development of titanium sheet alloys for welded structures working at high temperatures”, Weld. International. 30:389–394 7. Junaid, M. et al. 2017. “Study of microstructure, mechanical properties and residual stresses in full penetration electron beam welded Ti-5Al-2.5Sn alloy sheet.” Materials & Design. 139. .10.1016/j.matdes.2017.11.009. 8. https://www.twmperformance.com/index.php?route=common/home 9. http://www.dsweldingfabrication.com/ds-welding-welding_types.html